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Pharmacy PHARMACEUTICS CT Institute of Pharmaceutical sciences Jalandhar, INDIA AICTE , PCI approved
of shear. Capillary viscometer(Ostwald viscometer) Falling sphere viscometer Application:- Newtonian fluids
Multipoint viscometer:-Equipment work at a several rate
of shear. Cup and bob viscometer Cone and plate viscometer Application:- Non-Newtonian, Newtonian fluids
equation.
n1
=
p1t1 n2
p2t2
p1 -density of unknown liquid p2 - density of known liquid t1 -time of flow of unknown liquid t2 -time of flow of known liquid n2 viscosity of known liquid
constant temperature jacket with provision for water circulation is arranged around the glass tube.
The test liquid is placed in the glass chamber. A glass or steel ball is
dropped into the liquid and allowed to reach equilibrium with the
temperature of the outer jacket.
The tube with the jacket is then inverted, which places the ball at
the top of the inner glass tube. The time taken for the ball to fall b/w two mark is accurately measured
This process is repeated several times to obtain concurrent results.
t is the time interval in seconds for the ball to fall b/w the two
points, Sb and Sf are the specific gravity of the ball and fluid under examination
CUP AND BOB VISCOMETER This a multipoint viscometer and belongs to the category of rotational viscometers
to rotate and the torque resulting from the viscous drag is measured by a spring or sensor device in the derive of the bob
The number of revolutions and the torque represent the rate of shear
pseudoplastic system.
n= Kv w v Where w= weight placed on the hanger, shearing stress v= rpm, shear rate n= apparent viscosity of the fluid Kv =constant for the instrument
It possesses several advantages:The rate of shear is constant throughout the entire sample being
sheared.
The sample required is small 0.1 to 0.2 ml. Cleaning and filling is easy. Less time is required for temperature equilibrium.
Principle:
The cone is driven by a variable-speed motor and the sample is
sheared in the narrow gap b/w the stationary plate and the rotating cone.
The rate of shear in rpm is increased and decreased by a selector
A plot of rpm (rate of shear) v/s scale reading (shearing stress) may
n=C T
v Where C is the instrument constant T is the torque v is the speed of the cone
BROOKFIELD VISCOMETER
The Brookfield Viscometer is an instrument used for measuring the
a definite, constant speed while immersed in the sample. The degree of spindle lag is indicated on a rotating dial.