V-616A I/O SHEET

PROCESS STEPS Charging of batch from V-618A,V-619,T-512,T-519 VA-NVA NVA SOP YES EQUIPMENTS Distillation assembly,Vessls,Pump, DCS, LT, TI. OUTPUT Charge of batch FEATURES(Y) Accurate quantity of mass SPECIFICATIONS Acetone & crude Iso ratio 0.52 : 1 Qty : 13000-14000 Lts Top vapour temp increases from 30-55C Reflux flow 0-2000 Kg Reflux temp 30-40c Reflux flow 4500-5100 Kg Reflux temp 30-35c Isoflurane NMT4% Collection rate 90:01 Reflux flow 4800-5100 Kg/hr Collection of Rechargable Fraction in V-619 VA YES Distillation assembly, DCS, LT, TI. FT Rechargable Fraction Max collection upto 1700 Lts At the end of distillation lower collection flow rate DCEF NMT 200ppm Collection rate 90:01 Bottom fraction 10500-13500 Kg Stop steam & collect column holdup in V-616A NVA YES Distillation assembly, DCS, LT, TI. FT Empty out material from column Avoid loss of material Increase level of V-616A No vapours in V-616A To cool the reaction mass Material must be free of vapours Feed for next step ie., C-646B Zero reflux flow rate Drop in reflux & column Temp Reaction mass temp 35-45 c Stop steam supply NC Close steam CV & manual valves steam flow Zero DCS Contineous supply of steam C Constant supply of steam Steam flow upto 1000kg/hr DCS,GC INPUT(X) Crude Iso & Acetone C-NC C FEATURES mass must be at room temp Free from high vapours Constant supply of steam SPECIFICATIONS Temp between 35-45c TESTS DCS, GC

Apply steam & heat upto reflux

VA

YES

Distillation assembly, DCS, LT, TI,FT

Heat the mass

Reboiler temp increases from 35-60c Change in column temp & Start of reflux

Steam

Steam flow 1000 kg/hr

DCS

Maintain column still stabilize

VA

YES

Distillation assembly, DCS, LT, TI. FT

Stabilize the column

Constant Reflux flow & temperature

Contineous supply of steam

Constant supply of steam

Steam flow upto 1000 kg/hr

DCS

Collection of Discardable Fraction in V-556

VA

YES

Distillation assembly, DCS, LT, TI. FT

Discardable Fraction

Fraction contains CMF,CECMF,ACETONE ,FEFME max collection upto 1100 Lts

Contineous supply of steam

Constant supply of steam

Steam flow upto 1000kg/hr

DCS, GC

Apply cooling to V-616A

NVA

YES

Distillation assembly, DCS, LT, TI. FT

Cool the mass

Cooling tower water supply

NC

Constant supply of CTW

CTW temp 355C

NA

Transfer V-616A mass to V-618B

NVA

YES

Distillation assembly, DCS, LT, TI. FT

Empty out V-616A

DCEF : NMT 180 ppm CECMF : NMT 05 ppm

NC