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Pump#1 (EtAc)
Pump#2 (NaOH)
Pump Setting V#olume (mL) time (sec)
flowrate (L/s) Pump Setting V#olume (mL)
4
3
18.49 0.00016225
4
4
7
10
5.5
8.64 0.00069444
4.65
0.0011828
6.8
10
7.5
Pump 1 EtaC
0.0014
y = 0.0002x - 0.0005
R = 0.9994
0.0012
0.001
0.0008
0.0006
Pump 1 EtaC
0.0004
0.0002
0
0
10
Pump Setting #
15
time (sec)
flowrate (L/s)
18.97 0.00021086
8.77 0.00077537
5.41 0.00138632
Pump 2 NaOH
0.0016
y = 0.0002x - 0.0006
R = 0.9995
0.0014
0.0012
0.001
0.0008
Pump 2 NaOH
0.0006
0.0004
0.0002
0
0
10
Pump Setting #
15
Conductivity Calibration:
Conversion: 1S=0.001mS
For 50 mL of Solution
Conversion
Sodium Acetate
NaOH
Total
%
Target mass (g)
Actual mass (g)
Target mass (g)
Actual mass (g) Volume
100
0.04102
0
50
0.03692
0.002000
80
0.03281
0.004000
0.02871
0.006000
60
0.02461
0.007999
0.02051
0.009999
40
0.01641
0.011999
0.01231
0.013999
20
0.00820
0.015999
0.00410
0.017999
0
0
0.019999
Conversion (%)
100
80
60
Series1
40
Poly. (Series1)
20
0
0
0.5
1.5
2.5
S=0.001mS
Conductivity reading
mS
1289
1.289
1719
1.719
2340
2.34
2790
2.79
Order of Reaction:
Trial #2: 0.1M NaOH, 0.01M EtAc
Time (s)
0
10
20
30
40
50
60
70
80
90
100
110
120
130
140
150
160
170
180
190
200
210
220
230
240
250
260
270
280
290
300
310
320
330
Conductivity Reading
(mS)
Time (s)
11.83
11.81
11.76
11.55
11.32
11.2
11.05
10.87
10.71
10.56
10.43
10.31
10.22
10.13
10.06
10
9.93
9.89
9.84
9.79
9.75
9.71
9.66
9.63
9.58
9.57
9.54
9.51
9.48
9.46
9.44
9.42
9.4
9.38
0
10
20
30
40
50
60
70
80
90
100
110
120
130
140
150
160
170
180
190
200
210
220
230
240
250
260
270
280
290
300
310
320
330
Conductivity
Reading
(mS)
1.556
1.539
1.515
1.495
1.464
1.443
1.422
1.401
1.382
1.359
1.35
1.336
1.324
1.311
1.3
1.288
1.278
1.266
1.255
1.245
1.236
1.227
1.217
1.209
1.2
1.193
1.186
1.179
1.173
1.167
1.16
1.153
1.147
1.139
340
350
360
370
380
390
400
410
420
430
440
450
460
9.36
9.34
340
350
360
370
380
390
400
410
420
430
440
450
460
1.132
1.127
1.122
1.117
1.114
1.109
1.104
1.1
1.096
1.094
1.091
1.088
1.085
10
20
30
40
50
60
70
80
90
100
110
120
130
140
150
160
170
180
190
200
210
220
230
240
250
260
270
280
290
300
3.38
3.3
3.13
3
2.9
2.82
2.76
2.7
2.65
2.61
2.57
2.53
2.48
2.47
2.44
2.42
2.39
2.37
2.35
2.34
2.32
2.31
2.3
2.28
2.27
2.26
2.25
2.23
2.22
2.21
60
70
80
90
100
110
120
130
140
150
160
170
180
190
200
210
220
230
240
250
260
270
280
290
300
2.34
2.33
2.32
2.3
2.29
2.28
2.27
2.25
2.24
2.23
2.21
2.2
2.19
2.19
2.17
2.17
2.16
2.16
2.16
2.15
2.15
2.14
2.14
2.13
2.13
*** dont use temp 33, Not good data (I think NaOH wasn't added)
Trial #2: Temp=33
Time (s)
0
10
20
30
40
50
60
70
80
90
100
110
120
130
140
150
160
170
180
190
200
210
220
230
240
250
260
270
280
290
300
(Kt - K) = B
0
3.1659
3.378
3.298
3.128
2.998
2.898
2.818
2.758
2.698
2.648
2.608
2.568
2.528
2.478
2.468
2.438
2.418
2.388
2.368
2.348
2.338
2.318
2.308
2.298
2.278
2.268
2.258
2.248
2.228
2.218
2.208
0.07
0.15
0.32
0.45
0.55
0.63
0.69
0.75
0.8
0.84
0.88
0.92
0.97
0.98
1.01
1.03
1.06
1.08
1.1
1.11
1.13
1.14
1.15
1.17
1.18
1.19
1.2
1.22
1.23
1.24
3.0959
3.0159
2.8459
2.7159
2.6159
2.5359
2.4759
2.4159
2.3659
2.3259
2.2859
2.2459
2.1959
2.1859
2.1559
2.1359
2.1059
2.0859
2.0659
2.0559
2.0359
2.0259
2.0159
1.9959
1.9859
1.9759
1.9659
1.9459
1.9359
1.9259
0
-0.07
-0.09
-0.09
-0.09
-0.09
(Kt - K) = B
1.9759
2.0459
2.0659
2.0659
2.0659
2.0659
2.338
2.328
2.318
2.298
2.288
2.278
2.268
2.248
2.238
2.228
2.208
2.198
2.188
2.188
2.168
2.168
2.158
2.158
2.158
2.148
2.148
2.138
2.138
2.128
2.128
-0.08
-0.07
-0.06
-0.04
-0.03
-0.02
-0.01
0.01
0.02
0.03
0.05
0.06
0.07
0.07
0.09
0.09
0.1
0.1
0.1
0.11
0.11
0.12
0.12
0.13
0.13
2.0559
2.0459
2.0359
2.0159
2.0059
1.9959
1.9859
1.9659
1.9559
1.9459
1.9259
1.9159
1.9059
1.9059
1.8859
1.8859
1.8759
1.8759
1.8759
1.8659
1.8659
1.8559
1.8559
1.8459
1.8459
A/B
0
(0t)/(t ) Vs Time at 29
(0t)/(t ) Vs Time at 29
0.8
(0t)/(t )
y = 0.002x + 0.1063
0.6
0.4
0.2
0
0
100
200
300
Time (in s)
0.022610549
0.049736397
0.112442461
0.165690931
0.210252686
0.248432509
0.278686538
0.310443313
0.338137707
0.361150522
0.384968721
0.409635336
0.441732319
0.44832792
0.468481841
0.482232314
0.503347737
0.517762117
0.532455588
0.539909529
0.555037084
0.562712868
0.570464805
0.586201714
0.594189033
0.602257199
0.610407447
0.626959248
0.635363397
0.643854821
Conductivity Vs Time at
299 K
4
3
2
1
0
0
100
A/B
0
-0.034214771
-0.043564548
-0.043564548
-0.043564548
-0.043564548
200
Time (in s)
100
200
300
400
Time (s)
-0.038912398
-0.034214771
-0.029470996
-0.019842254
-0.01495588
-0.010020542
-0.0050355
0.005086729
0.010225472
0.015417031
0.025961888
0.031316875
0.036728055
0.036728055
0.047722573
0.047722573
0.053307746
0.053307746
0.053307746
0.058952784
0.058952784
0.064658656
0.064658656
0.07042635
0.07042635
y = 0.0004x - 0.0497
0.05
0
-0.05
-0.1
50
100
150
200
Time (s)
250
300
350
Vs Time at 299K
Vs Time at 299K
Linear (A/B)
Linear (A/B)
300
400
ivity Vs Time at
299 K
300
Time (in s)
400
350
CSTR
Trial #1
Flowrate
#8 pump setting
initial cond (mS)
2.81
Conductivity (mS)
1.282
Time (min)
42.37
Trial #2
Flowrate
#9 pump setting
initial cond (mS)
2.88
Conductivity (mS)
2.09
Time (min)
30.15
PFR
Trial #1
Flowrate
#8 pump setting
initial cond (mS)
3.55
Conductivity (mS)
1.6
Time (min)
8.4
Trial #2
Flowrate
#9 pump setting
initial cond (mS)
3.61
Conductivity (mS)
1.8
Time (min)
9.1
PFR
Trial #1:
Flow Rate
Time (s)
0
10
20
30
40
50
60
70
80
90
100
110
120
130
140
150
160
170
180
190
200
210
220
230
240
250
260
270
280
290
300
310
320
330
340
Cond (mS)
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0.05
0.34
1.2
3.06
5.32
7.64
10.15
12.25
13.67
13.36
12.46
11.86
350
360
370
380
390
400
410
420
430
440
450
460
470
480
490
500
510
520
530
540
550
560
570
10.86
8.99
7.75
6.25
5.33
4.27
3.55
2.96
2.31
1.96
1.58
1.16
1.02
0.7
0.42
0.32
0.15
0.1
0.05
0
0