Engineering Management Support, Inc.: West Lake OU-1

ENGINEERING MANAGEMENT SUPPORT, INC.
West Lake OU-1
STANDARD LEVEL IV
REPORT OF ANALYSIS
WORK ORDER #13-04132-0R
May 24,2013
EBERLINE ANALYTICAL/OAK RIDGE LABORATORY

OAK RIDGE, TN
TABLE OF CONTENTS
SECTION
DESCRIPTION
PAGE
Chain of Custody & pH Check Sheet
0004
II
Sample Acknowledgement
0012
III
Case Narrative
0015
IV
Analytical Results Summary
0019
Analytical Standards
0025
VI
Quality Control Sample Results Summary
0049
VII
Laboratory Technician's Notes
0060
VIII
Analytical Data (Isotopic Uranium)
0098
IX
Analytical Data (Isotopic Thorium)
0247
Analytical Data (Radium-226)
0361
XI
Analytical Data (Radium-228)
0470
XII
Barium-133 Analytical Tracer Data
0488
Last Page Number
0564
STANDARD OPERATING PROCEDURE
MP...001, Rev. 12
Effective: 10131112
Sample Receiving
Page 14 of14
Eberline Services -Oak Ridge Laboratory

LABORATORY DATA SUPPORT CHECKLIST
MP-001-3
1_3_-_0_4_1_3_2___
Eberline Services Work Order # _ _ _ _ _
The checklist items listed below are to be initialed by appropriate staff upon completion/verification.
Date for Partial
Initials
Date
Initials
'1/Jrt/i:~
Checklist Items
\(C.
Sample Log-In
S-1..2- B l~
Data Compilation
I{,~74? ,__v?
First Technical Data Review
1~1~ 0
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Second Technical Data Review
t:J
Data Entry/Electronic Deliverable
)!!/
Case Narrative
~P\(f~, ~.,..-
Electronic Deliverable Proof
gf. .l 1j
f"''lf
Sample>l\AJ"'Iyzed within Holding Time

Yes?
I No? I
~ 1 1 "'-
fVV"'i
Client in Possession of Data

: or Hrd Coov
Invoiced by Laboratory
Technical/Clerical Corrections, Signatures Needed, Problems, Etc
Date/Initials
Date package approved by:
Laboratory Manager
Date
\
CopyNo. _______
Radiochemistry Services
SECTION I
CHAIN OF CUSTODY
&
pH CHECK SHEET
13-04132
REC'D APR 18 2.013
Chain of Custody Record

Project Name: ~LA
Send Report To:~J
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Ebel11ne Services
601 SCarbo!o Road
Clak Rklge, TN 37830
1604
(865) 481-0683 Phone (865) 4834621 Fax
Project Number:
Sampler (Print Name):
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Address:
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Shipment Method:
j A) /
Laboratory Receiving:
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Internal
Work Order#
13-04132
Chain of
Custody
Lab Deadline
5/9/2013
EBERLINE
- ------ --- sE Rv ,-c E: s

Oak Ridge Laboratory
Sample
Fraction
HP 210 I 270
Detector Activity
04
38
05
38
45
06
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Printed: 4/18/2013 2:30PM
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Internal
BERL,NE
Chain of
Custody
SERVICES
Comments
Re-Analysis: 2Fxns 04, 06, 08, 10, 12, 14, 16, & 18 are
TOTAL
Original Lab Deadline: 05/16/13

Rerun Lab Deadline: 05/16/13
Work Order#
13-04132
Lab Deadline
See Comments
UUISO - Level 4
Analysis
WA
Sample Matrix
Sample
Fraction
Detector Activity
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
38
38
45
45
46
46
40
40
36
36
39
39
37
37
41
41

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EBERL.INE
SERVICES
Internal
Work Order#
Chain of
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Lab Deadline
5/9/2013
ThiSO - Level 4
Analysis
Water
Sample Matrix
Sample
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Comments
HP 210
270
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04
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13-04132
---
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Ptinted: 4/18/2013 2:30 PM -
EEIERLINE
SERVICES
Internal
Work Order#
Chain of
Custod
Lab Deadline
Ra226 - Level 4
Sample
Fraction
Comments
HP 210/270
Storage
Detector Activity
Location
04 _, ..
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38
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EBERLINE
- - - - . "SE_R_V_i_CE-S
Internal
Work Order#
13-04132
Chain of
Custody
Lab Deadline
5/9/2013
Water
Sample Matrix
Sample
Comments
",
04
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06
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Printed: 4118/2013 2:30 PM
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Page 1 of 1
Printed: 4/18/2013 1:00 PM
Internal Work Order
(Volumes, pH, & CPM)
SERVICES
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13-04132
Sample Receiving Report
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Date:
LJ/Is/1~
MP-001, Rev 5
Effective: 11/22/02
'n!{i 11
SECTION II
SAMPLE ACKNOWLEDGEMENT
B!U2
f_lient Name
Contract/
Po
Engineering Management Support, Inc.; West Lake OU-11

__ ,__ _
Prol!.c.!..~ame
----
lntemaiiD
Client\0
Date Received
sample Disp
ClientWO
West Lake OU-1
PojootT~---0--4--/18/2013
environmental
----,--
West Lake OU-1 i
Sample Date I Matrix
Storage
05/o9i2"o13
rolo~
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& "'~
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~~
-+---'Rc0quir~_d Turnaround Days
28
13-04132
-~--- o5/'1"5/2o'13
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05/16/2013
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04/18/13
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04/18/13
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04/18/13
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04/12/1311:18
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04/12/1311:18
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04/16/13 08:40
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04/16/13 08:40
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04/16/13 09:oo
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Totals Per Analysis (non QA samples)
1611616:16
Invoice
E: B
I;; R I..., IN
g:
SERVICES
I Oak Ridge Laboratory

601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: (865) 481-0683
Fax:
(865) 483-4621
olo
olo
I
Report Data
Paul V_ Rosasco, P.E.
7220 W.,;t Jelleroon Avenue.
"'
Contact
303-640--3426
lyn Fitzgerald
0
Paul
1 0
V. Rosasco, P.E.
Engineering Management Support. Inc

7220 West Jefferson Ave, Su~e 406
Su~e 406
lakewood, CO 80235
lakewood, CO 80235
Voice
Engineering Management Support, tnc
Vcice
Sample Log In Report
Voice
303-940-3426
'"
/303-601.--4255
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Printed: 4/18/2013 2:30 PM
STANDARD OPERATING PROCEDURE
MP-001, Rev.12
Effective: 10131112
Page 13 of14
Sample Receiving
Eberline Services- Oak Ridge Laboratory
WORK ORDER# _
SAMPLE RECEIPT CHECKLIST

MP-001-2
____,_1-=._3_-_0_4_1_3_2
SAMPLE MATRIX/MATRICES:
(CIRCLE ONE OR BOTH)

(/\QuEOUS')
NON-AQUEOUS
(CIRCLE EITHER YES, NO, OR N/A)

WERE SAMPLES
Received in good condttion?
1_]
Present on outside of package?
Y)
Unbroken on outside of package?
'()
Present on samples?
!'{)
Unbroken on samples?
Was chain of custody present upon sample receipt?
(y)
If aqueous, properly preserved
N/A
WERE CHAIN OF CUSTODY SEALS
IF THE RESPONSE TO ANY OF THE ABOVE IS NO, A DISCREPANT SAMPLE RECEIPT REPORT
(DSR) HAS BEEN ISSUED.
REMARKS:----------------------------
SIGNATURE:
Copy No. _ _ __
d<ol~.t\~
DATE:
q/18/1]
Radiochemistry SeJVices
SECTION III
CASE NARRATIVE
l\li.il15
~EBERLINE
EBERLINE ANALYTICAL CORPORATION

601 SCARBORO ROAD
OAK RIDGE, TENNESSEE 37830
PHONE (865) 481-0683
SERVICES
FAX (865) 483-4621
EBS-OR-35599
May 24,2013
Paul V. Rosasco, P.E.
Engineering Management Support, Inc.
7220 West Jefferson Ave, Suite 406
Lakewood, CO 80235
CASE NARRATIVE
Work Order# 13-04132-0R
SAMPLE RECEIPT
This work order contains eight water samples received 04/18/2013. All samples were analyzed as total
and dissolved for Isotopic Uranium, Isotopic Thorium and Radium-226/228.
CLIENTID
LABID
CLIENTID
LAB lD
D-14 TOT
D-14 DIS
PZ-112-AS TOT
PZ-112-AS DIS
PZ-202-SS TOT
PZ-202-SS DIS
DUP07TOT
DUP07 DIS
13-04132-04
13-04132-05
13-04132-06
13-04132-07
13-04132-08
13-04132-09
13-04132-10
13-04132-11
PZ-106-KS TOT
PZ-106-KS DIS
FB at PZ-100-KS TOT
FB at PZ-100-KS DIS
PZ-100-KS TOT
PZ-100-KS DIS
S-53 TOT
S-53 DIS
13-04132-12
13-04132-13
13-04132-14
13-04132-15
13-04132-16
13-04132-17
13-04132-18
13-04132-19
ANALYTICAL METHODS
Isotopic Uranium and Isotopic Thorium were analyzed using Method HASL 300, 4.5.2. Radium-226 was
analyzed using Method EPA 903.0. Radium-228 was analyzed using Method EPA 904.0.
Laboratory qualifiers are as follows:
J-
Indicates a situation where the result minus the error is less than the detection limit but greater
than zero.
U-
Indicates a situation where the result minus the error is less than or equal to zero.
ANALYTICAL RESULTS
Combined Standard Uncertainty is reported at 2-sigma value.
Page I of3
ANALYTICAL RESULTS CONTINUED

ISOTOPIC URANIUM
Samples were filtered to disassociate dissolved and total fractions. All samples were prepared by mixed
acid digestions as appropriate. Uranium was selectively extracted by ion exchange. Uranium was eluted,
micro-precipitated and mounted on micro-porous filter media. Sample activities were then determined by
alpha spectroscopy using energy specific regions of interest for Uranium-234, Uranium-235 and
Uranium-238. Chemical recovery was determined by the use of a Uranium-232 tracer. Activity of the
Uranium-232 tracer was determined by alpha spectroscopy using an energy specific region of interest.
I" Analytical Attempt
Samples demonstrated acceptable results for all Uranium analyses. Chemical recovery was slightly low
for sample fractions -05, -06, -07 and -18 (Client IDs: D-14 DIS, PZ-112-AS TOT, PZ-112-AS DIS and
S-53 TOT, respectively). Chemical recovery was acceptable for all other samples. The Uranium-234,
Uranium-235 and Uranium-238 method blank demonstrated acceptable results. Results for the Uranium234 and Uranium-238 duplicate demonstrated an acceptable relative percent difference and normalized
difference. Results for the Uranium-235 duplicate demonstrated a high relative percent difference;
however, normalized difference is within acceptable limits for the analytical technique. Results for the
Uranium-234 and Uranium-238 laboratory control sample demonstrated an acceptable percent recovery.
2"d Analytical Attempt
Sample fractions -05, -06, -07 and -18 (Client IDs: D-14 DIS, PZ-112-AS TOT, PZ-112-AS DIS and S53 TOT, respectively) were reanalyzed due to low chemical recoveries. Samples demonstrated
acceptable results for all Uranium analyses. Due to interferences chemical recovery was low for sample
fraction -18 (Client ID: S-53 TOT). Chemical recovery was acceptable for all other samples. The
Uranium-234, Uranium-235 and Uranium-238 method blank demonstrated acceptable results. Results for
the Uranium-234, Uranium-235 and Uranium-238 duplicate demonstrated a high relative percent
difference; however, normalized difference is within acceptable limits for the analytical technique.
Results for the Uranium-234 and Uranium-238 laboratory control sample demonstrated an acceptable
percent recovery.
ISOTOPIC THORIUM
acid digestions as appropriate. Thorium was selectively extracted by ion exchange. Thorium was eluted,
micro-precipitated and mounted on micro-porous filter media. Sample activities were then determined by
alpha spectroscopy using energy specific regions of interest for Thorium-228, Thorium-230 and Thorium232. Chemical recovery was determined by the use of a Thorium-229 tracer. Activity of the Thorium229 tracer was determined by alpha spectroscopy using an energy specific region of interest.
Samples demonstrated acceptable results for all Thorium analyses. Chemical recovery was acceptable for
all samples. The Thorium-228, Thorium-230 and Thorium-232 method blank demonstrated acceptable
results. Results for the Thorium-228 and Thorium-230 duplicate demonstrated a high relative percent
difference; however, normalized difference is within acceptable limits for the analytical technique.
Results for the Thorium-232 duplicate demonstrated an acceptable relative percent difference and
normalized difference. Results for the Thorium-228, Thorium-230 and Thorium-232 laboratory control
sample demonstrated an acceptable percent recovery.
Page 2 of3
ANALYTICAL RESULTS CONTINUED

RADIUM-226
acid digestions as appropriate. This was followed by selective sulfate precipitations of the Radium.
Samples were then mounted by semi-micro-precipitations onto micro-porous filters. Samples were
counted by alpha spectroscopy using an energy specific region of interest for Radium-226. Chemical
recovery was calculated by the use of a Barium-13 3 tracer, which was determined by HPGe gamma
spectroscopy.
Samples demonstrated acceptable results for all Radium-226 analyses. Due to interferences chemical
recovery was low for sample fraction -18 (Client ID: S-53 TOT). Chemical recovery was acceptable for
all other samples. The Radium-226 method blank demonstrated acceptable results. Results for the
Radium-226 duplicate demonstrated a high relative percent difference; however, normalized difference is
within acceptable limits for the analytical technique. Results for the Radium-226 laboratory control
RADIUM-228
Following alpha spectroscopy analysis of Radium-226, Barium/Radium Sulfate preCipitates were
redissolved and allowed for sufficient ingrowth of the Actinium-228 daughter. After ingrowth, Actinium228 was selectively precipitated. Precipitates were filtered and beta emissions for Actinium-228 were
then counted on a gas proportional counter. Chemical recovery was determined by the use of a Barium133 tracer, the activity of which was determined by HPGe gamma spectroscopy and an elemental Yttrium
carrier by gravimetric measurements. The product of these two recoveries was used to calculate chemical
yield.
Samples demonstrated acceptable results for all Radium-228 analyses. Due to interferences chemical
recovery was low for sample fraction -18 (Client ID: S-53 TOT). Chemical recovery was acceptable for
all other samples. The Radium-228 method blank demonstrated acceptable results. Results for the
Radium-228 duplicate demonstrated a high relative percent difference; however, normalized difference is
within acceptable limits for the analytical technique. Results for the Radium-228 laboratory control
CERTIFICATION OF ACCURACY
I certifY that this data report is in compliance with the terms and conditions of the Purchase Order, both
technically and for completeness, for other than the conditions detailed above. Release of the data
contained in this hard copy data package has been authorized by the cognizant project manager or his/her
designee to be accurate as verified by the following signature.
M.R. McDougall
Laboratory Manager
Date: 5/24/2013
Eberline Analytical wants and encourages your feedback regarding our performance providing radioanalytical services. Please
visit http://www.eberlineservices.com/client.htm to provide us with feedback on our services.
Page 3 of3
SECTION IV
ANALYTICAL RESULTS SUMMARY
Paul V. Rosasco, P .E.

Lakewood, CO 80235
Client Sam ole 10
l:ii!l
I;!~
N1
Project: West Lake OU-1

SDG: 1304132
Received: 04/18/2013
Matrix: Water
Lab Sam ole 10
Analvsis Date/Time
Analvte
LCS13-04132-01
LCS13-04132-01
LCS13-04132-01
LCS13-04132-01
LCS13-04132-01
LCS13-04132-01
LCS13-04132-01
LCS13-04132-01
LCS13-04132,01
LCS13-04132-01
LCS13-04132-01
13-04132-01
13-04132-01
13-04132-01
13-04132-01"
13-04132-01
13-04132-01
13-04132-01
13-04132-01
13-04132-01
13-04132-01
13-04132-01
05/15/2013 16:51 :46

05/21/201313:47:17
05/09/2013 16:28:50
05/09/2013 16:28:50
05/09/2013 16:28:50
05/09/2013 09:57:46
05/16/2013 12:25:05
05/09/2013 09:57:46
05/16/2013 12:25:05
05/09/2013 09:57:46
05/16/2013 12:25:05
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-234
Uranium-235
Uranium-235
Uranium-238
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
BLANK13-04132-02
BLANK13-04132-02
BLANK13-04132-02
BLANK13-04132-02
BLANK13-04132-02
BLANK13-04132-02
BLANK13-04132-02
BLANK13-04132-02
BLANK13-04132-02
BLANK13-04132-02
BLANK13-04132-02
13'04132-02
13-04132-02
13-04132-02
13-04132-02
13-04132-02
13-04132-02
13-04132-02
13-04132-02
13-04132-02
13-04132-02
13-04132-02
05/15/2013 16:51:43
05/21/2013 13:46:21
05/09/2013 16:28:52
05/09/2013 16:28:52
05/09/2013 16:28:52
05/09/2013 09:57:48
05/16/2013 15:38:27
05/09/2013 09:57:48
05/16/2013 15:38:27
05/09/2013 09:57:48
05/16/2013 15:38:27
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-234
Uranium-235
Uranium-235
Uranium-238
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
FB at PZ-1 00-KS TOT DUP

FB at PZ-1 00-KS TOT DUP
PZ-106-KS TOT DUP
PZ-1 06-KS TOT DUP
PZ-1 06-KS TOT DUP
PZ-106-KS TOT DUP
PZ-112-AS TOT DUP
PZ-106-KS TOT DUP
PZ-112-AS TOT DUP
PZ-1 06-KS TOT DUP
PZ-112-AS TOT DUP
13-04132-03
13-04132-03
13-04132-03
13-04132-03
13-04132-03
13-04132-03
13-04132-03
13-04132-03
13-04132-03
13-04132-03
13-04132-03
05/15/201316:51:43
05/21/2013 13:46:21
05/09/2013 16:28:46
05/09/201316:28:46
05/09/2013 16:28:46
05/09/2013 09:57:42
05/16/2013 15:38:28
05/09/2013 09:57:42
05/16/2013 15:38:28
05/09/2013 09:57:42
05/16/2013 15:38:28
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-234
Uranium-235
Uranium-235
Uranium-238
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
EBERh~~c~
Final Report of Analysis

Date: 5/24/2013
Page 1 of 5
Method
Result
Error
MDA
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
10.38
9.46
4.62
4.48
4.53
7.58
7.45
0.56
0.68
7.55
7.76
1.25
2.03
0.69
0.68
0.68
1.14
1.00
0.22
0.22
1.13
1.04
0.23
2.04
0.12
0.07
0.06
0.11
0.10
0.10
0.10
0.15
0.08
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.03
0.39
0.03
0.27
-0.02
0.06
0.06
0.09
0.06
0.04
0.01
O.Q7
0.34
O.Q7
0.15
0.04
0.09
0.08
0.11
0.09
0.07
0.04
0.15
0.69
0.14
0.13
0.11
0.13
0.14
0.13
0.14
0.12
0.10
4.5.2
4.5.2
4.5.2
4.5 ..2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.05
0.57
0.03
0.28
0.04
2.19
0.12
0.21
0.21
0.78
0.07
O.Q7
0.38
0.07
0.13
0.05
0.41
0.21
0.12
0.25
0.22
0.17
0.13
0.74
0.13
0.08
0.08
0.06
0.37
O.Q7
0.30
0.08
0.35

601 SCARBORO ROAD OAK RIDGE, TN 37830
865/481-0683
FAX 865/483-4621
Qualifier
Units
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
u
J
u
J
u
u
u
u
u
u
u
u
J
u
u
u
u
u
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1

Lakewood, CO 80235
Client Sam ole ID
Ia
1\ll
~... m.
Lab Sam ole ID Analvsis Date/Time
Analvte
13-04132-04
13-04132-04
13-04132-04
13-04132-04
13-04132-04
13-04132-04
13-04132-04
13-04132-04
05/15/201316:51:44
05/21/201313:46:22
05/09/2013 16:28:47
05/09/2013 16:28:47
05/09/2013 16:28:47
05/09/2013 09:57:44
05/09/2013 09:57:44
05/09/2013 09:57:44
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
D-14
D-14
D-14
D-14
D-14
D-14
D-14
D-14
13-04132-05
13-04132-05
13-04132-05
13-04132-05
13-04132-05
13-04132-05
13-04132-05
13-04132-05
05/15/2013 16:51 :45

05/21/2013 13:46:22
05/09/2013 16:28:48
05/09/2013 16:28:48
05/09/2013 16:28:48
05/16/2013 15:38:29
05/16/2013 15:38:29
05/16/201315:38:29
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
PZ-112-AS TOT
PZ-112-AS TOT
PZ-112-AS TOT
PZ-112-AS TOT
PZ-112-AS TOT
PZ-112-AS TOT
PZ-112-AS TOT
PZ-112-AS TOT
13-04132-06
13-04132-06
13-04132-06
13-04132-06
13-04132-06
13-04132-06
13-04132-06
13-04132-06
05/15/2013
05/21/2013
05/09/2013
05/09/2013
05/09/2013
05/16/2013
05/16/2013
05/16/2013
16:52:11
13:46:26
16:28:49
16:28:49
16:28:49
15:38:30
15:38:30
15:38:30
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
PZ-112-AS
PZ-112-AS
PZ-112-AS
PZ-112-AS
PZ-112-AS
PZ-112-AS
13-04132-07
13-04132-07
13-04132-07
13-04132-07
13-04132-07
13-04132-07
13-04132-07
13-04132-07
05/15/2013 16:52:12
05/21/2013 13:46:26
05/09/2013 16:29:24
05/09/2013 16:29:24
05/09/2013 16:29:24
05/16/2013 11:43:37
05/16/201311:43:37
05/16/2013 11 :43:37
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
DIS
DIS
DIS
DIS
DIS
DIS
DIS
DIS
4:EBERLINE
SERVICES

Date: 5/24/2013
Page 2 of 5
Method
D-14 TOT
D-14 TOT
D-14 TOT
D-14 TOT
D-14 TOT
D-14 TOT
D-14 TOT
D-14 TOT
DIS
DIS
DIS
DIS
DIS
DIS
PZ~112-AS DIS
PZ-112-AS DIS
!l~

SDG: 1304132
Matrix: Water
Result
Error
MDA
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
1.97
1.74
0.99
1.15
1.17
0.75
-0.02
1.05
0.46
0.55
0.28
0.30
0.30
0.39
0.11
0.47
0.17
1.00
0.12
0.05
O.Q7
0.26
0.26
0.18
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.79
1.39
0.05
0.16
0.00
0.27
0.21
0.71
0.30
0.45
O.Q7
0.10
0.03
0.59
0.50
0.82
0.22
0.80
0.12
0.08
0.06
1.15
1.05
1.07
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.95
2.24
0.11
0.19
0.05
0.08
0.06
0.09
0.38
0.50
0.11
0.11
O.Q7
0.24
0.17
0.19
0.17
0.84
0.16
0.10
0.10
0.51
0.40
0.38
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.74
1.05
0.01
0.20
O.o3
0.26
0.00
0.27
0.31
0.44
0.08
0.13
0.06
0.27
0.23
0.30
0.16
0.82
0.17
0.10
0.12
0.28
0.50
0.41

865/481-0683
FAX 865/483-4621
Qualifier
u
J
u
u
u
u
u
J
u
u
u
u
J
u
J
u
u
u
u
Units
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1

Lakewood, CO 80235
Client Sample ID
ti'&
~~~
1\ll

SDG: 1304132
Matrix: Water
Lab Sample ID
Analvsis Date/Time
Analvte
PZ-202-SS TOT
PZ-202-SS TOT
PZ-202-SS TOT
PZ-202-SS TOT
PZ-202-SS TOT
PZ-202-SS TOT
PZ-202-SS TOT
PZ-202-SS TOT
13-04132-08
13-04132-08
13-04132-08
13-04132-08
13-04132-08
13-04132-08
13-04132-08
13-04132-08
05/15/201316:52:14
05/21/2013 13:46:26
05/09/2013 16:29:25
05/09/2013 16:29:25
05/09/2013 16:29:25
05/09/2013 12:54:35
05/09/2013 12:54:35
05/09/2013 12:54:35
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
PZ-202-SS DIS
PZ-202-SS DIS
PZ-202-SS DIS
PZ-202-SS DIS
PZ-202-SS DIS
PZ-202-SS DIS
PZ-202-SS DIS
PZ-202-SS DIS
13-04132-09
13-04132-09
13-04132-09
13-04132-09
13-04132-09
13-04132-09
13-04132-09
13-04132-09
05/15/2013
05/21/2013
05/09/2013
05/09/2013
05/09/2013
05/09/2013
05/09/2013
05/09/2013
16:52:16
13:46:27
16:29:26
16:29:26
16:29:26
12:54:36
12:54:36
12:54:36
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
DUP07TOT
DUP07TOT
DUP07TOT
DUP07TOT
DUP07TOT
DUP07TOT
DUP07TOT
DUP07TOT
13-04132-10
13-04132-10
13-04132-10
13-04132-10
13-04132-10
13-04132-10
13-04132-10
13-04132-10
05/15/201316:52:17
05/21/201313:46:21
05/09/2013 16:29:27
05/09/2013 16:29:27
05/09/2013 16:29:27
05/09/201312:55:17
05/09/2013 12:55:17
05/09/2013 12:55:17
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
DUP07 DIS
DUP07 DIS
DUP07 DIS
DUP07 DIS
DUP07 DIS
DUP07 DIS
DUP07 DIS
DUP07 DIS
13-04132-11
13-04132-11
13-04132-11
13-04132-11
13-04132-11
13-04132-11
13-04132-11
13-04132-11
05/15/2013
05/21/2013
05/09/2013
05/09/2013
05/09/2013
05/09/2013
05/09/2013
05/09/2013
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
~EBERLINE
SERVICES
16:52:19
13:46:21
16:29:28
16:29:28
16:29:28
12:55:19
12:55:19
12:55:19

Date: 5/24/2013
Page 3 of 5
Result
Error
MDA
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.85
0.69
0.16
0.39
0.10
1.69
0.13
0.78
0.30
0.44
0.11
0.17
0.08
0.34
0.09
0.21
0.15
0.86
0.13
0.10
0.09
O.Q7
0.09
0.08
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.38
0.86
0.10
0.13
0.01
1.62
0.05
0.63
0.20
0.41
0.09
0.09
0.03
0.32
0.06
0.18
0.17
0.78
0.11
0.08
0.06
0.05
0.06
0.05
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.11
1.80
0.10
0.10
0.01
0.16
-0.01
0.03
0.81
0.65
0.08
0.08
0.03
0.16
0.10
0.08
0.21
1.20
0.10
0.09
0.06
0.17
0.21
0.17
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
2.31
2.47
-0.01
0.11
-0.01
0.23
0.04
0.13
0.60
0.56
0.04
0.08
0.03
0.19
0.12
0.14
0.21
0.95
0.11
O.Q7
O.Q7
0.17
0.26
0.15
Method

865/481-0683
FAX 865/483-4621
Qualifier
J
J
J
J
J
J
J
u
u
J
J
J
u
u
u
u
u
J
u
J
u
u
Units
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1

Lakewood, CO 80235
Client Sample ID
(dl\~
Analyte
05/15/2013
05/21/2013
05/09/2013
05/09/2013
05/09/2013
05/09/2013
05/09/2013
05/09/2013
16:52:20
13:46:21
16:29:29
16:29:29
16:29:29
12:55:21
12:55:21
12:55:21
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
PZ-106-KS
PZ-106-KS
PZ-106-KS
PZ-106-KS
PZ-106-KS
PZ-1 06-KS
PZ-106-KS
PZ-106-KS
13-04132-13
13-04132-13
13-04132-13
13-04132-13
13-04132-13
13-04132-13
13-04132-13
13-04132-13
05/15/2013 16:52:22
05/21/201313:46:22
05/09/2013 16:29:59
05/09/2013 16:29:59
05/09/2013 16:29:59
05/09/2013 12:55:23
05/09/2013 12:55:23
05/09/2013 12:55:23
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
13-04132-14
13-04132-14
13-04132-14
13-04132-14
13-04132-14
13-04132-14
13-04132-14
13-04132-14
05/15/2013
05/21/2013
05/09/2013
05/09/2013
05/09/2013
05/09/2013
05/09/2013
05/09/2013
16:52:24
13:47:07
16:30:00
16:30:00
16:30:00
12:55:25
12:55:25
12:55:25
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
13-04132-15
13-04132-15
13-04132-15
13-04132-15
13-04132-15
13-04132-15
13-04132-15
13-04132-15
05/15/2013
05/21/2013
05/09/2013
05/09/2013
05/09/2013
05/09/2013
05/09/2013
05/09/2013
16:52:25
13:47:07
16:29:55
16:29:55
16:29:55
12:55:28
12:55:28
12:55:28
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
DIS
DIS
DIS
DIS
DIS
DIS
DIS
DIS
at PZ-1 00-KS TOT

at PZ-1 00-KS TOT
at PZ-100-KS TOT
at PZ-100-KS TOT
at PZ-100-KS TOT
at PZ-100-KS TOT
at PZ-100-KS TOT
at PZ-1 00-KS TOT
EBERh~~c~

Date: 5/24/2013
Page 4 of 5
Result
Error
MDA
Qualifier
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.38
0.31
-0.01
0.09
0.04
2.25
0.07
0.86
0.20
0.43
0.04
0.08
0.05
0.40
0.16
0.89
0.12
0.09
u
u
O.D7
O.D7
0.05
0.09
0.22
O.D7
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.32
0.43
0.04
0.16
0.01
2.02
0.09
0.73
0.19
0.43
0.05
0.10
0.04
0.37
0.08
0.20
0.15
0.87
0.08
0.06
0.09
0.06
0.09
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.00
0.19
0.04
0.18
0.00
0.08
0.04
0.06
0.07
0.45
0.05
0.10
0.03
0.07
0.05
0.06
0.17
0.94
0.06
0.06
0.05
0.08
0.07
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.00
0.56
-0.01
0.17
0.00
0.07
0.04
-0.02
0.05
0.39
0.03
0.10
0.04
0.06
0.05
0.03
0.10
0.77
0.08
0.06
0.08
Method
13-04132-12
13-04132-12
13-04132-12
13-04132-12
13-04132-12
13-04132-12
13-04132-12
13-04132-12
FB at PZ-100-KS DIS
FB at PZ-100-KS DIS
FB at PZ-100-KS DIS
FB at PZ-1 00-KS DIS
FB at PZ-100-KS DIS
FB at PZ-100-KS DIS
1'\)
Analysis Date/Time
PZ-106-KS TOT
PZ-106-KS TOT
PZ-106-KS TOT
PZ-106-KS TOT
PZ-106-KS TOT
PZ-106-KS TOT
PZ-106-KS TOT
PZ-106-KS TOT
FB
FB
FB
FB
FB
FB
FB
FB
lt!lt
'1.!#
Lab Sample ID

SDG: 1304132
Matrix: Water
865/481-0683
u
u
J
u
J
O.D7
O.D7
O.D7
0.06
0.10

FAX 865/483-4621
u
u
u
u
J
u
u
u
J
u
u
J
u
u
Units
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1

Lakewood, CO 80235
Client Sample ID
l;ll~
t!!lr
~~~:II
$.~.
Lab Sample ID

SDG: 1304132
Matrix: Water
Analvsis Date/Time
Analvte
Method
PZ-100-KS TOT
PZ-100-KS TOT
PZ-100-KS TOT
PZ-1 00-KS TOT
PZ-100-KS TOT
PZ-100-KS TOT
PZ-100-KS TOT
PZ-100-KS TOT
13-04132-16
13-04132-16
13-04132-16
13-04132-16
13-04132-16
13-04132-16
13-04132-16
13-04132-16
05/15/2013
05/21/2013
05/09/2013
05/09/2013
05/09/2013
05/09/2013
05/09/2013
05/09/2013
16:52:27
13:47:08
16:29:57
16:29:57
16:29:57
12:55:30
12:55:30
12:55:30
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
PZ-1 00-KS
PZ-100-KS
PZ-1 00-KS
PZ-100-KS
PZ-100-KS
PZ-100-KS
PZ-100-KS
PZ-1 00-KS
13-04132-17
13-04132-17
13-04132-17
13-04132-17
13-04132-17
13-04132-17
13-04132-17
13-04132-17
05/15/2013
05/21/2013
05/09/2013
05/09/2013
05/09/2013
05/09/2013
05/09/2013
05/09/2013
16:52:29
13:47:09
16:30:07
16:30:07
16:30:07
12:55:33
12:55:33
12:55:33
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
S-53 TOT
S-53 TOT
S-53 TOT
S-53 TOT
S-53 TOT
S-53 TOT
S-53 TOT
S-53 TOT
13-04132-18
13-04132-18
13-04132-18
13-04132-18
13-04132-18
13-04132-18
13-04132-18
13-04132-18
05/15/201316:52:31
05/21/2013 13:47:31
05/09/2013 16:30:03
05/09/2013 16:30:03
05/09/2013 16:30:03
05/16/2013 15:38:31
05/16/201315:38:31
05/16/201315:38:31
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
S-53 DIS
S-53 DIS
S-53 DIS
S-53 DIS
S-53 DIS
S-53 DIS
S-53 DIS
S-53 DIS
13-04132-19
13-04132-19
13-04132-19
13-04132-19
13-04132-19
13-04132-19
13-04132-19
13-04132-19
05/15/2013 16:52:33
05/21/201313:47:32
05/09/2013 16:30:05
05/09/2013 16:30:05
05/09/2013 16:30:05
05/09/2013 12:55:39
05/09/2013 12:55:39
05/09/2013 12:55:39
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
DIS
DIS
DIS
DIS
DIS
DIS
DIS
DIS
EBERh~~c~

Date: 5/24/2013
Page 5 of5
Result
Error
MDA
Qualifier
Units
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.16
0.84
0.09
0.39
0.03
0.16
0.03
0.06
0.14
0.54
0.08
0.17
0.05
0.09
0.04
0.06
0.12
1.05
0.08
0.07
0.09
0.07
0.07
0.06
J
J
J
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.26
0.96
0.02
0.08
0.00
0.07
0.01
0.10
0.16 .
0.38
0.04
0.07
0.03
0.06
0.03
0.07
0.14
0.69
0.09
0.06
0.06
0.05
0.06
0.07
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.14
-2.53
19.95
19.58
19.05
45.30
11.37
53.49
0.31
4.71
3.92
3.85
3.75
19.89
7.53
22.91
0.62
10.29
0.12
0.13
0.18
3.63
4.81
3.29
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.84
1.46
0.03
0.22
0.11
5.90
0.40
4.74
0.33
0.62
0.05
0.12
0.08
0.82
0.16
0.69
0.14
1.15
0.09
0.07
O.Q7
0.07
0.08
0.05

601 SCARBoRo RoAD OAK RIDGE, TN 37830
865/481-0683
FAX 865/483-4621
u
.u
u
J
J
u
J
u
J
u
J
u
u
u
J
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
SECTIONV
ANALYTICAL STANDARDS
1i!lll25
Radionuclide:
U-238NAT
Half Life:
(4.468 0.005) x 109 years
Catalog No.:
7338
Source No.:
479-50
Customer:
TMA BBERLlNE
P.O.No.:
OR2778
Reference Date:
January 1 1995
12:00 PST.
Contained Radioactivity: (Total U) 8.016 ICi
Cnntained Radioactivity: (Total U) 297 kBq
Description of Solution
a. Mass of solution:
b. Chemical form:
c. Carrier content:
65.2896 gin a SO ml flame sealed ampoule

Uranyl Nitrate in H20
None
d. Density:
Approximately 1.3202
Radioimpurities
Refer to attached technical data sheet
Radioactive Daughters
Refer to attached technical data sheet
,-,
Radionuclide Concentration
'.
(Total U) 0.1228
.:.
f.LCi/g.
Method of Calibration
,,,, :.-
' _.,.
,-;;-_,-,
-Activity calculations are based upon known specific activity and mass.
--.
-:."
. >.;-.-
___
.-.. ,.,_________
Uncertainty of Measurement
a. Systematic uncertainty in instrument calibration:
b. Random uncertainty in assay:
-,._.
3.0%
0.0%
2.0%
3.6%
c. Random uncertainty in weighing(s):

d. Total uncertainty at the 99% confidence level:
NIST Traceability
This calibration is implicitly traceable to the National Institute of Standards and Teclmology.
Leak Test(s)
'
'
,,
.,_,:
See reverse side for Leak Test(s) applied to this source.

Notes
1. Nuclear data were taken from "Table of Radioactive Isotopes", edited by Virginia S. Shirley, 1986.
2. IPL participates in an NIST measurement a&SUrance prognun to e&ta.bliah and maintain implicit traceability for a Dumber of nuclides,
based on the blind assay (and later NIST certification) of Standard Reference Materials (As in NRC Regulatory Guide 4.15).
Ei$(1:/ AuA-7
YCONTROL
ISOTOPE PRODUCTS LA BORATORIES

3017 N. SAN FERNANDO BLVD.
_,
BuRBANK, CALIFORNIA
91504
818 8437000
818 8436168
FAX
'
,,,,_" .-.-
.... ....
_,
.;;.
-._,_
,.
,--,
...
'.,_.
._,,_, ..
;': ;- ~ ;-. ;:::. <,t;::~~~--5':~:1.2S'-.'_ _

. \
..
QUALITY CONTROL PROGRAM

MP-009
Rev.8; 11/01/03
Title: Radioactive Reference Standards Solutions & Records
RIDGE
RADIOACTIVE REFERENCE SOLUTIONS
PRIMARY DILUTION RECERTIFICATION
MP009
Reference Date!.
Ampoule /Solution Gross

9'7.:6400
Empty Ampoule < 32:5020
Solution Net
65.1380
8.0160
Total Activity in Ampoule
'111tf99.5
O:ool
Weight, Grams
Weight, Grams
Weight, Grams
1>CI
Chemical Com osition of Standard Solution
IDilution Instructions:
Dilution Solvent Used
Dilute to a volume ofj 1000:00
Certified Total Activity ofj
. . ;I
1.MHNO.
' _.3
1
Imilliliters
Which Eauals
1.780E+07jdpm at the date listed above

This activity concentration Is based on the original
And after dilution the activity of this solution is 1.77955E+D4Idpm/ml-eterenco date listed above: All activities are corrected
to the date and time of analysis by the laboratory data
processing software.
Expiration Date: September 6, 2013
Date: _ _:91=:26:::.;12::.:0:..:.1::.2,:::0:::::;00:::.
Date: --'i'l/c.::u.:=.r/c....;,"2....__
PROGRAM
~!;;; BER_h~!::'.!ii I QUALITY CONTROL
MP.OOS
Rev.8; 11/01103
Trtle: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES OAK RIDGE LABORATORY

RADIOACTIVE REFERENCE STANDARD SOLUTIONS
SECONDARY DILUTION RECERTIFICATION
,. ...
~Life, rears
:
Date
Half Life, lays
1""-'4:
!I
'I
Radionuclide oflnteresf,?~:~i:J
Parent Solution Cone. 1:7796E+04':. dpmlml
Reference Date
Chemical ComPOsition of Standard Solution

luraiWNitrat!iir1~HN03
Instructions:
!0:001
'#I:.,. . uc la< .-......... ,
.... I
"' -1t1i199s o:oo
11MHN03'
.. I
..
SECONDARY VOLUMETRIC DILUTION
Vol. Parent Solution: .: :;,;:, "4:oooo ml

Total Activity: 7.1182E+04 dpm
Final Volume:
1000;00 ml
7 .1182E+011 dpmtml
Final Activity Concentration:!
This activity concentration is based on the original

reference date listed above. All activities are
corrected to the date and time of analysis by the
data processing software.
NOTES:
..
as:
% =48.239 U-238 = 71.182 dpm/ml X 0.4!12<19 34.345 dpmlml
[lJ-~35 Atom % = 2.25
U-235 =71.182 dpm/miX 0.0225 = 1.602 dpm/ml
lu-234 Atom%= 49.501 U-238 = 71.182 dpm/ml X 0.<19501 = 35.236 dpm/ml
';_:;.;; ,
3.6%
Expiration Date:! September 6, 2013
Isotopic ratios from manufacturer's data sheet
~
Verified & Approved By
QCApproval
1'\
~.~~
)---......
-~tlit.AlU 1\
Date:
9/26/2012 0:00
Date:
ttft..f# 1,.-z.
I
.RECORD COPY
Tracer Solution for Environmental Analysis & Disequilibrium Studies
'
Product Description & Measurement Certificate

Description
Principal radionuclide:
Daughter Nuclide:
Measurement
Reference date:
Radioactive concentration U-232
which is equivalent to
01 March 2000
6.739E+03 becquerels per gram of solution
1.821~1 microcwies per gram of solution
Volume of solution
Total activity ofU-232
which is equivalent to
5.035 millilitres
3.6JE+04 becquerels
9.76~1 microcwies
Accuracy
Radionuclidic
Purity
uranium 232 (U-232)

Th-228
Product code: UDPl 0050

Batch Number: 921232/67
Method ofmeasurement (see reverse of this certificate)

Systematic uncertainty: 0.5%
Random uncertainty is: 0. 7%
Overall uncertainty in the radioactive concentration quoted above: 1.7%
Overall uncertainty is defined on the reverse of this certificate.
Any radioactive impwities measured are listed below, expressed as percentages
of the activity of the principle radionuclide at the referenc<> date .
Th-228 and daughter activity removed 2 Fe\12000
U-232 daughters activity will increase with time. By alpha 88% U-232, 12% daughters on 113/00
~ne
Isotopic
Purity
isotopic composition, expressed as atom per cent at the reference date .
1'iot measured
Chemical
Composition
Calculated weight ofU-232, 4.42E-08 grams, as 2M HN03 solution in a flame sealed glass vial.
This Tracer solution has been produced 'carrier free'.
Physical
Data
Recommended ha1flife of uranium 232: 6.980E+Ol years

Principle energies of alpha emissions (MeV): 5.263 31.7%, 5.320 68.0%
Branching ratio for alpha emission: I 00%
Calculated specific activity of uranium 232: 8.167E+OS Bq per microgram U-232.
Remarks
For safety information and notes to ensure correct usage by all persons handling this radio'lc!ive Tracer
solution please read the instructions accompanying the package.
ABA Technology operates a quality management system which has been independently audited and
approved to ISO 9001.
Approved
Signatory
Project Ref. AE2315
Roger Wiltshire
Prepared and characterised in the UK, for world wide distribution by Isotrak, AEA Technology, QSA.
Trkcert.wps 10/03/00
AEA TechnrJlogy is the trading name of AEA Technology Ififrg_ 2 9
~EBERl-IN!;; I

MP.009
S~~;RV1Ct:::$
Rev.B; 11/01/03
Trtle:
Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES -OAK RIDGE LABORATORY

PRIMARY DILUTION RECERTIFICA T/ON
MP009
12/13/2012 0:001
CURRENT DATE I
:.
. :_,,Ucj 0 ...:, CC 'l

.
I
SOLUTION
#I<
SOLUTION REFERENCE #IAEA!Amersham 921232167.
Principal Radionuclide
Half Life, Years
Half Life, Daxs
I ~2 u' 'I
2.630E+04I
1 'i':2ooE+o1l
I ..
Radionuclide~_:,: ::.!\U '', ..~
Reference Datal. :' .... -3t1/2ooo o:ool
Certified Activity ... 9.760.E~Q1 11Ci

Certified Concentration '< :. .: : 11Ci per gram
Ampoolo ,..,.., -~ Empty Ampoule :
Weight, Grams
Solution Net . . . . Weight, Grams
0.9760 11CI
Chemical Comoosition of Standard Solution
FP,'{NO~)e iri ?M l:lNb3 .. ' : ' ' :_... . . ..'.:.... :-,:_..
Dilution Instructions:
Dilute to a volume ofj . 1 000.00
Certified Total Activity of
o.s7aoj 11ci
... ...:;.
I2MHNo'
. -. . . . 3: ,..
.
:..~
Which Eauals
QC Approval
~--';,
\..~.1~1{, J\J ffi
. ..I
. 2.167E+06Idpm at the date listed above

This activity concentration Is based on Ute original
reference date listed above. All activities are corrected
Expiration Date: I December 7, 2013 I
;,:_
'I milliliters
And after dilution the activity of this solution Is !2.167E+03Jdpmlml
.._.
r\
'-'
Date:
Date:
12113/2012 0:00
tsb7
~Ef;;t_ERLJNE I QUALITY CONTROL PROGRAM

MP.Q09
S!<AVICO!:!>
Rev.6; 11/01103
EBERLINE SERVICES- OAK RIDGE LABORATORY

MP.009
Solution Reference #IAENAmersham921232167 1
Principal Radlonucllde
Half Life, Years
j . 7.200E+01J
. '32u. I
Radlonuclide of lntereslf':>.. _;<3~(r:-:,:: I

Parent Solution Conc.l <2.167E+03.'1dPmlml
~"
Date\ . ,,-. 1217/2012 0:001

'U'10a >: 1
Solution #I
Half Life, Dal!
.
. 2.630E+04l
Reference Date! :
-.:-
31112ooo:o:ool
.. > './.;' '.' ,.. . .< ..; . . , ;.,j
J2MHNOa
..,,,..
'

Vol. Parent Solution: ' . 10.0000 ml
Total Activity: . 2. 1670E+04 dpm
'1000:00 ml
Final Volume: .
. 2.1670E+01Jdpmlml

laboratory data processing software.
NOTES:
Expiration Date:! December 7, 2013
\.
QCApproval
~---~
~LUJ< li\
~
..__...
Date:
Date:
12113/2012 0:00
lafb2::
i
RTIF1CATE OF CALffiRATI~\\t
q\
.'"""'. . ~LPIIA . STANDARD SOLUTION" tj\,' '\ ~:~\\t'\\
~f::f:#::!=~===.l
01!'~~~~\l
Radionuclide
Th-230
Half Life:
(7.54 0.03) x 104 yeaiS
Catalog No.:
7230
Source No.:
388-116
b. Chemical form:
c. Carrier content:
d. Density:
Customer:
TMA EBER.LM~ fA\~'f};"'
P.O.No.:
TI4944
,~~
Reference Date:
November 1 1991
12:00 PST.
Contained Radioactivity:
1.036
J&Ci.
5.0042
Th(N03)4 in O.lN HN03
None added
1.0016
grams.
gram/ml @
2oc.
Radioimpurities
See attached technical data sheet
See attached teclmical data sheet
Radionuclide Concentration
0.207
Weighed aliquols of the solution were ossayed using a liquid scintillation oounter.
Unl!eliainty of Measurement
a. Systematic uncertainty in instruinent calibration:
c. Random uncertainty in weighing(&):
d. Total uncertainty at the 99% oonfidence level:
2.0%
0.5%
0.2%
2.7%
NJST Traceability
This calibration is implicitly traceable to the National Institote of Standards and Technology.
Notes
1. Nuclear data were taken from "Table of Isotopes, Seventh Edition, edited by Vi.Iginia S. Sbirley.
2. IPL participates in an NIST measurement assurance program to establish and maintain implicit
traceability for a nomber of nuclides, based on the blind assay(and later NIST certification) of
Standard Reference Materials. (As in NRC Regulatory Guide 4.15)
ISOTOPE PRODUCTS LABORATORIES

1800 No. Keystone Street.,
Burbank, California 91504
818 843 - 7000
\~
'-'

MP-ll09
Rev.8; 11/01/03

PRIMARY DILUTION RECERTIFICA T/ON
MP009
CURRENT DATEl
. 314/Z013 0:001
SOLUTION REFERENCE #"'IP"'.L""'' 3"'.B""B.c"":t""'t6<-.....-:....,,..,.._~...,,,........,
...,...,
;'I SOLUTION #[cvc:. :>T:h+.>>.:.'\:.CCI
Principal Radlonuclide
Half Life, Years
Half Life, Days
~M'Ii
<:1
1 7:54oE+o41
2.754E+o71
Reference Date! c.. <'1j/1/199lo:ool
Ampoule
/Solutiooln~~:~~;~~>j.{~,;em~;:;;;:;~
Grams
.
Grams
Empty~ -.
Solution Net .
4~
:Q:
Grams
01Ci
Chemical Composition of Standard Solution
DilUtion Solvent Used
Dilute to a volume otl'
Certified Total Activity ofl
.tooo:oo> :jmlllillters
1.036011-'Ci
Which Eauals
2;3QOE+OBidpm at the date listed above

This activity concentration Is basod on the original
And after dilution the activity of this solution is 2;300E+Q3jdpm/ml reference date listed above. All acttvitles are corrected
to the da~ and time of analysis by !he laboratory data
Expiration Date:
Recertified By
QCApproval
~ ~~.
......
~j ~\AJfA1
Date:
Date:
March 4, 2014 .
312112013 0:00
-f~!J.
~
I
Rev.8; 11/01/03

Reference Date
IDllutiion Instructions:
f.
i:A1/1119$1:1Ji!)o'f

Final Activity Concentrationf
2.2999E+01ldpmlml

NOTES:
Expiration Date:!
Recertified
Date:
Vartfled & Approved By
Date:
QCApproval
Date:
March 4, 2014
3/2112013 0:00
j.;).t ''3~{:~-t(p
7h-8
CERTIFICATE OF CALIBRATION
ALPHA STANDARD SOLUTION

~onuclide:
Th-232
Half Life:
(1.405 0.006) x 10'10 yeaiS
Catalog No.:
7232
Source No.:
435-104-2
b. Chemical form:
c. Carrier content:
d. Density:
TMA EBERLINE
Customer:
VH1632
P.O.No.:
Reference Date:
November 1 1993
12:00 PST.
(Th-232) 0.0933
,.ci.
(Th-232)
3.45
kBq.
ll.9712 g (in a 10 ml flame sealed amJ?.Oule)
Th(N 03)4 in waier
None added
Approx. 1.21
Radioimpurities
g/ml @20'C.
None detected (other than daughters).
Ra-228, Ac-228, Th-228, Ra-224, Rn-220, Po-216, Pb-212, Bi-212,Pp-212, Tl-208
Radionuclide Cuncentration
(Th-232) 0.00779
,.Cilg.
Activity calculations are based upon known specific activity and mass.
c. Random uncertsinty in weighing(s):
3.0%
0.0%
2.0%
3.6%
NIST Traceability
This calibration is implicitly traceable to the National Institute of Standards and Technology.
Leak Test(s)
See reverse side for Leak Test(s) applied to this source.
Notes
1. Nuclear da~ .~e~ 'taken from "t:abte Of Radioactive Isotopes"; edited by Virgi"nia s. Shirley, !986.
2. 1PL particip~tes in an NIST m~rement assurance program to establish and maintain implicit traceability for a number of nuclid~,
based on the blind assay (and later NIST certification) of Standard Reference Materials (As in NRC Regulatory Guide 4.15).
QUALITY CONTROL
Date Signed
1800 North Keystone Street
818 843. 7000
fHI135

MP-409
Rev.S; 1110/03
Tdfe: RadioacUve Reference Standards Solutions & Records

MP009
per gram
ICrti1fied Total Activity of(. "i} a:0933lf1Ci
Which eauals (., .:',':2.07JE+o5(dpm at the date listed above
And after dilution the activity of thi$ $Oiution isl2;071 E+02ldpmlml
This aGtivlty concentration Is based on the original

reference date listed above. All a<rtivltles ""' correcled
tothodate and time of analysis by the laboratory data
Expiration oate:l .otobet9.2otal
Date:
10/9/2012 0:00
----"====-
(EBERL_~_g: I QUALITY CONTROL PROGRAM

MP009
S"~RVIC:E-S
Rev.8; 1/10/03
Title: Radioactive Reference standards Solutions & Records

: ZZB &
Z>ZJh
MP-QI9
:#IIPL
I'Z .
Half Life, !!!fS
Datal
t#l
1; . . . .II
Radionuelide of lnterestl<'f'6 &232Th ::1

Parent Solution Cono.r 2:07E+o2. 'ldpm/ml
Reference Date
Chemical Comeosltlon of Standard Solution

.. .,.' ..
1Tn(N03) i~ 1% HN03 ..
Instructions:
.012 0:00 I
!b .... ,
-~
"
Half Life, 1ays
. 5.1:
tl
.:'
. . .
1111i19eao:ool
.I
11 % NitrieAeid

600:0000.ml
Vol. Parent Solution: .
Total Activity: 1.0365E+06 dpm
Final Volume:
1000;00ml
1.0355E+02Idpmlmi
Final Activity Connentration:l

NOTES:
Expiration Date: I . Octaoer e. 2013
Verified &Approved
8~
QCApproval
_A~Al J1
--
"'H'V
- \)
u l LJ"'
\1'
Date:
Data:
:0:00
II
,..,J,..z. .
I
Isotope Products
lh-18
24937 Avenue Tibbitts

Valencia, California 91355
Laboratories
An Eckert & Ziegler Company
Tel 6613091010
Fax 6612578303
ALPHA STANDARD SOLUTION
Th-229
7340 160 years
7229
867-54
Radionuclide:
Half-life:
Catalog No.:
Source No.:
Physical Description:
A. Mass of solution:
B. Chemical form:
C. Carrier content:
D. Density:
Customer:
P.O. No.:
Reference Date:
(Th-229 only)
EBERLINE SERVICES
00009633
15-Jan-02 12:00 PST
1.013
J!Ci
37.48
kBq
5.0147 g in 5 ml ftame-sealed ampoule

Th{NOs)4 in 0.1 M HN03
10~g Th/ml
1.0016 g/mL@ 20C.
Radioimpurities:
None detected (daughters in equilil:>rium)

Radionuclide Concentration:
0.2020
~Ci/g,
7.474
kBq/g
Method of Calibration:
This source was prepared from a weighed aliquot of solution whose activity in IJCi/g was determined
using gamma ray spectrometry.

Peak energy used for integration:
193.5 keV
Branching ratio used:
0.0441 gammas per decay
Uncertainty of Measurement:
A.
B.
C.
D.
Type A (random) uncertainty:

Type B (systematic) uncertainty:
Uncertainty in aliquot weighing:
Total uncertainty at the 99% confidence level:
0.7%
3.0%
0.0%
3.1%
Notes:
See reverse side for leak test(s) performed on this source.

IPL participates in a NIST measurement assurance program to establish and maintain implicit traceal:>ility
for a number of nuclides, based on the blind assay (and later NIST certification) of Standard Reference
Materials (As in NRC Regulatory Guide 4.15).
- Nuclear data was taken from IAEA Technical Report Series No. 261.
- This solution has a working life of 5 years.
Quality'C{;ntrol
Date Signed
IPL Ref. No.:
867-54
- - - - - - - - - - - - - - - - - - IS09001CERTIFIEP - - - - - - - - - - - - - - - - - -
Medical Imaging Laboratory

24937 Avenue Tibbitts Valencia, California 91355
Industrial Gauging Laboratory

1800 North Keystone Street Burbank, California 91504
~~ER!;-;,~~~~ QUALITY CONTROL PROGRAM

MP-009
Rev.7; 9/29/99
TIUe' RadioaCtive Reference StaMal'ds SoluUons & Records

MP-009
Solution Reference #JIPL86,7Cfi4 .
Principal Radionucllde
Half Life, Years
I.'J.34oE+o31
"''Th "I
Radionucllde of lntere~ .
Parent Solution Cone. '2;25E+03 .:,dpmlml
-~-
~t0,1M~f: . ;>
Date I
1119/2012 0:00 I
'fh,1Ba.. -I
Solution #1"
Half Life, Da;ts
2.681E+osl
Reference Date
I ..
111sJ2oo2 o:ool
.. .]
__
.,
__
!0.1MHNO
. - . . . . . 3. . :
"'" I
. 10.0000 ml
Vol. Parent Solution: .
Total ActiVIty: . 2.2490E+04 dpm
.. 1000.00 ml
Final Volume:
2.2490E+01ldpmiml

cPrrected to the date and time of analysis by the
NOTES:
Expiration Date:!
\>
QCApproval$
"
'-..J
October 9, 2013
Date:
11/912012 0:00
Date:
uhb"2i
I
,
E E I E R ' INE
~ ~------ -~~\nc~:e
MP009
Rev.S; 1/10/03
Title:

MP009
Reference Date) '
Ampoule /Solution Gross . 8.7752

Empty Ampoule ': 3.7591
5.0161
Solution Net
1.0130
1115i:woio:ool
Weight, Grams
Weight, Grams
Weight, Grams
J.LCi
.... h(N()~) 4 .in .().1 MHI\IO:i '
. I

Dilute to a volume ofl .1000.00 .!milliliters
Certified Total Activity of I
1.0130IJlCi
Which Eauals
2~249E+06Idpm at the date listed above
And after dilution the activity of this solution is I 2.249E+03Idpm/ml
This activity concentration is bassd on the original

reference date listed above. All activities are corrected
Expiration Date:
October 9, 2013
Date: _ _.!.11!!.19::::,1::20::.,:1.:2,:::0;.:::0:.:::,0
Date: -....!'!I-!;(IZIJ..{r!::.Z-:....-__
j}attonal 3Jnstitute of
~tanbarbs
&
~ecbno lo !l!'
terttftcate
.11", '
U.fYr,--t
~ 1: / '. ___ l' _(!
fi
~
-/-
-.
-:_
'
_.il;;
Standard Reference Material4251C

Bariurn-13$ Radioactivity ,Standard . ,
This Standard Reference ll<faterial(SRM) consis~ of radioactive. barium-133. cbloride,.llOncradioactive barium

chloride, and hydrochloric acid diSsolved in 5 niL of distilled water. The soiution is contain~ .in a flamesealed NIST borosilicate-glass ampoule. The SRM is intended for the calibration of ionization\ihaillbers and
soliq-state gamma-ray,spectromeqy.systems..
:
,,
Radiological Hazard
The
llmpoule contains bariuni-133 with~ total activity of approximately 2.5 MBq. Barium-133 decays
.by electron capture and during tile decay pr~ss X-rays and garpl!,1a;rays with energies from 4. to 400 ke V are
emitted. Most of these photons escape from the SRM ampoUle and can represent a radiati9n hazard.
Approximate unshielded dose rates at several distances (as of the reference time) are given in note [a]*.
Appropriate shielding and/or distance shoulq be us.ed to .l)lini:miz\>, pe.rscmnel exposure.,,The ,SRM ~hould be
.~e<;l only by persons qUalified to han?Je radioactivr material.. "
SRM
Chemical Hamrd
The SRM ampoule contains hydrochloric acid (HQ) with a concentration.pf 1 mole per Iiter.ofwater. The
SOlution is corrosive imd represents health hazard if it comes in COntact with,eyes OLSidn,, :If the ampoule
is to be opened to transfer the solution,.the recommended procedure.is given on page 2.
ampoule should
)Je opened ouly by persons qualified to handle both radioactive material and strong a.cid solution.
The
Storage and Handling

The SRM should be stored and used at a temperature between 5 and 65 c. The solution in an un~pened
ampoule should remain stable and homogeneous until at least June 2004.
The ampoule (or any subsequent container) should always be clearly marked as containing radioactive
material. If the ampoule is tr~rted it should be packed, marked, labeled, and shipped in accordance with
the applicable national, international, and carrier regulations. The solution in the ampoule is a dangerous
good (hazardous material) both because of the radioactivity and because of the strong acid.
Preparation
This Standard Reference Material was prepared in the Physics Laboratory, Ionizing Radiation Division,
Radioactivity Group, J.M.R. Hutchinson, Group Leader. The overall technical direction and physical
measurements leading to certification were provided by LL. Lucas of the Radioactivity Group and D.B. Golas,
Nuclear Energy Institute Research Associate.
The support aspects involved in the preparation, certification, and issuance of this SRM were coordinated
through the Standard Reference Materials Program by N.M. Trahey.
Gaithersburg, Maryland 20899
October 1994
Thomas E. Gills, Chief

Standard Reference Materials Program
*Notes and r~ferences_ an~. PD pages.$ and 6.

QCP.009
Rev.8; 11110/03
Title:
Radioactive Reference standards Solutions & Records

PRIMARY DILUTION RECERTIF/CA T/ON
QCP 009-1
SOLUTION
Certified Acllivillvl<'
Certified ConCEtntratic>n C
per gram
Ampoule /Solution
Empty AmjpOUIIe
Solution
Total Activity In
fDiilution Instructions:
Grams
Grams
Grams
Which Eauals I> ' 1A78E+oajdpm at the date listed above

And after dilution the activity of this solution isl1o478E+05Idpm/ml reference dam llsn.d above. All activities are corrected
to the dow and time of analysis by the laboratory data
Expiration Date:ISeptenil:!er 20,>20131
__
Date:
__
Date:
---".!l/.!:z~'I+=I..:Z:......_
...:::..:::.:..:.;:.:_
9/27/12
Rev.B: 11/10/03

''"'aa;
Radlonuclide of lnteres > '

Parent Solution Cone. ; 1A6E+05 dpm/ml
JDilutic>n Instructions:
Reference Date!;
.;',<911/1993o:ool
. .. .. I
l1MHCI

Vol. Parent Solution: ~'L . "25:0000 ml

Total Activity: 3.6950E+06. dpm
Final Volume . 1000:00 ml
NOTES:
3.6950E+03Idpm/ml

Expiration Date:! September 20, 2013
Date:
9/27112
__:::~~-
Date: _ _'1~/:;..t'1-'+f.:..::t2-::::..__
Radionuclide:
Half Life:
Catalog No.:
Source No.:
Ra-226
Customer:.
1600 7 years
7"126
453-26
Description of. Solution

b. Chemical form:
c. Carrier content:
d. Density:
TMA EBERLINE
VH1888
P,O.No.:
February 1 1994
12:00 PST.
Reference Date.:.
Contained Radioactivity: (Ra-226) 1.001 ~tCi.
Contained Radioactivity: (Ra-226)
37.0 kBq.
5.1864 g (in a 5 ml Flame Sealed Ampoule)
Ra(N03)2 in 1 N HN03
None added
1.0318
Radioimpurities
None detected(other than daughters)
Rn-222, Po-218, At-218, Pb-214, Bi-214, Po-214, Tl-210, Pb-210, Bi-210, Po-210 aud Tl-206.
Radionuelide Concentration
. (Ra-226) . 0.1929
~Cilg.
Weighed aliquots of the solution were assayed using gamma spectrometry:
Energy peak(s) integrated under: 186 keV.
Brancbilig ratio(s) used:
0.0351
gamma my~ per decay.
c. Random uncertainty in weighing(s):
3.4%
3.1%
0.2%
.4.6%
NIST Traceability
This calibration is implicitly traceable to the National Institute of Standards and Technology.
Leak Test(s)
See reverse side for Leak Test(s) applied to tbis source.
Notes
1. Nuclear data were _tabil ftom "Table of Radioactive Isotopes", edited by Vuginia S. Shirley, 1986.
2. IPL participates in an NIST measurement assurance program to eStablish and maintain implicit traceability for a num~r of m,tclides,
- -oased orrtlftfbliiiintssay-(&odlater NISTeeriifiCationrorstalidaro -p.ererenc~fMiiteriatS1AnnNRc-R.egumoeyomdir4; rs): -------
QUALITY CONTROL
/iA.. ~I
119/.f
Date Signed
1800 North Keystone Street
818 843 -7000
~EEIERL!NE I

MP009
SI!:RVIC~S
Rev.8; 11101103
Title:

MP009
CURRENT DATEI
11/9/2012 0:001
'. J
SOLUTION #I , i
'Riac5 ' . . , I
Half Life, Dal(S
5.844E+osi
SOLUTION REFERENCE #IIPL453226. :: . .

Prlnc~al Radionuclide
Half Life, Years
. " 2 ~Radium 1
1:aooi:+o3l
I
Reference Date I'
Radionuclide , ~~~R~;~dium
Certified Activity ..1:0.0.1 E.;,oo !'Ci
Certified Concentration :,.. ' . ' ' ..
)'Ci per gram
-.
. -:
2!1i19940:ooi
Amp~~
. . . .Ampoule
,-~... Grams
~
Empty
. . : : .. Weight,
Solution Net '
. . Weight, Grams
1.0010 )'CI
Chemical Comeosition of Standard Solution

F'Ra(I\IO'sJ2in',1MHNOi.'.
Dilute to a volume of!
Certified Total Activity of!
.I
''
ltMHNOa
'1000:00. '!milliliters
1:0010lJ.tCi
Which Eauals
2.222E+06ldpm at the date listed above

This activity concentration is based on tho original
And after dilution the activity of this solution lsi 2.222E+03ldpm/ml reference date listed above. All acUvlties are corrected
Expiration Date:! November 9, 2013

QCApproval
~::at\
11/9/2012
Date:
Date:
rrLz../rz..
I
Rev.B; 11/01/03
Title:

IDilutlc>n Instructions:

NOTES:
Final Activity Concentration:!,.'< ',)t4440E+01ldpmlml

Expiration Date:l November 9, 2013l
Date:
Date:
''
1119/2012 0:00
I
ft.z.f,z...
I
Rl\-\\
1380 Seaboard Industrial Blvd.
Atlanta, Georgia 30318 U.S.A.
ANALYTICS
Phone (404) 3528677

Fax
(404) 3522837
Standard Radionuclide Source
62680-416
Ra-228 5 mL Liquid in Flame Sealed Vial
was
prepared
This
standard
radionuclide
source
gravimetrically from a calibrated master solution.
The
master solution was calibrated using a germanium gamma
spectrometer system.
Radionuclide purity and calibration were checked using a
germanium gamma spectrometer system. The nuclear decay rate
and assay date for this source are given below.
ANALYTICS maintains traceability to the National Institute
of Standards and Technology through Measurements Assurance
Programs as described in USNRC Reg. Guide 4.15, Revision 1.
ISOTOPE:
CALIBRATION DATE:
Ra-228
2.585 E3
5.75 years
November 7, 2001 12:00 EST
TOTAL UNCERTAINTY*:
4.0%
ACTIVITY (dps) :
HALF-LIFE:
SYSTEMATIC:
3.0%
RANDOM:
1. 0%
*99% Confidence Level

Impurities: y-impurities (other than decay products) <0.1%
5.07198 grams 0.1M HCl solution with 50
P 0 NUMBER
~g/g
Ba carrier.
9508, Item 1 (Part #4339A)
SOURCE PREPARED BY:

M. D.
Q A APPROVED:
urrle, Radlochemlst

MP-009
Rev.S; 1/10/03
Tltfe:
EBERLINE SERVICES -OAK RIDGE LABORATORY

RECERTIFICATION
MP009
per gram
Certified Total Activity ofl;/()0!0$11\ill~ci
Which Eauals
I: 'f.'}c:'I;SS1E:+osldpm at the date listed above
And after dilution the activity of this solution 1siA:'55tE:r,Q2ldpm/ml
This activity concentnttion is based on the original

reference date listed above. All activfties are corrected
to the date and lime of analysis by the laboratory data

Expiration Date:!> /APtil12i"-2013
>'I
Date: _ __;4~/1~6:::.11!!2,___
Date:------Date: _....;;4"H/u.f~t.,p.IJJ.Z....:;;__
SECTION VI
QUALITY CONTROL SAMPLE RESULTS SUMMARY
Eberline Services
Analysis Control Chart
Printed: 5/10/2013 8:43AM

Page 1 of2
Wo
Ani3lYSis
Run
Activity Units
13-04132
UUISO
pCi
Aliauot Units
Client Name
Laboratory Control Sample

LCS
Measured
Nonnalized
Difference
Analyte
U-234
0.84
U-238
0.57
Known
I
~
csu
Result
Standard
ID
Standard
Standard
ACT(dpm)
Standard
Added (g)
~
I
1.26E+OO
U-Sa
I 3.52E+01 I 3.60E+OO
5.12E-01
7.55E+OO
1.25E+OO
U-Sa
I 3.44E+01 I 3.60E+OO I
5.12E-o1
Sample
Sample
Aliquot
Standard
93.29%
16.60%
100.00%
3.60%
8.12E+OO
2.92E-01
7.58E+OO
95.33%
16.62%
I 100.00%
3.60%
7.92E+OO
2.85E-01
Sample
Result
Matrix Spike
MSActual
%Rec
Normalized
Difference
Analyte
Expected
MSResult
Expected
MSUncert
Actual
MSResult
Actual
MSCSU
csu
Ul
Iii!!
Replicate
Result
Replicate
csu
csu
LCS Relative
Bias
LCS%R
2.48
2.25E+OO
4.31E-01
2.19E+OO
4.43E-01
0.93
OK
OK
OK
OK
9.61
8.56E-01
2.26E-Q1
7.78E-01
2.26E-01
0.95
OK
OK
OK
OK
98.31
7.26E-02
7.04E-02
2.13E-01
1.21E-o1
OK
OK
INV
OK
U-234
0.17
U-238
0.48
U-235
1.97
Ill!'!
Version
Standard
Added(g)
Original
RPD
Standard
Error%
Original
Result
Normalized
Difference
Standard
ACT(dpm)
QCSummary
Replicate Sample
Analyte
ID
LCSND
MS%R
MSND
RepRPD
RepND
Eberline Services
Printed: 5/10/2013 8:43AM

Page 2 of2
WO
Analysis
Run
Activitv Units
13-04132
UUISO
pCi
Aliauot Units
Client Name
Replicate Sample RPD
LCS % Recovery
130.00
40.00
120.00
35.00
110.00
30.00
100.00
25.00
20.00
90.00
15.00
80.00
10.00
7o.oot---------------cuc~ccc---------------r---------------cuc-c=---------------,
34
Lower Error
Upper Error
%R
LCL
Mean
UCL
73.09
113.50
93.29
80
100
120
I
I
I
I
238
75.11
115.54
95.33
80
100
120
5.00
0.00
t----------;c-;;;;-;---------,----------=
u-""'"'
Lower Error
Upper Error
RPD
CL
2.73
2.24
2.48
35
v-.i38
10.94
8.28
9.61
U-235
131.19
65.42
98.31
35
35
Normalized Difference
3.50 , - - - - - - - - - - - - - - - - - - - - - - - - - - - -
3.001------------------------2.50
+----------------------------
2.00
+----------------------------
1.50
+----------------------------
l:t~
~
W1
......
Version
No Matrix Spike
Eberline Services
Printed: 5/17/2013 9:19AM

Page 1 of 2
wo
Analysis
Run
ActivitY-Units
13-04132
UUISO
pCi
Aliauot Units
Client Name

Nonnalized
Difference
Analyte
LCS
Measured
csu
Measured
LCS
Expected
'
U-234
1.15
91.69% 115.25%
100.00%
uncert.
Expected
Known
3.60%
8.12E+OO
Known
Em"
2.92E-01
csu
7.45E+OO
1.14E+OO
'
U-238
0.26
9S.01%
15.14%
100.00%
3.60%
2.85E-01 1 7.76E+OO
7.92E+OO
Result
1.18E+OO
Standard
Standard
ACT(dpm)
ID
Standard
Standard
Added (g)
Em"
URSa
3.52E+01
3.60E+OO
5.12E-01
URSa
3.44E+01
3.60E+OO
5.12E-01
Matrix Spike
Nonnalized
Difference
Analyte
MS Actual
%Rec
Expected
MS Resuh
Expected
MSUncett
Actual
MS Result
Actual
MSCSU
Sample
Result
Sample
Sample
Aliquot
csu
N.l
Replicate
Result
LCS Relative
Replicate
RPD
Original
Result
Original
U-234
0.25
41.52
7.68E-02
2.43E-01
U-238
0.17
27.57
8.93E-02
! 1.93E-01
6.76E-02
1.69E-D1
U-235
0.98
5.53E-02 I 1.69E-01
2.06E-01
2.50E-01
Version
115.42
Standard
Error%
Standard
Added(g)
RepRPD
RepND
INV
OK
QCSummary
Normalized
Difference
l:.'il
1.111
Standard
ACT(dpm)
ID
---~
Replicate Sample
Analyte
Standard
csu
I 1.17E-01
csu
Bias
2.07E-01
0.92
0.98
LCS%R
LCSND
OK
OK
OK
OK
MS%R
MSND
OK
OK
INV
OK
NA
OK
Eberline Services
Printed: 5/1712013 9:19AM

Page 2 of 2
wo
AnaJYSIS
13-04132
UUISO
Run
-1
Activity Units
Aliguot Units
pCi
Client Name
LCS % Recovery
------1
130.00
~0.00
120.00
35.00
110.00
30.00
100.00
25.00
20.00
90.00
15.00
80.00-+
1000
70.00
Lower Error
Upper Error
%R
LCL
Mean
UCL
U-234
U-238
72.84
110.53
91.69
80
100
120
79.26
116.75
98.01
'"
0.00
lower Error
so
100
120
erError
RPD
CL
U-2:34
89.70
-6.66
41.52
35
U-238
59.40
-4.26
27.57
35
3_50 , - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -
2.50
+-----------------------+-----------------------------
2.00
+----------------------------
1.50
+-----------------------------
3.00
1.00
0.50
0.00
1:~1
!.Jl
!,,)
Version
No Matrix Spike
U-235
207.93
22.92
115.42
35
Eberline Services
Printed: 5/1012013 8:55AM

Page 1 of 2
--we
Analysis
ThiSO
13-04132
"""
Activity Units
Aliquot Units
Client Name
pCi

NonnU"d
Difference
Anatyte
csu
'
LCS
Measured
Measured
LCS
Expected
Uncert.
Expected
96.31%
17.73%.
100.00%
3.60%
TH-228
0.42
TH-230
2.09
82.71%
19.51%
100.00%
TH-232
0.64
94.54%
17.43%
100.00%
Known
Known
Em"
csu
Result
Standard
ID
Standard
ACT(dpm)
Standard
Error
Standard
Added (g)
4.80E+OO
1.73E-01
4.62E+OO
8.19E-01
Th-8b
1.04E+02
3.60E+OO
1.03E-01
2.70%
5.41E+OO
1.46E-01
4.48E+OO
8.74E-01
Th-1b
2.35E+01
2.70E+OO
5.11E-01
3.60%
4.80E+OO
1.73E-01
4.53E+OO
7.90E-01
Th-8b
1.04E+02
3.60E+OO
1.03E-01
Matrix Spike
Normalized
Difference
Analyte
MSActuat
%Rec
Expected
MS Result
Expected
MSUncert
Standard
Added {g)
Actual
MSResult
QCSummary
Replicate Sample
Normalized
Difference
RPD
Original
Result
Original
Replicate
Result
Replicate
csu
csu
LCS Relative
Bias
LCS%R
LCSND
TH-228
1.13
544.07
-1.37E-02
3.56E-02
2.97E-02
6.65E-02
0.96
OK
TH-230
2.33
99.38
9.47E-02
8.31E-02
2.82E-01
1.33E-01
0.83
TH-232
O.Q7
6.97
4.09E-02
5.33E-02
3.81E-02
5.17E-02
0.95
Anafyte
~!!!
ft~
!..11
~:-~
Version
MS%R
RepRPD
RepND
OK
NA
OK
OK
OK
NA
OK
OK
OK
NA
OK
MSND
Eberline Services
Printed: 5/10/2013 8:55AM

Page 2 of 2
wo
Analysis
Roo
Activitv Units
13-04132
ThiSO
pCi
AliQuot Units
Client Name
LCS % Recovery
130.00
40.00
12000
- - - - - - - - - - - - - - -UCL
35.00
110.00
30.00
100.00
25.00
20.00
90.00
15.00
80.00
- - - - - - ... LCL
10.00
70,00
--Lower Error
Upper Error
%R
LCL
Mean
UCL
TH-228
74.98
117.64
96.31
TH-230
60.50
104.92
82.71
80
80
100
120
100
120
5.00
TH-232
73.51
115.57
94.54
80
100
120
0.00
Lower Error
Uooer Error
RPD
CL
~ , ~~n
'' ,-"'"''-'
2285.14
-1197.00
544.07
35
.,.., ,
'' .-230
127.93
70_82
99.38
35
35
3.50,-----------------------3.00 +------~--------~---~-------
2.5ojl-----------------------2.00
+------r--1-------j
1.50+-----j
1.00+-----j
0.50
0.00
~1!1
(!-)
I:Ji
Ul
Version
I
TH-232
11.60
2.34
6.97
No Matrix Spike
Eberline Services
Printed: 5/16/201310:19 AM
Page 1 of 2
wo
AnalySis
Run
Activity Units
13-04132
Ra226
pCi
Aliauot Units
Client Name

Analyte
RA-226
csu
Normalized
Difference
LCS
Measured
Measured
LCS
Expected
Uncert.
Expected
Known
0.08
101.03%
24.31%
100.00%
4.60%
1.03E+01
Known
Result
csu
Standard
4.73E-01
1.04E+01
2.52E+OO
Ra-5b
Sample
Result
Sample
Sample
Aliquot
Standard
ID
Standard
ACT (dpm)
4.41 E+01
I
I
Standard
Error
I 4.60E+OO
Standard
Added (g)
5.18E-01
Matrix Spike
Normalized
Difference
Analyte
MSActuat
%Rec
Expected
MS Result
Expected
MSUncelt
Actual
MSResult
Actual
MSCSU
csu
RA-226
IW
!:...i!ll
!JU
Version
Standard
ACT(dpm)
Standard
Error%
Standard
Added(g)
RepRPD
RepND
INV
OK
QCSummary
Replicate Sample
Analyte
/D
Normalized
Difference
RPD
Original
Result
Original
Replicate
Result
Replicate
LCS Relative
csu
csu
Bias
0.82
175.30
3.00E-03
6.89E-02
4.56E-02
7.43E-02
1.01
LCS%R
OK
I
I
LCSND
OK
MS%R
MSND
Eberline Services
Printed: 5/16/201310:19 AM
Page 2 of 2
wo
Analysis
Run
Activitv Units
13-04132
Ra226
pCi
AliQUOt Units
Client Name
LCS % Recovery
130.00
40.00
120.00
35.00
110.00
30.00
100.00
25.00
20.00
9{).00
15,00
80.00
1o.oo
RA-226
Lower Error
Upper Error
%R
72.12
129.95
101.03
80
LCL
Mean
100
UCL
120
1000
'"'
o.oo
RA-226
Lower Error
Uooer Error
RPD
433.66
-83.07
175.30
35
CL
3.50~--------------------------
2.50-\--------------------------2.00-\--------------------------1.50 + - - - - - - - - - - - - - - - - - - - - - - - - 1.00+-------------------------
0.50-1----------0.00
Iii~
S~
(J'H
...
Version
' .... ,.. ......
No Matrix Spike
Eberline Services
Printed: 5/22/2013 8:11AM
Page 1 of 2
Wo
AnalYsis
Activitv Units
13-04132
Ra228
pCi
Aliquot Units
Client Name
1

Analyte
RA-228
csu
Normalized
Difference
LCS
Measured
Measured
LCS
Expected
Uncert.
Expected
Known
0.33
105.56%
31.21%
100.00%
5.10%
8.96E+OO
Known
='
Result
4.57E-01
9.46E+OO
Sample
Result
Sample
CSU
2.95E+OO
Standard
ID
Ra-11
Standard
ACT (dpm)
3.88E+01
I
I
Standard
Error
5.10E+OO
Standard
Added (g)
5.12E-01
Matrix Spike
Normalized
Difference
Ana/yte
MS Actual
Expected
MS Result
%RK
Expected
MS Uncert
Actuaf
MSResult
Actual
MSCSU
csu
RA-228
~
t2:11
UY
():)
Version
Nonnafized
Difference
RPD
1.23
99.19
Standard
ACT{dpm)
Standard
Error%
Standard
Added (g)
RepRPD
RepND
NA
OK
QCSummary
Replicate Sample
Analyte
Sampte
Aliquot
Original
Result
Original
Replicate
Result
Repficate
LCS Relative
csu
csu
Bias
1.92E-01
4.51E-01
5.71E-01
4.03E-01
1.06
LCS%R
LCSND
OK
OK
MS%R
MSND
Eberline Services
Printed: 5/22/2013 8:11AM

Page 2 of 2
wo
Aila!ysis
Roo
Activity Units
13-04132
Ra228
pCi
AliQUOt Units
Client Name
LCS % Recovery
130,00
40.00
120.00
3500
110.00
30,00
100.00
25.00
20.00
90.00
15 00
80.00
10.00
7o.oo
RA-228
LowerError
UpperError
%R
LCL
69.25
141.87
105.56
80
100
120
---Mean
1-
-UCL
. 00
o_oo
RA-228
154.67
99.19
3.50,------------------------3.00 +--------~--------~--------2.50
+-----------------------------
2.ooil---------~------------
1.sojl----------------------
t----------0.50 +------------1.00
0.00
~~
~
U1i
Version
No Matrix Spike
SECTION VII
LABORATORY TECHNICIAN'S NOTES
ISOUNOTES
Run 1
Printed: 5/3/2013 9:49AM
Page 1 of 1
}!9 E:_!'3 1::: Rl....._l N

~
J;:;
SERVICES
Work Order Analysis Notes
Date
Dept
' 1
05/03/13 09:49
PREP
User
JBARNARD
601 Scarboro Rd.

Oak Ridge, TN 37830
Voice: 865.481.0683
www.eberlineservices.com
Internal Work Order
Analysis Code
Run Number
13-04132
UUISO
1
Notes
ALIQUOTED AND FILTERED DISSOLVED FRACTIONS- ADDED SPIKES AND TRACERS- ADDED HN03
TO PRESERVE SAMPLES- DRIED SAMPLES DOWN
i!l862
Printed: 5/8/2013 6:12PM
Page 1 of 1
~E:BERI.,_INE
SERVICES
User
Oak Ridge LabQratory

601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
Internal Work Order

Analysis Code
Run Number
13-04132
UUISO
1
Date
Dept
05/03/13 09:49
PREP
JBARNARD
Notes
05/08/13 18:12
CHEM
JDEMELAS
Added concentrated HC! to sample beakers and heated to dryness; Added 20 ml 8N HCL to samples and
transferred to new, labeled CTubes, rinsing with 8N HC! to bring volume to 35 ml; Preconditioned resin
columns with 35 mi8N HCI; Centrifuged samples and loaded onto columns; Rinsed CTubes with 20 ml 8N
HCI, centrifuged as needed and loaded onto columns; Rinsed columns with 35 ml 8N HCI- 0.1N NH41, 35 ml
of 6.5N HCl- 0.04N HF, and 10 ml of 6.5N HCI; Eluted Uranium with 50 ml of 0.5N HCI into clean, labeled 100
ml beakers; Orieddown samples on hotplate; Dissolved samples in -10 ml of concentrated HC!; Transferred to
new, labeled CTubes with Dl H20. Set samples aside for later precipitation and filtering.
Printed: 5/9/2013 6:01AM
Page 1 of 1
~ E: E3 .E:: R hl~c~
Oak Ridge Lab<>ratory
--- .2""'
Date
05/03/13 09:49
--osiO~B/1"3"'1"8:1-2'"
Dept
PREP
User
JBARNARD
-----cH_E_M______ -----JDEMEiJ.:s--..----
601 Scarboro Rd.

Oak Ridge, TN 37830
Voice: 865.481.0683
Internal Work Order
Analysis Code
Run Number
13-04132
UUISO
1
Notes
AU QUOTED AND FILTERED DISSOLVED FRACTIONS- ADDED SPIKES AND TRACERS- ADDEO HN03
TO PRESERVE SAMPLES- DRIED SAMPLES OOWN
--- --ACfde<:tco-ncentrated HC! to sam-pte-beakers-and heate-dtOCTryn8SS; Added 20-rliTBN'HcL toS8mples and____ _
transferred to new, labeled C~Tubes, rinsing with SN HCl to bring volume to 35 ml; Preconditioned resin
columns with 35 ml 8N HCl; Centrifuged samples and loaded onto columns; Rinsed C- Tubes with 20 ml 8N
HCl, centrifuged as needed and loaded onto columns; Rinsed columns with 35 ml 8N HC!- 0.1 N NH4l, 35 ml
of 6.5N HCl- 0.04N HF, and 10 ml of 6.5N HCl; Eluted Uranium with SO ml of O.SN HCl into clean, labeled 100
ml beakers; Dried~down samples on hotplate; Dissolved samples in -10 ml of concentrated HCl; Transferred to
new, labeled C- Tubes with 01 H20. Set samples aside for later precipitation and filtering.
05/09/13 06:01
CHEM
RMARTZ
AOOED 0.1 ML NEODYMIUM CARRIER, 0.3 ML TITANOUS CHLORIDE, & 1 ML HF TO C-TUBES; LET SET
SIT IN ICE BATH FOR ONE HOUR SET UP FILTERS BY ADDING ALCOHOL & CARBON SUBSTRATE
THEN ADDED SAMPLES; WHEN SAMPLES WERE THROUGH FILTERS, ADDED 10 ML Dl H20 RINSES
FROM C-TUBES, REMOVED FILTERS, LET DRY IN DESSICATOR, THEN SENT SET TO COUNT ROOM.
Eberline Analytical
Printed: 5/9/2013 6:02AM

Page 1 of 1
Internal Work Order
13-04132
E:E3i;;~h~t';l;o~
Reagents
Analysis Code
UUISO
1lysi:
llc:Pri
..
Reagent
JD
Analyst
JD
013624P
Nitric Acid
Reagent Grade
013708P
Anion Exchange Resin
Reagent Grade
--------~----
HCI- HF
-----~
~-
1
Date
Recorded
JBARNARD
5/3/2013
JDEMELAS
5/8/2013
JDEMELAS
5/8/2013
--
f---
6.5N - 0.04N
-----~~-..-
Reagent
Concentration
Name
0138265
Run
--~-~-
013675D02
oyuo u~ nuo ~ Acid
0.5N
JDEMELAS
5/8/2013
0137345
, yu v~olloric Acid
6.5N
JDEMELAS
5/8/2013
013809P
Hydrochloric Acid
~-.----------~---------
-----~-----~-~--~--~~-------
0138395
Hydrochloric Acid
0138445
0132465
012809P
013221P
-----
HCI- NH41
8N- 0.1M
Carbon substrate
Solution
Ethyl Alcohol
---
---~~------~~-----
-----------
Reagent Grade
8N
-~-------~---- -------~------~~-------
!----
Hydrofluoric Acid
----
Neodymium Carrier
013434P
Titanous Chloride
------
-----
----~----
0131915
--
Reagent Grade
Reagent Grade
-------------
JDEMELAS
--JDEMELAS
-------
..
5/8/2013
5/8/2013
JDEMELAS
5/8/2013
RMARTZ
5/9/2013
RMARTZ
RMARTZ
5/9/2013
------ -----5/9/2013
1 mg/ml
RMARTZ
5/9/2013
Reagent Grade
RMARTZ
5/9/2013
llliil65
,:.._I'll.">
7
,.
; f,,,
I'I:~r'fhA
/7
LI-t.
...ro-ll\
;:
r-;:..
OCJt.t<;
n"i '11-
.:-1
~t"'
"--
,,, ""
<---
ilUilS7
I
f
).
I.Pl
\"\ 1\)
; s-\~ \o
-~
\-.
~n.,
(lj;
-H-.
...
I\~ o'; l1-t> .a.c .,."'')

Lt.c.n~
Ino--\ \'3Z A(~-'\\ 'i""' uU
.Sv..
f)
/)
--l
J.
_,
*'1..
"' ..
.I
J25-t
l?~
(' y ilL:.
?-1.
'Z. L.
'
-""') >~~
"
-~
f..Jp'
IU
uU
I~
--
------
-.
.--.:c ...
............
'"'
..
.. _
_.,
..
'--
..
.......
.....
>
df,l
"
ISOUNOTES
Run2
Printed: 5/13/2013 7:36AM
Page 1 of 1
~ t;:ai::::.Rbi,J?~"~
Date
Dept
05/13/13 07:36
PREP
I
I
User
JBARNARD

601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
lntemal Work Order
Analysis Code
Run Number
13-04132
UUJSO
Notes
ALIOUOTED AND FllTERED DISSOLVED FRACTIONS- ADDED SPIKES AND TRACERS- ADDED HN03
Printed: 5/15/2013 2:25PM
Page 1 of 1
~ e: a t:;;: ~b1N_t:;;:
SERVICES
#
1
Date
Dept
05/13/13 07:36
-:z- -a57i5ii3-i4:zs
PREP
-- CHEM--
User
JBARNARD
.......,_, ____________________________
RMARTZ
601 Scarboro Rd.

Oak Ridge, TN 37830
Voice: 865.481.0683
Internal Work Order 1

'"""'"'"''''""'"----
.... _. ____ ,,_ .
Analysis Code
Run Number
13-04132
.
UUISO
2
---
"'"--'""""-""'"'"------
Notes
AI,.IQUOTED AND Fll..TERED DISSOI..VED FRACTIONS- ADDED SPIKES AND TRACERS- ADDED HN03
TO PRESERVE SAMPI..ES- DRIED SAMPI..ES DOWN
--AiioEo:s-M"Lii-oi'coi'icENTRATED. Hci:-to8Eiii<ER8-i>:N5TooK fo-oRYNEss:-iioi5-E5-:::f51ii:Bof'
BN HCI.. TO BEAKERS AND AI..I..OWED TO COOL TRANSFERRED SAMPI..ES TO NEW, i..ABEI..ED CTUBES WITH BN HCL TO A VOLUMNE OF -35 MLS. PRECONDITIONED RESIN COLUMN WITH 35 ML BN
HCL & CENTRIFUGED SAMPLES; ADDED SAMPLES TO COLUMNS; AFTER SAMPLES RAN THROUGH
COLUMNS, ADDED 35 ML BN HCUNH41 & LET RUN THROUGH, FOLLOWED UP WITH ADDING 35 ML
6.5N HCU0.04N HF & THEN 10 ML 6.5N HCL. ELUTED SAMPLES WITH 50 ML 0.5N HCL INTO CLEAN
100 ML BEAKERS. TOOK SAMPLES TO DRYNESS ON HOTPI..ATE & ADDED 10 ML CONCENTRATED
HCL TO SAMPLES TRANSFERRED SAMPLES INTO C-TUBES WITH D.l. H20.
Printed: 5/16/2013 6:12AM
Page 1 of 1
)!J t;:: _.:=:: RL,.I !"-!_r;:::

~
601 Scarboro Rd.

Oak Ridge, TN 37830
Voic:e: 865.481.0683
www.eberlineservices.c:om
SERVICES
#
1
Date
Dept
05/13/13 07:36
PREP
User
JBARNARD
Internal Work Order
Analysis Code
Run Number
13-04132
UUISO
2
Notes
ALl QUOTED AND FILTERED DISSOLVED FRACTIONS- ADDED SPIKES AND TRACERS- ADDEO HN03
---ilo5ei5-:S"MLS OFCONCENT'Rilte5-fic[ro-8eii-KERSANo-tooi<l'i5-iiRYNE'ss:Jio6eo::i51iit:so
05/16/13 06:12
CHEM
RMARTZ
8N HCL TO BEAKERS AND ALLOWED TO COOL. TRANSFERRED SAMPLES TO NEW, LABELED CTUBES WITH 8N HCL TO A VOLUMNE OF -35 MLS. PRECONDITIONED RESIN COLUMN WITH 35 ML 8N
HCL & CENTRIFUGED SAMPLES; ADDED SAMPLES TO COLUMNS; AFTER SAMPLES RAN THROUGH
COLUMNS, ADDED 35 ML 8N HCUNH41 & LET RUN THROUGH, FOLLOWED UP WITH ADDING 35 ML
6.5N HCU0.04N HF & THEN 10 ML 6.5N HCL. ELUTED SAMPLES WITH 50 ML 0.5N HCL INTO CLEAN
100 ML BEAKERS. TOOK SAMPLES TO DRYNESS ON HOTPLATE & ADDED 10 ML CONCENTRATED
HCL TO SAMPLES; TRANSFERRED SAMPLES INTO C-TUBES WITH D.L H20.
ADDED 0.1 ML NEODYMIUM CARRIER, 0.3 ML TITANOUS CHLORIDE, & 1 ML HF TO C-TUBES; LET SET
SIT IN ICE BATH FOR ONE HOUR. SET UP FILTERS BY ADDING ALCOHOL & CARBON SUBSTRATE
THEN ADDEO SAMPLES; WHEN SAMPLES WERE THROUGH FILTERS, ADDED 10 ML 01 H20 RINSES
FROM C-TUBES, REMOVED FILTERS, LET DRY IN DESSICATOR, THEN SENT SET TO COUNT ROOM.
Eberline Analytical
----
----------- ..
'
Printed: 5/16/2013 6:15AM

Page 1 of 1
_____ ___
,
-----------~--
Internal Work Order
13-04132
.::;:: er;;:;Rh~~c~
Analysis Code
Reagents Used in an Analysis
UUISO
Reagent
ID
Reagent
Name
Reagent
Concentration
013797P
Nitric Acid
Reagent Grade
013708P
Run
Analyst
ID
I
I
JBARNARD
5/13/2013
Reagent Grade
RMARTZ
5/15/20131
HCI- HF
6.5N - 0.04N
RMARTZ
01385gs
HCI- NH41
8N - 0.1M
RMARTZ
5/15/2013
013675002
Hydrochloric Acid
0.5N
RMARTZ
5/15/2013
6.5N
RMARTZ
5/15/2013
8N
RMARTZ
5/15/2013
Solution
RMARTZ
5/16/2013
Reagent Grade
RMARTZ
5/16/2013
Reagent Grade
RMARTZ
5/16/2013
Rr-1:-RTZ - -
RMARTZ
5/16/2013
--------------~--
013841S
--~--~~-
Date
Recorded
..------
013853S
0138495
0132465
012809P
013221P
-----
--
Hydrochloric Acid
----Hydrochloric Acid
Carbon substrate
Ethyl Alcohol
.
Hydrofluoric Acid
------ ---
..
--
-------
-------~-----------
013191S
Neodymium Carrier
1 mg/ml
013434P
Titanous Chloride
Reagent Grade
5/15/2013
--
-----
5/16/2013
8!73
:--
.....
/1
~~
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--- -+--
ISOTHNOTES
Page 1 of 1
Printed: 5/3/2013 9:49AM
~
#
1
g __~_g_R _ ~~~~
Date
Dept
05/03/13 09:49
PREP
User
JBARNARO
601 Scarboro Rd.

Oak Ridge, TN 37830
Voice: 865.481.0683
Internal Work: Order

Analysis Code
Run Number
13-04132
ThiSO
1
Notes
..0
.b.
...........
$/&-
Printed: 5/8/2013 6:13PM
~I;;
Page 1 of 1
13
E:: RJ._.I_NE::
SERVICES
601 Scarboro Rd.

Oak Ridge, TN 37830
Voice: 865.4&;1.0683
Internal Work Order

Analysis Code
Run Number
13-04132
ThiSO
1
Date
Dept
05/03/13 09:49
PREP
JBARNARD
ALIQ~OTED
05/08/1318:13
CHEM
JDEMELAS
Added concentrated HN03 to sample beakers and heated to dryness; Added 20 ml 8N HN03 to samples and
transferred to new, labeled C-Tubes, adding 8N HN03 to bring volume to 35 ml; Preconditioned resin columns
with 50 ml 8N HN03; Centrifuged samples as needed, and passed through columns; Rinsed C-Tubes with 20
ml 8N HN03; Centrifuged rinsates and loaded onto columns; Rinsed columns with 40 ml 8N HN03; ElUted
Thorium with 50 ml of 8N HCI into clean, labeled 100-ml beakers; Dried-down samples on hotplate; Dissolved
samples in -10 ml of concentrated HCI; Transferred to new, labeled C-Tubes with deiononized water, bringing
volume to -15ml. Set samoles aside for later orecioitation and filterina.
User
Notes
AND FILTERED DISSOLVED FRACTIONS ADDED SPIKES AND TRACERS ADDED HN03
Printed: 5/9/2013 6:01AM
jfJ E::: ~ E;; R

~
Page 1 of 1
L I "! _!;;:
SERVICES
!'
Date
Dept
2 510811 3 1 8 1 3
---~~~
0 51
_..
: _ _
11 30 9 4 9
PREP
'
User
JBARNARD
CHEfVf"" "--JDEMELAS
05/09/13 06:01
CHEM
RMARTZ
601 Scarboro Rd.

Oak Ridge, TN 37830
Voice: 865.481.0683
Internal Work Order 1
......!. .
Analysis Code I
Run Number
13-04132
ThiSO
1
Notes
-
~~~~~~~~~V~N~:~~TL~~~~~~~~6~~~~~~~~~NS- ADDED SPIKES AND TRACERS- ADDED HN03

--Ad-Ci9d-cOncentrated HN03.i0-Sampi8.be8kers and-h8'8i8-dt0dryneSs; Added.20rilT8N HN03 tO samples andtransferred to new, labeled C-Tubes, adding 8N HN03 to bring volume to 35 ml; Preconditioned resin columns
with 50 ml 8N HN03; Centrifuged samples as needed, and passed through columns; Rinsed C-Tubes with 20
ml 8N HN03; Centrifuged rinsates and loaded onto columns; Rinsed columns with 40 ml 8N HN03; Eluted
Thorium with 50 m! of 8N HCI into clean, labeled 100-ml beakers; Dried-down samples on hotplate; Dissolved
samples in -10 ml of concentrated HCI; Transferred to new, labeled C-Tubes with deiononized water, bringing
volume to -15m!. Set samples aside for later precipitation and filtering.
ADDED 0.75 ML 0.1 MG/ML CERIUM CARRIER & 1 ML HF TOG-TUBES & LET SET SIT IN ICE BATH FOR
ONE HOUR; SET UP FILTERS BY ADDING ALCOHOL & CARBON SUBSTRATE THEN ADDED SAMPLES;
WHEN SAMPLES WERE THROUGH FILTERS, ADDED 10 ML Dl H20 RINSES FROM C-TUBES,
REMOVED FILTERS LET DRY IN OESSICATOR THEN SENT SET TO COUNT ROOM.
Eberline Analytical
Printed: 5/9/2013 6:02AM

Page 1 of 1
ThiSO

Reagent
ID
Reagent
Name
Reagent
Concentration
1
Analyst
ID
Date
Recorded
~~Ol'~"''c~~,,.A~>>n~--------~-~N~it~ri~c~A~c~id~----------------~-~R~ea~g~e~n~t~G~r~a~de~------~~JB~A~R~N~A~R~D~---~~5/3/2013
013708P
Reagent Grade
JDEMELAS
5/8/2013
013839S
Hydrochloric Acid
8N
JDEMELAS
5/8/2013
013809P
Hydrochloric Acid
Reagent Grade
JDEMELAS
5/8/2013
1------------ ----~--- +-------
--------- ------=--------------+------------+--'---'----
[-----------------+-------------------------------- -------------------1---------+-'--'------1
tiH\181
-~...:_:.....::.:-.=:.:~,--------------~--:.--,:~._.,:__.~.;_~-~;_o;_C::i_.,,{_""'j_...;,'~.;;:;:c:;:'::;.--~ ~:; ~---~.-<_;_:_..:;-;._;~;,_;~~-::;;;;~---~--;.;~.-.;.-~_,_~:_.;_;~---<~-~;_-
~cb~-~-~- --~- .
'
....
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. .-.
..
,,, .' '
. ... 1U!82
.~
=====1==-----~-J--~----~---~==r===~j
.
,.-.
:,,
....
RA-226 NOTES
Printed: 5/3/201312:44 PM
Page 1 of 1
""M; E;_s E
RL
l_f'.,!_E
SERVICES
#
1
..
Date
05/03/13 12:44
Dept
PREP
User
JBARNARD
601 Scarboro Rd.

Oak Ridge, TN 37830
Voice: 865.481.0683
Internal Work Order
Analysis Code
Run Number
13-04132
Ra226
1
Notes
AU QUOTED AND FILTERED DISSOLVED FRACTIONS~ ADDED SPIKES AND TRACERS- DRIED
SAMPLES 4AND 18 DOWN AND DIGESTED DUE TO SAMPLES BEING DIRTY~ FRACTION 18 WAS
EXTREMELY DIRTY~ PH'D SAMPLES- PRECIPITATED WITH BAAND PB CARRIERS AND AMMONIUM
SULFATE~ DECANTED SAMPLES AND CENTRIFUGED~ SUBMITTED RADIUM PRECIP TO
SEPARATIONS
Page 1 of 1
Printed: 511412013 4:58PM
~
#
~---~. E;J~--~-t~c-~
Date
Dept
05/03/13 12:44
PREP
JBARNARD
User
05/09/13 18:18
PREP
LWALKER
05/14/13 16:58
PREP
LWALKER
601 Scarboro Rd.

Oak Ridge, TN 37830
Voice: 865.481.0683
Internal Work Order
Analysis Code
Run Number
13-04132
Ra226
1
Notes
ALIQUOTED AND FILTERED DISSOLVED FRACTIONS- ADDED SPIKES AND TRACERS- DRIED
SAMPLES 4AND 16 DOWN AND DIGESTED DUE TO SAMPLES BEING DIRTY- FRACTION 16 WAS
EXTREMELY DIRTY- PH'D SAMPLES- PRECIPITATED WITH BAAND PB CARRIERS AND AMMONIUM
SULFATE- DECANTED SAMPLES AND CENTRIFUGED- SUBMITTED RADIUM PRECIP TO
SEPARATIONS
ADDED EDTA TO PRECIP-VORTEX-LET SIT OVERNIGHT TO DIGEST.
FOLLOWED STEPS 12.1 TO 12.6 IN AP-006 REV 12 FOR RA 226 ANALYSIS (SYRNGE FILTEREDPRECIP-FILTERED-DRIED-OBTAIN FINAL WEIGHT}-SUBMIT TO COUNT ROOM.
Printed: 5/15/2013 10:47 AM
Eberline Analytical
Page 1 of 1
EBERLINE
SERVICES
013376P
Ammonium Hydroxide
Reagent Grade
JBARNARO
5/3/2013
013575002
Ammonium Sulfate
200 mg/ml
JBARNARO
5/3/2013
012766014
Barium Carrier
1 mg/ml
JBARNARO
5/3/2013
012729007
Lead Carrier
166 mg/ml
JBARNARO
5/3/2013
013624P
Nitric Acid
Reagent Grade
JBARNARO
5/3/2013
013416P
Perchloric Acid
Reagent Grade
JBARNARO
5/3/2013
009098P
Sulfuric Acid
Reagent Grade
JBARNARO
5/3/201
013824S
EOTA
0.25M
LWALKER
011383P
Acetic Acid
Reagent Grade
LWALKER
013751001
Ammonium Sulfate
200
LWALKER
----+~)"--'-'-/IIJ"-'-'-f'?. _I~Lf2"}-74h'f-l 41
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An\ "Z.i'J \Ct'?
__ ~~$ _.L:2Q'-U2~~_(.._y_-_l~S fm~-1'~. I<,~ UvSl>..:.... b.-It_ ~
---+----1--
__________..__ ------------1--------t-- - - - - 1 - - - - - - 1 - - -
- ______.. ___ ,_. __ ..______ --+------1----- ---------------- -----,------+-----+-----+----+---
--+----- ------------- ------- ---1--------l-------1-----1--,

--+------ - - - -----------------t----+----1----1----+-----1-------------- - - - - ----- - - - - - - - - - - - - f - - - - - - - f - - - - - ' 1 - -
--+-----+--------- --------------------+------1------+-----}---
--+----1----------- -----------!----
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- - - - -.. - - - - - - - - f - - - - - - - - - - 1 - - - - - - l - - - - - - } - - - - l - - - ......
--f----t-------------------+-------1-----l------t-----l---!"----+------ . . - ---- --
----1-
- -..- - - - + - - - - 1 - - - - - t - - - + - - - - ; .
------~-------- -~--------1----1----+-----1-----.';:'
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----l---------------1--------+----+-------+---+-----?'
i
--- - - - - - - - - - - - - - - - - - - - - - - - - - ------t---~+-----1------'-?."
.::
. -.. -----.. ----- -------------- ----+------+----~----- T'(. ,,
____,--- -------..
'~--.:
~~--;::-:"
:--;-.--
. . ----- - --------
-
---------- - . - - - - - - - - - - 1 - - - -
-J
______ <
RA-228 NOTES
Printed: 5/3/2013 12:44 PM
Page 1 of 1
jt) !;:; 1::u;;:_~L l__t-,1_1;::

~
SERVICES
#
1
Date
Dept
05/03/13 12:44
PREP
User
JBARNARD

601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
Internal Work Order
Analysis Code
Run Number
13-04132
Ra228
1
Notes
SAMPLES 4 AND 18 DOWN AND DIGESTED DUE TO SAMPLES BEING DIRTY- FRACTION 18 WAS
SEPARATIONS
Printed: 5/20/2013 8:13PM
~
#
Page 1 of 1
E;_~;J__ ~__R.bltilc-~
User
Date
Dept
05103/13 12:44
PREP
JBARNARD
05/16/13 12:37
PREP
LWALKER
05/20/13 20:13
PREP
LWALKER
601 Scarboro Rd.

Oak Ridge 1 TN 37830
Voice: 865.481.0683
13-04132
Ra228
Internal Work Order
Analysis Code
Run Number
Notes
ALl QUOTED AND FILTERED DISSOLVED FRACTIONS- ADDED SPIKES AND TRACERS- DRIED
SAMPLES 4 AND 18 DOWN AND DIGESTED DUE TO SAMPLES BEING DIRTY- FRACTION 18 WAS
SEPARATIONS
RECEIVED FILTERS BACK FROM COUNT ROOM-PUT BACK INTO C-TUBES-ADDED EDTA AND
SWIRLEDLET SIT OVERNIGHT TO DIGEST.
FOLLOWED STEPS 12.1 TO 12.7 IN AP-007 REV 18 (CHEMICAL CLEANUP FOR RA 228)
.~'
}8)__
""
Page 1 of 1
Printed: 5/21/2013 1:09PM
~
E;; a
~
E:: R I,., I N 1:::

SERVICES
I
I

601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
Internal Work Order
Analysis Code
Run Number
13-04132
Ra228
1
#I
Date
05/03/13 12:44
PREP
JBARNARD
05/16/13 12:37
PREP
LWALKER
05/20f;:13;-:2;;;0;:::1"3c+-cp;;;R"'E"'P-t-c;LW=A"LK;;Eoc;R------l--;F"O"L,-LO"'W=E;;D:-;S:o;T"'E"'PS""1"2.71 "T"'o""'1""2.""7"1N""A"P-"""o"'o7;-R;;-E;;V=18"("'C"'H"'E"'M"'IC"'A"L""'C"'L""'EA=N"U"'P""'F"'O"'R"RA;-;;c2;;-;2;;;8,-)------11
05/21/13 13:09
Dept
CHEM
User
TSMITH
Notes
SAMPLES 4AND 18 DOWN AND DIGESTED DUE TO SAMPLES BEING DIRTY- FRACTION 18 WAS
EXTREMELY DIRTY- PH'D SAMPLES- PRECIPITATED WITH BA AND PB CARRIERS AND AMMONIUM
SEPARATIONS
RECEIVED FILTERS BACK FROM COUNT ROOM-PUT BACK INTO G- TUBES-ADDED EDTA AND
SWIRLED-LET SIT OVERNIGHT TO DIGEST.
Followed steps 12.7 to 12.15 in AP-007 rev. 17. (Precipitated samples, hot bathed, centrifuged, and discarded
supernate. Dissolved precip, precipitated samples, hot bathed, centrifuged, and discarded supernate.
Dissolved precip, precipitated and filtered samples, obtained final weights, covered with aluminum foil, and
took to count room l
Eberline Analytical
Printed: 5/21/2013 1:29PM

Page 1 of 1
~ !;:;~!"' Rh~t"o!'i
Internal Work Order
13-04132
Analysis Code
Ra228

Reagent
ID
Run
1---------
Reagent
Name
Reagent
Concentration
Analyst
ID
Date
Recorded
0
! _(J.Ol~:13T~l~77_6~~p~--+--A~mlflml1_'o:_rn~i:ull_lm":__H:!:Yf.C.d!':r:'l.ox~i~d_:e______~f--~
-:g~:':~"G~r~ad~e:._____j_~JB~A~R~N~A~R~D~-
5/3/2013
---+-----1
Ammonium Sulfate
200 mg/ml
JBARNARD
5/3/2013
------------------------------------------+----- --=---------- -------1-----------+____:_..:_______ _
r-
013575002
1-----------------1
012iot>Ll14
Barium Carrier
1 mg/ml
JBARNARO
5/3/2013
1--- - --------------------+---------------------------------------------+------------------------------- ---------------t--012729007
Lead Carrier
166 mg/ml
JBARNARD
5/3/2013
-------
-------------1----"-------t----------+--'---1
r--0_13_6_2_4_P_ _ _++_N_itr_ic_A_ci_d___________++_Re_a~g~e_n_t_G_r_a_d_e_ _ _ _r-_JB_A_R_N_A_R_D

_ _~_5j3/2013
013416P
Perchloric Acid
Reagent Grade
JBARNARO
5/3/2013
2%
LWALKER
5/20/2013
Reagent Grade
LWALKER
5/20/2013
10M
LWALKER
5/20/2013
-----+--------+-------009098P
Sulfuric Acid
Reagent Grade
JBARNARD
5/3/2013
-------------------------c------------------------------------- ------------------------ ----------------+--------------1
1-------------------011504023
------------------+-------
~mmonium
Sulfide
13797P
Nitric Acid
13690S
Sodium Hydroxide
---------
--------------------------- ----r----='---------+------j--------~
-----!
L_(l22~().~_:>_____
Y~tri ~'_11_-~arrier ______________ -~mg/m_l_____ _____ ---~WALK~--~0_!l~~_!l-~
~~?29009
1-
Lead Carrier
1.5 mg/ml
LWALKER
5/20/2013
0127170().5
Ammonium Oxalate_
5%
TSMITH
5/21/2013
013624009
Nitric Acid
1N
TSMITH
j_5/21/2013
3j'
--=:=== :
_
t==o~~6-~~~-=-- ----Nit_~~~:~~<J=:-~===~=====~ -6N _

~_(ll3690S
Sodium Hydroxide
L~oM
013065004
Sodium Hydroxide
18M
Ts~!TH___
___ _r_s;211~~~-~
TSMITH
5/21/~013
TSMITH
5/21/2013
.;_-__ ,
_.:-'..
. .
~s_;?~L*j;~"""--.:~_-;___~o:"---
-.
- -- - --- -- -------- I -- -- ----~-----'f--~~--1-----~~+---~-1---
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fiUi197-
. -.
SECTION VIII
ANALYTICAL DATA (ISOTOPIC URANIUM)
RUNl
Eberline Services
13-04132

Analysis Sheet
UUISO
Run 1
Internal
Fraction
Work Order
Analysis Code
-------Run
! Sample
UUJSQ
f-
Desc
Client
ID
~:~ l
Sample
Date
03
I DUPt--,
. -~~106:1<_~TO_T_ j .-~-1
1---------
~-14 ~OT
' TRG
West Lake OU-1
06
TRG
PZ-112-AS TOT
D-14 DIS
Report Level
01
TRG-,-
PZ-112-AS_DIS
Activity Units
pCi
08
TRG
PZ-202-SS TOT
Aliquot Units
09
TRG
PZ-202-SS
Method
EML
U-02 Modified
Instrument
I - Alpha Spectroscopy
1-- - - - -Type
--+
11
TRG
12
38
TQ4/12/13 11:05
38
04/12/13 11:05
45
04/12/13 11:18G-_oooo'E-:.:oo
45
04/12/1311:18
46
04/12/13 12:32~~-0000E+OO
46.
04/12/13 12:32
1-.0000E+OO
------
.T
---+-;
oo [
DUP07 DIS
40
04/12/13 oO:oor- 1.0000E+OO
36
04/15/13 15:59
1.0000E+OO
FB at PZ-1 00-KS TOT
39
04/16/13 08:40
1.0000E+OO
FB at PZ-100-KS DIS
39
I 04/16/13 08:40 I
1.0000E+OO
37
04/16/13 08:50
1.0000E+OO
TRG
Tracer Act (dpmlg)
19.089
15
TR~-
16
TRG
-+-
PZ-100-KS TOT
-----
17
TRG
PZ-100-KS DIS
37
04/16/13 08:50
1.0000E+OO
18
TRG
S-53 TOT
41
04/16/13 09:00
1.0000E+OO
TRG-+-
S-53_[l'~-----
41
04/16/13 09:00
1--1-----ll
1.0000E+OO
04/15/131~1.ooooE+o~
14
--+---------
..
36 ..
PZ-106-KS TOT
U-1 Oa
Carrier Cone (mglml)
1.ooooE.~~~
04/12/13 00:00
Radiometric Sol# I
--------j I
1.0000E+OO
40
PZ-106-KS DIS
.
DUP07 TOT
TRG
Carrier
1-
TRG
-~-OOE+OO
D;s---~
1
U232 ----II 13
Radiometric Tracer
f-
10
Sample
Aliquot
04/~~/1315:59 i-~~OOE+~~
WA
B~:~K---+-i ::~::~::::::: ~~~;:~~~~

---~------I=-----
05
Matrix I
~~_J_
Client I Engineering Management Support, Inc.
Login
CPM
::
I--
Date Received
4/18/2013
-----------------Lab Deadline
5/9/2013
Project I
Printed: 5/9/2013 6:02AM

Page 1 of3
19
['
I
-1
i
1.0000E+OO
'~
""''
1!!11
.., SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.
**Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
Eberline Services
Analysis Sheet
13-04132
Printed: 51912013 6:02AM

Page 2 of 3
UUISO
Run 1
Internal [ Sample
Fraction ; Desc
-~
Tracer
Aliquot (g)
~~---Tracer Total I
ACT (dpm)
_l_
TRG
~-07 JTRG I
I 08 I TRGT
09
10
.11
TRG
;~diametric
% Rec
0.5744
TRG
I_ _ _
I DO
f-~t
12
I Grav Carrier
, Added (ml)
::a_ T~~:1
11:'ll__
0.5941
-11.31
0.5911
11.3!
0.5793
11.1
0.5954 I
0.5586 I
11.4f
10.7 I
TRG
Radiometric
Tracer (pCi)
,--~ ~-:.: I ::: I

06
I
I
'
Grav Filter
Tare (g)
Grav Filter
Final (g)
Grav Filter
Net (g)
1 4 / TRG
1--
'
1--2.:._1
TRG
o.5ao3
11.1
:~ ~
11.2
11.0
0.58821
TRG
19
, TRG
.58
0.5772
Grav
Mean
SAF
SAF
% Rec
% Rec
1.
2.
i--
~-~--------1--t
-t--
0.00
-+-~-
--
~~--~-.-----J..----1----~+
-+--+~
I
11.1
1-
--+---...J-----l
+ - - I
~ f:- -=-L--+:-----+--
""SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.
---1-----l
+------
---1
-+----~------T---~~---i
l<.lr.
..j
'
aa
~~
0.'
----+----+------+-------+------+-----+--11.1
18
T -~ -I- I
--+'---t=-=L-=1
,
TRG
----+-------+-+--+----
13
1--
---+--- ~
0.00
+--~:00,
...,.. Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
Eberline Services
Analysis Sheet
13-04132
Printed: 5/9/2013 6:02AM

Page3of3
UUISO
Run 1
Internal
Fraction
I Sample
I Desc
Rough Prep
Date
-~~-+LCS
02
--
'
'
MBL
. 03-1 ~;'
04
TRG
'----- ----
,--,-+
~~TRG
I
-+--,___T
--~-----l_
,-------
06
RoughPrep
By
TRG
- - -[ - - ' - - - - - - - - -
07
I
'
'
Prep
Date
05/03/13
TRG
09
TRG
10
TRG
09
05/03/13 09:431
! 05/03/13 09:43_[
05/03/13 09:43
TRG
12
DO
----~-
13
TRG
14
TRG
15
TRG
16
TRG
17
TRG
05/03/13 09:43
'i
05/03/13 09:43
05/03/13 09:43
_,
=
__
L
=
~
-+
I
--
JBARNARD
i---
____
JBARNARD
05/03/13 09:43
JBARNARD
05/03/13 09:43
JBARNARD
' 05/03/13 09:43
JBARNARD
05/03/13 09:43
JBARNARD
TRG
19
TRG
05/03/13 09:43
--+
JBARNAR~
I
t_____.,_
________
----+
* SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.
1
__
+j_ +---
--I__----
....
1':.1
__-___
~~
l!'.il
'
I 0510~13 ' '431 JBARNARD

I
---
18
---~,---
JBARNARD
1
__
=J, - ----1
---'t----1
.=r =: . ---1
'
::;;: ::: I~:~~:t_
--+
f-'-----r
Sep t1
By
JBARNARD
JBARNARD
Sep t1
Date/Time
JBARNAR~
SeptO
By
~-,-~_, _ _ _ T _ _ _ _ _
05/03/13 09:43 - JBARNARD
--
JBARNARD
- 05/03/13 09:43,- JBARNARD
11
~ _,
05/03/13 09:43 JBARNARD '
'
08
SeptO
Date/Time
09:43~RNAR~
I 05ro~13 43
TRG
Prep
By
Eberline Services
~
~
0:
.g
0
"
.~
~
~
<(
"'
U-234
LCS
LCS
pCi/1
7.58E+OO
1.14E+OO
1.08E-01
02
U-234
MBL
BLANK
pCi/1
6.33E-02
S.SOE-02
1.33E-01
03
U-234
DUP
PZ-106-KS TOT
pCi/1
2.19E+OO
4.14E-01
5.62E-02
04
U-234
TRG
D-14 TOT
pCi/1
7.50E-01
3.94E-01
2.64E-01
OK
en
05
U-234
TRG
D-14 DIS
pCill
1.97E-01
3.39E-01
5.90E-01
OK
::J
::J
06
U-234
TRG
PZ-112-AS TOT
pCI/1
-4.29E-02
1.72E-01
4.41E-01
OK
07
U-234
TRG
PZ-112-AS DIS
pCi/1
6.37E-01
4.58E-01
4.53E-01
OK
08
U-234
TRG
PZ-202-5S TOT
pCi/1
1.69E+OO
3.37E-01
6.98E-02
OK
09
U-234
TRG
PZ-202-5S DIS
pCi/1
1.62E+OO
3.17E-01
4.80E-02
OK
10
U-234
TRG
DUP07TOT
pCi/1
1.55E-01
1.62E-01
1.69E-01
OK
11
U-234
TRG
DUP07 DIS
pCI/1
2.33E-01
1.86E-01
1.67E-01
OK
12
U-234
DO
PZ-1 06-KS TOT
pCi/1
2.25E+OO
4.00E-01
4.91E-02
OK
.;
.E
13
U-234
TRG
PZ-106-KS DIS
pCi/1
2.02E+OO
3.69E-01
5.62E-02
OK
t:0
14
U-234
TRG
FB
at PZ-100-KS TOT
pCi/1
7.58E-02
6.60E-02
7.57E-02
OK
"'".c
15
U-234
TRG
FB
at PZ-100-KS DIS
pCi/1
7.38E-02
6.13E-02
7.14E-02
OK
16
U-234
TRG
PZ-100-KS TOT
pCi/1
1.62E-01
9.38E-02
6.82E-02
OK
c
:;;
"'"'
17
U-234
TRG
PZ-100-KS DIS
pCi/1
7.02E-02
5.84E-02
5.02E-02
OK
."'c
18
U-234
TRG
S-53 TOT
pCi/1
1.14E+01
7.37E+OO
2.13E+OO
INV
19
U-234
TRG
S-53 DIS
pCi/1
5.90E+OO
8.20E-01
7.25E-02
OK
Units
c.
c.
"'
;:
;:;,
c
w
'~
.....
~~$
t.l
Results
Error Estimate
MDA
LCS
Known
8.12E+OO
LCS
LCS
%R
Flag
93.29
OK
RPD
Flag
MDA
Flag
Blank
Flag
OK
OK
T""
ill
Sample
Activity
01
Work Order: 13-04132-UUIS0-1
Client
Identification
Nuclide
Printed: 5/10/2013 8:43 AM

Page 1 of 3
Deso
a-!l'!:
~
Lob
Fraction
Preliminary Data Report & Analytical Calculations
OK
OK
OK
Eberline Services
,:
~
~
0:
.g
0
(J
.!!/
...~
~
<(
Nuclide
01
U-234
LCS
04/18/13 00:00
1.00E+OO
81.94
0.00
0.00
02
U-234
MBL
04/18/13 00:00
1.QOE+OO
56.59
0.00
0.00
03
U-234
DUP
04/15/1315:59
1.00E+OO
103.70
0.00
0.00
04
U-234
TRG
04/12/1311:05
1.00E+OO
33.64
0.00
0.00
en
05
U-234
TRG
04/1211311:05
1.00E+OO
14.80
0.00
0.00
:::l
:::l
06
U-234
TRG
04/1211311:18
1.00E+OO
18.79
0.00
0.00
07
U-234
TRG
04/12/1311:18
1.00E+OO
23.14
0.00
0.00
08
U-234
TRG
04/1211312:32
1.00E+OO
124.13
0.00
0.00
09
U-234
TRG
04/1211312:32
1.00E+OO
118.63
0.00
0.00
.,~
10
U-234
TRG
04/12113 00:00
1.00E+OO
35.91
0.00
0.00
11
U-234
TRG
04/12113 00:00
1.00E+OO
40.96
0.00
o.oo
12
U-234
DO
04/15/1315:59
1.00E+OO
123.48
0.00
0.00
13
U-234
TRG
04/15/1315:59
1.00E+OO
126.72
0.00
0.00
t:
0
c.
c.
14
U-234
TRG
04/16/13 08:40
1.00E+OO
110.S2
0.00
0.00
15
U-234
TRG
04/16/13 08:40
1.00E+OO
123.82
0.00
0.00
"
E
""'
16
U-234
TRG
04/16/13 08:50
1.00E+OO
110.70
0.00
0.00
17
U-234
TRG
04/16/13 08:50
1.00E+OO
116.03
0.00
0.00
c"'
c
18
U-234
TRG
04/16/13 09:00
1.00E+OO
4.17
0.00
0.00
""
.5
19
U-234
TRG
04/16/13 09:00
1.00E+OO
120.51
0.00
0.00
Sample
"'"
Sample
Date
Sample
Aliquot
Radiometric
%Rec
G"v
Mean
%Rec
%Rec
SAF
Sep to
Sep t1
Date!Time
DatefTime
"r""
-!:
0
Printed: 5/10/2013 8:43AM

Page 2 of 3
Lob
Fraction
l
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ill
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w
~~
~~~,
t:~
tlii.
'
Eberline Services
Lab
Nuclide
Fraction
Printed: 5/10/2013 8:43AM

Page 3 of 3
Desc
Counting
DatefTime
Sample
Halflife
(days)
Detect
Carrier
Count
Time
Counts
Bkg
Eff
CPM
01
U-234
LCS
05/09/13 09:57
A_ Spec
Alpha_041
170 4.63 E+02
7.00 E.03
19.8
02
U234
MBL
05/09/13 09:57
A_Spec
Alpha_042
170 2.49 E+OO
3.00 E03
18.5
03
U234
DUP
05/09/13 09:57
A_ Spec
Alpha_044
170 1.63 E+02
1.00 E03
19
04
U234
TRG
05109/13 09:57
A_Spec
Alpha_046
170 1.70 E+01
0.00 E+OO
17.9
U)
05
U-234
TRG
05/09/13 09:57
A_Spec
Alpha_047
170 2.00 E+OO
0.00 E+OO
18.2
::::l
::::l
06
U234
TRG
05109/13 09:57
A_Spec
Alpha_048
170 -5.10 E01
3.00 E.03
16.8
07
U-234
TRG
05/09/13 12:54
A_Spec
Alpha_025
170 9.64 E+OO
8.00 E03
17.4
08
U-234
TRG
05/09/13 12:54
A_ Spec
Alpha_027
170 1.36 E+02
4.00 E03
17.3
i!
09
U234
TRG
05/09/13 12:54
A_Spec
Alpha_029
170 1.41 E+02
1.00 E.03
19.5
10
U-234
TRG
05/09/1312:55
A_Spec
Alpha_o33
170 3.83 E+oo
1.00 E03
18.2
11
U-234
TRG
05/09/1312:55
A_Spec
Alpha_034
170 6.66 E+OO
2.oo E03
18.6
12
U234
DO
05109113 12:55
A_Spec
Alpha_035
170 1.91 E+02
1.00 E.03
18.3
.;
.E
t!
13
U234
TRG
05109/1312:55
A_Spec
Alpha_037
170 1.72 E+02
2.00 E03
17.8
14
U-234
TRG
05/09/1312:55
A_Spec
Alpha_040
170 6.00 E+OO
o.oo E+OO
19
-...
15
U-234
TRG
05/09/13 12:55
A_Spec
Alpha_041
170 6.81 E+OO
7.00 E03
19.8
16
U234
TRG
05109/13 12:55
A_Spec
Alpha_042
170 1.25 E+01
3.00 E03
18.5
17
U-234
TRG
05109/1312:55
A_Spec
Alpha_044
170 5.83 E+OO
1.00 E03
19
C)
18
U-234
TRG
05109/1312:55
A_Spec
Alpha_046
170 3.20 E+01
0.00 E+DO
17.9
19
U234
TRG
05/09113 12:55
A_Spec
Alpha_047
170 4.88 E+02
0.00 E+OO
18.2
0:
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0
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~
~
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---
- - - - -L
---
----
----
----
'--
Eberline Services
0:
Lob
Fraction
Nuclide
Printed: 5/10/2013 8:43AM

Page 1 of 3

Sample
Desc
Client
Activity
Identification
Units
01
U-238
LCS
LCS
pCi/1
02
U-238
MBL
BLANK
03
U-238
DUP
PZ-106-KS TOT
Results
Error Estimate
MDA
7.55E+OO
1.13E+OO
1.46E-01
pCi/1
4.20E-02
7.14E-02
1.21 E-01
pCi/1
7.78E-01
2.19E-01
8.04E-02
LCS
LCS
LCS
Known
%R
Flag
95.33
OK
7.92E+OO
RPO
Flag
MOA
Flog
OK
OK
OK
04
U-238
TRG
D-14 TOT
pCi/1
1.05E+OO
4.68E-01
1.83E-01
05
U-238
TRG
D-14 DIS
pCill
3.76E-01
3.99E-01
4.09E-01
OK
06
U-238
TRG
PZ-112-AS TOT
pCi/1
2.23E-01
2.93E-01
4.00E-01
OK
07
U-238
TRG
PZ-112-AS DIS
pCill
O.OOE+OO
1.82E-01
3.95E-01
OK
-e
OS
U-238
TRG
PZ-202-SS TOT
pCill
7.76E-01
2.11E01
7.77E-02
OK
"/!
09
U-238
TRG
PZ-202-SS DIS
pCi/1
6.28E-01
1.79E-01
4.78E-02
OK
10
U-238
TRG
DUP07TOT
pCIII
3.35E-02
8.04E02
1.68E-01
OK
11
U-238
TRG
DUP07 DIS
pCill
1.33E-01
1.39E01
1.45E-01
OK
12
U-238
DO
PZ-106-KS TOT
pCill
8.56E-01
2.18E-01
7.03E-02
OK
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13
U-238
TRG
PZ-106-KS DIS
pCi/1
7.25E-01
1.97E01
7.02E-02
OK
14
U-238
TRG
FB at PZ-100-KS TOT
pCill
5.65E-02
5.59E-02
6.60E-02
OK
15
U-238
TRG
FB at PZ-100-KS DIS
pCill
-2.22E-02
2.62E-02
9.64E-02
OK
16
U-238
TRG
PZ-100-KS TOT
pCill
6.03E-02
5.74E-02
6.18E-02
OK
17
U-238
TRG
PZ-1 00-KS DIS
pCill
9.58E-02
7.12E-02
7.18E-02
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1.83E+01
1.12E+01
1.48E+OO
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4.74E+OO
6.9DE01
5.03E-02
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U-238
LCS
04118113 00:00
1.00E+OO
81.94
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U-238
MBL
04/18113 00:00
1.00E+OO
56.59
0.00
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DUP
04/1511315:59
1.00E+OO
103.70
0.00
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U-238
TRG
0411211311:05
1.00E+OO
33.64
0.00
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TRG
0411211311:05
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14.80
0.00
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06
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TRG
0411211311:18
1.00E+OO
18.79
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TRG
04/1211311:18
1.00E+OO
23.14
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U-238
TRG
04/1211312:32
1.00E+OO
124.13
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TRG
04112113 12:32
1.00E+OO
118.63
0.00
0.00
10
U-238
TRG
04112113 00:00
1.00E+OO
35.91
0.00
0.00
11
U-238
TRG
04112113 00:00
1.00E+OO
40.96
0.00
0.00
12
U-238
DO
04/1511315:59
1.00E+OO
123.48
0.00
0.00
13
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TRG
04/1511315:59
1.DOE+OO
126.72
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TRG
04/16113 08:40
1.00E+OO
110.62
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0.00
15
U-238
TRG
04116113 08:40
1.00E+OO
123.82
0.00
0.00
16
U-238
TRG
04116113 08:50
1.00E+OO
110.70
0.00
0.00
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17
U-238
TRG
04/16113 08:50
1.00E+OO
116.03
0.00
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TRG
04116113 09:00
1.00E+OO
4.17
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04116113 09:00
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120.51
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Nuclide
Sample
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Datemme
01
U-238
LCS
02
U238
03
Halflife
Count
Bkg
Detect
Carrier
05/09/13 09:57
A_Spec
Alpha_041
170 4.63 E+02
1.80 E-02
19.8
MBL
05/09/13 09:57
A_Spec
Alpha_042
170 1.66 E+OO
2.00 E-03
18.5
U-238
DUP
05/09/13 09:57
A_Spec
Alpha_044
170 5.80 E+01
0.00 E+OO
19
04
U-238
TRG
05/09/13 09:57
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Alpha_046
170 2.38 E+01
1.00 E-03
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(days)
Time
Counts
CPM
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U-238
TRG
05/09/13 09:57
A_ Spec
Alpha_047
170 3.83 E+OO
1.00 E-03
18.2
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06
U-238
TRG
05/09/13 09:57
A_Spec
Alpha_048
170 2.66 E+OO
2.00 E-03
16.8
07
U-238
TRG
05/09/13 12:54
A_Spec
Alpha_025
170 1.00 E+OO
0.00 E+OO
17.4
08
U-238
TRG
05/09/13 12:54
A_Spec
Alpha_027
170 6.30 E+01
6.00 E-03
17.3
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U-238
TRG
05/09/1312:54
A_Spec
Alpha_029
170 5.48 E+01
1.00 E-03
19.5
10
U-238
TRG
05/09/1312:55
A_Spec
Alpha_033
170 8.30 E-01
1.00 E-03
18.2
11
U-238
TRG
05/09/1312:55
A_Spec
Alpha_034
170 3.83 E+OO
1.00 E-03
18.6
12
U-238
DO
05/09/1312:55
A_Spec
Alpha_035
170 7.30 E+01
0.00 E+OO
18.3
13
U-238
TRG
05/09/13 12:55
A_Spec
Alpha_037
170 6.20 E+01
0.00 E+OO
17.8
14
U-238
TRG
05/09/1312:55
A_Spec
Alpha_040
170 4.49 E+OO
3.00 E-03
19
15
U-238
TRG
05/09/1312:55
A_Spec
Alpha_041
170 -2.06 E+OO
1.80 E-02
19.8
16
U-238
TRG
05/09/1312:55
A_Spec
Alpha_042
170 4.66 E+OO
2.00 E-03
18.5
17
U-238
TRG
05/09/1312:55
A_ Spec
Alpha_044
170 8.00 E+OO
0.00 E+OO
19
18
U-238
TRG
05/09/13 12:55
A_Spec
Alpha_046
170 5.18 E+01
1.00 E-03
17.9
19
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TRG
05/09/13 12:55
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170 3.94 E+02
1.00 E-03
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8.87E-02
1.08E-01
1.31E-01
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U-235
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PZ-106-KS TOT
pCi/1
2.13E-01
1.20E-01
6.93E-02
04
U-235
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1.10E-01
2.60E-01
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U-235
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2.49E-01
6.37E-01
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TRG
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2.88E-01
6.22E-01
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5.38E-02
1.65E-01
3.90E-01
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pCi/1
1.27E-01
9.14E-02
8.61E-02
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09
U-235
TRG
PZ-202-SS DIS
pCi/1
5.44E-02
5.61E-02
5.92E-02
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10
U-235
TRG
DUP07TOT
pCi/1
-8.50E-03
9.94E-02
2.09E-01
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11
U-235
TRG
DUP07 DIS
pCi/1
4.31E-02
1.20E-01
2.58E-01
OK
12
U-235
DO
PZ-1 06-KS TOT
pCi/1
7.26E-02
7.02E-02
8.71E-02
OK
13
U-235
TRG
PZ-1 06-KS DIS
pCi/1
8.70E-02
7.57E-02
8.69E-02
OK
14
U-235
TRG
FB
at PZ-100-KS TOT
pCJ/1
4.41E-02
5.34E-02
6.50E-02
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15
U-235
TRG
FB
at PZ-100-KS DIS
pCifl
3.56E-02
4.60E-02
6.39E-02
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16
U-235
TRG
PZ-100-KS TOT
pCi/1
2.93E-02
4.49E-02
6.69E-02
OK
17
U-235
TRG
PZ-100-KS DIS
pCi/1
1.23E-02
2.95E-02
6.19E-02
OK
18
U-235
TRG
S-53 TOT
pCi/1
4.67E+OO
3.83E+OO
2.10E+OO
INV
19
U-235
TRG
S-53 DIS
pCi/1
3.95E-01
1.58E-01
7.83E-02
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Sample
Date
U-235
LCS
04118113 00:00
1.00E+OO
81.94
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02
U-235
MBL
04118113 00:00
1.00E+OO
56.59
0.00
0.00
03
U-235
CUP
0411511315:59
1.00E+OO
103.70
0.00
0.00
04
U-235
TRG
0411211311:05
1.00E+OO
33.64
0.00
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0411211311:05
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0411211311:18
1.00E+OO
18.79
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U-235
TRG
0411211311:18
1.00E+OO
23.14
0.00
0.00
08
U-235
TRG
04112113 12:32
1.00E+OO
124.13
0.00
0.00
09
U-235
TRG
0411211312:32
1.00E+OO
118.63
0.00
0.00
10
U-235
TRG
04112113 00:00
1.00E+OO
35.91
0.00
0.00
11
U-235
TRG
04112113 00:00
1.00E+OO
40.96
0.00
0.00
12
U-235
DO
0411511315:59
1.00E+OO
123.48
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TRG
0411511315:59
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126.72
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04116113 08:40
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110.S2
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04116113 08:40
1.00E+OO
123.82
0.00
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16
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TRG
04116113 08:50
1.00E+OO
110.70
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17
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TRG
04116113 08:50
1.00E+OO
116.03
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04116113 09:00
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4.17
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04116/13 09:00
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120.51
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05/09113 09:57
A_Spec
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170 2.77 E+01
2.00 E-ll3
19.8
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05/09/13 09:57
A_Spec
Alpha_042
170 2.83 E+OO
1.00 E-03
18.5
U-235
DUP
05109/13 09:57
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Alpha_044
170 1.28 E+01
1.00 E-03
19
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05/09113 09:57
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170 -3.40 E-01
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05/09113 09:57
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170 -5.10 E-01
3.00 E-03
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05/09113 09:57
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170 1.00 E+OO
0.00 E+OO
16.8
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TRG
0510911312:54
A_Spec
Alpha_025
170 6.60 E-01
2.00 E-03
17.4
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U-235
TRG
05/0911312:54
A_Spec
Alpha_027
170 8.32 E+OO
4.00 E-03
17.3
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U-235
TRG
05109113 12:54
A_Spec
Alpha_029
170 3.83 E+OO
1.00 E-03
19.5
10
U-235
TRG
05109/1312:55
A_ Spec
Alpha_033
170 1.70 E-01
1.00 E-03
18.2
11
U-235
TRG
05/09/1312:55
A_Spec
Alpha_034
170 1.00 E+OO
0.00 E+OO
18.6
12
U-235
DO
05109113 12:55
A_Spec
Alpha_035
170 5.00 E+OO
0.00 E+OO
18.3
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U-235
TRG
0510911312:55
A_Spec
Alpha_037
170 6.00 E+OO
0.00 E+OO
17.8
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U-235
TRG
05109/1312:55
A_Spec
Alpha_040
170 2.83 E+OO
1.00 E-03
19
15
U-235
TRG
0510911312:55
A_Spec
Alpha_041
170 2.66 E+OO
2.00 E-03
19.8
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05109/1312:55
A_Spec
Alpha_042
170 1.83 E+OO
1.00 E-03
18.5
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U-235
TRG
05/09113 12:55
A_Spec
Alpha_044
170 8.30 E-01
1.00 E-03
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05/09113 12:55
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170 1.07 E+01
2.00 E-03
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10.9647
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11.2835
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11.1804
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11.3656
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11.2778
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5/3/2013 9:42
JBARNARD
LCS & Matrix Spikes

Isotope
Page 1 of 1
Printed: 5/3/2013 9:43AM
Spike and Tracer Worksheet
Sol#
Activity
dpmlg
Solution
Date
Approx
Addition
LCS
MS
LCSD
MSD
Volume
Used(g)
Volume
Used(g)
Volume
Used{g)
Volume
Used(g)
Witness Initials
LCS
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MS
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Estimate
U-234
U-8a
35.240
5/3/2013
0.500
0.5118
0.292
0.001
0.000
U-238
U-Sa
34.350
5/3/2013
0.500
0.5118
0.285
0.00
0.000
Tracers
fraction
l<ll
i<..~.
f.<~~>
!.~
Isotope
Sol#
Activity
dpm!g
MSD
Erro'
Estimate
oool
oool
Added
pCi
Solution !
Date
Volume
Used(g)
Approx
Addition
Tracer
0.00
0.000
0.000
0.00
0.000
LCS
U-232
U-10a
19.089
5/3/2013
0.6073
0.6300
02
U-232
U-10a
19.089
5/3/2013
0.6047
0.6300
0.6073 9
03
U-232
U-10a
19.089
5/3/2013
0.6001
0.6300
0.6047
0.6300
-0.6001
~i
04
U-232
U-10a
05
U-232
U-10a
19.089 '
5/3/2013
. 0.5958
0.6300
06
U-232
U-10a
19.089
5/3/2013
0.5744
0.6300
07
U-232
U-10a
19.089
5/3/2013
0.5941
0.6300
-0. 571f:':, :J
-(i ~ 5958 ;.i
-0.5744 '9
-(3= 5941 .::;_,
08
U-232
U-10a
19.089
5/3/2013
0.5911
0.6300
-0.5911 9
-121.5793 s
09
U-232
U-10a
19.089
5/3/2013
0.5793
0.6300
10
U-232
U-10a
19.089
5/3/2013
0.5857
0.6300
11
U-232
U-1Da
19.089
5/3/2013
0.5954
0.6300
12
U-232
U-10a
19.089
5/3/2013
0.5586
0.6300
13
U-232
U-10a
19.089
5/3/2013
0.5908
0.6300
0.6300
19.089
5/3/2013
0.5716
14
U-232
U-10a
19.089
5/3/2013
0.5864.
15
U-232
U-10a
19.089
5/3/2013
0.5803
0.6300
16
U-232
U-10a
19.089
5/3/2013
0.5882
0.6300
17
U-232
U-10a
19.089
5/3/2013
0.5827
0.6300
18
U-232
U-10a
19.089
5/3/20131
0.5810
0.6300
19
U-232
U-10a
19.089
5/3/20131
0.5772.
0.6300
-13.5>E;I!S7
-0~
ra. 511:::
5954 '=I
Matrix Spike
-0. ::;s::;t. 3
-0. 59~3B :1
-0.5864 :1
-0. 58[13 '3
-0.5882 '3
-0.5:327 9
'-0~5810 9
-0.5772 9
Error
Estimate
0.000
Balance Printer Tapes

1
01
Version 2.0 08/99
Known
pCi
:1
Eberline Analytical
Analysis Code
Rpt Units
Lab Deadline
Technician
UUISO
liters
5/9/2013
JBARNARD
Sample
Muffle Data
Client ID
Type
Ratio
Post/Pre
LCS
BLANK
PZ-106-KS TOT
D-14 TOT
D-14 DIS
PZ-112-AS TOT
PZ-112-AS DIS
PZ-202-5S TOT
PZ-202-SS DIS
DUP07TOT
DUP07 DIS
PZ-106-KS TOT
PZ-106-KS DIS
FB at PZ-100-KS TOT
FB at PZ-100-KS DIS
PZ-100-KS TOT
PZ-1 00-KS DIS
S-53 TOT
S-53 DIS
LCS
MBL
DUP
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
DO
TRG
TRG
TRG
TRG
TRG
TRG
TRG
Work Ord
13-04132
Lab
Fraction
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
No of Oils
Data
t Data
Oil Fact~)
Ratio
D'""''
,b~.
Technician:
Aliquot
1.
1.
I
---------
Net Equ
1.
MS.
Aliquot
I Data
H-3 Solids Only
Net Equlv
(ml)
H3 Oist
Aliq
l-1.
1.
1.
1.0000E+OO
1.0000E+OO
1.
1.
1.
1.
1.
1.
1.
1.
1.
1.
1.
---
1.
I
-
---
--
--
Comments
...~~
Printed: 5/3/2013 9:43AM

Page 1 of 1
Aliquot Worksheet
~-:s~Date:
-r-3 I
--
1.
1.
1.
1:00POE+OO
1.0000E+OO
1.
1.
1.0000E+OO
1.0000E+OO
1.
-.--
-l
Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:
SPIKE
\\OR-ALPHA1\Canberra\ApexAlpha\Root\Data\00000575
1304132A-UU
01
Shelf 2
U iso
Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:
Alpha_041
05026930A
91087
System Bkgd 56377
<not performed>
Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:
1.000E+000 +/- O.OOOE+OOO liter

5/9/2013
6:52:37 AM
5/9/2013
9:57:46 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chern. Recovery Factor:
U232_UU-10A
0.607 mL
0.1621 +/- 0.0098
0.1978 +/- 0.0034 on 12/16/2012
0.8194 +/- 0.0517
Control Certificate Name: Natu U-SA

Chern. Recov. of Control:
U-238
Peak Match Tolerance:
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.263
4. 718
4.398
4.137
T
Net
Pk Area
0.929240 +/-
AREA
0.076392
REPORT
Pk Area
Error %
317.66
462.81
27.66
462.94
5:49:31 PM
Ambient
Backgnd
0.34
1.19
0.34
3.06
11.00
9.12
37.53
9.14
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
13.6
32.1
3.0
8.5
Tracer Peak used for Effective Efficiency
NUCLIDE ANALYSIS RESULTS

Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.989
0.987
0.999
0.984
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.20E+000
7.58E+OOO
5.59E-001
7.55E+000
+I+I+I+I-
6.19E-001
1.14E+000
2.20E-001
1.13E+000
MDA
(pCi/liter
7.83E-002
l. 08E-001
9.66E-002
l. 46E-001
+I+I+I+I-
9.31E-003
l.28E-002
l.15E-002
l. 73E-002
5/fcfl~
B115
0000057535.CNF
Live Time :10200.000 sec
Real Time :10200.400 sec
start:
1:3452. 7(kev)
stop : 1024:6S06.6(kev)
Acq. start :Thu May 09 09:57:46 2013
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Channel Data Report
5/9/2013
Page
3:55:45 1m
*******************************************************
*****
p E C T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
01
Elapsed Live time:

Elapsed Real Time:
10200
10200
Channell------l-------l-------l-------l-------l-------l-------l-------1
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15
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0
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1
1
2
8
9
10
11
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1
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0
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1
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1
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1
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1
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0
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0
0
0
1
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4
4
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8
4
12
6
13
4
0
1
0
0
0
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2
lii117
Channel Data Report

369:
5/9/2013
2
Sample Title:
3:55:45
2
Page
~M
01
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8
11
10
7
0
0
0
0
0
0
0
0
0
1
0
0
1
2
3
0
3
0
2
4
11
7
5
0
0
0
0
0
0
0
0
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0
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0
0
0
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2
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7
7
7
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11
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0
0
0
0
0
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0
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0
0
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0
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0
0
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0
0
0
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9
4
9
8
4
3
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
mua
Channel Data Report

801:
5/9/2013
0
Sample Title:
Page
3:55:45 :E'M
0
01
809:
817:
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833:
841:
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857:
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945:
953:
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969:
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1001:
1009:
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0
0
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0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
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0
0
0
0
0
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0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
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0
0
0
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0
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0
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0
0
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0
0
0
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Ul119
pex-Aipha
Sample Description:
Spectrum File:
Sample Geometry:
BLANK
1304132A-UU
02
Shelf 2
u iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_042
05026930B
84185
System Bkgd 56378
<not performed>
Sample Size:
Sample Date/Time:

5/9/2013
6:52:37 AM
5/9/2013
9:57:48 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.605 mL
0.1045 +/- 0.0077
0.1846 +/- 0.0032 on 12/16/2012
0.5659 +/- 0.0429
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.289
4.745
4.445
4.151
Net
Pk Area
AREA
REPORT
Pk Area
Error %
203.83
2.49
2.83
1.66
5:49:29 PM
Ambient
Backgnd
13.74
138.29
120.53
169.38
0.17
0.51
0.17
0.34
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
4.6
3.0
3.0
3.0
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.999
0.998
0.975
0. 992
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.18E+000
6.33E-002
8.87E-002
4.20E-002
+I+I+I+I-
7.49E-001
8.80E-002
1. 08E-001
7.14E-002
AG
~(Oil~
MDA
(pCi/liter
1. 06E-001
1. 33E-001
1. 31E-001
1.21E-001
+I+I+I+I-
1.53E-002
1. 93E-002
1. 89E-002
1. 75E-002
0000057536.CNF
Live Time 10200.000 sec
Real Time 10200.500 sec
start:
1 3450.2(kev)
stop : 1024 6505.5(kev)
Acq. start Thu May 09 09:57:48 2013
60
55
50
45
40
35
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ROI Type: 1
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5000
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5500
6000
ROI Type: 3
6500
Channel Data Report
5/9/2013
Page
3:55:55 l!'M
*******************************************************
*****
p E C T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
02
Elapsed Live time:

Elapsed Real Time:
10200
10201
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
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169:
177:
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fg1 ??
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-{g123
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Sample Description:
Spectrum File:
Sample Geometry:
PZ-106-KS TOT-DUP
1304132A-UU
03
Shelf 2
u iso
Detector Name:
Env. Background:
Reagent Blank:
A1pha_044
04026481B
84168
System Bkgd 56379
<not performed>
Sample Size:
Sample Date/Time:
O.OOOE+OOO liter
1. OOOE+OOO +/4/15/2013
6:52:37 AM
9:57:42 AM
5/9/2013
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.600 mL
0.1972 +/- 0.0111
0.1902 +/- 0.0033 on 12/16/2012
1.0370 +/- 0.0609
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.274
4.727
4.406
4.135
Net
Pk Area
AREA
REPORT
Ambient
Backgnd
Pk Area
Error %'
381.83
162.83
12.83
58.00
5:49:26 PM
0.17
0.17
0.17
0.00
10.03
15.37
55.14
25.96
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
5.5
12.5
3.0
3.7
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.994
0.991
0.997
0.983
5302.50*
4761. 50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.14E+000
2.19E+000
2.13E-001
7.78E-001
+I+I+!+I-
5.66E-001
4.14E-001
1.20E-001
2.19E-001
AG.
Sl(ojl)
MDA
(pCi/liter
5.62E-002
5.62E-002
6.93E-002
8.04E-002
+I+I+I+I-
6.18E-003
6.18E-003
7.62E-003
8.84E-003
0000057537.CNF
start:
1:3447.9(kev)
stop : 1014:6485. 9(kev)
Acq. start :Thu May 09 09:57:42 2013
60
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50
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40
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ROI Type: 1
5000
Energy(kev)
!!I,
6000
5500
ROI Type: 3
Channel Data Report
5/9/2013
3:56:03
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"M
*******************************************************
*****
p E C T R A L
DATA
R E P 0 R T
*****
*******************************************************
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0
0
0
Sample Description:
Spectrum File:
Sample Geometry:
D-14 TOT
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000575
1304132A-UU
04
Shelf 2
u iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_046
04026482B
58762
System Bkgd 56380
<not performed>
Sample Size:
Sample Date/Time:
l.OOOE+OOO +/- O.OOOE+OOO liter

6:52:37 AM
4/12/2013
5/9/2013
9:57:44 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-lOA
0.572 mL
0.0602 +/- 0.0059
0.1789 +/- 0.0031 on 12/16/2012
0.3364 +/- 0.0335
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.271
4. 721
4.396
4.151
T
Net
Pk Area
111.00
17.00
-0.34
23.83
AREA
5:49:23 PM
REPORT
Pk Area
Error %"
18.69
48.92
592.90
40.32
Ambient
Backgnd
0.00
0.00
0.34
0.17
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
5.1
3.7
0.0
3.0
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.993
0.988
0.999
0.992
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
4.90E+000
7.50E-001
-1.85E-002
1.05E+ODO
+I+I+I+I-
9.42E-001
3.94E-001
l.lOE- 001
4.68E-001
AG
5/ rof C!:J
MDA
(pCi/liter
2.65E-001
2.64E-001
2.60E-001
1. 83E- 001
+I+I+I+I-
5.09E-002
5.08E-002
5.00E-002
3.52E-002
0000057534.CNF

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Channel Data Report
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3:56:11 PM
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*****
E C T R A L
DATA
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*****
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Channel Data Report

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11133
Channel Data Report

801:
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Sample Title:
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ex-AiphaTM
Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:
Env. Background:
PZ-202-SS TOT
1304132A-UU
08
Shelf 2
u iso
Alpha_027
27
System Bkgd 56370
Reagent Blank:
<not performed>
1. OOOE+OOO +/- O.OOOE+OOO liter

6:52:37 AM
4/12/2013
12:54:35 PM
5/9/2013
170.0 minutes
170.0 minutes
Sample Size:
Sample Date/Time:
U232 UU-10A
0.591 mL
0.2144 +/- 0.0117
0.1728 +/- 0.0032 on 12/15/2012
1.2413 +/- 0.0717
0.150 MeV
Tracer Certificate:
Tracer Quantity:
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.283
4.733
4.423
4.156
Net
Pk Area
AREA
REPORT
Pk Area
Error %
408.98
136.32
8.32
62.98
2:27:41 PM
Ambient
Backgnd
9.71
16.84
71.13
24.93
1. 02
0.68
0.68
1. 02
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
27.1
12.4
3.2
6.2
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.997
0.994
0.990
0.994
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.07E+000
1. 69E+000
1.27E-001
7.76E-001
+I+I+I+I-
5.42E-001
3.37E-001
9.14E-002
2.11E-001
MDA
(pCi/liter
7.81E-002
6.98E-002
8.61E-002
7.77E-002
+I+I+I+I-
8.35E-003
7.47E-003
9.22E-003
8.31E-003
A&
5(to{IJ
3135
0000057556.CNF
Start:
1:3402.4(kev)
stop : 1024:6658.!(kev)
Acq. Start :Thu May 09 12:54:35 2013
60
5
50
35
....,
v>
s:::
::::s
25
!llil
....
!,.J:
0)
ROI Type: 1
ROI Type: 3
Channel Data Report
5/9/2013
Page
3:56:45 PM
*******************************************************
S P E C T R A L
DATA
R E P 0 R T
*****
*****
*******************************************************
Sample Title:
08
Elapsed Live time:

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!137
Channel Data Report

369:
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Channel Data Report

801:
5/9/2013
0
Sample Title:
Page
3:56:45 l"M
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4/12/2013
6:52:37 AM
5/9/2013
12:54:36 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232_UU-10A
0.579 mL
0.2308 +/- 0.0123
0.1945 +/- 0.0036 on 12/15/2012
1.1863 +I- 0.0670
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.281
4.731
4.378
4.151
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REPORT
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Error %
Net
Pk Area
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140.83
3.83
54.83
2:30:02 PM
9.45
16.53
102.72
26.52
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Reagent
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FWHM
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0.68
0.17
0.17
0.17
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
20.8
4.8
3.1
4.7
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Id
Conf.
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U-234
U-235
U-238
0.997
0.993
1. 000
0.992
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
4.97E+OOO
1.62E+OOO
5.44E-002
6.28E-001
+I+I+I+I-
5.20E-001
3.17E-001
5.61E-002
1. 79E-001
/+;&
5/ro/J
MDA
(pCi/liter
6.49E-002
4.80E-002
5.92E-002
4.78E-002
+I+I+I+I-
6.80E-003
5.03E-003
6.20E-003
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Channel Data Report

801:
5/9/2013
0
Sample Title:
3:56:53 PM
0
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Sample Description:
Spectrum File:
Sample Geometry:
DUP07 TOT
1304132A-UU
10
Shelf 2
U iso
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Alpha_033
04026479A
91132
System Bkgd 56372
<not performed>
Sample Size:
Sample Date/Time:
1.000E+OOO +/- O.OOOE+OOO liter

6:52:37 AM
4/12/2013
5/9/2013
12:55:17 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232_UU-10A
0.586 mL
0.0655 +/- 0.0061
0.1825 +/- 0.0032 on 12/16/2012
0.3591 +/- 0.0339
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.290
4.709
4.398
4.205
Net
Pk Area
123.83
3.83
-0.17
0.83
AREA
5:49:18 PM
REPORT
Pk Area
Error %
17.63
102.72
1169.4
239.53
Ambient
Backgnd
0.17
0.17
0.17
0.17
FWHM
(keV)
Reagent
Backgnd
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O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
3.4
3.0
0.0
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Nuclide
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Conf.
Energy
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U-234
U-235
U-238
0.999
0.981
0.999
0.997
5302.50*
4761.50*
4385.50*
4184.40*
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1.55E-001
-8.50E-003
3.35E-002
+I+I+I+I-
9.14E-001
1.62E-001
9.94E-002
8.04E-002
MDA
(pCi/liter
1.69E-001
1. 69E-001
2.09E-001
1. 68E-001
+I+I+I+I-
3.08E-002
3.08E-002
3.80E-002
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6500
Channel Data Report
5/9/2013
3:57:01 PM
Page
*******************************************************
*****
E C T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
10
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Channel Data Report

801:
5/9/2013
0
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Channel Data Report

801:
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3:57:11 l!'M
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6:52:37 AM
5/9/2013
12:55:21 PM
170.0 minutes
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0.559 mL
0.2254 +/- 0.0123
0.1826 +/- 0.0032 on 12/16/2012
1.2348 +/- 0.0709
0.150 MeV
PEAK
Energy
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Nuclide
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U-234
U-235
U-238
5.298
4.756
4.402
4.170
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5.00
73.00
5:49:42 PM
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96.02
23.10
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Channel Data Report
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801:
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Sample Description:
Spectrum File:
Sample Geometry:
PZ-106-KS DIS
1304132A-UU
13
Shelf 2
U iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_037
04026478A
91133
system Bkgd 56375
<not performed>
Sample Size:
Sample Date/Time:

6:52:37 AM
4/15/2013
12:55:23 PM
5/9/2013
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.591 mL
0.2259 +!0.0121
0.1783 +/- 0.0033 on 1/26/2013
1.2672 +/- 0.0717
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.276
4.734
4.389
4.158
T
Net
Pk Area
AREA
REPORT
Pk Area
Error %
430.66
171.66
6.00
62.00
3:28:25 PM
Ambient
Backgnd
0.34
0.34
0.00
0.00
9.45
14.98
86.43
25.09
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
6.0
16.1
2.9
3.3
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.995
0.995
1. 000
0.995
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.06E+000
2.02E+000
8.70E-002
7.25E-001
+I+!+I+I-
5.30E-001
3.69E-001
7.57E-002
1. 97E- 001
fiG
s(rq!J
MDA
(pCi/liter
5.62E-002
5.62E-002
8.69E-002
7.02E-002
+I+I+I+I-
5.89E-003
5.88E-003
9.10E-003
7.35E-003
0000057561.CNF
Start:
1 3463.5(kev)
Stop : 1024 6468.5(kev)
Acq. start Tho May 09 12:55:23 2013
60
55
50
45
40
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ROI Type: 1
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Channel Data Report
5/9/2013
Page
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R E P 0 R T
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ex-Alpha
Sample Description:
Spectrum File:
FB AT PZ-100-KS TOT
1304132A-UU
14
Shelf 2
u iso
Sample Geometry:
Detector Name:
Env. Background:
Alpha_040
060273968
91135
System Bkgd 56376
<not performed>
Reagent Blank:
Sample Size:

4/16/2013
6:52:37 AM
5/9/2013
12:55:25 PM
170.0 minutes
Sample Date/Time:
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232_UU-10A
0.586 mL
0.2102 +/- 0.0116
0.1900 +/- 0.0033 on 12/16/2012
1.1062 +/- 0.0640
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
Net
Pk Area
5.278
4.717
4. 370
4.071
397.66
6.00
2.83
4.49
AREA
5:49:33 PM
REPORT
Pk Area
Ambient
Reagent
Error %
Backgnd
Backgnd
0.34
0.00
0.17
0.51
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
9.83
86.43
120.53
98.45
FWHM
(keV)
12.8
3.0
3.0
5.9

Id
Conf.
Energy
Nuclide
U-232
U-234
U-235
U-238
0.996
0.986
0.998
0.913
5302.50*
4761.50*
4385.50*
4184.40*
(keV)
Activity
(pCi/liter )
5.03E+OOO
7.58E-002
4.41E-002
5.65E-002
+I+I+I+I-
5.44E-001
6.60E-002
5.34E-002
5.59E-002
MDA
(pCi/liter
6.04E-002
7.57E-002
6.50E-002
6.60E-002
+I+I+I+1-
6.54E-003
8.19E-003
7.04E-003
7.14E-003
If(,
s !toft:;
t11165
0000057562.CNF
start:
l:l459.0(kev)
stop : 1014:6497.l(kev)
Acq. Start :Thu May 09 12:55:25 2013
60
55
50
45
40
35
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5000
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5500
6000
ROI Type: 3
6500
Channel Data Report
5/9/2013
3:57:37 PM
Page
*******************************************************
*****
p E C T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
14
Elapsed Live time:

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369:
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801:
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0
Sample Title:
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Ui169
Sample Description:
Spectrum File:
Sample Geometry:
FB AT PZ-100-KS DIS
\\OR-AIPHA1\Canberra\ApexAlpha\Root\Data\00000575
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15
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Alpha_041
05026930A
91087
System Bkgd 56377
<not performed>
Sample Size:
Sample Date/Time:

6:52:37 AM
4/16/2013
5/9/2013
12:55:28 PM
170.0 minutes
l70. 0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.580 mL
0.2450 +/- 0.0128
0.1978 +/- 0.0034 on 12/16/2012
1.2382 +/- 0.0679
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.282
4.730
4.383
4.142
Net
Pk Area
458.66
6.81
2.66
-2.06
AREA
5:49:31 PM
REPORT
Pk Area
Error %
Ambient
Backgnd
0.34
1.19
0.34
3.06
9.16
82.43
128.85
117.31
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
32.0
3.0
3.0
3.0
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.997
0.993
1.000
0.987
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
4.97E+OOO
7.38E-002
3.56E-002
-2.22E-002
+I+I+I+I-
5.08E-001
6.13E-002
4.60E-002
2.62E-002
~
Sjto/t~
MDA
(pCi/liter
5.19E-002
7.14E-002
6.39E-002
9.64E-002
+I+I+I+I-
5.29E-003
7.29E-003
6.52E-003
9.84E-003
0000057566.CNF
60
t::

start:
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stop: 1024:6506.6(kev)
Acq. Start :Thu May 09 12:55:28 20ll
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6500
Channel Data Report
5/9/2013
3:57:47 PM
Page
*******************************************************
*****
p E
T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
15
Elapsed Live time:

Elapsed Real Time:
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Channel Data Report

369:
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!\l! 73
Channel Data Report

801:
5/9/2013
0
Sample Title:
Page
3:57:47 l"M
0
15
Channell------l-------l-------1-------l-------l-------l-------l-------l
809:
817:
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865:
873:
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Sample Description:
Spectrum File:
Sample Geometry:
PZ-100-KS TOT
1304132A-UU
16
Shelf 2
U iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_042
050269308
84185
System Bkgd 56378
<not performed>
Sample Size:
Sample Date/Time:

4/16/2013
6:52:37 AM
5/9/2013
12:55:30 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.588 mL
0.2044 +/- 0.0114
0.1846 +/- 0.0032 on 12/16/2012
1.1070 +/- 0.0647
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.280
4.740
4.461
4.149
Net
Pk Area
AREA
REPORT
Pk Area
Error %
387.83
12.49
1. 83
4.66
5:49:29 PM
Ambient
Backgnd
0.17
0.51
0.17
0.34
9.96
56.77
152.56
94.59
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
15.7
3.0
3.0
3.0

Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.996
0.997
0. 960
0.991
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.04E+OOO
1. 62E- 001
2.93E-002
6.03E-002
+I+I+I+I-
5.51E-001
9.38E-002
4.49E-002
5.74E-002
MDA
(pCi/liter
5.43E-002
6.82E-002
6.69E-002
6.18E-002
+I+I+I+I-
5. 93E- 003
7.45E-003
7.31E-003
6.76E-003
AG
:5 (tr;,/t 3
m175
0000057567.CNF
Start:
I: 3450, 2(kev)
stop : 1024:6505.5(kev)
Acq. Start :Thu May 09 12:55:30 2013
60
55
50
45
40
35
....,
V>
<=
8"' 30
25
20
15
:'IIi
~iii]
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10
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5
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ROI Type: 1
1 ~11
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5000
Energy(kev)
ji
, 1
5500
6000
ROI Type: 3
6500
Channel Data Report
5/9/2013
Page
3:57:58 PM
*******************************************************
S P E C T R A L
DATA
R E P 0 R T
*****
*****
*******************************************************
Sample Title:
16
Elapsed Live time:

Elapsed Real Time:
10200
10200
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n1177
Channel Data Report

369:
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Sample Title:
Page
3:57:58 PM
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,{~178
Channel Data Report

801:
5/9/2013
0
Sample Title:
3:57:58
0
Page
~M
16
809:
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mt79
ex-AiphaTM
Sample Description:
Spectrum File:
Sample Geometry:
PZ-100-KS DIS
1304132A-UU
17
Shelf 2
U iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_044
04026481B
84168
System Bkgd 56379
<not performed>
Sample Size:
Sample Date/Time:

4/16/2013
6:52:37 AM
5/9/2013
12:55:33 PM
170.0 minutes
170. 0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.583 mL
0.2207 +/- 0.0120
0.1902 +/- 0.0033 on 12/16/2012
1.1603 +/- 0.0661
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.267
4.737
4.481
4.142
Net
Pk Area
AREA
REPORT
Pk Area
Error %
414.83
5.83
0.83
8.00
5:49:26 PM
9.63
82.55
239.53
73.50
Reagent
Backgnd
Ambient
Backgnd
0.17
0.17
0.17
0.00
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
4.6
3.0
3.0
3.0
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.991
0.996
0.937
0.987
5302.50*
4761. 50*
4385.50*
4184.40*
Activity
(pCi/liter )
4.99E+OOO
7.02E-002
1. 23E- 002
9.58E-002
+I+I+I+I-
5. 31E-001
5.84E-002
2.95E-002
7.12E-002
AG,
5fr<>ft)
MDA
(pCi/liter
5.02E-002
5.02E-002
6.19E-002
7.18E-002
+I+I+I+I-
5.34E-003
5.34E-003
6.58E-003
7.64E-003
0000057563.CNF
start:
13447,9(kev)
stop : 1024 6485,9(kev)
60
55
50
45
40
35
"'
c
+-'
8"' 30
25
20
~~~~!~~~~ .
15
l~j!
10
!. .
/Iii ~ I
Iii,
I:' 'll II
ljAI
~~ 'l
i.
'
3500
...
4000
4500
Ill!
())
.,~.i,
ROI Type: 1
5000
Energy(kev)
5500
6000
ROI Type: 3
Channel Data Report
5/9/2013
3:58:07 PM
Page
*******************************************************
*****
p E C T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
17
Elapsed Live time:

Elapsed Real Time:
10200
10200
Channell------l-------1-------l-------l-------l-------l-------l-------l
1:
9:
17:
25:
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65:
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Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:
Env. Background:
Reagent Blank:
S-53 DIS
1304132A-UU
19
Shelf 2
u iso
Alpha_047
02030596A
91086
System Bkgd 56381
<not performed>

6:52:37 AM
4/16/2013
5/9/2013
12:55:39 PM
170.0 minutes
Sample Size:
Sample Date/Time:
170.0 minutes
U232_UU-10A
0.577 mL
0.2195 +/- 0.0120
0.1822 +/- 0.0032 on 12/16/2012
1.2051 +/- 0.0691
0.150 MeV
Tracer Certificate:
Tracer Quantity:
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.274
4.722
4.401
4.146
Net
Pk Area
AREA
REPORT
Pk Area
Error %
408.83
488.00
26.49
393.83
5:49:21 PM
Ambient
Backgnd
Reagent
Backgnd
0.17
0.00
0.51
0.17
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
9.70
8.88
38.51
9.88
FWHM
(keV)
20.9
11.8
5.9
25.4

Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.994
0.989
0.998
0.990
5302.50*
4761. 50*
4385.50*
4184.40*
Activity
(pCi/liter )
4.95E+OOO
5.90E+OOO
3.95E-001
4.74E+OOO
+I+I+I+I-
5.29E-001
8.20E-001
1.58E-001
6.90E-001
MDA
(pCi/liter
5.05E-002
7.25E-002
7.83E-002
5.03E-002
+I+I+I+I-
5.40E-003
7.75E-003
8.37E-003
5.37E-003
ptJ
6 (r~"~lt'J
lll185
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Channel Data Report
5/9/2013
3:58:28 PM
Page
*******************************************************
*****
p E C T R A L
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R E P 0 R T
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m1as
Page 1 of 2
5/9/2013
5:53:04 AM
ex-AI ha
QA SUMMARY REPORT
Review Of QA Results - Pulser Check
Date
Time
: 5/9/2013
: 5:53:04 AM
CHAMBER
Alpha 001
Alpha 002
Alpha 003
Alpha 004
Alpha 005
Alpha 006
Alpha 007
Alpha 008
Alpha 009
Alpha 010
Alpha Oil
Alpha 012
Alpha 013
Alpha 014
Alpha 015
Alpha 016
Alpha 017
Alpha 018
Alpha 019
Alpha 020
Alpha 021
Alpha 022
Alpha 023
Alpha 024
Alpha 025
Alpha 026
Alpha 027
Alpha 028
Alpha 029
Alpha 030
Alpha 031
Alpha 032
Alpha 033
Alpha 034
Alpha 035
Alpha 036
Alpha 037
Alpha 038
Alpha 039
Alpha 040
Alpha 041
Alpha 042
DEVICE
2lf
21f
21f
21f
2lf
2lf
21f
21f
21f
21f
21f
2lf
21f
21f
21f
21f
AIM730
AIM730
AlM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AJM730
AIM730
AIM730
AIM730
AIM730
AIM730
Alpha Analyst I OODC
Alpha Analyst! OODC
Alpha Analyst!OODC
Alpha Analyst! OODC
Alpha Analyst!OODC
Alpha Analyst! OODC
Alpha Analyst! OODC
Alpha Analyst!OODC
Alpha AnalystiOODC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
FLAG
Not Done
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Not Done
Not Done
Passed
Passed
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Passed
Not Done
Not Done
Not Done
Passed
Not Done
Passed
Passed
Not Done
Passed
Not Done
Passed
Not Done
Not Done
Not Done
Passed
Passed
Passed
Not Done
Passed
Not Done
Not Done
Passed
. Passed
Passed
DATE
5/9/2013 5:34:02 AM
5/9/2013 5:34:02 AM
5/9/2013 5:34:03 AM
5/9/2013 5:34:04 AM
5/9/2013 5:34:05 AM
5/9/2013 5:34:06 AM
5/9/2013 5:34:07 AM
5/9/2013 5:34:08 AM
5/9/2013 5:34:08 AM
5/9/2013 5:34:09 AM
5/9/2013 5:34:10 AM
5/9/2013 5:34:11 AM
5/9/2013 5:34:12 AM
5/9/2013 5:34:13 AM
5/9/2013 5:34:15 AM
5/9/2013 5:34: 16 AM
5/9/2013 5:34:18 AM
5/9/2013 5:34:20 AM
5/9/2013 5:34:21 AM
Page 2 of 2
Review of QA Results - Pulser Cheek

5/9/2013
CHAMBER
Alpha 043
Alpha 044
Alpha 045
Alpha 046
Alpha 047
Alpha 048
DEVICE
Alpha Analyst! OODC
Alpha Analyst! OODC
Alpha Analyst!OODC
Alpha Analyst! OODC
Alpha Analyst! OODC
Alpha Analyst! OODC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
FLAG
Not Done
Passed
Not Done
Passed
Passed
Passed
55304 AM
DATE
5/9/2013 5:34:23 AM
5/9/2013 5:34:25 AM
5/9/2013 5:34:27 AM
5/9/2013 5:34:29 AM
APPROVED BY:
APPROVAL DATE:
--.J-(--'f.'--1.---'-'//~)
1191
Library Listing Report
6/12/12
Page
12:17:04 PM
*************************************************************************
*****
L I B R A R Y L I S T I N G R E P 0 R T
*****
*************************************************************************
Nuclide Library Title:
Uranium
Nuclide Library Description:

Nuclide
Name
Half-Life
(Seconds)
U-232
U-234
U-235
U-238
2.174E+009
7.731E+012
2.221E+016
1.410E+017
U-232,-234,-235,-238
Energy
(keV )
Energy
Uncert. (keV
5302.500*
4761.500*
4385.500*
4184.400*
0.000
0.000
0.000
0.000
* = key line
TOTALS:
Nuclides
Energy Lines
Yield
(%)
99.8000
99.8000
80.9000
100.2300
Yield
Uncert. (Abs. +-)
0. 0000
0.0000
0. 0000
0.0000
RUN2
Eberline Services
Analysis Sheet
13-04132
Printed: 5116/2013 6:15AM

Page 1 of 3
UUISO
Run 2
Work Order
Analysis Code
Internal I Sample
Fraction j Desc
I '
UUISO
01
LCS
ID
1
Login
CPM
Sample
Date
I
'
LCS
-----
Run
Date Received
Client
4/18/2013
Sample
Aliquot
04/18/13 00:00
1.0000E+OO
04/18/13 00:00
1.0000E+OO
02
MBL
BLANK
03
DUP
PZ-112-AS TOT
45
04/12/13 11:18
2.5000E-01
05
TRG
D-14 DIS
38
i 04/12/13 11 :05
2.5000E-01
06
DO
PZ-112-AS TOT
04/12/1311:18
2.5000E-01
45
04/12/1311:18
2.5000E-01
41
04/16/13 09:00
Lab Deadline
--
Client
5/9/2013
Project
West Lake OU-1
Report Level
Activity Units
pCi
Aliquot Units
' -07
18
TRG
TRG
PZ-112-AS DIS
-
---
S-53 TOT
2.5000E-01
I
I
--
Matrix
45
..
r--
r-----
-----
WA
-
Method
EML U-02 Modified
--
1Instrument Type
Alpha Spectroscopy
Radiometric Tracer
U-232
Radiometric Sol#
U-10a
Tracer Act (dpm/g)
19.084
I-
Carrier
--
Carrier Cone (mg/ml)
~
a
'Lll""
g.:'.:'Ji,
"'SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.
Eberline Services
Analysis Sheet
Printed: 511612013 6:15AM

Page 2 of 3
13-04132
UUISO
Run 2
Internal
Fraction
Sample
Desc
01
LCS
Tracer
Aliquot (g)
Tracer Total
ACT (dpm)
Radiometric
Tracer (pCi)
0.6100
'
03
05
o.ool
0.6099
11.6
Grav Filter
Tare (g)
Grav Filter
Final (g)
0.6090
DUP
'
TRG'
0.6112
11.7
0.6089
11.6
18
TRG
0.6088
11.6
1--=1 ~
SAF
SAF
1.
2.
o.oo,
--
-------
'-
-------
'
0.00
-
'
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--
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-~--
0.00
--
TRG
Ii
--
0.00
11.6
07
Mean
%Rec
Grav
%Rec
--
0.6080
DO
Grav Filter
Net(g)
0.00
11.6
06
Grav Carrier
Added(ml)
%Rec
11.6
--
--
!Radiometric
i
!
MBL
02
'
0.001
---
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'
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Analysis Sheet
Printed: 5/16/2013 6:15AM

Page 3 of 3
13-04132
UUISO
Run 2
Internal
Fraction
Sample
Desc
I
1
'
Prep
Date
By
05/13/13 07:33
I!
Septo
By
-1
05/13/13 07:33
Sep t1
By
05/13/13 07:33
JBARNARD
---------
iI
I
05/13/13 07:33 ! JBARNARD

-
05/13/13 07:33
JBARNARD
05/13/13 07:33
JBARNARD
----
TRG
I
-----
II
'
II
--
--
---
!
--
--
-- I
--
--
--
'
--
'
--
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--
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JBARNARD
----
DO
JBARNARD
-----
----
Sep 11
Date/Time
-----
TRG
18
SeptO
Date/Time
I JBARNARD
-----
07
Prep
05/13/13 07:33
MBL
TRG
05
By
DUP
03
06
Rough Prep
LCS
01
02
Rough Prep
Date
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01
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Identification
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Units
U-234
LCS
LCS
pCi/1
7.45E+OO
1.00E+OO
9.69E-02
U-234
MBL
BLANK
pCill
5.81E-02
8.34E-02
1.36E-01
2.07E-01
3.72E-01
--
Results
Error Estimate
MDA
LCS
Known
8.12E+OO
LCS
%R
LCS
Flag
91.69
OK
RPD
MDA
Flag
Flag
Blank
Flag
OK
OK
OK
U-234
05
U-234
Cl)
06
U-234
: :;)
::;)
07
U-234
18
U-234
Sample
Desc
03
Printed: 5/17/2013 9:19AM

Page 1 of 3
Nuclide
Fraction
OK
INV
DUP
PZ-112-AS TOT
pCi/1
1.17E-01
TRG
D-14 DIS
pCi/1
2.70E-01 i
5.86E-01
1.15E+OO
INV
..
'
DO
PZ-112-AS TOT
pCi/1
7.68E-02
2.43E-01
5.14E-01
OK
TRG
PZ-112-AS DIS
pCi/1
2.61E-01
2.70E-01
2.84E-01
OK
TRG
S-53 TOT
pCill
4.53E+01
1.99E+01
3.63E+OO
INV
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Printed: 5/17/2013 9:19AM

Page 2 of 3
Sample
Sample
Date
"~'
01
U-234
02
U-234
MBL
03
U-234
DUP
05
U-234
LCS
Sample
Aliquot
Radiometric
%Rec
'
Grav
Mean
%Rec
%Rec
1.00E+OO
112.41
0.00
0.00
04/18/13 00:00
1.00E+OO
83.89
0.00
0.00
04/12/1311:18
2.50E-01
105.09
04/18/13 00:00
Sep to
DatefTime
SAF
----
Sept1
Date/Tlme
'
'
---0.00
0.00
---04/12/1311:05
TRG
2.50E-01
29.90
o.oo!
06
U-234
07
U-234
18
U-234
DO
I
' TRG
0.00
- ---
04/12/13 11:18
2.50E.Q1
90.50.
0.00
0.00
04/12/13 11:18
2.50E.Q1
81.92
0.00
0.00
04/16/13 09:00
2.50E.Q1
7.89
0.00
0.00
''
---
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Date/Time
Halflife
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Detect
Carrier
Count
Time
U-234
LCS
05/16/1312:25
A_Spec
Alpha_014
170.02 5.82 E+02
1.10 E-02
18.5
02
U-234
MBL
05/16/13 15:38
A_ Spec
Alpha_022
170.02 2.81 E+OO
7.00 E-03
15.3
03
U-234
DUP
05/16/13 15:38
A_Spec
Alpha_oM 170.02 1.98 E+OO
6.00 E-03
17.1
----
-----
05
--- - - - -
U-234
;'
TRG
05/16/13 15:38
DO
05/16/1315:38
A_Spec
Alpha_025
170.02 1.32 E+OO
4.00 E-03
17.4
A_Spec
Alpha_027
170 1.13 E+OO
1.10 E-02
17.3
1.00 E-03
19
3.00 E-03
19.5
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06
~
~
07
U-234
TRG
05/16/1311:43
A_Spec
Alpha_044
170 3.83 E+OO
18
U-234
TRG
05/16/13 15:38
A_Spec
Alpha_029
170.02 6.55 E+01
U-234
'
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01
-~
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CPM
Counts
f-----
:!:
Printed: 5/17/2013 9:19AM

Page 3 of 3
'
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U-238
Activity
Client
Identification
Desc
LCS
LCS
Error Estimate
Results
Units
7.76E+OO
pCi/1
'
1.04E+OO
---
MDA
7.63E-02
MBL
pCi/1
BLANK
1.36E-02
U-238
DUP
4.15E-02
PZ-112-AS TOT
pCi/1
7.92E+OO
'
LCS
%R
LCS
RPD
Flag
Flag
98.01
OK
1.69E-011
U-238
TRG
D-14 DIS
pCi/1
7.11E-01
8.20E-01
1.07E+OO
U-238
DO
PZ-112-AS TOT
pCi/1
8.93E-02
1.93E-01
3.81E-01
07
U-238
TRG
PZ-112-AS DIS
pCi/1
2.72E-01
2.99E-01
4.07E-01
18
U-238
TRG
S-53 TOT
pCi/1
5.35E+01
2.29E+01
3.29E+OO
'
-~
.,
.5
Flag
--
OK
OK
INV
''
OK
I
I-~~
INV
OK
i
OK
INV
i
.
Blank
"E
'
-~
OK
05 i
06
MDA
Flag
---
3.52E-01
9.84E-02
6.76E-02
LCS
Known
--
--
U-238
03
Nuclide
Fraction
Printed: 5/17/2013 9:19AM

Page 1 of 3
i.
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Sample
Date
01
U-238
LCS
04/18/13 00:00
02
U-238
MBL
04/18/13 00:00
03
U-238
DUP
-e
06
..
07
Radiometric
Sample
Aliquot
'
Grav
%Rec
%Rec
Mean
%Rec
1.00E+OO
112.41
0.00
1.00E+OO
83.89
0.00
2.50E-01
105.09
0.00
'
04/12/1311:18
--
0.00
--
..
0.00
..
..
04/12/1311:05
2.50E-01
29.901
0.00
0.00
U-238
DO
04/12/1311:18
2.50E-01
90.50
0.00
o.ool
U-238
TRG
04/12/1311:18
2.50E-01
81.92
0.00
0.00
U-238
TRG
04/16/13 09:00
2.50E-01
7.89
0.00
0.00
'
18
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DatefTime
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SAF
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05
Printed: 5/17/2013 9:19AM

Page 2 of3
Nuclide
Fraction
0:
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~
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0
0
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..
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Lab
02
03
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Alpha_014
170.0216.09 E+02
Bkg
CPM
Eff
5.00 E-03
18.5
15.3
05/16/1315:38
Counts
Time
A_Spec
Alpha_022i 170.02 6.60 E-01
2.00 E-03
Alpha_024
170.02 1.15 E+OO
5.00 E-03
A_Spec
Alpha_025
170.02 3.49 E+OO
3.00 E-03
17.4
en
06
U-238
DO
05/16/13 15:38
A_ Spec
Alpha_027
170 1.32 E+OO
4.00 E-03
17.3
~
~
07
U-238
TRG
05/16/13 11:43
A_Spec
Alpha_044
170 4.00 E+OO
0.00 E+OO
19
=-+
05/16/13 15:38
A_Spec
'Aipha_029
170.02 7.77 E+01
2.00 E-03
19.5
18
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05/16/1315:38
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U-238
05/16/13 12:25
05
.;
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LCS
Halflife
(days)
A_Spec
ill
1::
DatefTime
05/16/13 15:38
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Printed: 5/17/2013 9:19AM

Page 3 of 3
Nuclide
Fraction
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Desc
Client
Identification
Activity
01
U-235
LCS
LCS
pCi/1
02
U-235
03
Printed: 5/17/2013 9:19AM

Page 1 of 3
Results
Units
6.76E-01
Error Estimate
BLANK
5.91E-02
pCifl
U-235
TRG
06
U-235
DO
07
U-235
18
U-235
'
LCS
Known
LCS
%R
2.06E-01
pCi/1
Flag
OK
1.44E-01
2.50E-01
MOA
NA
3.04E-01
OK
..
2.10E-01
5.04E-01
1.05E+OO
INV
pCi/1
5.53E-02
1.69E-01
4.01E-01
OK
pCi/1
O.OOE+OO
2.33E-01
5.04E-01
pCi/1
PZ-112-AS TOT
PZ-112-AS DIS
OK
-
D-14 DIS
Blank
Flag
OK
I'
PZ-112-AS TOT
RPO
Flag
LCS
Flag
8.85E-02
---
05
..
MBL
- -DUP
1.04E-01
2.18E-011
-----
U-235
MOA
TRG
S-53 TOT
TRG
pCill
1.14E+01
7.53E+OO
OK
'
4.81E+OO
INV
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Date
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LCS
04118/13 00:00
02
U-235
U-235
MBL
04118113 00:00
03
U-235
DUP
04/1211311:18
U-235
TRG
0411211311:05
i'
05
'
Grav
%Rec
Mean
'
SAF
%Rec
1.00E+ool
112.41
0.00
1.00E+OO '
83.89
0.00
0.00
2.50E-01
105.09
0.00
0.00
2.50E-01
29.90
0.00
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U-235
18
U-235
DO
04/1211311:18
2.50E-01
90.50
0.00
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0.00
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TRG
04/12113 11:18
2.50E-01
81.92
0.00
0.00
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04116113 09:00
2.50E-01
7.89
0.00
0.001
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Printed: 5/17/2013 9:19AM

Page 2 of 3
Nuclide
01 i
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Internal Work Order
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5/13/2013 7:33
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1.0000E+OO
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06
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18
Printed: 5/13/2013 7:34AM

Page 1 of 1
Aliquot Worksheet
Technician:
Date:
L/L-~
H-3 Solids Only

Water Added
(ml)
H3 Dist
Aliq
Sample Description:
Spectrum File:
Sample Geometry:
SPIKE
1304132B-UU
01
Shelf 2
U iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_014
14
System Bkgd 56975
<not performed>
Sample Size:
Sample Date/Time:

7:27:01 AM
5/16/2013
5/16/2013 12:25:05 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232_UU-10A
0.610 mL
0.2075 +/- 0.0114
0.1846 +/- 0.0034 on 12/15/2012 11:26:44 AM
1.1241 +/- 0.0650
Control Certificate Name: NatU U-SA

U-238
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.266
4. 726
4.401
4.146
T
Net
Pk Area
0.955375 +/-
AREA
REPORT
Pk Area
Error %
408.28
582.13
42.81
609.15
0.071124
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9.74
8.14
30.44
7.95
2.72
1. 87
1.19
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O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
35.2
18.9
3.7
26.4
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Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.991
0.991
0.998
0.990
5302.50*
4761. 50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.22E+000
7.45E+000
6.76E-001
7.76E+000
+!+I+I+I-
5.61E-001
1.00E+000
2.18E-001
1.04E+000
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1.10E-001
9.69E-002
1. 04E-001
7.63E-002
+I+I+I+I-
1.18E-002
1. 04E- 002
1.12E- 002
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5/17/2013
Page
5:12:45 AM
*******************************************************
*****
p E C T R A L
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*****
*******************************************************
Sample Title:
01
Elapsed Live time:

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9
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22
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18
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6
8
8
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20
28
7
0
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~1"211
Channel Data Report

369:
5/17/2013
1
Sample Title:
Page
5:12:45 AM
3
01
377:
385:
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409:
417:
425:
433:
441:
449:
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513:
521:
529:
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Channel Data Report

801:
5/17/2013
0
Sample Title:
Page
5:12:45 AM
0
01
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1213
ex-AiphaTM
Sample Geometry:
BLANK
1304132B-UU
02
Shelf 2
U iso
Detector Name:
Env. Background:
Alpha_022
Sample Description:
Spectrum File:
22
System Bkgd 56977
Reagent Blank:
<not performed>

5/16/2013
7:27:01 AM
5/16/2013
3:38:27 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.610 mL
0.1285 +/- 0.0086
0.1531 +/- 0.0029 on 12/15/2012
0.8389 +/- 0.0587
0.150 MeV
Sample Size:
Sample Date/Time:
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
Net
Pk Area
REPORT
Ambient
Backgnd
Pk Area
Error %
252.79
2.81
2.32
0.66
5.270
4.683
4. 366
4.048
AREA
1:57:26 PM
12.39
142.99
149.13
305.45
2.21
1.19
0.68
0.34
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
7.9
3.1
3.1
3.1

Id
Conf.
Energy
Nuclide
U-232
U-234
U-235
U-238
0.993
0.957
0.997
0.876
5302.50*
4761. 50*
4385.50*
4184.40*
(keV)
Activity
(pCi/liter )
5.22E+OOO
5.81E-002
5.91E-002
1. 36E-002
+I+I+I+I-
6.89E-001
8.34E-002
8.85E-002
4.15E-002
t>G
S/f7/(J
MDA
(pCi/liter
1. 65E- 001
1.36E-001
1.44E-001
9.84E-002
+I+I+I+I-
2.18E-002
1.80E-002
1.90E-002
1.30E-002
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pex-AiphaTM
PZ-112-AS TOT-DUP
\\OR-ALPHA1\Canberra\ApexA1pha\Root\Data\00000582
1304132B-UU
03
Shelf 2
u iso
Detector Name:
A1pha_024
Sample Description:
Spectrum File:
Sample Geometry:

Env. Background:
24
System Bkgd 56978
Reagent Blank:
<not performed>
2.500E-001 +/- O.OOOE+OOO liter

4/12/2013
7:27:01 AM
5/16/2013
3:38:28 PM
Sample Size:
Sample Date/Time:
170.0 minutes
170.0 minutes
U232 UU-10A
0.609 mL
0.1797 +/- 0.0104
0.1710 +/- 0.0032 on 12/15/2012
1.0509 +/- 0.0642
0.150 MeV
Tracer Certificate:
Tracer Quantity:
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.284
4.740
4.412
4.182
Net
Pk Area
353.13
1. 98
2.83
1.15
AREA
2:02:15 PM
REPORT
Pk Area
Ambient
Error %
Backgnd
Reagent
Backgnd
1.87
1. 02
0.17
0.85
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
10.46
176.35
120.54
249.61
FWHM
(keV)
27.6
3.1
3.1
3.1
Nuclide
Id
Con.
Energy
(keV)
U-232
U-234
U-235
U-238
0.998
0.997
0.995
1. 000
5302.50*
4761. 50*
4385.50*
4184.40*
Activity
(pCi/liter )
2.09E+001
1.17E-001
2. 06E-001
6.76E-002
+I+I+I+I-
2.38E+000
2.07E-001
2.50E-001
1.69E-001
MDA
(pCi/liter
4.48E-001
3.72E-001
3.04E-001
3.52E-001
+I+I+I+I-
5.10E-002
4.24E-002
3.47E-002
4.01E-002
AU
s/nf/'3
m219
0000058263.CNF
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60
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pex-Aipha
Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:
Env. Background:
Reagent Blank:
D-14 DIS
13041328-UU
05
Shelf 2
iso
Alpha_025
25
System Bkgd 56979
<not performed>
Sample Size:
Sample Date/Time:

4/12/2013
7:27:01 AM
5/16/2013
3:38:29 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.611 mL
0.0519 +/- 0.0053
0.1736 +/- 0.0032 on 12/15/2012
0.2990 +1- 0.0310
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.265
4.774
4.488
4.110
Net
Pk Area
AREA
REPORT
Pk Area
Error%'
102.32
1. 32
0.83
3.49
1:57:27 PM
Ambient
Backgnd
19.45
215.98
239.54
113.53
0.68
0.68
0.17
0.51
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
8.6
3.1
3.1
3.1
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.990
0.999
0.927
0.962
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
2.10E+001
2.70E-001
2.10E-001
7.11E-001
+I+I+I+I-
AG
4.18E+000
5.86E-001
5.04E-001
8.20E-001
s(n/t~
MDA
(pCi/liter
1.16E+000
1.15E+000
1.05E+000
1. 07E+000
+I+I+I+I-
2.31E-001
2.30E-001
2.10E-001
2.14E-001
0000058265.CNF

Start:
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stop : 1024:6615.8(kev)
Acq. Start :Thu May 16 15:38:29 2013
60 II5550
4540
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6500
Channel Data Report
5/17/2013
Page
5:13:06 AM
*******************************************************
*****
S P E C T R A L
DATA
R E P 0 R T
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1227
Channel Data Report

801:
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Sample Title:
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Sample Description:
Spectrum File:
Sample Geometry:
PZ-112-AS TOT
1304132B-UU
06
Shelf 2
U iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_027
27
System Bkgd 56980
<not performed>
Sample Size:
Sample Date/Time:

4/12/2013
7:27:01 AM
3:38:30 PM
5/16/2013
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232_UU-10A
0.608 mL
0.1563 +/- 0.0096
0.1728 +/- 0.0032 on 12/15/2012
0.9050 +!- 0.0584
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.271
4.759
4.303
4.150
T
Net
Pk Area
AREA
REPORT
Pk Area
Error %
306.64
1.13
0.66
1.32
2:27:41 PM
11.22
315.94
305.43
215.97
FWHM
(keV)
Ambient
Backgnd
Reagent
Backgnd
1. 36
1.87
0.34
0.68
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
28.4
3.2
3.2
3.2
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.993
1. 000
0.953
0.992
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
2.08E+001
7.68E-002
5.53E-002
8.93E-002
+I+I+I+I-
KG
2.52E+000
2.43E-001
1. 69E-001
1.93E-001
5( (111~
MDA
(pCi/liter
4.66E-001
5.14E-001
4.01E-001
3.81E-001
+I+I+I+I-
5.64E-002
6.22E-002
4.85E-002
4.61E-002
0000058266.CNF
start:
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Stop : 1024:6658.1(kev)
Acq. Start :Thu May 16 15:38:30 2013
60
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6500
Channel Data Report
5/17/2013
Page
5:13:14 AM
*******************************************************
*****
p E C T R A L
DATA
R E P 0 R T
*****
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Sample Title:
06
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Channel Data Report

369:
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t\1232
Channel Data Report

801:
5/17/2013
Sample Title:
Page
5:13:14 AM
0
06
Channell------I-------I-------I-------1-------I-------I-------I-------J
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Sample Description:
Spectrum File:
Sample Geometry:
u iso
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Reagent Blank:
Alpha_044
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84168
System Bkgd 56989
<not performed>
PZ-112-AS DIS
1304132B-UU
07
Shelf 2
Sample Size:
Sample Date/Time:

4/12/2013
7:27:01 AM
5/16/2013 11:43:37 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232_UU-10A
0.609 mL
0.1558 +/- 0.0096
0.1902 +/- 0.0033 on 12/16/2012
0.8192 +/- 0.0525
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.279
4.706
4.398
4.108
T
Net
Pk Area
AREA
REPORT
Pk Area
Error %
306.00
3.83
0.00
4.00
5:49:26 PM
Amhient
Backgnd
Reagent
Backgnd
0.00
0.17
0.00
0.00
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
11.22
102.72
1960.0
109.57
FWHM
(keV)
20.0
3.0
0.0
3.0
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.996
0.978
0.999
0.959
5302.50*
4761. 50*
4385.50*
4184.40*
Activity
(pCi/liter )
2.09E+001
2.61E-001
O.OOE+OOO
2.72E-001
+/+/+/+/-
2.53E+000
2.70E-001
2.33E-001
2.99E-001
s{r7/l)
MDA
(pCi/liter
4.09E-001
2.84E-001
5.04E-001
4.07E-001
+I+I+I+I-
4.95E-002
3.44E-002
6.10E-002
4.92E-002
0000058247.CNF
Rea1 Time 10200.400 sec
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10
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0
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J.l,
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I.
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4000
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Energy(kev)
5500
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Ull
ROI Type: 1
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Channel Data Report
5/17/2013
Page
5:13:20 AM
*******************************************************
*****
E C T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
07
Elapsed Live time:

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m236
Channel Data Report

369:
5/17/2013
0
Sample Title:
Page
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Channel Data Report

801:
5/17/2013
0
Sample Title:
Page
5:13:20 AM
0
07
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-S238
Sample Description:
Spectrum File:
Sample Geometry:
S-53 TOT
1304132B-UU
18
Shelf 2
u iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_029
29
System Bkgd 56981
<not performed>
Sample Size:
Sample Date/Time:

4/16/2013
7:27:01 AM
5/16/2013
3:38:31 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.609 mL
0.0154 +/- 0. 0029
0.1945 +/- 0.0036 on 12/15/2012
0.0789 +1- 0.0148
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
Net
Pk Area
5.246
4.681
4.429
4.105
AREA
REPORT
Pk Area
Error %
30.15
65.49
13.32
77.66
2:30:02 PM
Ambient
Backgnd
36.28
24.33
55.28
22.30
0.85
0.51
0.68
0.34
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
3. 9
9.3
3.1
3.6

Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.978
0.955
0.987
0.956
5302.50*
4761. 50*
4385.50*
4184.40*
Activity
(pCi/liter )
2.09E+001
4.53E+001
1.14E+001
5.35E+001
+I+I+I+I-
7.63E+000
1.99E+001
7.53E+000
2.29E+001
AG
5/17/0
MDA
(pCi/liter
4.15E+OOO
3.63E+000
4.81E+OOO
3.29E+OOO
+I+I+I+I-
1.52E+000
1. 33E+000
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15
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3500
4500
4000
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li:!!
ROI Type: 1
5000
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6000
5500
ROI Type: 3
6500
Channel Data Report
5/17/2013
Page
5:13:29 AM
*******************************************************
*****
p E C T R A L
DATA
R E p 0 R T
*****
*******************************************************
Sample Title:
18
Elapsed Live time:

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0
1
0
1
1
0
1
2
1
1
0
2
1
2
0
0
0
0
0
0
0
1
1
1
1
1
1
1
1
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
1
0
0
0
0
0
1
1
2
0
0
0
1
2
2
1
0
0
0
0
0
1
0
0
0
0
0
0
1
1
1
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
1
1
0
1
0
2
3
0
1
0
0
1
0
0
0
0
0
0
0
0
0
0
1
2
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
2
0
1
0
0
1
0
1
0
1
1
0
0
2
3
0
0
0
1
0
1
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
1
0
2
0
0
0
0
0
0
0
0
0
0
0
1
2
2
1
0
1
2
0
2
0
0
0
0
0
0
0
0
0
0
1
1
1
2
1
0
0
0
0
1
0
0
0
0
0
1
1
0
0
0
0
0
0
0
1
0
0
0
0
3
3
1
4
2
0
1
0
0
0
0
0
0
0
0
0
0
1
0
1
0
0
!12111
Channel Data Report

369:
5/17/2013
1
Sample Title:
Page
5:13:29 AM
0
18
377:
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1
0
3
1
0
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1
0
0
1
0
1
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1
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1
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2
2
0
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1
0
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0
2
1
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0
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0
1
1
1
0
0
0
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0
0
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0
0
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0
0
0
0
0
0
0
0
1
0
2
2
1
0
0
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
0
0
0
1
0
0
1
0
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
2
0
4
4
0
3
1
0
0
0
0
0
0
1
0
0
0
0
0
0
0
1
0
0
0
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
4
1
0
0
0
2
0
0
0
0
0
1
0
0
0
0
0
1
0
0
0
2
1
0
0
0
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
4
1
0
0
1
1
0
0
0
0
0
0
0
0
0
1
0
1
0
0
0
0
0
0
1
1
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2
2
2
0
2
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1
0
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
fQ2i12
Channel Data Report

801:
5/17/2013
0
Sample Title:
Page
5:13:29 AM
0
18
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945:
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961:
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977:
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993:
1001:
1009:
1017:
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Page 1 of 2
5/16/2013 5:55:31 AM
ha
QA SUMMARY REPORT
Date
Time
: 5/16/2013
: 5:55:31 AM
CHAMBER
Alpha 001
Alpha 002
Alpha 003
Alpha 004
Alpha 005
Alpha 006
Alpha 007
Alpha 008
Alpha 009
Alpha 010
Alpha 011
Alpha 012
Alpha 013
Alpha 014
Alpha 015
Alpha 016
Alpha 017
Alpha 018
Alpha 019
Alpha 020
Alpha 021
Alpha 022
Alpha 023
Alpha 024
Alpha 025
Alpha 026
Alpha 027
Alpha 028
Alpha 029
Alpha 030
Alpha 031
Alpha 032
Alpha 033
Alpha 034
Alpha 035
Alpha 036
Alpha 037
Alpha 038
Alpha 039
Alpha 040
Alpha 041
Alpha 042
DEVICE
21f
2lf
2lf
21f
2lf
21f
2lf
2lf
21f
21f
21f
21f
2lf
21f
21f
21f
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
Alpha AnalystlOODC
Alpha Analyst!OODC
Alpha Analyst! OODC
Alpha Analyst! OODC
Alpha AnalystlOODC
Alpha Analyst100DC
Alpha Analyst100DC
Alpha Analyst!OODC
Alpha Analyst!OODC
Alpha Analyst! OODC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
FLAG
Not Done
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Not Done
Not Done
Passed
Passed
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Passed
Passed
Not Done
Not Done
Passed
Not Done
Passed
Passed
Not Done
Passed
Not Done
Passed
Not Done
Not Done
Not Done
Passed
Passed
Passed
Passed
Passed
Passed
Passed
Passed
Passed
Passed
DATE
5116/2013 5:33:32 AM
5/16/2013 5:33:33 AM
5116/2013 5:33:34 AM
5116/2013 5:33:35 AM
5/16/2013 5:33:36 AM
5116/2013 5:33:37 AM
5/16/2013 5:33:37 AM
5116/2013 5:33:38 AM
5116/2013 5:33:39 AM
5116/2013 5:33:40 AM
5/16/2013 5:33:41 AM
5116/2013 5:33:42 AM
5116/2013 5:33:42 AM
5116/2013
5116/2013
5116/2013
5116/2013
5/16/2013
5116/2013
5/16/2013
5116/2013
5/16/2013
5116/2013
5:33:44 AM
5:33:45 AM
5:33:46 AM
5:33:48 AM
5:33:49 AM
5:33:51 AM
5:33:52 AM
5:33:54 AM
5:33:56 AM
5:33:57 AM
Page 2 of 2
Review of QA Results - Pulser Check

5/16/2013 5:55:31 AM
CHAMBER
Alpha 043
Alpha 044
Alpha 045
Alpha 046
Alpha 047
Alpha 048
DEVICE
Alpha Analyst! OODC
Alpha Analyst! OODC
Alpha Analyst 1OODC
Alpha-Analyst 1OODC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
APPROVED BY:
APPROVAL DATE:
FLAG
Passed
Passed
Passed
Passed
Passed
Passed
DATE
5/11/2013 10:55:58 AM
5116/2013 5:33:59 AM
5116/2013 5:34:01 AM
5/16/2013 5:34:02 AM
5/16/2013 5:34:04 AM
5/16/2013 5:34:06 AM
6/12/12
Page
12:17:04 PM
*************************************************************************
LIBRARY
*****
LISTING
REPORT
*****
*************************************************************************
Uranium

Nuclide
Name
Half-Life
(Seconds)
U-232
U-234
U-235
U-238
2.174E+009
7.731E+012
2.221E+016
1.410E+017
U-232,-234,-235,-238
Energy
(kev l
Energy
Uncert. (kev
5302.500*
4761.500*
4385.500*
4184.400*
0.000
0.000
0.000
0.000
* = key line
TOTALS:
Nuclides
Energy Lines
Yield
(%)
99.8000
99.8000
80.9000
100.2300
Yield
Uncert. (Abs. +-)
0.0000
0.0000
0. 0000
0.0000
SECTION IX
ANALYTICAL DATA (ISOTOPIC THORIUM)
8247
Eberline Services
Analysis Sheet
13-04132
Printed: 5/9/2013 6:02AM

Page 1 of3
ThiSO
Run 1
ThiSO
Analysis Code
Internal
Fractlon
I ,
Work Order
Sample
Desc ,
Client
ID
LCS
01
LCS
-~;----MBL
Run
I ----
4/18/2013
....
Date Received
-
03
'
5/9/2013
Lab Deadline
04
. ------
Client
Project
West Lake OU-1

--
Report Level
Activity Units
06
PZ-106-KS TOT
TRG
D-14 DIS
-I
----
I
I
--
Matrix
Method
WA
45
1.0000E+OO
---
04/12/13 11 :05
EML Th-01 Modified
TRG
PZ-112-AS DIS
45
TRG
PZ-202-SS TOT
04/12/13 11:05
Alpha Spectroscopy
Th-229
' TRG I
PZ-202-SS DIS
10
TRG
DUP07 TOT
TRG
::=f,oo
TRG
Th-18a
1.0000E+OO
----------
04/12/13 11:18
1.0000E+OO
04/12/1311:18 I
1.0000E+OO
04/12/1312:32
1.0000E+OO
04/12/13 12:32
1.0000E+OO
04/12/13 00:00
1.0000E+OO
04/12/13 00:00
1.0000E+OO
..
36
04/15/13 15:59
1.0000E+OO
36
04/15/13 15:59
1.0000E+OO
04/16/13 08:40
1.0000E+OO
46
09
11
1.0000E+OO
--
46
40
-
DUP07 DIS
40
I
I
.-
PZ-106-KS TOT
__
PZ-106-KS DIS
---
f-Radiometric Sol#
--Tracer Act (dpm/g)
38
---
Radiometric Tracer
04/15/13 15:59
--~-----
PZ-112-AS TOT
r--
--------
Instrument Type
38
TRG I
_,_,
1.0000E+OO
------------------~~---
------
08
04/18/13 00:00
07
.
1_0000E+OO
36
...
D-14 TOT
--
Aliquot
f----
pCi
Aliquot Units
--
-------
----
Sample
----~18/13 00:00
1 TRG
05
-----
Sample
Date
CPM
BLANK
I
. DUP I
f-----~~--
Login
14
TRG
FB at PZ-100-KS TOT
39
15
TRG
FB at PZ-100-KS DIS
39
04/16/13 08:40
1.0000E+OO
16
TRG
PZ-100-KS TOT
37
04/16/13 08:50
1.0000E+OO
--
22.467
-
--
Carrier
....
--
17
TRG
PZ-100-KS DIS
18
TRG
S-53 TOT
37
04/16/13 08:50
1.0000E+OO
04/16/13 09:00
1.0000E+OO
41
f----
19
TRG
41
S-53 DIS
-
04/16/13 09:00
1.0000E+OO
I
I
ill!~
r'J
~-
0:1
"'"'Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
13-04132
Printed: 5/9/2013 6:02AM
Page2of3
ThiSO
Run 1
Tracer Total
ACT(dpm)
Radiometric
Tracer (pCi)
2o~:__~
5.4
-+---
5.41:::
-1----
-+ '"1. -_ - -o.oo,
08
10
5.3
0.2387 .
5.4
0.2396 '
5.4
-TRG
L::: I :.: ::::: I

14
151
0.2357
-- 0.2381
TRG
TRG
~1 ::::~-
,_17
TRG I
I TRG I
~RG I
19
TRG
5.31
5.3
-_-
Grav Filter
Grav
Mean
Net(g)
%Rec
% Rec
----
SAF
2*
l-----1
i
I
r ---
--+---------t-
0 -00
J_____o:ooI
~~-~
I
-+
--+--
-1,-----j
-~1-
i .
--
0.00
0~00
5.3
0.2385
5.41
0.00
0.23191
5.2
0.00
0.2368
''__(_
--
0.001
+I-I
-t---. _j_
I
J__[__-+---1-----1
I
--+--I
llr:p_jl
~~
+-~-
llell
~--
--
--
-l-t
----1 -
SAF
1*
0.00
0.2379
Grav Filter
Final (g)
0.00!
-
:: .
--t
--
---+-
- ,- -
16
--t-
Tare (g)
-~- -~
5.4
TRGl 0.2379_1
~
-
.j
5.3
.
Grav Filter
o~~t-_,-~.-----
---
Radiometric Grav Carrier

% Rec
Added (ml)
""SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.
,.... Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
Eberline Services
Analysis Sheet
13-04132
Printed: 5/9/2013 6:02AM

Page 3 of 3
ThiSO
Run 1
I
Internal
Fraction
01
Sample
Desc
Rough Prep
Date
----
02
Prep
Date
By
t
LCS
Rough Prep
MBL
04
DUP
- -- - - - - - -
TRG
--
05
TRG
-
06
TRG
-----
07
TRG
08
TRG
f---
09
10
TRG
TRG
--
t
--=
i
Prep
By
05/03/13 09:39
05/03/13 09:3g . JBARNARD
'
0510~1309'39
0&0~13 00039
05/03/13 09:39
- -
Sep tO
Sep t1
Date/Time
By
Sep t1
By
JBARNARD
jr=
----------- ---
----,---------
-------
. J!-NARDi__
~--
JBARNARD_ JBARNARD
09,39 ' JBARNARD
05/03/13 09:39
JBARNARD
05/03/13 09:39
JBARNARD
----
t=-I
I-
--
----
TRG
12
DO
13
TRG
14
TRG
15
TRG
16
TRG
17
TRG
18
19
JBARNA~--
05/03/13 09:39
JBARNARD
..
~-
I
--
----
JBARNARD
05/03/13 09:39
JBARNARD
--
'
05/03/13 09:39
JBARNARD
05/03/13 09:39
JBARNARD I
05/03/13 09:39
JBARNARD
----
--
05/03/13 09:39
05/03/13 09:39
''
05/03/13 09:39
TRG
TRG
JBARNARD
---
JBARNARD
05/03/13 09:39
----
11
l=t
--
----
'
_ -
'
I
Ia
~~J
U~
t!~
.. SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.
'
--~
I
I
'
05/03/13 09:39
JBARNARD
05/03/13 09:39
0510~13
Sep tO
Date/Time
--
03
.... Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
Eberline Services
Activity
Units
TH-228
LCS
LCS
pCi/1
4.62E+OO
6.94E-01
1.20E01
02
TH-228
MBL
BLANK
pCi/1
2.84E-02
7.23E.02
1.44E.Q1
03
TH228
DUP
PZ-1 06-KS TOT
pCill
2.97E02
6.64E-02
1.26E01
04
TH-228
TRG
014 TOT
pCi/1
9.92E-01
2.79E-01
1.23E-01
OK
05
TH-228
TRG
D-14 DIS
pCi/1
4.50E-02
6.88E02
1.18E-01
OK
06
TH-228
TRG
PZ-112-AS TOT
pCi/1
1.12E-01
1.08E-01
1.57E-01
OK
07
TH-228
TRG
PZ-112-AS DIS
pCi/1
1.11E-02
7.75E.02
1.71E-01
OK
'
~
08
TH-228
TRG
PZ-202-5S TOT
pCi/1
1.56E.01
1.12E.01
1.30E-01
OK
t:
09
TH-228
TRG
PZ-202-5S DIS
pCI/1
9.92E.02
8.79E-02
1.09E-01
OK
10
TH-228
TRG
DUP07TOT
pCi/1
1.01E-01
8.38E.02
1.01 E-01
OK
11
TH-228
TRG
DUP07 DIS
pCi/1
-1.36E-02
4.00E.02
1.15E-01
OK
12
TH-228
DO
PZ-106-KS TOT
pCi/1
-1.37E-02
3.55E.02
1.19E-01
OK
13
TH-228
TRG
PZ-1 06-KS DIS
pCi/1
3.79E.02
5.28E.02
7.98E-02
OK
14
TH-228
TRG
FB
at PZ-100-KS TOT
pCi/1
3.74E.02
4.55E-02
5.52E-02
OK
15
TH-228
TRG
FB
at PZ-100-KS DIS
pCi/1
-9.17E.03
2.80E.02
7.61E-02
OK
"
16
TH-228
TRG
PZ-100-KS TOT
pCi/1
8.52E-02
7.64E.02
8.15E-02
OK
17
TH-228
TRG
PZ-100-KS DIS
pCi/1
1.67E-02
4.18E.02
8.70E-02
OK
C1
18
TH-228
TRG
S-53 TOT
pCI/1
1.99E+01
3.92E+OO
1.16E-01
OK
19
TH-228
TRG
S-53 DIS
pCi/1
3.09E.02
5.02E-02
8.61E-02
OK
0:
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Work Order: 13-04132-ThiS0-1
Client
Identification
Nuclide
Printed: 5/10/2013 8:55AM

Page 1 of 3
Sample
Deso
Lb
Fraction
Results
Error Estimate
MDA
LCS
Known
4.80E+OO
LCS
%R
LCS
Flag
96.31
OK
RPD
Flag
MOA
Flag
OK
OK
NA
OK
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Lob
Fraction
Nuclide
Printed: 5/10/2013 8:55AM

Page 2 of 3
Sample
Desc
Sample
Sample
Radiometric
Date
Aliquot
%Rec
Grav
% Rec
Mean
%Rec
SAF
01
TH-228
LCS
04/18/13 00:00
1.00E+OO
131.02
0.00
0.00
02
TH-228
MBL
04/18/13 00:00
1.00E+OO
77.99
0.00
0.00
03
TH-228
DUP
04/15/13 15:59
1.00E+OO
105.22
0.00
0.00
04
TH-228
TRG
04/12/1311:05
1.00E+OO
103.87
0.00
0.00
05
TH-228
TRG
04/12/1311:05
1.00E+OO
106.20
0.00
0.00
06
TH-228
TRG
04/12/1311:18
1.00E+OO
97.23
0.00
0.00
07
TH-228
TRG
04/12/1311:18
1.00E+OO
82.97
0.00
0.00
08
TH-228
TRG
04/12/1312:32
1.00E+OO
117.13
0.00
0.00
i!
09
TH-228
TRG
04/12/1312:32
1.00E+OO
103.89
0.00
0.00
10
TH-228
TRG
04/12/13 00:00
1.00E+OO
113.95
0.00
0.00
11
TH-228
TRG
04/12/13 00:00
1.00E+OO
122.99
0.00
0.00
12
TH-228
DO
04/15/1315:59
1.00E+OO
88.57
0.00
0.00
..;
13
TH-228
TRG
04/15/1315:59
1.00E+OO
97.84
0.00
0.00
1:!
14
TH-228
TRG
04/16/13 08:40
1.00E+OO
110.55
0.00
0.00
15
TH-228
TRG
04/16/13 08:40
1.00E+OO
110.22
0.00
0.00
16
TH-228
TRG
04116/13 08:50
1.00E+OO
98.05
0.00
0.00
17
TH-228
TRG
04/16/13 08:50
1.00E+OO
98.23
0.00
0.00
"'c
18
TH-228
TRG
04/16/13 09:00
1.00E+OO
70.77
0.00
0.00
"
19
TH-228
TRG
04/16/13 09:00
1.00E+OO
102.22
0.00
0.00
Sep to
Sep t1
Date/Time
DatefTime
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DatefTime
TH-228
LCS
02
TH-228
03
Halflife
(days)
Count
Bkg
A_Spec
Alpha_003
170 3.98 E+02
2.70 E-02
17.5
MBL
05109113 16:28
A_Spec
Alpha_004
170 1.62 E+OO
1.40 E-02
19.4
TH-228
DUP
0510911316:28
A_Spec
Alpha_010
170 2.26 E+OO
2.20 E-02
19.7
04
TH-228
TRG
0510911316:28
A_Spec
Alpha_011
170.02 7.46 E+01
2.00 E-02
05
TH-228
TRG
0510911316:28
A_Spec
Alpha_013
170.02 3.28 E+OO
1.60 E-02
18.7
06
TH-228
TRG
0510911316;28
A_ Spec
Alph'\...014
170 7.41 E+OO
2.70 E-02
18.5
07
TH-228
TRG
0510911316:29
A_Spec
Alpha_018
170 6.00 E-01
2.00 E-02
17.8
08
TH-228
TRG
0510911316:29
A_Spec
Alpha_022
170 1.03 E+01
1.60 E-02
15.3
09
TH-228
TRG
0510911316:29
A_Spec
Alpha_024
170 6.47 E+OO
9.00 E-03
17.1
10
TH-228
TRG
05109113 16:29
A_Spec
Alpha_025
170 7.30 E+OO
1.00 E02
17.4
11
TH-228
TRG
05109113 16:29
A_Spec
Alpha_027
170 -1.06 E+OO
1.80 E-02
17.3
12
TH-228
DO
0510911316:29
A_Spec
Alpha_029
170 -8.70 E-01
1.10 E-02
19.5
13
TH-228
TRG
0510911316:29
A_Spec
Alpha_033
170 2.49 E+OO
3.00 E-03
18.2
t:0
14
TH-228
TRG
0510911316:30
A_Spec
Alpha_034
170 2.83 E+OO
1.00 E-03
18.6
"'c
15
TH-228
TRG
0510911316:29
A_Spec
Alpha_035
170 -6.80 E-01
4.00 E-03
18.3
16
TH-228
TRG
05109113 16:29
A_ Spec
Alpha_037
170 5.49 E+OO
3.00 E-03
17.8
..
17
TH-228
TRG
05109113 16:30
A_Spec
Alpha_040
170 1.15 E+OO
5.00 E-03
19
C>
18
TH-228
TRG
05109113 16:30
A_Spec
Alpha_041
170 1.03 E+03
5.00 E-03
19.8
"
19
TH-228
TRG
05109/1316:30
A_Spec
Alpha_042
170 215 E+OO
5.00 E-03
18.5
Counts
Time
en
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Desc
Sample
0510911316:28
01
Carrier
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Nuclide
Printed: 5/10/2013 8:55AM

Page 3 of 3
Detect
~t:
~
Lob
Fraction
--
19.7
Eberline Services
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Printed: 5/10/2013 8:55AM

Page 1 of 3
LCS
%R
LCS
RPD
MDA
Blank
Flag
Flag
Flag
Flag
82.71
OK
Lb
Fraction
Nuclide
Sample
Desc
Client
Identification
Activity
01
TH-230
LCS
LCS
pCi/1
4.48E+OO
6.76E01
7.31E02
02
TH230
MBL
BLANK
pCi/1
2.65E-01
1.51 E-01
1.33E01
03
TH-230
DUP
PZ-106-KS TOT
pCi/1
2.82E-01
1.29E01
S.OSE-02
04
TH-230
TRG
D-14 TOT
pCI/1
1.15E+OO
3.00E01
5.41E02
OK
en
05
TH-230
TRG
D-14 DIS
pCi/1
1.65E-01
9.84E-02
7.54E-02
OK
J:
06
TH-230
TRG
PZ-112-AS TOT
pCi/1
1.89E-01
1.14E-01
9.74E-02
OK
07
TH230
TRG
PZ112AS DIS
pCi/1
2.04E-01
1.28E-01
1.02E-01
OK
-e'
08
TH-230
TRG
PZ-202-5S TOT
pCI/1
3.94E-01
1.67E-01
1.01E-01
OK
i!
09
TH-230
TRG
PZ202-5S DIS
pCi/1
1.27E-01
9.07E-02
7.84E-02
OK
10
TH-230
TRG
DUP07TOT
pCi/1
1.05E-01
8.15E-02
8.84E-02
OK
11
TH-230
TRG
DUP07 DIS
pCi/1
1.06E-01
7.56E-02
6.56E-02
OK
12
TH-230
DO
PZ-106-KS TOT
pCi/1
9.47E-02
8.23E-02
9.22E-02
OK
d
.E
13
TH-230
TRG
PZ106KS DIS
pCi/1
1.61E-01
1.00E-01
6.20E-02
OK
14
TH-230
TRG
FB at PZ-100-KS TOT
pCi/1
1.77E-01
9.90E-02
6.19E-02
OK
-..
15
TH-230
TRG
FB at PZ-100-KS DIS
pCifl
1.67E-01
9.71E-02
6.31E-02
OK
16
TH-230
TRG
PZ100-KS TOT
pCi/1
3.90E-01
1.65E-01
7.26E-02
OK
17
TH-230
TRG
PZ-100-KS DIS
pCi/1
8.29E-02
6.98E-02
5.94E-02
OK
18
TH-230
TRG
S-53 TOT
pCi/1
1.96E+01
3.85E+OO
1.35E-01
OK
19
TH-230
TRG
S-53 DIS
pCI/1
2.20E-01
1.16E01
6.73E-02
OK
"'
.g
0
(.)
-~
~
~
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Units
Results
Error Estimate
MDA
LCS
Known
5.41E+OO
OK
OK
"f"'"
1-
NA
OK
~
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Lob
Nuclide
Sample
Desc
Sample
Sample
Dote
Allquot
01
TH-230
LCS
04/18/13 00:00
1.00E+OO
131.02
0.00
0.00
02
TH230
MBL
04/18/13 00:00
1.00E+OO
77.99
0.00
0.00
03
TH-230
DUP
04/15/1315:59
1.00E+OO
105.22
0.00
0.00
04
TH230
TRG
04/12/1311:05
1.00E+OO
103.87
0.00
0.00
05
TH-230
TRG
04/12/1311:05
1.00E+OO
106.20
0.00
0.00
06
TH-230
TRG
04/12/1311:18
1.00E+OO
97.23
0.00
0.00
07
TH-230
TRG
04/12/13 11:18
1.00E+OO
82.97
0.00
0.00
'
08
TH-230
TRG
04/12/1312:32
1.00E+OO
117.13
0.00
0.00
"!:
09
TH-230
TRG
04/12/13 12:32
1.00E+OO
103.89
0.00
0.00
10
TH-230
TRG
04/12/13 00:00
1.00E+OO
113.95
0.00
0.00
11
TH-230
TRG
04/12/13 00:00
1.00E+OO
122.99
0.00
0.00
12
TH-230
DO
04/15/1315:59
1.00E+OO
88.57
0.00
0.00
.;
.E
13
TH-230
TRG
04/15/1315:59
1.00E+OO
97.84
0.00
0.00
t!
0
14
TH-230
TRG
04/16/13 08:40
1.00E+OO
110.55
0.00
0.00
"
15
TH-230
TRG
04/16/13 08:40
1.00E+OO
110.22
0.00
0.00
"E
16
TH-230
TRG
04/16/13 08:50
1.00E+OO
98.05
0.00
0.00
17
TH-230
TRG
04/16/13 08:50
1.00E+OO
98.23
0.00
0.00
"'c
18
TH-230
TRG
04/16/13 09:00
1.00E+OO
70.77
0.00
0.00
"
19
TH-230
TRG
04/16/13 09:00
1.00E+OO
102.22
0.00
0.00
0:
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0
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%Rec
G'"
Mean
%Rec
%Rec
SAF
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Printed: 5/10/2013 8:55AM

Page 2 of 3
Eberline Services
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Sample
Deso
Counting
Halflife
DatefTime
(days)
01
TH-230
LCS
02
TH-230
03
Count
Carrier
05/09/13 16:28
A_Spec
Alpha_003
170 3.86 E+02
6.00 E.03
17.5
MBL
05/09/1316:28
A_Spec
Alpha_004
170 1.51 E+01
1.10 E02
19.4
TH-230
DUP
05/09/1316:28
A_Spec
Alpha_010
170 2.20 E+01
6.00 E-03
19.7
04
TH-230
TRG
05/09/13 16:28
A_Spec
Alpha_011
170.02 8.88 E+01
1.00 E-03
19.7
05
TH-230
TRG
05/09/1316:28
A_Spec
Alpha_013
170.02 1.23 E+01
4.00 E-03
18.7
Counts
Time
llll
CPM
Eff
A_Spec
Alpha_014
170 1.28 E+01
7.00 E03
18.5
07
TH-230
TRG
05/09/13 16:29
A_Spec
Alpha_018
170 1.13E+01
4.00 E.03
17.8
08
TH-230
TRG
05/09/13 16:29
A_Spec
Alpha_022
170 2.66 E+01
8.00 E-03
15.3
09
TH-230
TRG
05/09/1316:29
A_Spec
Alpha_024
170 8.49 E+OO
3.00 E03
17.1
10
TH230
TRG
05/09/1316:29
A_Spec
Alpha_025
170 7.81 E+OO
7.00 E03
17.4
11
TH-230
TRG
05/09/13 16:29
A_Spec
Alpha_027
170 8.49 E+OO
3.00 E-03
17.3
12
TH-230
DO
05/09/1316:29
A_Spec
Alpha_029
170 6.15 E+OO
5.00 E-03
19.5
13
TH-230
TRG
05/09/1316:29
A_Spec
Alpha_033
170 1.08 E+01
1.00 E.03
18.2
..:0
14
TH-230
TRG
05/09/1316:30
A_Spec
Alpha_034
170 1.37 E+01
2.00 E-03
18.6
15
TH-230
TRG
05/0911316:29
A_Spec
Alpha_035
170 1.27 E+01
2.00 E-03
18.3
16
TH-230
TRG
05/09113 16:29
A_ Spec
Alpha_037
170 2.57 E+01
2.00 E-03
17.8
17
TH-230
TRG
05109113 16:30
A_Spec
Alpha_040
170 5.83 E+OO
1.00 E.03
19
18
TH-230
TRG
0510911316:30
A_Spec
Alpha_041
170 1.03 E+03
9.00 E-03
19.8
19
TH-230
TRG
05109113 16:30
A_Spec
Alpha_042
170 1.57 E+01
2.00 E-03
"
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Detect
05/09/1316:28
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Nuclide
TRG
Q.
Q.
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Lob
Fraction
TH-230
.E
06
1-
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Printed: 5/10/2013 8:55AM

Page 3 of 3
"r'"
1-~
I
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18.5
Eberline Services
Lab
Fraction
Nuclide
01
Printed: 5/10/2013 8:55AM

Page 1 of 3
Sample
Desc
Client
Identification
Activity
TH-232
LCS
LCS
pCi/1
4.53E+OO
6.82E-01
6.08E-02
02
TH-232
MBL
BLANK
pCi/1
-1.79E-02
3.73E-02
1.10E-01
03
TH-232
DUP
PZ-1 06-KS TOT
pCi/1
3.81E-02
5.16E-02
8.06E-02
04
TH-232
TRG
D-14 TOT
pCi/1
1.17E+OO
3.04E-01
6.7BE-02
OK
05
TH-232
TRG
D-14 DIS
pCi/1
-2.27E-03
2.65E-02
5.57E-02
OK
06
TH-232
TRG
PZ-112-AS TOT
pCI/1
5.12E-02
6.69E-02
1.05E-01
OK
07
TH-232
TRG
PZ-112-AS DIS
pCi/1
2.95E-02
6.36E-02
1.23E-01
OK
08
TH-232
TRG
PZ-202-SS TOT
pCi/1
1.03E-01
8.45E-02
9.31E-02
OK
-!!
09
TH-232
TRG
PZ-202-SS DIS
pCifl
1.24E-02
2.97E-02
6.22E-02
OK
10
TH-232
TRG
DUP07TOT
pCi/1
1.11E-02
2.67E-02
5.59E-02
OK
11
TH-232
TRG
DUP07 DIS
pCi/1
-6.36E-03
2.55E-02
6.54E-02
OK
12
TH-232
DO
PZ-106-KS TOT
pCi/1
4.09E-02
5.32E-02
7.35E-02
OK
13
TH-232
TRG
PZ-106-KS DIS
pCi/1
1.4BE-02
4.12E-02
B.SOE-02
OK
1:!
14
TH-232
TRG
FB
at PZ-100-KS TOT
pCi/1
-2.20E-03
2.57E-02
5.39E-02
OK
"
c
"E
""'
15
TH-232
TRG
FB
at PZ-100-KS DIS
pCi/1
O.OOE+OO
3.65E-02
7.89E-02
OK
16
TH-232
TRG
PZ-100-KS TOT
pCi/1
3.03E-02
5.17E-02
9.09E-02
OK
17
TH-232
TRG
PZ-100-KS DIS
pCi/1
-2.41E-03
2.82E-02
5.92E-02
OK
"'c
18
TH-232
TRG
S-53 TOT
pCi/1
1.90E+01
3.75E+OO
1.78E-01
OK
"
19
TH-232
TRG
S-53 DIS
pCi/1
1.08E-01
S.OOE-02
6.71E-02
OK
0:
.g
0
lJ
-~
~
~
<t
Units
Results
Error Estimate
MDA
LCS
Known
4.80E+OO
LCS
%R
LCS
Flag
94.54
OK
RPD
MDA
Blank
Flag
Flag
Flag
OK
OK
en
-
.s:::
1-
NA
OK
"'s
1::
ill
E
0
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..:;;.
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c
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Eberline Services
0:
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0
<>
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;;
-.:"
Nuclide
Sample
Desc
Sample
01
TH-232
LCS
04118/13 00:00
1.00E+OO
131.02
0.00
0.00
02
TH-232
MBL
04118/13 00:00
1.00E+OO
77.99
0.00
0.00
03
TH-232
DUP
04/1511315:59
1.00E+OO
105.22
0.00
0.00
04
TH-232
TRG
0411211311:05
1.00E+OO
103.87
0.00
0.00
en
05
TH-232
TRG
04112/1311:05
1.00E+OO
106.20
0.00
0.00
J:
06
TH-232
TRG
04/1211311:18
1.00E+OO
97.23
0.00
0.00
07
TH-232
TRG
0411211311:18
1.00E+OO
82.97
0.00
0.00
08
TH-232
TRG
04/1211312:32
1.00E+OO
117.13
0.00
0.00
09
TH-232
TRG
04/1211312:32
1.00E+OO
103.89
0.00
0.00
10
TH-232
TRG
04112113 00:00
1.00E+OO
113.95
0.00
0.00
11
TH-232
TRG
04112113 00:00
1.00E+OO
122.99
0.00
0.00
12
TH-232
DO
04115/13 15:59
1.00E+OO
88.57
0.00
0.00
13
TH-232
TRG
04/15/1315:59
1.00E+OO
97.84
0.00
0.00
t:
14
TH-232
TRG
04116113 08:40
1.00E+OO
110.55
0.00
0.00
15
TH-232
TRG
04116113 08:40
1.00E+OO
110.22
0.00
0.00
16
TH-232
TRG
04116/13 08:50
1.00E+OO
98.05
0.00
0.00
17
TH-232
TRG
04116/13 08:50
1.00E+OO
98.23
0.00
0.00
18
TH-232
TRG
04116113 09:00
1.00E+OO
70.77
0.00
0.00
19
TH-232
TRG
04116/13 09:00
1.00E+OO
102.22
0.00
0.00
Sample
Aliquot
Radiometric
%Rec
Mean
%Rec
Grav
% Rec
SAF
-I-
ill
.5
0
c.
c.
"
c
"E
""'
c"
:;;
"
(/l
"'c
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w
~
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tll
~~)
Sep t1
Date/Time
't:
SeptO
DaterTime
~
-~
Date
T""
Printed: 5/10/2013 8:55 AM

Page 2 of 3
Lb
Fraction
0
~
Eberline Services
~
-~
~
~
"
.,-~
Date/Time
TH-232
LCS
02
TH-232
03
01
Halflife
{days)
Count
Time
A_Spec
Alpha_003
170 3.91 E+02
3.00 E-03
17.5
MBL
05/09/1316:28
A_Spec
Alpha_004
170 -1.02 E+OO
6.00 E-03
19.4
TH-232
DUP
05/09/1316:28
A_Spec
Alpha_010
170 2.98 E+OO
6.00 E03
19.7
04
TH-232
TRG
05/09/13 16:28
A_Spec
Alpha_011
170.02 9.05 E+01
3.00 E-03
19.7
Cl)
05
TH-232
TRG
05/09/1316:28
A_Spec
Alpha_013
170.02 -1.70 E-01
1.00 E-03
18.7
J:
06
TH-232
TRG
05/09/13 16:28
A_Spec
Alpha_014
170 3.47 E+OO
9.00 E-03
18.5
07
TH-232
TRG
05/09/13 16:29
A_Spec
Alpha_018
170 1.64 E+OO
8.00 E-03
17.8
08
TH-232
TRG
05/09/13 16:29
A_Spec
Alpha_022
170 6.98 E+OO
6.00 E-03
15.3
1-
Counts
Bkg
05/09/1316:28
~
"!:
Counting
Desc
Nuclide
Carrier
" """
(J
Sample
Lb
Fraction
Printed: 5/10/2013 8:55AM

Page 3 of 3
Detect
-1:0
CPM
Eff
'
I'
09
TH-232
TRG
05/09/13 16:29
A_ Spec
Alpha_024
170 8.30 E-01
1.00 E-03
17.1
10
TH-232
TRG
05/09/1316:29
A_Spec
Alpha_025
170 8.30 E-01
1.00 E-03
17.4
11
TH-232
TRG
05/09/13 16:29
A_Spec
Alpha_027
170 -5.10 E-01
3.00 E-03
17.3
12
TH-232
DO
05/09/1316:29
A_Spec
Alpha_029
170 2.66 E+OO
2.00 E-03
19.5
13
TH-232
TRG
05/09/13 16:29
A_Spec
Alpha_033
170 1.00 E+OO
0.00 E+OO
18.2
14
TH-232
TRG
05/09/13 16:30
A_Spec
Alpha_034
170 -1.70 E-01
1.00 E-03
18.6
Ul
15
TH-232
TRG
05/09/13 16:29
A_Spec
Alpha_035
170 1.00 E+OO
0.00 E+OO
18.3
16
TH-232
TRG
05/09/1316:29
A_Spec
Alpha_037
170 2.00 E+OO
0.00 E+OO
17.8
17
TH-232
TRG
05/09/1316:30
A_Spec
Alpha_040
170 -1.70 E-01
1.00 E-03
19
."'c.,
18
TH-232
TRG
05/09/13 16:30
A_Spec
Alpha_041
170 1.01 E+03
2.10 E-02
19.8
"
19
TH-232
TRG
05/09/1316:30
A_Spec
Alpha_042
170 7.66 E+OO
2.00 E-03
18.5
ill
.;
E
-i
Q.
Q.
:I
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"E
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..
:;;
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;;,
c
w
c
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Count Room Report

13-04132-ThiS0-1 (pCi/1) in WA
Tracer ID: Th-18a
Printed: 5/9/2013 6:02AM
Page 1 of 1
/ t \(l-"
Internal
Fraction .
f{..
Sample
Desc
I
1
~: i ~:-+ -
:o~___ii~-~4_~)
---~
TRG
Client
ID
.:, . .
Sample
Aliquot
I!
::;;:;;:::::~_::::-r
PZ-106-KS TOT __ : 04/15/1315:5;-+- 1.0000
PZ-112-ASTOT~2/131~-:18
1
::::::::::::
1.0000
:::::~
Tracer
Aliquot(g)
:::
I
I
0.2403____
_1-~ooo __
1o4t12~~3 11:0~0000
D-14 DIS
~-~ ::: J :~~;:_:: :~~-
I
1
D-14TOT ___ TQ4112/1311:05
-~ tTRG-~
~
I
Sample
Date
TRG
Pz-202-ss Dis
- o4t1211312:32T1:oooo
TRG
DUP07TOT
04/12/1300:oo
DUP07 DIS
' 04/12/13 00:00
_rnr
__
r--11\_:rRG .
--;--DO
PZ-106-KS TOT
$! L..2:__J__2_~-- PZ~106-KS DIS
;'
::::::
::::::
'
o.2387
5.3629
19
'"l """"'
~G
S-53 DIS
'
I'IJ
en
il!ll
~~~I
~000
_ t--0.2378 I
~15/1315:5~___1~0000 .I
--=I~04/16/13 09:oo
-0.2374
0.238~
o.2357
04/16/13 09:00 '

I
1.0000
0.00
~ ~-~-
SAF
2*
____
--
__ _
J_. 0.0~- ~--_-j--1~~~--1
__
_o.oo~-
o.ootf=.-1
5.33~--~_j_~- 0.00 .
~ ~~
----
,:,,.,
"'"" I
0.2379
5.3449
0.2385
5.3584
0.2319
5.2101 1_
1.oooo
---1
E---- r::F t---=I
~_
0.2396
SAF
1*
o.oo_j
5.35~ ____
0.2383
-5.3202
1.oooo
~~:
5.27081
0.2368
I=~-~~~FBatPZ-100-KSD~S- I <W'"""'"'I ;.oooo\16 1 _nroy_-~z-1oo-Ks To-r____ . 04/16/13 o8:5~~-oo~o [

~ TRG r
PZ-100-KS DIS
04/16/13 08:50 - 1.0000
"_ I
04/15/1315:59
%Rec
-5.3988t~-- ---,--- 0-.o-o-t!-_-_-~
i Radiometric I
Radiometric
Tracer(pC1}
'::: .
0.2346
1o
Tracer
ACT(dpm)
_I
=+
____
,_
o.oo f-----t----o.oo .I
0.00
o.oo-t---
5.3202+------~-{l.QQ~t----t---i
0.2368
I
--r-
_j_
Eberline Services
Internal Work Order
Run
Analysis Code
Date
Technician
13-04132
ThiSO
5/3/2013 9:37
JBARNARD
LCS & Matrix Spikes
Activity
dpmlg
Isotope
Sol#
Th-228
Th-8b
103.560
Th-230
Th-1b
23.525
Th-8b
Th-232
Page 1 of 1
Printed: 5/3/2013 9:39AM
Solution
Date
1
103.560
I Addition
Approx
LCS
MS
LCSD
MSD
Volume
Used(g)
Volume
Used(g)
Volume
Used(g)
Volume
Used (g)
LCS
0.100
0.1028
4.80
5/3/2013
0.500
0.5109
5.41!
0.100
4.80
0.1028
MS
Error
Estimate
Known
pCi
5/3/2013
5/3/2013
fraction
Isotope
Sol#
Volume
Used(g}
Approx
Addition
5/3/2013
0.4848
0.2200
Th-18a
22.467
5/3/2013
0.2425
0.2200
Th-229
Th-18a
22.467
5/3/2013
0.2403
0.2200
04
Th-229
Th-18a
22.467
5/3/2013
0.2346
0.2200
05
Th-229
Th-18a
22.467
5/3/2013
0.2383
0.2200
Th-229
Th-18a
22.467
5/3/2013
0.2368
0.2200
07
Th-229
Th-18a
22.467
5/3/2013
<r.2392
0.2200
08
Th-229
Th-18a
22.467
5/3/2013
0.2379
0.2200
0.2387
0.2200
Th-229
Th-18a
02
Th-229
03
06
'
22.467
..en
~
Estimate
Added
pCi
0.000
0.00
0.000
0.00
0.146
o.ooi
0.000
oooi
oooi
0.000
0.00
0.173
0.00
0.000
5/3/2013
0~ 4848
0.000
0.00
'3
0.2425 g
-0.2403 '3
0~ ~H09 '3
102f.: Sl
-(1.2346 '3
-0.2383 g
(1.
-0.2368 '3
-0~ 2392
-0.:2379
'3
23~:7
Sl
Th-229
Th-18a
10
Th-229
Th-18a
22.467
5/3/2013
0.23.96
0.2200
11
Th-229
Th-18a
22.467
5/3/2013
0.2374
0.2200
12
Th-229
Th-18a
22.467
5/3/2013
0.2378.
0.2200
13
Th-229
Th-18a
22.467
5/3/2013
0.2383
0.2200
-0. 237B 3
-0. 23::~:3; '3
14
Th-229
Th-18a
22.467
5/3/2013
0.2357
0.2200
-0. 2357
-0=2381
-0.
-0 .. 2396 9
-ra ~
15
Th-229
Th-18a
22.4671
5/3/2013
0.2381
0.2200
16
Th-229
Th-18a
22.467
5/3/2013
0.2379
0.2200
17
Th-229
Th-18a
22.467
5/3/2013
0.2385
0.2200
18
Th-229
Th-18a
22.467
5/3/2013
0.2319
0.2200
19
Th-22~_Th18a
22.467
5/3/2013
0.2368
0.2200
:::;.:$74
lUI
.,,
-0.23?9 9
-0.2385 '3
-0.2319 '3
Error
Estimate
0.000
0.000
~
LCS
Tracer
09
Version 2.0 08/99
MSD
Error
Known
pCi
0.00!
-121 :2369 -:=;~
till
M
LCSD
Error
Estimate

Solution
Date
22.467
01
Added
pCi
0.173
Tracers
Activity
dpmlg
Witness Initials
Matrix Spike
0.000
Eberline Analytical
Work Order
13-04132
Lab
Fraction
I 1
Engineering Management Support, In<:.
Client ID
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
DO
TRG
TRG
TRG
TRG
TRG
TRG
TRG
Analysis Code
Rpt Units
Lab Deadline
Technician
ThiSO
liters
5/9/2013
JBARNARD
Dilution Data
Muffle Data
Sample
Type
LCS
MBL
DUP
LCS
BLANK
PZ-106-KS TOT
D-14 TOT
D-14 DIS
PZ-112-AS TOT
PZ-112-AS DIS
PZ-202-SS TOT
PZ-202-SS DIS
DUP07TOT
DUP07 DIS
PZ-106-KS TOT
PZ-1 06-KS DIS
FB at PZ-100-KS TOT
FB at PZ-100-KS DIS
PZ-100-KS TOT
PZ-100-KS DIS
S-53 TOT
S-53 DIS
Printed: 5/3/2013 9:41AM

Page 1 of 1
Aliquot Worksheet
Ratio
Post/Pre
No of Oils
Aliquot Data
Oil Factor
Ratio
Aliquot
.
..
..
.-.
'"
. ...
-.
..
. . .
.
.
....
. ..
.
..
.. ..
. . .
.
i
I
MS Aliquot Data
: -.-Net Ecjuiv
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO ' '
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO .
1.0000E+OO
1.0000E+OO
1.0000E+OO
Aliquot
H-3 Solids Only

Water Added
(ml)
Net Equiv
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
H3 Dist
Aliq
----~
...
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
..
.....
----~
.... - - -
..
.> ..
. .
'
. /.
-- - -
-- L _ _
---
Comments
~~
m
N
Technician:
<.
P:,J
Date:
ex-Alpha
Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:
Env. Background:
SPIKE
1304132A-TH
01
Shelf 2
Th iso
Alpha_003
3
System Bkgd 56360
Reagent Blank:
<not performed>

5/9/2013
7:22:02 AM
5/9/2013
4:28:50 PM
l70. 0 minutes
170.0 minutes
Sample Size:
Sample Date/Time:
Th229 TH-18A
0.485 mL
0.2288 +!- 0.0132
0.1746 +/- 0.0033 on 12/15/2012 11:26:47 AM
1.3102 +/- 0.0795
Tracer Certificate:
Tracer Quantity:
Control Certificate Name: NatTh Th-8

TH-232
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.768
5.381
4.875
4.641
3.967
0.945409 +/-
AREA
0.077895
REPORT
Net
Pk Area
Ambient
Reagent
Pk Area
Error %
Backgnd
Backgnd
13.09
398.41
423.64
385.98
391.49
62.93
9.89
9.54
9.99
9.91
3.91
4.59
1.36
1. 02
0.51
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
3.0
42.9
6.8
9.1
24.2
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.965
0.998
1. 000
0.995
0.995
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
1.55E-001
4.62E+000
4.93E+000
4.48E+000
4.53E+000
+!+I+I+I+I-
9.94E-002
6.94E-001
5.58E-001
6.76E-001
6.82E-001
MDA
(pCi/liter
1.16E-001
1.20E-001
7.98E-002
7.31E-002
6.08E-002
+!+I+I+I+I-
1.31E-002
1.35E-002
9.02E-003
8.27E-003
6.87E-003
5/ fo/t3
-rD-263
0000057570.CNF
Start:
13498.4(kev)
Stop : 1024 6549.5(kev)
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40
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Channel Data Report
5/10/2013
Page
5:01:23 AM
****i**************************************************
*****
p E C T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
01
Elapsed Live time:

Elapsed Real Time:
10200
10200
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:
10200
0
0
0
0
1
0
0
0
0
0
1
1
0
0
3
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3
6
11
21
6
0
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1
1
0
0
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10200
0
0
0
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2
1
2
0
1
1
4
5
7
10
18
5
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0
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0
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0
3
5
8
8
16
4
1
0
0
0
0
1
1
0
0
0
0
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0
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0
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0
0
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0
0
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0
1
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5
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14
11
1
0
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0
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0
0
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0
4
0
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1
2
0
0
0
0
0
0
0
0
0
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0
0
1
2
0
3
3
3
2
9
7
17
0
0
0
0
1
0
1
0
0
0
0
0
0
0
0
0
1
0
0
1
0
4
1
1
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
2
3
3
9
11
12
9
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
1
1
2
1
0
0
0
0
0
1
0
0
0
0
0
0
1
0
1
4
5
3
8
12
8
0
0
0
0
0
0
0
0
1
0
0
0
0
0
1
0
0
0
0
0
0
0
4
7
0
0
0
0
0
1
1
0
0
0
0
0
0
2
2
1
3
8
9
10
11
10
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lll266
Channel Data Report

801:
5/10/2013
0
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Page
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~267
ex-AiphaTM
Sample Description:
Spectrum File:
Sample Geometry:
BLANK
Detector Name:
Env. Background:
Reagent Blank:
Alpha_004
1304132A-TH
02
Shelf 2
Th iso
System Bkgd 56361

<not performed>


5/9/2013
7:22:02 AM
5/9/2013
4:28:52 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.243 mL
0.1513 +/- 0.0137
0.1940 +/- 0.0036 on 12/15/2012 11:26:46 AM
0.7799 +/- 0.0718
0.175 MeV
Sample Size:
Sample Date/Time:
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.913
5.327
4.861
4.632
3.947
Net
Pk Area
-0.87
1.62
140.15
15.13
-1.02
AREA
REPORT
Pk Area
Error %
Ambient
Backgnd
1.87
2.38
0.85
1. 87
1. 02
258.63
253.92
16.61
53.91
208.15
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
2.9
2.9
3.7
2.9
0.0
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.979
0.973
0.999
0.992
0.987
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
-1. 56E-002
2.84E-002
2.47E+000
2.65E-001
-1.79E-002
+I+I+I+I+I-
4.05E-002
7.23E-002
4.36E-001
1. 51E- 001
3.73E-002
MDA
(pCi/liter
1.36E-001
1.44E-001
1.05E-001
1.33E-001
1.10E-001
+!+I+I+I+I-
2.41E-002
2.54E-002
1. 86E- 002
2.35E-002
1.95E-002
A4
5"/to/ /}
lil2S8
0000057571.CNF
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6500
Channel Data Report
5/10/2013
5:01:!H. 1oM
Page
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Sample Title:
02
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Channel Data Report

369:
5/10/2013
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Sample Title:
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'i271
Channel Data Report

801:
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0
Sample Title:
Page
5:01:31 AM
0
02
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:fii-272
Sample Description:
Spectrum File:
Sample Geometry:
PZ-106-KS TOT-DUP
1304132A-TH
03
Shelf 2
Th iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_OlO
10
System Bkgd 56362
<not performed>
Sample Size:
Sample Date/Time:

4/15/2013
7:22:02 AM
4:28:46 PM
5/9/2013
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.240 mL
0.2070 +/- 0.0164
0.1967 +/- 0.0036 on 12/15/2012 11:26:40 AM
1.0522 +/- 0.0856
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.812
5.327
4.886
4.629
3.998
Net
Pk Area
AREA
REPORT
Pk Area
Error %
2.77
2.26
189.96
21.98
2.98
Ambient
Backgnd
181. 07
223.40
14.31
42.93
134.36
3.23
3.74
2.04
1. 02
1. 02
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
2.9
2.9
6.1
5.9
2.9

Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.992
0.972
0.999
0.990
1.000
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
3.64E-002
2.97E-002
2.44E+000
2.82E-001
3.81E-002
+I+I+I+I+I-
6.62E-002
6.64E-002
3.80E-001
1.29E-001
5.16E-002
MDA
(pCi/liter
1.20E-001
1.26E-001
1.00E-001
B.OBE-002
8.06E-002
+I+I+I+I+I-
1. 86E-002
1. 96E- 002
1.56E-002
1.26E-002
1. 25E-002
Au
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/,
!,
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""
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1Ji'27-6
Channel Data Report

801:
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AM
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8.277
ex-AiphaTM
Sample Geometry:
D-14 TOT
1304132A-TH
04
Shelf 2
Th iso
Detector Name:
Alpha_011
Sample Description:
Spectrum File:

Env. Background:
11
System Bkgd 56363
Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

4/12/2013
7:22:02 AM
5/9/2013
4:28:47 PM
170.0 minutes
l70.0 minutes
Th229_TH-18A
0.235 mL
0.2049 +/- 0.0165
0.1973 +/- 0.0042 on 12/15/2012 11:28:06 AM
1.0387 +/- 0.0863
0.175 MeV
Tracer Certificate:
Tracer Quantity:
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
Net
Pk Area
5.906
5.380
4.880
4.631
3.970
AREA
REPORT
Pk Area
Error %
3.13
74.60
183.64
88.83
90.49
Ambient
Backgnd
144.41
23.29
14.53
20.82
20.67
l. 87
3.40
1.36
0.17
0.51
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
2.7
2.7
10.2
2.9
8.4

Id
Conf.
Energy
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
0.984
0.998
l. 000
0.991
0.996
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
(keV)
Activity
(pCi/liter )
4.16E-002
9.92E-001
2.39E+OOO
l.15E+OOO
l.17E+OOO
+I+I+I+I+I-
6.04E-002
2.79E-001
3.76E-001
3.00E-001
3.04E-001
MDA
(pCi/liter
1.01E-001
l.23E-001
8.91E-002
5.41E-002
6.78E-002
+I+I+I+I+I-
l.58E-002
1.94E-002
l.40E-002
8.51E-003
l. 07E- 002
IG
'Sfro/t?
-el27S
0000057569.CNF
Start:
1 3645.8(kev)
Stop : 1014 6374.l(kev)
60
55
50
45
40
35
.....
"'
r:::
8 30
25
20
15
10
5
0
!JA
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4000
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Ul
ROI Type: 1
5000
Energy(kev)
6000
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ROI Type: 3
Channel Data Report
5/10/2013
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5:01:4'!' l'.M
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ill282
ex-AiphaTM
Sample Description:
Spectrum File:
Sample Geometry:
D-14 DIS
1304132A-TH
05
Shelf 2
Th iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_013
13
System Bkgd 56364
<not performed>
1. OOOE+OOO +/O.OOOE+OOO liter

7:22:02 AM
4/12/2013
4:28:48 PM
5/9/2013
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.238 mL
0.1985 +/- 0.0160
0.1869 +/- 0.0035 on 12/15/2012 11:26:45 AM
1.0620 +/- 0.0879
0.175 MeV
Sample Size:
Sample Date/Time:
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.794
5.368
4.869
4.633
3. 971
Net
Pk Area
4.13
3.28
180.66
12.32
-0.17
AREA
REPORT
Pk Area
Ambient
Error %
Backgnd
Reagent
Backgnd
1. 87
2. 72
0.34
0.68
0.17
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
119.29
151.92
14.60
57.62
1169.3
FWHM
(keV)
2.8
2.8
8.9
2.8
0.0
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.984
0.995
1.000
0.992
0. 997
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
5.67E-002
4.50E-002
2.42E+000
1. 65E-001
-2.27E-003
+I+I+I+I+I-
6.82E-002
6.88E-002
3.83E-001
9.84E-002
2.65E-002
~
S/ro(t~
MDA
(pCi/liter
1. 04E-001
1.18E-001
6.41E-002
7.54E-002
5.57E-002
+I+I+I+I+I-
1. 64E- 002
1. 86E-002
1. 01E-002
1.19E-002
8.81E-003
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Channel Data Report

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nl286
Channel Data Report

801:
5/10/2013
0
Sample Title:
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Ul287
ex-AiphaTM
Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:
Env. Background:
PZ-112-AS TOT
1304132A-TH
06
Shelf 2
Th iso
Alpha_014
14
System Bkgd 56365
Reagent Blank:
<not performed>

4/12/2013
7:22:02 AM
5/9/2013
4:28:49 PM
Sample Size:
Sample Date/Time:
170.0 minutes
170.0 minutes
Th229 TH-18A
0.237 mL
0.1795 +/- 0.0152
0.1846 +/- 0.0034 on 12/15/2012 11:26:44 AM
0.9723 +/- 0.0844
0.175 MeV
Tracer Certificate:
Tracer Quantity:
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.858
5.333
4.873
4.626
3.965
AREA
REPORT
Net
Pk Area
Ambient
Pk Area
Error %
Backgnd
Reagent
Backgnd
2.55
4.59
1. 70
1.19
1.53
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
3.45
7.41
162.30
12.81
3.47
144.10
94.56
15.48
57.66
129.54
FWHM
(keV)
2.9
2.9
3.9
2.9
2.9

Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
1. 000
0.977
1.000
0.989
0.995
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
5.24E-002
1.12E-001
2.41E+OOO
1. 89E-001
5.12E-002
+I+I+I+I+I-
7.60E-002
1.08E-001
4.00E-001
1.14E-001
6.69E-002
MDA
(pCi/liter
1.27E-001
1.57E-001
1.09E-001
9.74E-002
1.05E-001
+I+I+I+I+I-
2.12E-002
2.61E-002
1. 81E-002
1. 62E- 002
1. 75E-002
ftG
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Channel Data Report
5/10/2013
Page
5:02:04 AM
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*****
p E C T R A L
DATA
R E P 0 R T
*****
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06
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Channel Data Report

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fi!_n--a
c.- 1...
Channel Data Report

801:
5/10/2013
0
Sample Title:
Page
5:02:04 AM
0
06
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8292
Sample Description:
Spectrum File:
Sample Geometry:
PZ-112-AS DIS
1304132A-TH
07
Shelf 2
Th iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_018
18
System Bkgd 56366
<not performed>
Sample Size:
Sample Date/Time:

4/12/2013
7:22:02 AM
5/9/2013
4:29:24 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.239 mL
0.1474 +/- 0.0136
0.1776 +/- 0.0033 on 12/15/2012
0.8297 +/- 0.0779
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.874
5. 314
4.874
4.676
3. 964
Net
Pk Area
AREA
REPORT
Pk Area
Error %
1.96
0.60
134.64
11.32
1.64
1:57:26 PM
208.49
698.88
16.99
60.27
214.83
Ambient
Backgnd
Reagent
Backgnd
FWHM
(keV)
2.04
3.40
1. 36
0.68
1.36
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
3.1
3.1
7.6
3.1
3.1

Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.997
0.962
1.000
1.000
0.994
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
3.62E-002
l.llE-002
2.43E+000
2.04E-001
2.95E-002
+I+I+I+I+I-
7.58E-002
7.75E-002
4.39E-001
1.28E-001
6.36E-002
MDA
(pCi/liter
1.44E-001
1. 71E-001
1. 24E-001
1. 02E-001
1.23E-001
+I+I+I+I+I-
2.60E-002
3.09E-002
2.23E-002
1. 83E-002
2.22E-002
1\&
.S/ro/17
til293
0000057574.CNF
Start:
13404.1(kev)
stop : 1024 6604.2(kev)
60555045-1-4035....,
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8 30-
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I
6500
Channel Data Report
5/10/2013
Page
5:02:15 1.M
*******************************************************
*****
p E C T R A L
DATA
R E p 0 R T
*****
*******************************************************
Sample Title:
07
Elapsed Live time:

Elapsed Real Time:
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369:
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fJ2S6
Channel Data Report

801:
5/10/2013
0
Sample Title:
Page
5:02:15 AM
0
07
809:
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825:
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841:
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993:
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0
0
0
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0
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0
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0
0
0
0
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0
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0
0
0
0
1
0
1
0
0
1
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pex-Aipha
Sample Description:
Sample Geometry:
PZ-202-SS TOT
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\OOOOOS7S
1304132A-TH
08
Shelf 2
Th iso
Detector Name:
Env. Background:
Alpha_022
Spectrum File:
22
System Bkgd S6367
Reagent Blank:
<not performed>

4/12/2013
7:22:02 AM
S/9/2013
4:29:2S PM
170.0 minutes
170.0 minutes
Sample Size-:
Sample Date/Time:
Th229 TH-18A
0.238 mL
0.1794 +/- 0.01S2
0.1S31 +/- 0.0029 on 12/1S/2012
1.1713 +/- 0.101S
0.17S MeV
Tracer Certificate:
Tracer Quantity:
PEAK
Nuclide
Energy
(MeV)
TH-227
TH-228
TH-229
TH-230
TH-232
S.8SO
S.34S
4.862
4.647
3.971
AREA
REPORT
Net
Pk Area
Pk Area
Error %
3.13
10.28
162.98
26.64
6.98
1:S7:26 PM
144.40
69.96
1S.41
39.09
80.28
Ambient
Backgnd
Reagent
Backgnd
FWHM
(keV)
1. 87
2.72
1. 02
1. 36
1. 02
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
3.1
3.1
3.9
6.2
3.1
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
1.000
0.984
0.999
0.997
0.997
S8SO.OO*
S400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
4.7SE-002
1.S6E-001
2.42E+000
3.94E-001
1.03E-001
+I+I+I+I+I-
6.91E-002
1.12E-001
4.01E-001
1.67E-001
8.4SE-002
S/to/l3
MDA
(pCi/liter
1.1SE-001
1.30E-001
9.35E-002
1. 01E-001
9.31E-002
+I+I+I+I+I-
1. 90E-002
2.16E-002
1. SSE- 002
1. 68E- 002
1. S4E- 002
0000057575.CNF
start:
1:342U(kev)
stop : 1024:6608.8(kev)
Acq, start :Thu May 09 16:29:25 2013
60555045
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6500
Channel Data Report
5/10/2013
Page
5:02:23 AM
*******************************************************
*****
P E C T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
08
Elapsed Live time:

Elapsed Real Time:
10200
10200
1:
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m.Jm1
Channel Data Report

801:
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0
Sample Title:
Page
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Sample Description:
Spectrum File:
Sample Geometry:
PZ-202-SS DIS
1304132A-TH
09
Shelf 2
Th iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_024
24
System Bkgd 56368
<not performed>
Sample Size:
Sample Date/Time:

7:22:02 AM
4/12/2013
4:29:26 PM
5/9/2013
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229_TH-18A
0.239 mL
0.1777 +/- 0.0151
0.1710 +/- 0.0032 on 12/15/2012
1.0389 +/- 0.0901
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.823
5.357
4.856
4.657
3.913
Net
Pk Area
AREA
REPORT
Pk Area
Error %
4.47
6.47
161.98
8.49
0.83
2:02:15 PM
109.71
87.07
15.46
69.59
239.53
Ambient
Backgnd
1. 53
1.53
1. 02
0.51
0.17
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
3.1
3.1
4.3
3.1
3.1

Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.996
0.990
0.999
0.999
0.964
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
6.85E-002
9.92E-002
2.43E+OOO
1.27E-001
1.24E-002
+I+I+I+I+I-
7.60E-002
8.79E-002
4.03E-001
9.07E-002
2.97E-002
PiG
S{to{(~
MDA
(pCi/liter
1.09E-001
1.09E-001
9.44E-002
7.84E-002
6.22E-002
+I+I+I+I+I-
1.81E-002
1. 81E- 002
1.57E-002
1.30E-002
1.03E-002
0000057576.CNF
60
55

Start:
1:341!.6(kev)
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Acq. Start :Thu May 09 16:29:26 2013
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Channel Data Report
5/10/2013
Page
5:02:31 AM
*******************************************************
S P E C T R A L
DATA
R E P 0 R T
*****
*****
*******************************************************
Sample Title:
09
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0
0
0
ex-AiphaTM
Sample Geometry:
DUP07 TOT
1304132A-TH
10
Shelf 2
Th iso
Detector Name:
Alpha_025
Sample Description:
Spectrum File:
Env. Background:
Reagent Blank:
25
System Bkgd 56369
<not performed>

4/12/2013
7:22:02 AM
4:29:27 PM
5/9/2013
170.0 minutes
170.0 minutes
Sample Size:
Sample Date/Time:
Th229 TH-18A
0.240 mL
0.1978 +/- 0.0160
0.1736 +/- 0.0032 on 12/15/2012
1.1395 +/- 0.0945
0.175 MeV
Tracer Certificate:
Tracer Quantity:
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.792
5.337
4.887
4.607
4.027
Net
Pk Area
0.13
7.30
180.98
7.81
0.83
AREA
REPORT
Pk Area
Ambient
Error %
Backgnd
2294.8
81.83
14.62
76.13
239.53
1:57:27 PM
1. 87
1. 70
1. 02
1.19
0.17
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
3.1
3.1
5.5
4.7
3.1
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.983
0.980
0.999
0.978
0.995
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
1. 79E-003 +I- 4.11E-002
1. 01E-001 +I- 8.38E-002
2.44E+OOO +1- 3.86E-001
1. 05E-001 +I- 8.15E-002
l.llE-002 +I- 2.67E-002
S/ro/6
MDA
(pCi/liter
1. 04E- 001
1.01E-001
8.48E-002
8.84E-002
5.59E-002
+I+I+I+I+I-
1. 65E-002
1. 60E- 002
1.34E-002
1.40E-002
8.85E-003
0000057577.CNF
Start:
1:3405.9(kev)
Stop : 1024:66!5.8(kev)
Acq. start :Thu May 09 16:29:27 2013
60+
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6500
Channel Data Report
5/10/2013
Page
5:02:39 AM
*******************************************************
*****
p E C T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
10
Elapsed Live time:

Elapsed Real Time:
10200
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Channel Data Report

369:
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0
Sample Title:
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lll311
Channel Data Report

801:
5/10/2013
0
Sample Title:
5:02:~,
Page
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0
10
809:
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1~312
pex-AiphaTM
Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:
Env. Background:
Reagent Blank:
DUP07 DIS
1304132A-TH
11
Shelf 2
Th iso
Alpha_027
27
System Bkgd 56370
<not performed>
Sample Size:
Sample Date/Time:

4/12/2013
7:22:02 AM
4:29:28 PM
5/9/2013
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.237 mL
0.2125 +/- 0.0167
0.1728 +/- 0.0032 on 12/15/2012
1.2299 +/- 0.0995
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.908
5.385
4.861
4.658
3.947
Net
Pk Area
0.79
-1.06
192.64
8.49
-0.51
AREA
2:27:41 PM
REPORT
Pk Area
Error %
455.84
293.54
14.18
69.59
400.63
Ambient
Backgnd
2.21
3.06
1.36
0.51
0.51
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
3.2
3.2
6.9
3.2
0.0
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.983
0.999
0.999
0.999
0.987
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/1iter )
1. 01E-002
-1.36E-002
2.41E+OOO
1. 06E-001
-6.36E-003
+I+I+I+I+I-
4.62E-002
4.00E-002
3. 72E-001
7.56E-002
2.55E-002
A&5'/rc{rJ,
MDA
(pCi/liter
1. 03E- 001
1.15E-001
8.59E-002
6.56E-002
6.54E-002
+I+I+I+I+I-
1. 58E-002
1.77E-002
1.33E-002
1. 01E-002
1. 01E-002
0000057578.CNF
Start:
l:l402.4(kev)
stop : 1024:665B.l(kev)
Acq. start :Thu May 09 16:29:28 2013
60-.155-1150-
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6500
Channel Data Report
5/l0/201_3
Page
5:02:49 AM
1_
*******************************************************
*****
p E C T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
Elapsed Live time:

Elapsed Real Time:
l0200
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9:
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tli315
Channel Data Report

369:
5/10/2013
0
Sample Title:
Page
5:02:49 AM
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11
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801:
5/10/2013
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Sample Title:
5:02:4~
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29
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<not performed>
4/15/2013
7:22:02 AM
4:29:29 PM
5/9/2013
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0.175 MeV
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TH-230
TH-232
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85.19
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O.OOE+OOO
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3.1
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3.1
3.1
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TH-228
TH-229
TH-230
TH-232
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1. 000
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0.987
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5400.00*
4872.00*
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3997.00*
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4.09E-002
+I+I+I+I+I-
6.48E-002
3.55E-002
4.07E-001
8.23E-002
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1.19E-001
8.11E-002
9.22E-002
7.35E-002
+I+I+I+I+I-
2.07E-002
2.01E-002
1.36E-002
1.55E-002
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Channel Data Report

801:
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Sample Title:
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5:02:57 AM
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Sample Description:
Spectrum File:
Sample Geometry:
PZ-106-KS DIS
\\OR-ALPHA1\Canherra\ApexAlpha\Root\Data\00000575
1304132A-TH
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04026479A
91132
System Bkgd 56372
<not performed>
Sample Size:
Sample Date/Time:

7:22:02 AM
4/15/2013
4:29:59 PM
5/9/2013
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.238 mL
0.1785 +/- 0.0151
0.1825 +/- 0.0032 on 12/16/2012
0.9784 +/- 0.0844
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.749
5.385
4.865
4.655
3.950
AREA
REPORT
Pk Area
Error %
Net
Pk Area
1.15
2.49
162.49
10.83
1. 00
5:49:18 PM
249.59
138.29
15.40
60.10
277.19
Ambient
Backgnd
0.85
0.51
0.51
0.17
0.00
FWHM
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O.OOE+OOO
O.OOE+OOO
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O.OOE+OOO
3.0
3.0
3.6
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3.0

Nuclide
Id
Conf.
Energy
(keV)
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TH-228
TH-229
TH-230
TH-232
0.948
0.999
1.000
0.999
0.988
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
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1.75E-002
3.79E-002
2.42E+000
1. 61E-001
1.48E-002
+I+I+I+I+I-
4.39E-002
5.28E-002
4.01E-001
1.00E-001
4.12E-002
MDA
(pCi/liter
9.13E-002
7.98E-002
7.83E-002
6.20E-002
8.90E-002
+I+I+I+I+I-
1.51E-002
1.32E-002
1.30E-002
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6500
Channel Data Report
5/10/2013
Page
5:03:05 AM
*******************************************************
S P E C T R A L
R E P 0 R T
DATA
*****
*****
*******************************************************
Sample Title:
13
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Channel Data Report

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lll327
Sample Description:
Spectrum File:
Sample Geometry:
FB AT PZ-100-KS TOT
1304132A-TH
14
Shelf 2
Th iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_034
04026479B
91136
System Bkgd 56373
<not performed>
Sample Size:
Sample Date/Time:

4/16/2013
7:22:02 AM
5/9/2013
4:30:00 PM
170. 0 minutes
170. o minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.236 mL
0.2051 +/0.0164
0.1856 +/- 0.0032 on 12/16/2012
1.1055 +/- 0.0904
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.810
5.334
4.884
4.634
3.947
Net
Pk Area
3.83
2.83
184.66
13.66
-0.17
AREA
5:49:43 PM
REPORT
Ambient
Backgnd
Pk Area
Error %
102.72
120.53
14.44
53.80
1169.4
0.17
0.17
0.34
0.34
0.17
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
3.0
3.0
6.6
4.5
0.0
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Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.992
0.977
0.999
0.992
0.987
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
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5.08E-002
3.74E-002
2.40E+000
1.77E-001
-2.20E-003
+I+I+I+I+I-
5.28E-002
4.55E-002
3.75E-001
9.90E-002
2.57E-002
A&
{(~ (]J
MDA
(pCi/liter
5.54E-002
5.52E-002
6.21E-002
6.19E-002
5.39E-002
+I+I+I+I+!-
8.68E-003
8.65E-003
9.72E-003
9.69E-003
8.44E-003
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I I Ill I
Channel Data Report
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~332
ex-Alpha
Sample Geometry:
FB AT PZ-100-KS DIS
\\OR-AlPHA1\Canberra\ApexAlpha\Root\Data\00000575
1304132A-TH
15
Shelf 2
Th iso
Detector Name:
Env. Background:
Alpha_035
04026477A
58771
System Bkgd 56374
Sample Description:
Spectrum File:
Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

4/16/2013
7:22:02 AM
5/9/2013
4:29:55 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.238 mL
0.2012 +/- 0.0162
0.1826 +/- 0.0032 on 12/16/2012
1.1022 +/- 0.0906
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5. 791
5. 299
4.907
4.615
3.949
Net
Pk Area
0.98
-0.68
183.00
12.66
0.00
AREA
5:49:42 PM
REPORT
FWHM
(keV)
Pk Area
Ambient
Reagent
Error %
Backgnd
Backgnd
1. 02
0.68
0.00
0.34
0.00
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
294.85
304.44
14.53
55.94
1960.0
2.9
0.0
8.1
2.9
0.0
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.982
0. 949
0. 994
0.983
0.988
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
1. 33E-002
-9.17E-003
2.42E+OOO
1. 67E- 001
O.OOE+OOO
+I+I+I+I+I-
3.92E-002
2.80E-002
3.81E-001
9.71E-002
3.6SE-002
MDA
(pCi/liter
8.53E-002
7.61E-002
7.93E-002
6.31E-002
7.89E-002
+I+I+!+I+I-
1. 34E-002
1.20E-002
1.25E-002
9.93E-003
1. 24E-002
0000057583.CNF
start:
I: 3463 .4(kev)
Stop : 1024:6473.5(kev)
Acq. Start :Thu May 09 16:29:55 2013
60
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Channel Data Report
5/10/2013
Page
5:03:25 AM
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*****
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801:
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1337
ex-Alpha
Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:
Env. Background:
Reagent Blank:
PZ-100-KS TOT
1304132A-TH
16
Shelf 2
Th iso
Alpha_037
04026478A
91133
System Bkgd 56375

<not performed>


4/16/2013
7:22:02 AM
5/9/2013
4:29:57 PM
170. 0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.238 mL
0.1748 +/- 0-0149
0.1783 +/- 0.0033 on 1/26/2013
0.9805 +/- 0.0855
0.175 MeV
Sample Size:
Sample Date/Time:
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.853
5.315
4.861
4-645
3.988
AREA
REPORT
Pk Area
Error %'
Net
Pk Area
4.83
5.49
158.83
25.66
2.00
3:28:25 PM
91.00
88.08
15.56
38.99
169.74
FWHM
(keV)
Backgnd
Reagent
Backgnd
0.17
0.51
0.17
0.34
0.00
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
Ambient
2.9
2.9
5.9
4.4
2.9
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
1.000
0-963
0.999
0.996
1. 000
5850.00*
5400.00*
4872- 00*
4672.00*
3997.00*
Activity
(pCi/liter )
7.52E-002
8.52E-002
2.42E+OOO
3.90E-001
3.03E-002
+I+I+I+I+I-
6.96E-002
7.64E-002
4.04E-001
1. 65E-001
5.17E-002
MDA
(pCi/liter
6.50E-002
8.15E-002
6.36E-002
7.26E-002
9.09E-002
+I+I+I+I+I-
1.09E-002
1. 36E-002
1.06E-002
1. 21E-002
1. 52E-002
A-G-
S/ro/t!:J
B3.38
0000057580.CNF
1-Live Time :10200.000 sec
Rea1 Time :10200.300 sec
start:
1:3463. S(kev)
Stop : 1024:6468.5(kev)
Acq. Start :Thu May 09 16:29:57 2013
60
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Channel Data Report
5/10/2013
Page
5:03:34 AM
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-~3-41
Channel Data Report

SOl:
5/l0/20l3
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Sample Description:
Spectrum File:
Sample Geometry:
PZ-100-KS DIS
1304132A-TH
17
Shelf 2
Th iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_040
060273968
91135
System Bkgd 56376
<not performed>
Sample Size:
Sample Date/Time:
l. OOOE+OOO +/- O.OOOE+OOO liter

4/16/2013
7:22:02 AM
5/9/2013
4:30:07 PM
170.0 minutes
l70.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.238 mL
0.1866 +/- 0.0155
0.1900 +/- 0.0033 on 12/16/2012
0.9823 +!- 0.0832
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.731
5.355
4.882
4.536
3.946
Net
Pk Area
0.49
1.15
170.00
5.83
-0.17
AREA
5:49:33 PM
REPORT
Pk Area
Error %
Anlbient
Backgnd
416.98
249.59
15.08
82.55
1169.4
0.51
0.85
0.00
0.17
0.17
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
3.0
3.0
3.7
3.0
0.0

Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.929
0.990
0.999
0.908
0.987
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
7.15E-003
1.67E-002
2.43E+000
8.29E-002
-2.41E-003
+I+I+I+I+I-
2.98E-002
4.18E-002
3.94E-001
6.98E-002
2.82E-002
/\(;,
5/ro/!'J
MDA
(pCi/liter
7.66E-002
8.70E-002
8.55E-002
5.94E-002
5.92E-002
+I+I+I+I+I-
l. 24E-002
l.41E-002
1.39E-002
9.65E-003
9.63E-003
0000057584.CNF
Start:
1:3459.0(kev)
stop : 1024:6497.3(kev)
Acq. start :Thu May 09 16:30:07 2013
60
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'
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I>
"'
ROI Type: 1
5000
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6500
Channel Data Report
5/10/2013
Page
5:03:43 AM
*******************************************************
*****
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R E P 0 R T
*****
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Sample Title:
17
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fg346
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801:
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Sample Title:
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5:03:43 AM
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pex-AiphaTM
Sample Geometry:
S-53 TOT
1304132A-TH
18
Shelf 2
Th iso
Detector Name:
Env. Background:
Alpha_041
05026930A
91087
System Bkgd 56377
Sample Description:
Spectrum File:
Reagent Blank:
<not performed>

4/16/2013
7:22:02 AM
4:30:03 PM
5/9/2013
170.0 minutes
Sample Size:
Sample Date/Time:
170.0 minutes
Th229 TH-18A
0.232 mL
0.1400 +/- 0.0133
0.1978 +/- 0.0034 on 12/16/2012
0.7077 +/- 0.0686
0.175 MeV
Tracer Certificate:
Tracer Quantity:
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.865
5.362
4.884
4.622
3.948
Net
Pk Area
56.49
1029.15
124.00
1032.47
1006.43
AREA
5:49:31 PM
REPORT
Pk Area
Ambient
Error %
Backgnd
Reagent
Backgnd
FWHM
(kev)
26.22
6.11
17.67
6.11
6.19
0.51
0.85
0.00
1. 53
3.57
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
3.0
34.3
3.0
74.6
11.5
NOCLIDE ANALYSIS RESULTS
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.999
0.992
0.999
0.987
0.987
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
1.10E+000
1.99E+001
2.36E+000
1.96E+001
1.90E+001
+I+I+I+I+I-
3.54E-001
3.92E+000
4.41E-001
3.85E+000
3.75E+000
AG
5jtoj!J
MDA
(pCi/liter
1.02E-001
1.16E-001
1.14E-001
1.35E-001
1.78E-001
+I+I+I+I+I-
1.91E-002
2.17E-002
2.13E-002
2.52E-002
3.34E-002
0000057585.CNF
Live Time
Real Time
start:
I
stop : 1024
10200.000 sec
10200.300 sec
3452./(kev)
6506.6(kev)
Acq. start rhu May 09 16:30:03 2013
60
55
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6500
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Channel Data Report
5/10/2013
Page
5:03:54 AM
*******************************************************
*****
p E
T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
18
Elapsed Live time:

Elapsed Real Time:
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:mJscrJ
Channel Data Report

369:
5/10/2013
8
Sample Title:
10
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mJS1
Channel Data Report

801:
5/10/2013
2
Sample Title:
Page
5:03:54 AM
0
18
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'fi1352
pex-Aipha
Sample Description:
Spectrum File:
Sample Geometry:
S-53 DIS
1304132A-TH
19
Shelf 2
Th iso
Detector Name:
Env. Background:
Alpha_042
05026930B
84185
System Bkgd 56378
Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

7:22:02 AM
4/16/2013
4:30:05 PM
5/9/2013
170.0 minutes
170.0 minutes
Th229 TH-18A
0.237 mL
0.1887 +/- 0.0156
0.1846 +/- 0.0032 on 12/16/2012
1.0222 +/- 0.0864
0.175 MeV
Tracer Certificate:
Tracer Quantity:
PEAK
Energy
Nuclide
(MeV)
TH-227
TH-228
TH-229
TH-230
TH-232
5.782
5.356
4.887
4.596
3.982
Net
Pk Area
5.83
2.15
170.66
15.66
7.66
AREA
5:49:29 PM
REPORT
Pk Area
Ambient
Error %
Backgnd
0.17
0.85
0.34
0.34
0.34
82.55
161.66
15.02
50.15
72.63
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
4.5
3.0
6.5
4.5
3.0
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.976
0.990
0.999
0.971
0.999
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
8.41E-002
3.09E-002
2.41E+OOO
2.20E-001
1. 08E-001
+I+I+I+I+I-
7.08E-002
5.02E-002
3.90E-001
1.16E-001
8.00E-002
MDA
(pCi/liter
6.02E-002
8.61E-002
6.75E-002
6.73E-002
6.71E-002
+I+I+I+I+I-
9.76E-003
1.39E-002
1.09E-002
1. 09E-002
1.09E-002
i353
0000057586.CNF
start:
13450.2(kev)
stop : 1024 6505.5(kev)
60
55
50
45
40
35
V)
+-'
<=
::::1
8 30
25
20
15
10
5
0
'
3500
4000
4500
5000
Energy(kev)
jl,
5500
6000
~~I
tll
.\J'.I.."ii,
ROI Type: 1
ROI Type: 3
6500
Channel Data Report
5/10/2013
Page
5:04:03 AM
*******************************************************
*****
p E C T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
19
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Channel Data Report

801:
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5:04:03 AM
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19
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t\1357
Page 1 of 2
5/9/2013
5:53:04 AM
ha
QA SUMMARY REPORT
Date
Time
: 5/9/2013
: 5:53:04 AM
CHAMBER
Alpha 001
Alpha 002
Alpha 003
Alpha 004
Alpha 005
Alpha 006
Alpha 007
Alpha 008
Alpha 009
Alpha 010
Alpha 011
Alpha 012
Alpha 013
Alpha 014
Alpha 015
Alpha 016
Alpha 017
Alpha 018
Alpha 019
Alpha 020
Alpha 021
Alpha 022
Alpha 023
Alpha 024
Alpha 025
Alpha 026
Alpha 027
Alpha 028
Alpha 029
Alpha 030
Alpha 031
Alpha 032
Alpha 033
Alpha 034
Alpha 035
Alpha 036
Alpha 037
Alpha 038
Alpha 039
Alpha 040
Alpha 041
Alpha 042
DEVICE
21f
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
AIM730
AIM730
AlM730
AIM730
AlM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
Alpha Analyst! OODC
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha Analyst! OODC
Alpha Analyst! OODC
Alpha Analyst! OODC
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha AnalystlOODC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
FLAG
Not Done
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Not Done
Not Done
Passed
Passed
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Passed
Not Done
Not Done
Not Done
Passed
Not Done
Passed
Passed
Not Done
Passed
Not Done
Passed
Not Done
Not Done
Not Done
Passed
Passed
Passed
Not Done
Passed
Not Done
Not Done
Passed
Passed
Passed
DATE
5/9/2013 5:34:02 AM
5/9/2013 5:34:02 AM
5/9/2013 5:34:03 AM
5/9/2013 5:34:04 AM
5/9/2013 5:34:05 AM
5/9/2013 5:34:06 AM
5/9/2013 5:34:07 AM
5/9/2013 5:34:08 AM
5/9/2013 5:34:08 AM
5/9/2013 5:34:09 AM
5/9/2013 5:34:10 AM
5/9/2013 5:34:11 AM
5/9/2013 5:34:12 AM
5/9/2013 5:34:13 AM
5/9/2013 5:34:15 AM
5/9/2013 5:34:16 AM
5/9/2013 5:34:18 AM
5/9/2013 5:34:20 AM
5/9/2013 5:34:21 AM
Page 2 of 2
Review of QA Results - Pulser Cheek

5/9/2013
CHAMBER
Aloha 043
Alnha 044
Aloha 045
AlOha 046
Aloha 047
AlOha 048
DEVICE
AlOha Analvstl OODC
Aloha Analyst! OODC
AlOha AnalYst! OODC
Aloha Analyst! OODC
Aloha AnalystlOODC
Alnha Analyst! OODC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
FLAG
Not Done
Passed
Not Done
Passed
Passed
Passed
55304 AM
DATE
5/9/2013 5:34:23 AM
5/9/2013 5:34:25 AM
5/9/2013 5:34:27 AM
5/9/2013 5:34:29 AM
APPROVED BY:
APPROVAL DATE:
(Ill!)
8359
6/12/12
Page
12:16:29 PM
*************************************************************************
*****
L I B R A R Y
L I S T I N G
R E P 0 R T
*****
*************************************************************************
Thorium
Nuclide
Name
Half-Life
(Seconds)
Energy
(keV )
TH-227
TH-228
TH-229
TH-230
TH-232
6.873E+008
6.034E+007
2.487E+011
2.379E+012
4.434E+017
5850.000*
5400.000*
4872.000*
4672.000*
3997.000*
Th-227,-228,-229,-230,-232
Energy
Uncert. (kev
0.000
0.000
0.000
0.000
0.000
= key line
TOTALS:
Nuclides
Energy Lines
Yield
(%)
97.5000
99.9400
99.5200
99.8200
100.0000
Yield
Uncert. (Abs. +-)
0.0000
0.0000
0.0000
0.0000
0.0000
SECTION X
ANALYTICAL DATA (RADIUM-226)
t!l361
Eberline Services
Analysis Sheet
Printed: 5/15/2013 10:47 AM

Page 1 of 3
13-04132
Ra226
Run 1
Internal
Fraction
Sample
Desc
Client
Login
ID
CPM
Ra226
01
LCS
.LCS
04/18/13 00:00
1.0000E+OO
02
MBL
BLANK
04/18/13 00:00
1.5000E+OO
4/18/2013
03
DUP
FB atPZc100-KS TOT
39
04/16/13 08:40
1.5000E+OO
5/9/2013
04
TRG
D-14TOT
38
04/12/1311:05
1.5000E+OO
05
TRG
.. D-14 DIS
38
04/12/13 11:05
1.5000E+OO
West Lake OU-1
06
TRG
PZ-112-AS TOT
45
04/12/1311:18
1.5000E+OO
Report Level
07
TRG
PZ-112-AS DIS
45
04/12/1311:18
1.5000E+OO
Activity Units
pCi
08
TRG
PZ-202-SS TOT
46
04/12/13 12:32
1.5000E+OO
Aliquot Units
09
TRG
PZ-202-SS DIS
46
04/12/13 12:32
1.5000E+OO
WA
10
TRG
DUP07 TOT
40
04/12/13 00:00
1.5000E+OO
EPA 903.0 Modified
11
TRG
DUP07 DIS
40
04/12/13 00:00
1.5000E+OO
Alpha Spectroscopy
12
TRG
PZ-106-KS TOT
36
04/15/13 15:59
1.5000E+OO
Radiometric Tracer
Ba-133
13
TRG
PZ-106-KS DIS
36
04/15/13 15:59
1.5000E+OO
Radiometric Sol#
Ba-6a
14
DO
FB at PZ-100-KS TOT
39
04/16/13 08:40
1.5000E+OO
Tracer Act (dpm/g)
1007.586
15
TRG
FB at PZ-100-KS DIS
39
04/16/13 08:40
1.5000E+OO
Carrier
16
TRG
PZ-100-KS TOT
37
04/16/13 08:50
1.5000E+OO
17
TRG
PZ-100-KS DIS
37
04/16/13 08:50
1.5000E+OO
TRG
S-53 TOT
41
04/16/13 09:00
1.0000E+OO
S-53 DIS
41
04/16/13 09:00
1.0000E+OO
Work Order
Analysis Code
Run
Date Received
Lab Deadline
Client
Project
Matrix
Method
Instrument Type
18
19
TRG
Sample
Date
Sample
Aliquot
'
!
'
t~"ll
~~
U''~
,"" -SAF1 js u~ctJOr .Gro_ss hlptJa and .all-other
radionuclides~ .$AF.2.is used tor. Gross;B.eta only;.
,-"".Actual mass. exceeded:t~e,calibration curve range. Results should be qualified as appropriate.
Eberline Services
Analysis Sheet
Printed: 5/15/201310:47 AM
13-04132
Page 2 of 3
Ra226
Run 1
Internal
Fraction
Sample
Desc
01
LCS
0.9178
924.8
376.7
90.43
0.0226
0.0291
0.0065
02
MBL
0.9119
918.8
435.6
105.25
0.0228
0.0293
03
DUP
0.9044
911.3
367.4
89.51
0.0221
04
TRG
0.8976
904.4
342.7
84.12
05
TRG
0.8990
905.8
388.6
06
TRG
0.9014
908.2
07
TRG
0.8989
08
TRG
09
Tracer
Aliquot(g)
Tracer Total
ACT(dpm)
Radiometric
Tracer (pCi)

%Rec
Added(ml)
Grav Filter
Net(g)
Grav
%Rec
Mean
%Rec
SAF
1'
2'
90.43
2.34
1.00
0.0065
105.25
2.34
1.00
0.0280
0.0059
89.51
2.12
1.00
0.0224
0.0289
0.0065
84.12
2.34
1.00
95.24
0.0224
0.0300
0.0076
95.24
2.66
1.oo
398.8
97.48
0.0226
0.0389
0.0163
97.48
8.24
1.00
905.7
413.1
101.25
0.0221
0.0326
0.0105
101.25
3.44
1.00
0.9009
907.7
354.5
86.70
0.0221
0.0289
0.0068
86.70
2.44
1.00
TRG
0.9009
907.7
371.2
90.78
0.0223
0.0297
0.0074
90.78
2.61
1.00
10
TRG
0.9017
908.5
297.1
72.60
0.0223
0.0309
0.0086
72.60
2.91
1.00
11
TRG
0.8997
906.5
375.3
91.91
0.0222
0.0330
0.0108
91.91
3.54
1.00
12
TRG
0.9013
908.1
389.2
95.14
0.0223
0.0305
0.0082
95.14
2.82
1.00
13
TRG
0.8996
906.4
390.1
95.54
0.0223
0.0308
0.0085
95.54
2.89
1.00
14
DO
0.9002
907.0
347.7
85.10
0.0227
0.0288
0.0061
85.10
2.20
1.00
15
TRG
0.9008
907.6
393.1
96.15
0.0220
0.0286
0.0066
96.15
2.37
1.00
16
TRG
0.9023
909.1
338.0
82.53
0.0226
0.0296
0.0070
82.53
2.50
1.00
17
TRG
0.8744
881.0
401.5
101.17
0.0226
0.0298
0.0072
101.17
2.55
1.00
18
TRG
0.9038
910.7
55.5
13.52
0.0230
0.0231
0.0001
13.52 -3.53
1.00
19
TRG
0.9067
913.6
402.8
97.88
0.0221
0.0282
0.0061
97.88
1.00
~.~
Grav Filter
Final (g)
SAF
......
5~-
Grav Filter
Tare (g)
.*
SAF1 is u.sectfor,.Gross AlpJta.andall other radionuclides. SAF2 is usedJor.-Gross
2.20
._l_
Beta:.only-~\:;,. :.=.t~Actual mass-exceeded-the calibration- ourve-range.
Restll_ts should be qualified as: appropriate_.,
':
~;:i-:c,} i(i..
Eberline Services
Analysis Sheet
13-04132
Ra226
Printed: 5/15/201310:47 AM
Page 3 of 3
Run 1
Internal
Fraction
Sample
Desc
01
Rough Prep
Date
Rough Prep
Prep
Prep
SepW
By
Date
By
Date/Time
Sep to
By
LCS
05/03/13 12:34
JBARNARD
05/14/13 12:52
LWALKER
02
MBL
05/03/13 12:34
JBARNARD
05/14/13 12:52
LWALKER
03
DUP
05/03/13 12:34
JBARNARD
05/14/13 12:52
LWALKER
04
TRG
05/03/13 12:34
JBARNARD
05/14/13 12:52
LWALKER
05
TRG
05/03/13 12:34
JBARNARD
05/14/13 12:52
LWALKER
06
TRG
05/03/13 12:34
JBARNARD
05/14/13 12:52
LWALKER
07
TRG
05/03/13 12:34
JBARNARD
05/14/13 12:52
LWALKER
08
TRG
05/03/13 12:34
JBARNARD
05/14/13 12:52
LWALKER
09
TRG
05/03/13 12:34
JBARNARD
05/14/13 12:52
LWALKER
10
TRG
05/03/13 12:34
JBARNARD
05/14/13 12:52
LWALKER
11
TRG
05/03/13 12:34
JBARNARD
05/14/13 12:52
LWALKER
12
TRG
05/03/13 12:34
JBARNARD
05/14/13 12:52
LWALKER
13
TRG
05/03/13 12:34
JBARNARD
05/14/13 12:52
LWALKER
14
DO
05/03/13 12:34
JBARNARD
05/14/13 12:52
LWALKER
15
TRG
05/03/13 12:34
JBARNARD
05/14/13 12:52
LWALKER
16
TRG
05/03/13 12:34
JBARNARD
05/14/13 12:52
LWALKER
17
TRG
05/03/13 12:34
JBARNARD
05/14/13 12:52
LWALKER
18
TRG
05/03/13 12:34
JBARNARD
05/14/13 12:52
LWALKER
19
TRG
05/03/13 12:34
JBARNARD
05/14/1312:52
LWALKER
Sep t1
Sep t1
By
Date/Time
--
~~~
t1ri
.t;.'j,
* SAF1d~--Y~~"-for
Gros_~.>8.1p!la and all other radionuclides.
SAF2 is use_d)QcG,ross Bet;ason_ly. . **Actual mass exceeded the ealibratio_n,euiV~ range ..,R.e.sults should be qualified. as appropriate.
h_~{}->.r--_
1.;v
Eberline Services
Work Order: 13-04132-Ra226-1
Lob
Fraction
Nuclide
01
RA-226
Sample
Client
Activity
Desc
Identification
Units
LCS
LCS
-~------
02
,
0:
~
CD
N
N
-1:0
l)
-~
~
cu
~
~
0::
<>:
---
03
DUP
pCi/1
FB at PZ-100-KS TOT
_________________ ____
,.
04
RA-226
05
RA-226
06
RA-226
0~14
TRG
------
----~-
'
.1:"'s
ill
10
11
--------
TOT
pCi/1
c.
c.
:::
rtJ
...."'
~
TRG
pCI/1
0-14 DIS
TRG
RA-226
PZ-112-AS TOT
14
-~----
TRG
PZ-112-AS DIS
7.47E-02
1.54E-01
1.03E+01'
16
-~----
18
------
19
I'
4.56E-02
7.37E-02
1.27E-01
-- . ---- -- ------- - 1.97E+OO
4.55E-01
1.66E-01
--
LCS
RPD
Flag
LCS
Flag
%R
~~031
--
MDA
Flag
3.00E-01
9.47E-01
OK
-- ----
INV
OK
OK
OK
2.19E-01
3.83E-01
--
7.42E-01
pCI/1
3.09E-01
8.53E-01
pCi/1
RA-226
RA-226
--
3.04E-01
--111-
PZ-202-SS DIS
TRG
-------------RA-226
TRG
--~----
pCi/1
DUP07 TOT
OUP07 DIS
TRG
TRG
RA-226
---------~--~
---------
pCi/1
1.57E-01
1.54E-01
RA-226
RA-226
----
RA-226
,-
- - - - t---
RA-226
pCi/1
PZ~100~KS
TRG
DIS
TRG
pCI/1
S-53 TOT
!----------~-----
RA-226
TRG
-
2.04E-01
1.60E-01
OK
----
OK
OK
OK
-- --------
OK
1.48E-01
6.89E-02
-----
OK
1.75E-01
4.69E-02
1.64E-01
--
OK
9.84E-02
1---------- -2.60E-01
.....
1.36E-01
OK
1.17E-01
S-53 DIS
pCi/1
1.42E-Q1
1.45E-01
3.12E-01
- - - 1--
OK
6.1BE-01
OK
1.36E-01
OK
-- -pCI/1
- - --
1.65E-01
----
-~----l--------
-~-
--
----------- t-~-------- -------- , - - - - - - - - - - --------- ------
--~----------
---------
2.07E-Q1
-4.01 E-03
~-
PZ-100-KS TOT
TRG
6.01 E-01
1.92E-01
3.00E-03
pCi/1
--
OK
~---
......
---- 1-----
FB at PZ-100-KS DIS
TRG
OK
------
- --t-
3.23E-01
pCi/1
-----
2.08E-01
- ----
3.77E-01
pCi/1
RA-226
=t--~=-
- - - - - - ---------- - -
FB at PZ-100-KS TOT
DO
--
S.OBE-01
1.69E-01
---~------ ~--~
i
,---
------- t----~---
PZ-106-KS DIS
TRG
----~----- ---~------~~-----------~--
-~---
2.31E+OO
pCI/1
- - - - - - - -t----PZ-106-KS TOT
2.03E-01
4.11 E+OO
----- ----- ---- - - - - - ---- -----
RA-226
3.81 E-01
pCI/1
- - - - - - - - - - - -- ---
OK
1.66E-01
--
8.44E-01
3.28E-01
Blank
Flag
OK
OK
-------- - -
- - - - - - - - - - - - - ---
15
17
;;,
c
w
2.73E-02
t------ ------------ - - -
PZ-202-SS TOT
TRG
RA-226
-----
---~~-
"c
- - -
2.33E-01
7.92E-01
pCi/1
----~---------
13
----
::;;
"'c
1.25E+OO
LCS
Known
-------------
-----------~
1.04E+01
---- -..... _ -------
------ 1----
12
t-.;
.E
MDA
------ !---
07
09
pCi/1
----
-----
08
-~
-- - - -
~-
'!:
t.n
BLANK
- - - --
1..111
RA-226
---
'
~-~~
MBL
------
Error Estimate
-----~
~-~=-
RA-226
Results
pCi/1
------~----
T"'
------ -------
Printed: 5/16/2013 10:19 AM

Page 1 of 3
OK
Eberline Services
02
or-
.g
8
c.o
.~
~
~
Sample
Desc
Sample
Date
. _ RA:=26-
_1-_cs
04/18/13 oo:oo
j_ 1.0~_+0~
04/18/13 00:00
1.50E+OO
N
N
ca
0::
RA-226
~:---1-~~~:~~~--
1----
-~-~
1-
Sample
Aliquot
----~--
TRG
::::::::::::--
----- ----~
1
1
Radiometric
% Rec
Mean
%Rec
9Q.43
100.00
0.00
105.25
----.
------------
TRG
04/12/1311:05
1.50E+00----~95.24
TRG
04/12/1311:18
1.50E+OO
07
RA-226
TRG
04/12/13 11:18
1.50E+OO
---4
~--
1.50E+OO
~~"'"
97.48
5/14/201312:52
101.25
.,..... ----
O.ooj
86.70
---5/14/2013 12:52
ill
.;
.5
~---:~:---~~-:~:-:-:
1-:-:; ::::::::
04/16/13 08:40
c.
c.
"
c:
.."'
Cl
'C)
=~
"'c
'S,
c
w
~~
ll
Ill
95.1t-
1.50E+OO
95.54
0.00
95.14
1.50E+OO
85.10
04/16/13 08:40
1.505+00
16 I .. RA-22-"-~l---T_R_G-!---~~04/16/13 08:50
TRG
RA-226
17
1.50E+OO
04/16/13 08:50
0.00
95.54
19
04/16/13 09:00
---
0.00
85.10
5/14/201312:52
0.00
96.15
5/14/2013 12:52
0.00
82.53
5/141201312:52
--82.53
---101.17
5/14/2013 12:52
1.~;3--- ~-----~00 --~5~
5/14/2013 12:52
TRG
5/14/201312:52
--
1.50E+OOI
100.001
1---+--------I---J--~"~~t--~-t-~
TRG
04/16/13 09:00
RA-226
18
RA-226
5/14/2013 12:52
-------
-~~~--~~-~~~- - - -
(/)
"'E
~--------~------- ---~~-
1.~oeool
-----
'i
------~
1.00E+OO
----
0.00
---~-----
97.88
----
----------j
---J
-5/14/201312:52
5/14/201312:52
1:
.. -
5/14/201312:52
-5/14/2013 12:52
!.s
.,JI
5/14/2013 12:52
--
5/14/2013 12:52
------t-~--t-~~~~-+~~-- -~--J
0.00
--- .
04/12/13 12:32
0.00
-----TRG
Sep t1
DatefTime
--~'~----T~----~-------]
---~-L-~-
-~~---
RA-226
SeptO
Date/Time
::::~:::, --~~j -~~-:If ---~:~~J -==r : : : : : ::::~~~-~~ --~~==~:
RA-226
08
SAF
0.00
RA-226
...
Grav
%Rec
90.4~
......... _
06
1-----
~t;
Printed: 5/16/2013 10:19 AM

Page 2 of 3
Work Order: 13-04132-Ra226-1
Nuclide
Lob
Fraction
01
0.00
--
-------97.88
5/14/201312:52
Eberline Services
~
~
Lob
__01 1
1---
02
~
-~
"
(0
N
N
n:s
0::
!
~
.;
.5
c.
c.
"'"
"""
E
"'"'
~
:;:
"'
0>
~
""
~
a,
~
w
t,,)l
!:V'l
-4J
j.
~-~R,;
08
RA-226
tTRG
::
15
f-16
;;;.:;--2;
Alpha_010
170.0+.30 E+OO
___ T_____
-----
A_Spec
Alpha_011
17012.15 E+OO
05/15/13 16:51
A_Spec
Alpha_013
170 7.50 E+01
-~~;~~~;~---;--~:51-
A_ Spec
Alpha_01~ ---
1701;.96
TRG
--- ...
A_Spec
05/~;/13 16:52
_-
-;;:_~pe~---
05/15/1316:52
---------.----. - - - -..
A_Spec
--
-------- - - - - - . .
05/15/1316:52
. .... ____ ----
TRG _-~~1-5~3
16:52
Alpha_033
Alpha__
034--~ ::27 E+01 _2.0~~~
Alpha_035
-----
A_Spec
Alpha_036
A_Spec
~~::-037
------
---
170 3.13 E+01

---
170 '1.48 E+01
------
4.00 E-03
----- - - - - -
----
7.00 E-03
--------
1~-0-, 1.03 E+o~_:oo E-0~--13.00 E-03
RA-226
TRG
05/15/13 16:52
A_ Spec
Alpha_039
170 11.41 E+01
15.00 E-03
TRG
05/15/1316:52
A_Spec
Alpha_042
17011.70 E-01
1.00 E-03
-=~*= :~::::~ I~ - 1- ~:=-~~::r-:: :~:: ;~:

RA-226
--E
TRG ____
TRG
----;,;
18.2
17015.85 E+01
RA-226
18.7
170 2.38 E+01
Alpha_038
. _
118
19
--
E+~~--- 1.40 E-02
A_Spec
----1
6.00 E-03
05/15/1316:52
~-=
19.7
19.7
TRG
19.4
-----
RA-226
RA-226
Eff
CPM
_______ .______!_____
05/15/13 16:52
--
Bkg
Counts
05/15/1316:51
...... """
l17t--~;;.--}~RG ~-~-_"_5/~5~~316:52
1----.
A_Spec
--------------------- !----
--RA~226
RA-226
Count
Time
Carrier
I A_sp~c .. Alpha~~~~--17~~2f-~4 e+o2 ~.oo e-o3
---
05/15/1316:51
TRG -
I 07
--
o5/15/~316:;-
Detect
------------------------ - --- -r---
RA-226
RA-226
Halflife
(days)
-----
TRG
12
__
MBL
--t---
RA-226
11
.,=
lil;!l
RA-226
06
1Q-
Date/Time
- - - " ----------. -----
1---
,Qs_
09
"!:
Counting
Desc
;,..._2~~--r-Lc~-
--------------
Sample
03
04
Printed: 5/16/2013 10:19 AM

Page 3 of 3
Work Order: 13-04132-Ra226-1
Nuclide
Fraction
-r-
"-''" ....~
--
A_Spec_
-;,.!'"
~~ha_045 _-1-;~
__
17.2
r;:.
19.7
,;;-0--J-1.-0-0-E--0-3--.J-
1.03 E+01
4.00
E~;--
18.5
19
17.9 --j
05/15/13-16:5=-1
A_Spe~ 1Aipha_~46 ~-7011.32 e+oo
4.oo e-o3 ---1
17.9
05/15/1316:52
A_Spec
1.00 E-03
18.2
-- ---------
----- -
--
Alpha_047
---
170 2.58 E+01
+-
-f
l
I
Count Room Report

13-04132-Ra226-1 (pCi/1) in WA
Tracer ID: Ba-6a
Printed: 5115/201310:48 AM
Page 1 of1
)~
~~
Internal
Fraction
Sample
Desc
Client
ID
Sample
Date
Sample
Aliquot
01
LCS
LCS
04/18/13 00:00
1.0000
0.9178
924.7624
376.7000
02
MBL
BLANK
04/18/13 00:00
1.5000
0.9119
918.8177
DUP
FB at PZ-100-KS TOT
04/16/13 08:40
1.5000
0.9044
TRG
D-14 TOT
04/12/13 11:05
1.5000
05
TRG
D-14 DIS
04/12/1311:05
06
TRG
PZ-112-AS TOT
07
TRG
08
Tracer
Radiometric
ACT(dpm)
Tracer (pCi)
SAF
1'
SAF
90.43
2.34
1.00
435.6000
105.25
2.34
1.00
911.2608
367.4000
89.51
2.12
1.00
0.8976
904.4092
342.7000
84.12
2.34
1.00
1.5000
0.8990
905.8198
388.6000
95.24
2.66
1.00
04/12/1311:18
1.5000
0.9014
908.2380
398.8000
97.48
)n;(
1.00
PZ-112-AS DIS
04/12/13 11:18
1.5000
0.8989
905.7191
413.1000
101.25
3.44
1.00
TRG
PZ-202-SS TOT
04/12/13 12:32
1.5000
0.9009
907.7342
354.5000
86.70
2.44
1.00
09
TRG
PZ-202-SS DIS
04/12/13 12:32
1.5000
0.9009
907.7342
371.2000
90.78
2.61
1.00
10
TRG
DUP07TOT
04/12/13 00:00
1.5000
0.9017
908.5403
297.1000
72.60
2.91
1.00
03
04
--
Tracer
'
Aliquot(g)
Radiometric
%Rec
2'
11
TRG
DUP07 DIS
04/12/13 00:00
1.5000
0.8997
906.5251
375.3000
91.91
3.54
1.00
12
TRG
PZ-1 06-KS TOT
04/15/13 15:59
1.5000
0.9013
908.1373
389.2000
95.14
2.82
1.00
13
TRG
PZ-1 06-KS DIS
04/15/13 15:59
1.5000
0.8996
906.4244
390.1000
95.54
2.89
1.00
14
DO
FB at PZ-100-KS TOT
04/16/13 08:40
1.5000
0.9002
907.0289
347.7000
85.10
2.20
1.00
15
TRG
FB at PZ-100-KS DIS
04/16/13 08:40
1.5000
0.9008
907.6335
393.1000
96.15
2.37
1.00
16
TRG
PZ-1 00-KS TOT
04/16/13 08:50
1.5000
0.9023
909.1448
338.0000
82.53
2.50
1.00
17
TRG
PZ-100-KS DIS
04/16/13 08:50
1.5000
0.8744
881.0332
401.5000
101.17
2-15
1.00
18
TRG
S-53 TOT
04/16/13 09:00
1.0000
0.9038
910.6562
55.4800
13.52
~'"
1.00
TRG
S-53 DIS
04/~6/13 o9:oo
1.0000
0.9067
913.5782
402.8000
97.88
2.20
1.00
19
'
..
1
-
'
...
--
(.;~
Oil
IJ)
-_._,
\;:r-::c~
. -;-.:.<)
c;r-'-::,
~"~-
..,":-";,:
' ;"i
_,::,:\"~-"':-.
._,,f~~
Eberline Services
Internal Work Order
Run
Analysis Code
Date
Technician
13-04132
Ra226
5/3/2013 12:33
JBARNARD
LCS & Matrix Spikes

Isotope
Solution
Date
Sol#
Ra-226
Page 1 of 1
Printed: 5/31201312:34 PM
5/3/2013
Ra-5b
Approx
Addition
0.500
LCS
MS
LCSD
MSD
Volume
Used(g)
Volume
Used(g)
Volume
Used(g)
Volume
Used(g)
0.5176
Techni ian Initials
LCS
Known
pCi
10.28
~---
MS
Error
Estimate
0.473
Added
pCi
0.00
- ...
LCSD
I Estimate
Error
1
0.000
Tracers
Activity
dpmlg
Volume
Used (g)
Approx
Addition
Sol#
01
Ba-133 i
Ba-6a
1007.586
5/3/2013
0.9178
1.0100
02
Ba-133
Ba-6a
1007.586
5/3/2013
0.9119
1.0100
03
Ba-133
Ba-6a
1007.586
5/3/2013
0.9044
1.0100
04
Ba-133
Ba-6a
1007.586
5/3/2013
0.8976
1.0100
OS
Ba-133
Ba-6a
1007.586
5/3/2013
0.8990
1.0100
06
Ba-133
Ba-6a
1007.586
5/3/2013
0.9014
1.0100
07
Ba-133
Ba-6a
1007.586
5/3/2013
0.8989
1.0100
08
Ba-133
Ba-6a
1007.586
5/3/2013
0.9009
1.0100
09
Ba-133
Ba-6a
1007.586
5/3/2013
0.9009
1.0100
10
Ba-133
Ba-6a
1007.586
5/3/2013
.0.9017
1.0100
11
Ba-133
Ba-6a
1007.586
5/3/2013
0.8997
1.0100
12
Ba-133
Ba-6a
1007.586
5/3/2013
0.9013
1.0100
13
Ba-133
Ba-6a
1007.586
5/3/2013
0.8996
1.0100
14
Ba-133
Ba-6a
1007.586
5/3/2013
0.9002
1.0100
15
Ba-133
Ba-6a
1007.586
5/3/2013
0.9008
1.0100
16
Ba-133
Ba-6a
1007.586
5/3/2013
0:9023
1.0100
17
Ba-133
Ba-6a
1007.586
5/3/2013
0.8744
1.0100
18
Ba-133
Ba-6a
1007.586
5/3/2013
0.9038
1.0100
Ba-6a
1007586
5/3/2013
0.9067
1.0100
Tracer
Iii!
m
I.!!
Version 2.0 08/99
0.00
Added
pCi
0.000
LCS
o.5i76 '3
0.5121 <;I
Matrix Spike
-0
I-ll
MSD
Error
Estimate

Solution
Date
Isotope
19
Known
pCi
.- L
fraction
Witness Initials
0.00
Effor
Estimate
0.000
Eberline Analytical
Work Ord
13-04132
Lab
Fraction
Client ID
01
02
Analysis Code
Rpt Units
Lab Deadline
Technician
Ra226
liters
5/9/2013
JBARNARD
Sample
Muffle Data
03
04
05
06
07
D-14 DIS
PZ-112-AS TOT
PZ-112-AS DIS
TRG
TRG
TRG
08
09
PZ-202-SS TOT
PZ-202-SS DIS
TRG
TRG
10
11
12
13
14
DUP07TOT
DUP07 DIS
PZ-1 06-KS TOT
PZ-106-KS DIS
FB at PZ-100-KS TOT
TRG
TRG
TRG
TRG
DO
FB at PZ-100-KS DIS
PZ-100-KS TOT
PZ-1 00-KS DIS
TRG
TRG
TRG
17
18
S-53 TOT
19
S-53 DIS
No of Oils
Oil Factor
..
DUP
TRG
Aliquot Data
... .
MBL
TRG
TRG
Dilution Data
Ratio
PoSt/Pre
Type
LCS
LCS
BLANK
FB at PZ-100-KS TOT
D-14 TOT
15
16
Ratio
.
..
..
'
...
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
.
.
:
'
. '. >
..:
..
..
.
.
.
. .....
..
....
...
. .
.
.::
...
..
'.
Comments
!.<~
Technician:
Aliquot
MS Aliquot Data
I, -_:~Net Equiv
H-3 Solids Only
. .. <
Water Added
(ml)
-:_ :Net Equiv
Aliquot
H3 Dist
Aliq
1.0000E+OO I . .1:0000E+OO
1.5000E+OO
1.5000E+OO
1.soooE+oo
1.5000E+OO
Ia
Printed: 5/3/2013 12:35 PM

Page 1 of 1
Aliquot Worksheet
.=:s.J Date:~
--
..
1:5000E+OO
1.5000E+Oo
1.5000E+OO
1.soooE+oo
1.5000E+OO
1.5000E+OO
1.5000E+OO I : .HOOOE+OO
1.soooE+oo
i'.J>OOOE+OO
1.5000E+OO 1.5000E+OO
1.5000E+OO
1.5000E+OO
1.soooE+oo
1.soooE+oo
1.5000E+OO
. .1.5000E+OO
1.soooE+oo
1.5000E+OO
1.5000E+OO
1.0000E+OO
1.0000E+OO
1:5000E+OO
1.5000E+OO
1.5000E+OO
J.OOOOE+OO
1.0000E+OO
~
.
..
.
. ..
-
-'
'
Eberline Services - Oak Ridge

Version 1.0 9/1999
Printed: 5/14/2013 4:53PM

Page 1 of 1
Gravimetric Worksheet
Analysis
Work Order
Gravimetric
Carrier
Code
Carrier Cone
Technician
(mg/ml)
Ra226
TRetec Engineering Management Support, Inc.
Fraction
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
Client 10
LCS
BLANK
DUP
D-14 TOT
D-14 DIS
PZ-112-AS TOT
PZ-112-AS DIS
PZ-202-SS TOT
PZ-202-SS DIS
DUP07 TOT
DUP07 DIS
PZ-1 06-KS TOT
PZ-106-KS DIS
PZ-100-KS TOT
PZ-100-KS DIS
S-53 TOT
S-53 DIS
Sample
LWALKER
Filter Data
Carrier Data
Carrier Added
Filter Tare
(ml)
(g)
Type
LCS
MBL
DUP
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
DO
TRG
TRG
TRG
TRG
TRG
Gravimetric
Filter Final
(g)
0.o226
0.0228
0.0221
0.0224
0.0224
0.0226
0.0221
0.0221
0.0223
0.0223
0.0222
0.0223
0.0223
0.0227
0.0220
0.0226 '
0.0226
0.0230
0.0221
0.0291
0.0293
0.0280
0.0289
0.0300
0.0389
0.0326
0.0289
0.0297
0.0309
0.0330
0.0305
0.0308
0.0288
0.0286
0.0296
0.0298
0.0231
0.0282
Filter Net
(g)
>
.-
L__
!:ill
!..!
-.JI
....
Technician:
,d uJoilv
Date:
014, /3
0.0065
0.0065
0.0059
0.0065
0.00(6
0.0163
0.0105
0.0068
0.0074
0.0086
0.0108
0.0082
0.0085
0.0061
0.0066
0.0070
0.0072
0.0001
. 0.0061
..
Recovery
.
....
..
....
- .
_.. - ..
-
pex-AiphaTM
Sample Description:
Spectrum File:
Sample Geometry:
SPIKE
1304132A-RA
01
Shelf 2
Ra
Detector Name:
Alpha_004
Env. Background:
Reagent Blank:
System Bkgd 56971
<not performed>

Generic Div. Factor:
2.340E+OOO
5/15/2013 12:52:18 PM
5/15/2013
4:51:46 PM
170.0 minutes
170.0 minutes
Sample Size:
Generic Mult. Factor:
Sample Date/Time:
0.9043 +/0.1940 +/0.1755 +/-

0.0000
0.0036 on 12/15/2012 11:26:46 AM
0.0032
Control Certificate Name: Ra226_Ra-5b

RA-226
0.431755 +/Peak Match Tolerance:
0.350 MeV
PEAK
Nuclide
Energy
(MeV)
RA-224
RA-226
5.532
4. 693
Net
Pk Area
459.45
293.81
1. OOOE+OOO
AREA
0.029464
REPORT
FWHM
(keV)
Pk Area
Ambient
Reagent
Error %
Backgnd
Backgnd
9.17
11.46
2.55
1.19
O.OOE+OOO
O.OOE+OOO
5.0
9.8

Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.970
0.989
5685.50*
4785.00*
Activity
(pCi/liter )
1.76E+001 +/- 7.60E+002
1.04E+001 +/- 1.25E+000
MDA
(pCi/liter
3.22E-001 +/- 1.39E+001
2.33E-001 +/- 8.38E-003
0000058219.CNF
start:
1:3493.l{kev)
Stop : 1024:6486.9(kev)
ACq. Start :"'d '"'Y 15 16:51:46 2013
55
45
Vl
+-'
:::>
0
ll'.l!
~~JI
"'''~
(,.;
ROI Type: 1
Channel Data Report
5/16/2013
Page
5:22:40 AM
*******************************************************
*****
P E C T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
01
Elapsed Live time:

Elapsed Real Time:
10201
10201
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145;
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:
10201
1
1
0
0
1
4
2
1
1
4
0
3
1
2
0
4
1
4
2
3
2
2
1
2
4
4
7
0
3
2
0
0
2
3
1
2
1
2
4
5
3
2
4
1
5
10201
1
2
3
4
0
3
3
1
2
3
1
0
1
1
1
4
2
1
1
3
1
1
3
2
3
2
5
1
1
1
1
2
3
2
3
2
3
5
2
5
2
6
2
2
1
0
1
4
0
0
1
3
2
0
4
1
1
1
3
1
2
0
5
1
0
1
3
1
2
2
1
1
3
2
1
3
5
0
4
2
3
3
2
2
1
5
10
1
4
5
3
2
1
2
0
2
1
1
0
2
1
1
3
2
2
3
1
1
2
5
5
2
4
0
5
1
4
0
0
1
0
1
3
1
3
6
1
1
2
2
4
4
2
4
4
3
2
1
1
0
0
0
3
2
2
5
0
0
1
4
3
4
4
1
1
5
3
3
1
1
2
2
1
0
3
2
2
3
3
3
5
5
2
4
3
3
6
6
3
1
7
7
0
0
1
2
1
0
2
1
1
2
2
2
0
1
2
4
1
2
4
2
2
2
0
2
3
3
2
4
3
1
1
3
4
3
2
1
1
0
1
3
4
2
1
2
7
1
4
1
0
0
1
0
4
1
1
2
3
1
1
0
3
1
2
2
5
4
2
1
4
5
2
2
4
5
2
2
3
0
3
4
3
2
2
1
2
3
7
3
5
5
2
2
3
1
4
0
0
3
0
0
0
1
2
1
2
2
2
2
3
0
2
3
3
2
3
1
1
0
4
1
4
2
5
1
1
1
1
1
1
3
3
7
2
3
2
6
1
0
3
m.37-4
Channel Data Report

369:
5/16/2013
4
Sample Title:
Page
5:22:40 AM
2
01
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:
7
2
2
4
3
4
5
4
3
3
1
7
4
2
2
5
1
2
4
6
3
5
0
3
5
2
3
3
6
2
8
6
6
5
6
3
5
4
6
7
4
4
4
6
4
6
6
5
3
7
3
3
4
3
3
3
4
3
2
6
4
5
0
2
1
2
2
3
2
2
3
6
3
5
5
4
4
1
5
4
5
4
4
7
4
4
9
0
2
6
3
5
4
5
4
1
4
5
4
2
0
4
4
3
2
2
0
2
5
6
1
2
1
2
2
2
1
2
2
4
1
5
0
1
1
5
3
4
3
4
2
2
2
3
6
5
2
2
3
3
3
7
2
3
5
2
4
1
6
2
5
5
5
7
2
1
3
9
2
5
2
5
3
6
0
4
2
1
4
1
5
1
1
3
3
3
3
5
6
3
2
3
5
6
3
6
5
6
5
4
3
1
6
2
8
4
2
9
5
3
9
4
3
8
4
1
2
4
6
0
4
6
1
4
2
7
1
2
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Channel Data Report

801:
5/16/2013
7
Sample Title:
Page
5:22:40 AM
3
01
809:
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2
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0
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4
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1
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7
3
1
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2
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2
2
9
3
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4
1
3
1
3
2
1
3
0
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1
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1
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2
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1
0
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5
3
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8
2
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3
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1
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0
1
3
2
pex-Aipha
Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:
Env. Background:
BLANK
1304132A-RA
02
Shelf 2
Ra
Alpha_010
10
System Bkgd 56972
Reagent Blank:
<not performed>

2.340E+000
5/15/2013 12:52:18 PM
5/15/2013
4:51:43 PM
170.0 minutes
170.0 minutes
Sample Size:
Sample Date/Time:
1.0000 +!0.1967 +/0.1967 +/-
0.350 MeV

PEAK
Nuclide
Energy
(MeV)
RA-224
RA-226
0.0000
0.0036 on 12/15/2012 11:26:40 AM
0.0036
AREA
REPORT
Net
Pk Area
Pk Area
Error %
5.464
4.543
0.24
1. 30
1. OOOE+OOO
1972.2
273.47
Ambient
Backgnd
4.76
1. 70
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
2.9
2.9
Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.938
0.926
5685.50*
4785.00*
Activity
(pCi/liter )
5.46E-003 +/- 2.59E-001
2.73E-002 +/- 7.47E-002
MDA
(pCi/liter
2.39E-001 +/- 1.03E+001
1.54E-001 +/- 5.52E-003
0000058155.CNF
start:
1:3505. 7(kev)
Stop : 1024:6498.0(kev)
Acq. Start :wed May 15 16:51:43 2013
60i
5550
If-
4540
35
~
If-
<=
:::>
8 3025 If20-
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!, !
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6500
Channel Data Report
5/16/2013
Page
5:22:49 AM
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*****
p E C T R A L
DATA
R E p 0 R T
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Sample Title:
02
Elapsed Live time:

Elapsed Real Time:
10201
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Channel Data Report

801:
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0
Sample Title:
Page
5:22:49 AM
0
02
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Spectrum File:
Sample Geometry:
Detector Name:
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FB AT PZ-100-KS TOT DUP

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03
Shelf 2
Ra
Alpha_011
11
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2.120E+000
5/14/2013 12:52:18 PM
4:51:43 PM
5/15/2013
170.0 minutes
17 0. 0 minutes
Sample Size:
Sample Date/Time:
0.8951 +/0.1973 +/0.1766 +/-

PEAK
Energy
(MeV)
Net
Pk Area
5.465
4.677
RA-224
RA-226
0.0000
0.0042 on 12/15/2012 11:28:06 AM
0.0037
0.350 MeV
Nuclide
1. OOOE+OOO
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2.15
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Reagent
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0.85
O.OOE+OOO
O.OOE+OOO
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161.66
2.7
2.7
Nuclide
Id
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Energy
(keV)
RA-224
RA-226
0.938
0.985
5685.50*
4785.00*
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MDA
(pCi/liter
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1.27E-001 +/- 5.24E-003
U!3S2
0000058157.CNF
60-

start:
1:364S.8(kev)
stop : !Ol4:6374.l(kev)
Acq. Start :wed May 15 16:51:43 2013
55
5045
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Channel Data Report
5/16/2013
Page
5:22:55 AM
*******************************************************
*****
P E C T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
03
Elapsed Live time:

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10200
10200
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Channel Data Report

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83-85
Channel Data Report

801:
5/16/2013
0
Sample Title:
Page
5:22:55 AM
0
03
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ex-AiphaTM
Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:
Env. Background:
D-14 TOT
1304132A-RA
04
Shelf 2
Ra
Alpha_Ol3
13
System Bkgd 56974
<not performed>
Reagent Blank:

2.340E+000
S/14/2013 12:52:18 PM
4:51:44 PM
5/15/2013
170.0 minutes
17 0. 0 minutes
Sample Size:
Sample Date/Time:
0.8412 +/0.1869 +/0.1572 +/-

Energy
(MeV)
RA-224
RA-226
0.0000
0.0035 on 12/15/2012 11:26:45 AM
0.0029
0.350 MeV
PEAK
Nuclide
1.000E+000
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4.616
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74.98
AREA
REPORT
Pk Area
Ambient
Error %
Backgnd
52.41
22.81
1. 02
3.06
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
2.8
2.8
Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.954
0.963
5685.50*
4785.00*
Activity
(pCi/liter )
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1.97E+000 +/- 4.55E-001
MDA
(pCi/liter
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1.66E-001 +/- 6.00E-003
Q387
0000058158.CNF
Start:
1 3547. S(kev)
Stop : 1024 6438.1(kev)
Acq. start wed May 15 16:51:44 2013
60
55
50
45
40
35
....,
"'
<=
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25
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15
10
5
0
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4000
tl!l
(})
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ROI Type: 1
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5000
Energy(kev)
5500
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Channel Data Report
5/16/2013
Page
5:23:02 AM
*******************************************************
*****
p E C T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
04
Elapsed Live time:

Elapsed Real Time:
10200
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137:
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Channel Data Report

369:
5/16/2013
0
Sample Title:
Page
5:23:02 AM
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Channel Data Report

801:
5/16/2013
0
Sample Title:
Page
5:23:02 AM
0
04
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Sample Description:
Spectrum File:
Sample Geometry:
D-14 DIS
1304132A-RA
05
Shelf 2
Ra
Detector Name:
Env. Background:
Reagent Blank:
Alpha_014
14
System Bkgd 56975
<not performed>
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Sample Date/Time:

2.660E+000
5/14/2013 12:52:18 PM
5/15/2013
4:51:45 PM
170.0 minutes
170.0 minutes
0.9524 +/0.1846 +/0.1758 +/-

PEAK
Energy
(MeV)
RA-224
RA-226
0.0000
0.0034 on 12/15/2012 11:26:44 AM
0.0033
0.350 MeV
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1.000E+000
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29.62
92.09
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2.38
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Backgnd
FWHM
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O.OOE+OOO
O.OOE+OOO
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2.9
Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.975
0.973
5685.50*
4785.00*
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MDA
(pCi/liter
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l\1392
0000058154.CNF
Start:
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stop : 1024:6512.2(kev)
Acq. Start :wed May 15 16:51:45 2013
60555045
40-
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:::s
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25201510+
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II
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6500
Channel Data Report
5/16/2013
Page
5:23:08 AM
*******************************************************
*****
E C T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
05
Elapsed Live time:

Elapsed Real Time:
10200
10200
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17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
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113:
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801:
5/16/2013
0
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91132
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5/14/2013 12:52:18 PM
4:52:11 PM
5/15/2013
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RA-224
RA-226
5:49:18 PM
0.350 MeV
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0.0000
0.0032 on 12/16/2012
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RA-226
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4785.00*
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Channel Data Report

801:
5/16/2013
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Sample Title:
Page
5:23:15 AM
0
06
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1
ex-AiphaTM
PZ-112-AS DIS
1304132A-RA
07
Shelf 2
Ra
Detector Name:
Env. Background:
Alpha_034
040264798
91136
System Bkgd 56983
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Sample Geometry:
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<not performed>
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3.440E+000
5/14/2013 12:52:18 PM
4:52:12 PM
5/15/2013
170.0 minutes
1.0000 +/0.1856 +/0.1856 +/-
0.350 MeV
PEAK
Energy
(MeV)
RA-224
RA-226
1. OOOE+OOO
170.0 minutes

Nuclide
ftl~i
Net
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5.495
4.618
0.0000
0.0032 on 12/16/2012
0.0032
AREA
REPORT
Pk Area
Error %
3.66
22.66
107.87
41.53
5:49:43 PM
Ambient
Backgnd
Reagent
Backgnd
0.34
0.34
O.OOE+OOO
O.OOE+OOO
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3.0
4.5
Nuclide
Id
Con.
Energy
(keV)
RA-224
RA-226
0.953
0.964
5685.50*
4785.00*
Activity
(pCi/liter )
1.57E-001 +/- 4.75E+001

7.42E-001 +/- 3.09E-001
MDA
(pCi/liter
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1.57E-001 +/- 5.34E-003
0000058164.CNF
Start:
13439.1(kev)
Stop : 1024 6479.9(kev)
Acq. Start wed May 15 16:52:12 2013
4500
5000
Energy(kev)
5500
6000
Channel Data Report
5/16/2013
Page
5:23:23 AM
*******************************************************
*****
p E C T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
07
Elapsed Live time:

Elapsed Real Time:
10200
10200
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
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801:
5/16/2013
Sample Title:
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5/14/2013 12:52:18 PM
5/15/2013
4:52:16 PM
170.0 minutes
170.0 minutes
Sample Size:
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PEAK
Energy
(MeV)
RA-224
RA-226
2:01:29 PM
0.350 MeV
Nuclide
0.0000
0.0034 on 4/20/2013
0.0031
1. OOOE+OOO
REPORT
Pk Area
Error %
Net
Pk Area
2.32
14.81
5.515
4.599
AREA
149.12
53.27
Ambient
Backgnd
0.68
1.19
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
3.0
3.0
Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.962
0.956
5685.50*
4785.00*
Activity
(pCi/liter )
7.82E-002 +/- 2.37E+001

3.81E-001 +/- 2.03E-001
MDA
(pCi/liter
l.90E-001 +/- 5.75E+00l
1.69E-001 +/- 5.75E-003
~(((...__..-
0000058166.CNF
start:
I: 3451.8(kev)
Stop : 1024:6478.4(kev)
Acq. Start :wed May 15 16:52:16 2013
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Channel Data Report
5/16/2013
Page
5:23:35 AM
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*****
E C T R A L
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~4'15
Channel Data Report

801:
5/16/2013
0
Sample Title:
Page
5:23:35 AM
0
09
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Sample Description:
Spectrum File:
Sample Geometry:
DUP07 TOT
1304132A-RA
10
Shelf 2
Ra
Detector Name:
Env. Background:
Reagent Blank:
Alpha_037
04026478A
91133
System Bkgd 56985
<not performed>
Sample Size:
Sample Date/Time:
1.500E+000 +/O.OOOE+OOO liter

2.910E+000
5/14/2013 12:52:18 PM
5/15/2013
4:52:17 PM
170.0 minutes
170.0 minutes

0.7260 +/0.1783 +/0.1294 +/-
Energy
(MeV)
RA-224
RA-226
5.536
4.594
3:28:25 PM
0.350 MeV
PEAK
Nuclide
0.0000
0.0033 on 1/26/2013
0.0024
1. OOOE+OOO
Net
Pk Area
AREA
REPORT
Pk Area
Error %
16.66
103.49
48.59
19.32
Ambient
Backgnd
0.34
0.51
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
2.9
2.9
Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0. 971
0.953
5685.50*
4785.00*
Activity
(pCi/liter )
8.68E-001 +/- 2.62E+002

4.11E+000 +/- 8.08E-001
MDA
(pCi/liter
2.49E-001 +/- 7.53E+001
2.08E-001 +/- 7.59E-003
:fiL417
0000058162.CNF
start:
1:3463. 5(kev)
stop : 1024:6468.5(kev)
ACq. Start :wed May 15 16:52:17 2013
60
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Channel Data Report
5/16/2013
Page
5:23:42 AM
*******************************************************
*****
E C T R A L
DATA
R E P 0 R T
*****
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Sample Title:
10
Elapsed Live time:

Elapsed Real Time:
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Channel[------l-------l-------l-------l-------l-------l-------1-------[
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Channel Data Report

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Channel Data Report

801:
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DUP07 DIS
1304132A-RA
Detector Name:
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Alpha_038
04026478B
91134
System Bkgd 55208
<not performed>
11
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Ra
Sample Size:
Sample Date/Time:

3.540E+000
5/14/2013 12:52:18 PM
5/15/2013
4:52:19 PM
170.0 minutes
170.0 minutes

0.9191 +/0.1722 +/0.1582 +/-
Energy
(MeV)
RA-224
RA-226
5:13:35 PM
0.350 MeV
PEAK
Nuclide
0.0000
0.0030 on 5/11/2013
0.0028
1. OOOE+OOO
Net
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4.606
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REPORT
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Error %
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58.49
55.94
25.76
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Backgnd
0.34
0.51
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Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
5.9
3.0

Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.960
0.959
5685.50*
4785.00*
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6.56E-001 +/- 1.99E+002
2.31E+000 +/- 6.01E-001
MDA
(pCi/liter
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2.07E-001 +/- 7.14E-003
U22
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Channel Data Report
5/16/2013
Page
5:23:48 AM
*******************************************************
*****
p E
T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
11
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Channel Data Report

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801:
5/16/2013
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Sample Title:
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11
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12
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06027396A
83109
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5/14/2013 12:52:18 PM
5/15/2013
4:52:20 PM
170.0 minutes
170.0 minutes
0.9514 +/0.1965 +/0.1870 +/-

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Energy
(MeV)
RA-224
RA-226
2:01:25 PM
0.350 MeV
Nuclide
0.0000
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4785.00*
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5500
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6000
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Channel Data Report
5/16/2013
Page
5:23:57 AM
*******************************************************
*****
p E C T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
12
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Channel Data Report

801:
5/16/2013
0
Sample Title:
Page
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0
12
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91135
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5/14/2013 12:52:18 PM
5/15/2013
4:52:22 PM
170.0 minutes
170.0 minutes
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RA-224
RA-226
5:49:33 PM
0.350 MeV
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0.0000
0.0033 on 12/16/2012
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O.OOE+OOO
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RA-226
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4785.00*
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Channel Data Report
5/16/2013
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*******************************************************
*****
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Sample Title:
13
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Channel Data Report

801:
5/16/2013
0
Sample Title:
Page
5:24:03 AM
0
13
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Sample Description:
Spectrum File:
Sample Geometry:
FB AT PZ-100-KS TOT
1304132A-RA
14
Shelf 2
Ra
Detector Name:
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Alpha_041
05026930A
91087
System Bkgd 56987
<not performed>
2.200E+000
5/14/2013 12:52:18 PM
4:52:24 PM
5/15/2013
170.0 minutes
1.70.0 minutes
Sample Size:
Sample Date/Time:
0.8510 +/0.1978 +/0.1684 +/-

PEAK
Energy
(MeV)
RA-224
RA-226
5:49:31 PM
0.350 MeV
Nuclide
0.0000
0.0034 on 12/16/2012
0.0029
1. OOOE+OOO
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Error %
Net
Pk Area
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4.659
AREA
0.15
0.13
1397.8
2295.4
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Reagent
Backgnd
0.85
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O.OOE+OOO
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3.0
3.0
Nuclide
Id
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Energy
(keV)
RA-224
RA-226
0.898
0.979
5685.50*
4785.00*
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MDA
(pCi/liter
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(II)
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6000
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Channel Data Report
5/16/2013
Page
5:24:11 AM
*******************************************************
*****
E C T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
14
Elapsed Live time:

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Channel Data Report

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14
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Channel Data Report

801:
5/16/2013
0
Sample Title:
Page
5:24:11 AM
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14
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84185
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2.370E+000
5/14/2013 12:52:18 PM
5/15/2013
4:52:25 PM
170.0 minutes
170.0 minutes
Sample Date/Time:
0.9615 +/0.1846 +/0.1775 +/-

PEAK
Energy
(MeV)
RA-224
RA-226
5:49:29 PM
0.350 MeV
Nuclide
0.0000
0.0032 on 12/16/2012
0.0031
1.000E+000
Net
Pk Area
5.529
4.603
-0.51
-0.17
AREA
REPORT
Pk Area
Error %
400.63
1169.4
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Backgnd
0.51
0.17
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
0.0
0.0
NUCLIDE ANAIYSIS RESULTS

Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.968
0.958
5685.50*
4785.00*
Activity
(pCi/liter )
-1.58E-002 +/- 4.77E+000
-4.01E-003 +/- 4.69E-002
MDA
(pCi/liter
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9.84E-002 +/- 3.35E-003
000005817l.CNF
start:
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6055
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Channel Data Report
5/16/2013
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15
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Channel Data Report

369:
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Channel Data Report

801:
5/16/2013
0
Sample Title:
Page
5:24:18 AM
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15
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Sample Description:
Spectrum File:
Sample Geometry:
PZ-100-KS TOT
1304132A-RA
16
Shelf 2
Ra
Detector Name:
Env. Background:
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Alpha_044
04026481B
84168
System Bkgd 56989
<not performed>
2.500E+000
5/14/2013 12:52:18 PM
5/15/2013
4:52:27 PM
170.0 minutes
170.0 minutes
Sample Size:
Sample Date/Time:
0.8253 +/0.1902 +/0.1569 +/-

PEAK
Energy
(MeV)
RA-224
RA-226
5:49:26 PM
0.350 MeV
Nuclide
0.0000
0.0033 on 12/16/2012
0.0027
1.000E+000
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5.485
4.606
AREA
REPORT
Pk Area
Error %
1.32
5.83
215.97
82.55
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Backgnd
Reagent
Backgnd
FWHM
(keV)
0.68
0.17
O.OOE+OOO
O.OOE+OOO
3.0
3.0
Nuclide
Id
Con.
Energy
(keV)
RA-224
RA-226
0.948
0.959
5685.50*
4785.00*
Activity
(pCi/liter )
4.87E-002 +/- 1.47E+001
1.64E-001 +/- 1.36E-001
MDA
(pCi/liter
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1.17E-001 +/- 4.01E-003
fil-447
0000058169.CNF

Start:
1:3447.9(kev)
stop : 1024:6485, 9(kev)
Acq. Start :wed May 15 16:52:27 2013
6055
so!
45
40 r
35
Vl
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c:
8 30 r
25
20
15-
10!
5QI
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3500
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t:ii.
(1)
ROI Type: 1
II
4000
II
II
II:
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t.
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I_
5000
Energy(kev)
_L
__!L__ I j_L
5500
II
__L___j_
6000
II
I 1
Channel Data Report
5/16/2013
Page
5:24:27 AM
*******************************************************
*****
S P E C T R A L
DATA
R E P 0 R T
*****
*******************************************************
Sample Title:
16
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Channel Data Report

801:
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6.451
Sample Description:
Spectrum File:
Sample Geometry:
PZ-100-KS DIS
1304132A-RA
17
Shelf 2
Ra
Detector Name:
Env. Background:
Reagent Blank:
Alpha_045
04026482A
91131
System Bkgd 46594
<not performed>
Sample Size:
Sample Date/Time:

2.550E+000
5/14/2013 12:52:18 PM
4:52:29 PM
5/15/2013
170.0 minutes
170. 0 minutes

1.0000 +/0.1790 +/0.1790 +/-
Energy
(MeV)
RA-224
RA-226
2:04:04 PM
0.350 MeV
PEAK
Nuclide
0.0000
0.0032 on 12/29/2012
0.0032
1. OOOE+OOO
Net
Pk Area
5.568
4.542
7.00
10.32
AREA
REPORT
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
FWHM
(keV)
79.20
63.32
0.00
0.68
O.OOE+OOO
O.OOE+OOO
3.0
3.0

Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.982
0.926
5685.50*
4785.00*
Activity
(pCi/liter )
2.31E-001 +/- 6.99E+001
2.60E-001 +/- 1.65E-001
MDA
(pCi/liter
1.98E-001 +/- 5.99E+001
1.42E-001 +/- 5.00E-003
0000058160.CNF
Start:
1:3456.0(kev)
stop : 1024:6502.6(kev)
Acq. Start :wed May 15 16:52:29 2013
60
5550
1::
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40
35
....s::
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Channel Data Report
5/16/2013
Page
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p E
T R A L
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R E P 0 R T
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ex-AiphaTM
Sample Description:
S-53 TOT
1304132A-RA
18
Shelf 2
Ra
Detector Name:
Env. Background:
Alpha_046
040264823
58762
System Bkgd 56990
Spectrum File:
Sample Geometry:
Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:
1. OOOE+OOO +/-
O.OOOE+OOO liter
5/14/2013 12:52:18 PM
5/15/2013
4:52:31 PM
170.0 minutes
170.0 minutes
0.1352 +/0.1789 +/0.0242 +!-

PEAK
Energy
(MeV)
RA-224
RA-226
5.496
4.521
5:49:23 PM
0.350 MeV
Nuclide
0.0000
0.0031 on 12/16/2012
0.0004
Net
Pk Area
3.83
1. 32
AREA
REPORT
Pk Area
Ambient
Reagent
Error %
Backgnd
Backgnd
0.17
0.68
O.OOE+OOO
O.OOE+OOO
102.72
215.97
FWHM
(keV)
3.0
3.0

Nuclide
RA-224
RA-226
Id
Conf.
Energy
(keV)
0.954
5685.50*
4785.00*
0. 913
Activity
(pCi/liter )
5.50E-001 +/- 1.66E+002
1.45E-001 +/- 3.12E-001
MDA
(pCi/liter
6.00E-001 +/- 1.81E+002

6.18E-001 +/- 2.13E-002
-Ub!57
0000058159.CNF
start:
1:3453.7(kev)
Stop : 1024:65!5.4(kev)
Acq. Start :wed May 15 16:52:31 2013
60!
50+
45
40
35
Vl
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~ 30-f
2520-f
1510-l=
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fJ(I
ROI Type: 1
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Ll___L I
1\_j_ Ali_ I. __ _____l_ !.

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5500
_L_____j_
Ail
6000
I I
6500
Channel Data Report
5/16/2013
Page
5:24:40 AM
*******************************************************
S P E C T R A L
DATA
R E P 0 R T
*****
*****
*******************************************************
Sample Title:
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U6ID
Channel Data Report

801:
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pex-AiphaTM
Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:
Env. Background:
Reagent Blank:
S-53 DIS
1304132A-RA
19
Shelf 2
Ra
Alpha_047
02030596A
91086
System Bkgd 56991
<not performed>
Sample Size:

2.200E+000
5/14/2013 12:52:18 PM
4:52:33 PM
5/15/2013
170.0 minutes
Sample Date/Time:
l70.0 minutes
0.9788 +/0.1822 +/0.1783 +/-

PEAK
Energy
(MeV)
RA-224
RA-226
0.0000
0.0032 on 12/16/2012
0.0031
5:49:21 PM
0.350 MeV
Nuclide
1.000E+000
Net
Pk Area
5.479
4.655
10.66
25.83
AREA
REPORT
Pk Area
Ambient
Error %
Backgnd
61.14
38.71
0.34
0.17
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
2.9
2.9
Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.946
0.978
5685.50*
4785.00*
Activity
(pCi/liter )
4.57E-001 +/- 1.38E+002
8.44E-001 +/- 3.28E-001
MDA
(pCi/liter
2.05E-001 +/- 6.20E+001
1.36E-001 +/- 4.68E-003
0000058172.CNF
start:
1:3457.9(kev)
stop : 1024:6467. 7(kev)
Acq. Start :wed May 15 16:52:33 2013
60
55
50
45
40
35
....,
V>
c:
8 30
25
20
15
10
5
0
'
3500
~
f"-
tl"l
!,)
ROI Type: 1
'
4000
4500
5000
Energy(kev)
5500
6000
Channel Data Report
5/16/2013
Page
5:24:46 AM
*******************************************************
*****
S P E C T R A L
DATA
R E P 0 R T
*****
*******************************************************
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Page 1 of 2
5/15/2013 5:50:13 AM
ex-AI ha
QA SUMMARY REPORT
Date
Time
: 5/15/2013
: 5:50:13 AM
CHAMBER
AljJ_ha 00 I
Alpha 002
AljJ_ha 003
Alpha 004
Alpha 005
Alpha 006
Alpha 007
AljJ_ha 008
Alpha 009
Alpha 010
Alpha Oil
Alpha 012
Alpha 013
Alpha 014
Alpha 015
Alpha 016
Alpha 017
Alpha 018
Alpha 019
Alpha 020
Alpha 021
AljJ_ha 022
Alpha 023
Alpha 024
Alpha 025
Alpha 026
Alpha 027
Alpha 028
Alpha 029
Alpha 030
Alpha 031
Alpha 032
Alpha 033
Alpha 034
Alpha 035
Alpha 036
Alpha 037
Aipha 038
Alpha 039
Alpha 040
Alpha 041
Alpha 042
DEVICE
2Jf
21f
2Jf
2Jf
21f
21f
21f
21f
2Jf
2Jf
21f
2Jf
21f
21f
2Jf
2Jf
AIM730
AIM730
AIM730
AIM730
AJM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
Alpha AnalystJOODC
Alpha AnalystJOODC
Alpha AnalystJOODC
Alpha Analyst IOODC
Alpha Analyst IOODC
Alpha Analyst IOODC
Alpha Analyst IOODC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
FLAG
Not Done
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Not Done
Not Done
Passed
Passed
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Passed
Passed
Not Done
Not Done
Passed
Not Done
Passed
Passed
Not Done
Passed
Not Done
Passed
Not Done
Not Done
Not Done
Passed
Passed
Passed
Passed
Passed
Passed
Passed
Passed
Passed
Passed
DATE
5/15/2013 5:32:39 AM
5/15/2013 5:32:40 AM
5/15/2013 5:32:41 AM
5115/2013 5:32:42 AM
5/15/2013 5:32:43 AM
5/15/2013 5:32:43 AM
5/15/2013 5:32:44 AM
5/15/2013 5:32:45 AM
5/15/2013 5:32:46 AM
5/15/2013 5:32:47 AM
5/15/2013 5:32:47 AM
5/15/2013 5:32:48 AM
5115/2013 5:32:49 AM
5115/2013
5/15/2013
5115/2013
5/15/2013
5/15/2013
5/15/2013
5/15/2013
5/15/2013
5/15/2013
5/15/2013
5:32:50 AM
5:32:52 AM
5:32:53 AM
5:32:55 AM
5:32:57 AM
5:32:58 AM
5:33:00 AM
5:33:03 AM
5:33:05 AM
5:33:07 AM
-8467
Page 2 of 2
CHAMBER
Alpha 043
Alpha 044
AljJha 045
Alpha 046
Alpha 047
Alpha 048
Review of QA Results - Pulser Check
DEVICE
Alpha Analyst!OODC
Alpha Analyst! OODC
Alpha Analyst!OODC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
FLAG
Passed
Passed
Passed
Passed
Passed
Passed
APPROVED BY:
APPROVAL DATE:
s-
\I
{il]
511512013 55013 AM
DATE
511112013 10:55:58 AM
5/1512013 5:33:09 AM .
511512013 5:33:12 AM
5/15/2013 5:33:15 AM
5/15/2013 5:33:18 AM
5115/2013 5:33:20 AM
6/12/12
Page
12:16:17 PM
*************************************************************************
L I B R A R Y
*****
L I S T I N G
R E P 0 R T
*****
*************************************************************************
Radium

Nuclide
Name
Half-Life
(Seconds)
Energy
(keV )
P0-218
RN-222
RA-226
5.049E+Ol0
5.049E+010
5.049E+Ol0
6003.000*
5490.000*
4785.000*
* = key
TOTALS:
Ra-226, Po-218, Rn-222

Energy
Uncert. (keV
0.000
0.000
0.000
line
3
Nuclides
Energy Lines
Yield
(%)
99.9800
99.9200
100.0000
Yield
Uncert. (Abs. +-)
0.0000
0.0000
0.0000
SECTION XI
ANALYTICAL DATA (RADIUM-228)
Eberline Services
Analysis Sheet
Printed: 5/21/20131:2g PM
Page 1 of3
13-04132
Ra228
Run 1
f----
03
5/9/2013
Lab Deadline
r-------
West Lake OU-1

,_
-
Report Level
...
--
05
Matrix
'
Login
CPM
I
I
i
LCS
..
DUP
FB at PZ-100-KS TOT
TRG
D-14 DIS
PZ-112-AS DIS
I
WA
10
38
Sample
Date
I
I
Sample
Aliquot
04/18/13 00:00
1.0000E+OO
04/18/13 00:00
1.5000E+OO
04/16/13 08:40
1.5000E+OO
04/12/13 11:05
1.5000E+OO
....
TRG
I!
t-39
D-14 TOT
07
BLANK
PZ-112-AS TOT
09
t-----
Client
ID
TRG
...
Aliquot Units
06
08
pCi
. Activity Units
Desc
-~TRG
J--
Project
~--~
02
MBL
4/18/2013
Date Received
I Sample I
'
Ra228
Analysis Code
--Run
Client
Internal
Fraction
~~!Iii I
Work Order
II
38
45
PZ-202-SS TOT
46
i
PZ-202-SS DIS
46
TRG
DUP07TOT
40
1.5000E+OO
,_
1.5000E+OO
...-
04/12/13 12:32
1.5000E+OO
... _
1.5000E+OO
! 04/12/13 00:00
Method
..
,,_
DUP07 DIS
40
04/12/13 00:00
PZ-106-KS TOT
36
04/15/1315:59 .
TRG
PZ-106-KS DIS
DO
FB at PZ-100-KS TOT
EPA 904.0 Modified
11
TRG
Alpha/Beta GPC
12
' TRG
13
14
Instrument Type
--
Ba-133
Radiometric Tracer
----Radiometric Sol#
----.--
Ba-6a
..
Tracer Act (dpm/g)
15
1007.586
-.-
_,
Carrier
-Carrier Cone (mg/ml)
--
16
Yttirum
'
TR~FB at PZ-100-KS DIS

TRG
PZ-1 00-KS TOT
..- - -
34
--
TRG
18
. TRG
S~3TOT
-=j
19
TRG
S-53 DIS
__j
PZ-10_0-KS DIS
--"-
1.5000E+OO
-
1.~000E+OO
, 04/15/1315:59
1.5000E+OO
04/16/13 08:40
1.5000E+OO
17
-----
*16/13
37
--+-
~.5000E+OO
04/16/13 08:50
1.5000E+OO
__
37
41
41
l--l
--
04/16/13 08:50
1_.5000E+OO
04116/1309"0
1.0000EOO
04/16/13 09:00
1.0000E+OO
1<11
t~l,
""'~
li-"""
--
1.5000E+OO
2/13 12:32
TRG
..
~2/1311:18
45
..- - -
1.5000E+OO
04/12/13 11:18 _l
_,,
TRG
04/12/13 11 :05
.... Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
Eberline Services
Oak Ridge laboratory
Analysis Sheet
Printed: 5/21/2013 1:29PM

Page 2 of 3
13-04132
Ra228
Run 1
Internal
Fraction
01
Sample
Desc .
Tracer Total
ACT(dpm)
Tracer
Aliquot (g)
0.9178
LCS
Radiometric
Tracer (pCi)
924.8
Grav Filter
Tare (g)

% Rec
, Added (ml)
376.7
90.43
2.000
0.0934
'
Grav Filter
Final (g)
0.1485
I'
Grav Filter
Net(g)
0.0551
Grav
%Rec
81.031
..
02
' MBL
0.9119 I
918.8
435.6
105.25
2.000
0.0939
0.0934
'
03
DUP
0.9044
04
TRG
0.8976
r----
05
I-06
TRG,
0.8990
367.4
89.51
904.4
342.7
84.12
2.000
388.6
..
95.24
2.000
TRG
0.8989
905.7
413.1
101.25
TRG
0.9009
907.7 '
354.5
r-
TRG
10
TRG
11
TRG
0.9009
0.9017
907.7
I
....
0.8997
...
371.2
86.70
0.0937
~0.0938
90.78
1.00
0.1499'
0.0560:i
82.35
73.71
1.00
1.00
0.1474
0.0540
79.41
66.80
1.oo
79.71
75.91. 1.00
1.00
80.29
78.27
1.00
1.00
81.47
82.49
1.00
1.00
71.27
1.00
1.00
75.16 1 1.00
1.00
0.1477
0.0542
_____j_
0.1483
0.0546
....
0.1488
0.0554
0.1496
0.0559
82.21
0.1501
0.0563
82.79
0.0933
0.1495
0.0562
82.65
60.00
1.00
1.00
9~375.3!
91.91
2.oooi
0.0941
0.1508
0.0567
83.38
76.63
1.00
1.00
908.1
389.2 '
95.14
2.000
0.0940
0.1511
0.0571 i
83.97
79.89
1.00
1.00
390.1
95.54
2.0001
0.0937
0.1507
0.0570
83.82
80.09
1.00
1.00
2.0~0.0940
0.1515
0.0575
84.56
71.96
1.00
1.00
2.000!
0.1507
0.0569
83.68
80.45
1.00
1.00
297.1
13
TRG
0.8996
906.4
14
DO
0.9002
907.0
347.7
85.10
0.9008
907.6
393.1
96.151
'
..
16
TRG
0.9023
909.1
17
TRG
0.8744
881.0
338.0
82.53
2.000
0.0938
'
...
0.0935
0.1501
0.0566
68.70
1.00
1.00
84.56
85.55
1.00
1.00
83.24
-
401.5
101.17
"
2.000
0.0913
0.1488
0.0575
..
18
TRG
0.9038
910.7
55.5
13.52
2.0001
0.0968
0.1545
0.0577
84.85
11.48
1.00
1.00
19
TRG
0.9067
913.6
402.8
97.88
2.000
0.0969
0.1538
0.0569
83.68
81.90
1.00
1.00
r---
I
1:!!!
t.J.
~..,J
1.00
---
1-----
72.60
908.5
o.9013
r---
1.00
1----
..
2.000:
TRG
TRG I
73.28i 1.00
1.00
..
0.0934
12
15
2.
86.21
--
09
SAF
1.
81.91
..
08
0.0935
~0937
97.48
..
07
SAF
0.0557
'
r-
398.8
---
908.2
0.9014
0.1493
..
905.8
TRG
911.3
!
2.000!
...
0.0936
Mean
%Rec
"SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.
"'*Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
Eberline Services
Analysis Sheet
Printed: 5/21/20131:29 PM
Page 3 of 3
13-04132
Ra228
Run 1
Internal
Fraction
01
Sample
Desc
Rough Prep
Date
MBL
03
DUP
04
TRG
By
'
LCS
02
RoughPrep
Prep
Date
Prep
Sep tO
Datemme
Sep t1
Date/Time
Sept1
05/14/13 12:53 i LWALKER
05/21/1310:00
TSMITH
05/14/13 12:53
LWALKER
05/21/13 1o:oo
JBARNARD
05/14/13 12:53
LWALKER
05/21/13 10:00
05/03/13 12:33
JBARNARD
0~1~1312'53
LWALKER
05/21/13 10:00
05/03/13 12:33
JBARNARD
05/14/1312:53
LWALKER
05/21/13 10:00 '
By
05/03/13 12:33
JBARNARD
~~
06
TRG
07
TRG
08
--
JBARNARD
---: 1---I
05/14/13 12:53
05/03/13 12:33
JBARNARD
05/14/13 12:53
05/03/13 12:33
JBARNARD
05/14/1312:53
TRG
05/03/13 12:33
10
--
11
--
LWALKER
05/21/13 10:00
TSMITH
LWALKER
05/21/13 10:00
TSMITH
05/14/13 12:53 ' LWALKER
05/21/1310:00
~~~
05/21/13 10:00
TSMITH
--
--
TSMITH
05/03/13 12:33
JBARNARD
05/14/1312:53
05/03/13 12:33
JBARNARD
05/14/13 12:53 i LWALKER
05/21/1310ili~MITH
JBARNARD
05/14/13 12:53
LWALKER
05/21/13 10:00
TSMITH
05/03/13 12:33
JBARNARD
05/14/13 12:53
LWALKER
05/21/13 10:00
TSMITH
TSMITH
LWALKER
TRG
12
'
05/21/1310:00
""
TRG
1----
TSMITH
'
--
JBARNARD
--
TSMITH
LWALKER
09
TSMITH
----
"
05/03/13 12:33
TRG
TSMITH
---
+----
By
' 05/03/13 12:33
By
I
05/03/13 12:33 ' JBARNARD
Septo
TRG
05/03/13 12:33
-
'
--
13
TRG
14
DO
05/03/13 12:33
JBARNARD
05/14/1312:53
LWALKER
05/21/13 10:00
15
TRG
05/03/13 12:33
JBARNARD
05/14/13 12:53
LWALKER
05/21/1310:00
16
TRG
05/03/13 12:33
JBARNARD
05/14/13 12:53
LWALKER
05/21/13 10:00
17
TRG
05/03/13 12:33
18
TRG
19
TRG
TSMITH
TSMITH
-
05/21/1310:00
TSMITH
LWALKER
05/21/13 10:00
TSMITH
LWALKER
05/21/13 10:00
TSMITH
JBARNARD
05/14/13 12:53
LWALKER
05/03/13 12:33
JBARNARD
05/14/13 12:53
05/03/13 12:33
JBARNARD
05/14/13 12:53
--
li!l
l
~~
Ll
Eberline Services
..
Fraction
'\)
0:
,
-1l
8
.~
~
I
01
Nuclide
RA-228
Work Order: 13-04132-Ra228-1
Sample
Results
Oesc
LCS
1- 02- i - - - -!--RA-228
pCi/1
""'" --031_ AA~"n Ioo

co -~~
N
ctl
0:::
:::::
+:::
------------ ---1---- -----------..

06 I
RA-228
, :: (-:::::-
~;,
1---0-~
10
l-11-
-~
I TRG ______ PZ-112-AS TOT_
I ::: ----
"'
-------
J
..;
.s
12
13
RA-228
LCS
RPO
MDA
%R
Flag
Flag
Flag
2.03E+00~=~4=~00J_~~6E+OO
3.86E-01
3.43E-011
105.56
J
;
.
;
----+---
6.89E-01
::~~~:~:: :~:
--------
------------ -----
-~--~~-L
..
I ___
---~---
---
I pclti-~~24E.:_oo'_~~-o1 8.3~~~~l----- J _____ .__
-----
-----
. I
----DUPO~~~~---
pCI/1
1.80E+OO
6.47E-01
--;CI/1
2.47E+OO
5.58EO;t---9.48E-01
------- . -- ..... --- . ,,_i___ ...
1.20E+OO
TRG
_PZ__10_6_-~_TO_T_________ pCI/1 _ _ _a.1_5E-01
4.31E-01
8.86E~1~------
RA-228
TRG
PZ-106-KS DIS
4.27E~1
8.65E~1
..
1:
:;:
"'
1:
'I:
1:
a,
1:
L!J
<!1
$.:ca.
"'"'~J
r.~.
-~NV I
-j
~ OK
O<
::
~----!
OK
-
OK
-
OK
--~.......-~-
OK
-
-- +------+---+--OK
--------
OK
OK
-
t
0
c.
c.
"'"
"E"
..""'
Blank
Flag
OK
l ..... --
,_.. _. , -------- . ----,------- . +.
4.33E-01
-t------+-
RA-228
pCi/1
...
~ __
___
--l----
::::;-t~~:9~~~:~ -~:~::::: :::::::+--- -1-- --+

---j-----1-
---- ---
DUP07 TOT
--------
LCS
9.46-E+OO
RA-2-~-~------- TR~- ----------~~:~o-~~-ss_D_I~-------------- _ _PG_~_-8.63"3--4-.1~-~~1- ---~--B-4E-01

RA228
LCS
Known
:::::::: ____
---------------1
-----------..-----!_- .. __ ----
MOA
Error Estimate
'""':'"~"''- "" '

;;,~:1 ,;;;~, ~;~~~~:------- --;~~--~-~;E:Co s.s4E~1
______ _
Printed: 5/22/2013 8:11AM

Page 1 of 3
OK
-
FB at PZ-100-KS DIS
:G
:G
pCI/1
5.61E-011
-~~;~0~~-;-T-OT -- -- - -~~~~--r ~-~:~ E~1
3.92E01
5.35E-01
OK
7.71E01
~~5E+O~ _ _ --_-~;..---~-+--
I_____Pz-.100K~~~~-- -~-~ ___ s_:sE_~~f-_3.7710:~ _::~=:~

R~
~~_53 TOT
~~Ill I 2-~E+O~ 4.71_":"0 1.03E+01
tG I
S-53 DIS
I pC~46E+OO 6.15E-01 1.15E+OO
_:G
--r-----r--
__ _1__
1
- -.
OK
+
. -~
OK
____j
INV I
1--OK I
~
__
Eberlirie Services
Lob
Work Order: 13-04132-Ra228-1
Sample
Desc
Nuclide
Fraction
01
Printed: 5/22/2013 8:11 AM

Page 2 of 3
I LCS
RA-228
Sample
Sample
Date
Aliquot
04/18/13 00:00
Radiometric
%Rec
1.00E+OOI
Grav
% Rec
9D.431
Sep to
Date/Time
Mean
%Rec
81.031
73.281
Sep t1
DatefTime
1.
----+~~~-- __ o~~~~~~:~;-l1~o~_oo!.~--~~-;~ ~~~11_ -=- -_;;~t

:~: :::-:::::~:::: ::~~~?a~ ----;~:~;j'_ ---:~::: --- --::::~~--::
----~
~I ~11
02
RA-228
----
03
RA228
-- --
..,
~
0
-~
"'
co
N
N
ns
0:::
04
RA-228
[~l-~
oi'
------+---
08
I
!
-----1
"!:
09
----------
-~
10 I
"'
11
--------
:2
ill
----
RA-228
~
0
c.
c.
:;
~zr_
14 ;
RA-228
1.
04/12/1311:18
78.27
1.
1.50E+OO
RA-228
16
RA-228
I-----+
____
--_-_-
"0>
:!! I I -----+
17 I
::;;
1.50E+~O
04/12/1311:18
TRG
04/12/1312:32
1.50E+OO
90.78
------ i'
TRG
04/12/13 00:00
1.50E+OO
72.60
04/12/13 00:00
1.50E+OO
---
04/15/1315:59
~-- 1.5oeoo
__
04/15/13 15:59
1.50E+OO
95.541
,:;;:;;,
"'"]
--- - - -------- -r--- --rI --- -
-+~
TRG
-~~- .. _0.,4~16/~-~-~;,~-0-
__
tl
til
82.49
1.
------r- -------
--":"! ---~2.21-l-
TRG
~~/16/13 08:40
_---J+--=TR=G~-t-~-o4_11_:'1_3_o_8:5Q
1.50E+OO
11.21
1.
82.79,
75.161
1.
82.65~'
60.00[
1.
76.631
1.
--8;~~
-=- ~~i--=_7_9._8_9c-_1_._-+-t
83.821
,;.,F"
80.09
_ _ _ _ _ _ __
5/14/2013 12:531
1.00
-- --------1
5/21/2013 10:00
-~~~---1.0~- ---5/-141"2"01~~;,5;+ --~;;;;201~~
---~8 -----~0.45
_____:_6.15
1_.5_o_e+~
_____
RA-228
. ------+--~~04/16/1308:50
__ _j___1-50E+OO
ll t ~9 L_
--J
81.47~
101.25
--------11 --
------- - - - - - -
0>1 I ----j
18 I -------~-RA-228
o4/16/13o9:o~
e1
80.29
-~oo
"
"
w
97.481
------------------- . ----r - --- -- - - - -
---~---_J ----
"
15 TI ___
"'" ___
"
E
75.91
w'~"""
~-~~===-_j_,-~~-L
d
.E
~I
--
RA-228
---~-----
-'~
RA-228
--
04/12/13 11:05__ ,_.._1.5o~~oo _____ 95.~--------79.711-
--- - - - -- --- -
RA-228
'
- - - - - - - - - - --------- -------' .. - - - - - ------ - - -
TRG
TRG
1.
---
TRG
RA-228
--
__
__
TRG I
5/14/201312:~~ --- _5121/2013 10:00
__ 68.70
1.oo
5/14/2013 12:53
5/21/201310:oo
---~4.56 ------~-55
1.00
5/14/201312:53
____5121/201310:00
1.ooj
5/1412o1312:53
---~~~2o~2 o:oo
-~2.51---- 8:3.:24~~---
_
___101.17
13.5-=~---~~r--
1.ooe+oo
04/16/1309:0~ j_~OOE+OO~-1
RA-228
1.00
_97:i
11.48
--~3.68J _ _ _ 81.90 --~

I
5/14/2013.:2:5~---- 5/21/201310~
Eberline Services
Lab
;r~
~I
0
u
-~
"'
co
N
N
ns
0:::
Sample
Desc
--1
RA-228
. LCS
-----+------
~~E:
-~
RA-228
Counting
Halflife
(days)
Date/Time
i
05/21/1313:47
---------+-----M8L ____o5/21/1313:~6
~ __ _ _
-t
~ ~: -.--::( -J1:~- ~-~~::~~;:~:~~=-~--03
II
RA228
DUP
I
I
Bkg
CPM
Counts
177
. _ 1:0!1j
Eff
1.41
---- ----------------
A2
I
301
81
---------- -1---L~-411~~ -_A1L84110R
Time
0.4626
--~ 1 :~166666 ~~-~~7~6146 0.8333333331
0.4699
---.:;~~,-;;;l--8~~:::::~-r-~:----r---;;~----~::~ ::::::::::1 ::::::

---~;or-
~~~ ---0~~21/13~;4~---r - - - - t
342 1.;;;3333J- 0.4754
_I----------~---- --- ----- - -----~--------r---07
RA-228
~ TRG 05/21/1313:46
, L84110R
82
1201
248 1.283333333
0.4658
----r------- -- ---r--- --------- ------------o6
~~2;~
05/21/13 13:46
L84110A
Count
Carrier
Detect
--------
1
------~-
---~!____'--_ ~_:_~2~
09
RA-228
'!;
: TRG
I
05/21/~ ~3~46
r~:_ __o:l2~/1313:46
TRG
__
10
.,
RA-22s___
21/1313:46
ill
u
,:
.5
0
__B3
L84110R
-1-____
1 __
~----
84
OA.??o
~ nn~--
n"'"'" ,..,,
120 _
1
-----1 L841~~;r
~~ol
__L841_'"R_ _c1 ____ ___

C2
- j_
14
120
_ __182
o oAna
1.~66_~~~67
192
- - - - - - - - - - - - _____ _j
~: ---:~:- :;:+--;~:~;~ - =---~-- ~ :
c.
c.
-"
L8_411_"R
05/21/13 13:46
~---------- ---------------------------
1-
-~--
Printed: 5/22/2013 8:11 AM

Page 3 of 3
Work Order: 13-04132-Ra228-1
Nuclide
Fraction
01
--
0.4713_
0.4773
-----
294 1.466666667
0.4705
'
l} =;;: ::::; ~::

120
384 1.483333333
0.4676
r<
tJJ
~I
.."
16
Cl
..
17
Cl
18
:;;
c
"
a,
c
w
c
!
-~
19
[::~
~~~::::;.=
~,~~:
~~ltF
:;;~t1
:::
.
L---- - -----------T-----~------I
1;:
---------
RA-228
TRG
05/21/13 13:47
':".:"~-----
TRG ___ -"5/21/13
13
L84110A
:47
02
-~~~--'-~r
L84110A
1
12;f-
189
1.75
0.4682
222 1.116666667
0.474~
Count Room Report

Internal
Fraction
Sample
Desc
Client
ID
01
LCS
LCS
02
MBL
-
BLANK
0~-tDUP
-04
TRG
Sample
Aliquot
Sample
Date
04/18/13 00:00
FB at PZ-100-KS TOT
D-14 TOT
05
I TRG
D-14 DIS
06
! TRG
PZ-112-AS TOT
07~G
Page 1 of 1
Tracer
Tracer
Aliquot{g)
ACT{dpm)
1.0000
0.9178
924.7624
04/18/13 00:00
1.5000
0.9119
04/16/13 08:40
1.5000
04/12/13 11 :05
1.5000
'
PZ-112-AS DIS
'
Radiometric
Tracer (pCi)
1.5000
SAF
2.
1.00
1.00
918.8177
435.6000
105.25
1.00
1.00
0.9044
911.2608
367.4000
89.51
1.00
1.00
0.8976
904.4092
342.7000
84.12
1.00
1.00
1.00
1.00
905.8198
0.8990
~/~2/1311:1~00
908.2380
0.9014
0.8989
388.6000
'
95.24
~MOOO=t
905.7191
413.1000
TRG
PZ-202-SS TOT
' 04/12/1312:32
1.5000
0.9009
907.73421
354.5000
iTRG[
PZ-202-SS DIS
04/12/13 12:32
1.5000
0.9009
907.7342
371.2000
08
1.5000
04/12/1311:18
SAF
%Rec
90.43
04/12/13 11:05
Radiometric
376.7000
---+-t
-09
Printed: 5/21/2013 1:29PM
13-04132-Ra228-1 (pCi/1) in WA
Tracer 10: Ba-6a
'::r
1.00
~-' 'OC
1.00
1.00
1.00
1.00
1.00
1.00
I _90.7S ..
10
TRG
DUP07TOT
04/12/13 00:00
1.5000
0.9017
908.5~ 297.1000 .
72.60
1.00
1.00 .
11
! TRG .
DUP07 DIS
04/12/13 00:00
1.5000
0.8997
906.5251
91.91
1.00
1.00
95.14
1.00
1.00
12
i TRG
PZ-106-KS TOT
13
TRG
PZ-106-KS DIS
04/15/13 15:59
DO
FB at PZ-100-KS TOT
FB at PZ-100-KS DIS
14
--
TRG
15
16
'
17
18
375.3000
'
0.9013 .
389.2000
1.5~8.8996
906.4244
390.1000
95.54
1.00
1.00
04/16/13 08:40
1.5000
0.9002
907.0289
347.7000
85.10
1.00
1.00
' 04/16/13 08:40
1.5000
0.9008
907.6335
393.1000
96.15
1.00
1.00
1.5000
0.9023
909.1448
338.0000
82.53
1.00
1.00
1.5000
0.8744
881.0332
401.5000
101.17
1.00
1.00
04/16/13 09:00
1.0000
0.9038
910.6562
55.4800
13.52
1.00
1.00
04/16/13 09:00
1.0000
0.9067
913.5782
402.8000
97.88
1.00
1.oo
1.5000
..
'
908.1373
04/15/1315:59
TRG
PZ-100-KS TOT
04/16/13 08:50
TRG
PZ-100-KS DIS
. 04/16/1308:50
TRG
S-53 TOT
19
TRG
S-53 DIS
tlifl
.1>;
-..!
~J
Eberline Services
Internal Work Order
Run
Analysis Code
Date
Technician
13-04132
Ra228
5/3/2013 12:30
JBARNARD
LCS & Matrix Spikes

Activity I Solution
Isotope
Sol#
Ra-228
Ra-11
dpmlg
38.839
Date
5/3/2013
Approx
Addition
0.510
LCS
MS
LCSD
MSD
Volume
Used(g)
Volume
Used(g)
Volume
Used(g)
Volume
Used{g)
0.5121
Activity
dpmlg
8.96
Volume
Used{g)
Approx
Addition
Isotope
So/#
01
Ba-133
Ba-6a
1007.586
5/3/2013
0.9178
1.0100
02
Ba-133
Ba-6a
1007.586
5/3/2013
09119
1.0100
03
Ba-133
Ba-6a
1007.586
5/3/2013
0.9044
1.0100
04
Ba-133
Ba-6a
1007.586
5/3/2013
0.8976
1.0100
OS
Ba-133
Ba-6a
1007.586
5/3/2013
0.8990
1.0100
06
Ba-133
Ba-6a
1007.586
5/3/2013
0.9014
1.0100
07
Ba-133
Ba-6a
1007.586
5/3/2013
0.8989
1.0100
08
Ba-133
Ba-6a
1007.586
5/3/2013
0.9009
1.0100
09
Ba-133
Ba-6a
1007.586
5/3/2013
0.9009
1.0100
10
Ba-133
Ba-6a
1007.586
5/3/2013
0.9017
1.0100
11
Ba-133
Ba-6a
1007.586
5/3/2013
0.8997
1.0100
12
Ba-133
Ba-6a
1007.586
5/3/2013
0.9013
1.0100
13
Ba-133
Ba-6a
1007.586i
5/3/2013
0.8996
1.0100
14
Ba-133
Ba-6a
1007.586
5/3/2013
0.9002
1.0100
15
Ba-133
Ba-6a
1007.586
5/3/2013
0.9008
1.0100
16
Ba-133
Ba-6a
1007.586
5/3/2013
0.9023
1.0100
17
Ba-133
Ba-6a
1007.586
5/3/2013 .
0.8744
1.0100
1007.586
5/3/2013
0.9038
1.0100
1007.586
5/3/2013
0.9067
1.0100
19
Ba-133
Ba-6a
Ba-6a
~:o.
~,l
00
Version 2.0 08/99
MS
Error
Estimate
0.457
Added
pCi
0.00
LCSD
Error
Estimate
0.000
----
MSD
Error
Estimate
Known
pCi
0.00
0.000

Solution
Date
fraction
Ba-133
Witness Initials
LCS
Known
pCi
Tracers
18
Page 1 of 1
Printed: 51312013 12:33 PM
Tracer
LCS
Matrix Spike
Added
pCi
0.00
I Estimate
Error
0.000
Eberline Analytical
Work Order
13-04132
Lab
Fraction
Client 10
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
LCS
BLANK
FB at PZ-100-KS TOT
D-14 TOT
D-14 DIS
PZ-112-AS TOT
PZ-112-AS DIS
PZ-202-SS TOT
PZ-202-SS DIS
DUP07TOT
DUP07 DIS
PZ-106-KS TOT
PZ-1 06-KS DIS
FB at PZ-100-KS TOT
FB at PZ-100-KS DIS
PZ-1 00-KS TOT
PZ-100-KS DIS
S-53 TOT
S-53 DIS
Printed: 5/3/201312:36 PM
Page 1 of 1
Aliquot Worksheet
Analysis Code
Rpt Units
Lab Deadline
Technician
Ra228
liters
5/9/2013
JBARNARD
Sample
Muffle Data
Ratio
R
1
...
Type
LCS
MBL
DUP
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
DO
TRG
TRG
TRG
TRG
TRG
Dilution Data
No of Oils
Post/Pre
Aliquot Data
Oil Factor
Ratio
. .
:.
:: ..
..
.
.
. .
...
. ..
.
. ..
..
..
>
.
......
..
.
.
..
.
..
..
.
'
>
,..
Aliquot
NetEquiv ..
1.0000E+OO
1.0000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO 1:5000E+OO
1.5000E+OO < 1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
.
Comments
!21!1
gt~
"'~.JI
tlOr
Technician
:)Date
53,~
MS Aliquot Data
H-3 Solids Only
'
N~t_Equiv'
Aliquot
:___. .
--
.. .....
.
..
.
...
<
'
Water Added
H3 Oist
(ml)
Aliq
Eberline Services - Oak Ridge

Version 1.0 9/1999
Work Order
TRetec Engineering Management Support, Inc.
Sample
Analysis
Code
Gravimetric
Carrier
Carrier Cone
Ra228
Yttirum
34.0000
Carrier Data
Carrier Added
Fraction
01
02
03
04
05
---06
07
08
09
10
11
12
~-
~14
f-:Js 16
17
18
f-~9
l:i'Ji!
t:a.
~~)
!iii
Technician:
Client ID
LCS
BLANK
DUP
D-14 TOT
D-14 DIS
PZ-112-AS TOT
PZ-112-AS DIS
PZ-202-SS TOT
PZ-202-SS DIS
DUP07 TOT
DUP07 DIS
PZ-106,KS TOT - PZ-1 06-KS DIS
PZ-1 00-KS TOT
PZ-1 00-KS DIS
S-53 TOT
S-53 DIS
Printed: 5/21/2013 1:29PM

Page 1 of 1
Gravimetric Worksheet
Type
LCS
MBL
DUP
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
DO
TRG
TRG TRG
TRG
TRG
(ml)
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
(mglml)
Filter Data
Filter Tare
(g)
0.0934
0.0936
0.0939 ;
0.0934
0.0935
0.0937
0.0934
0.0937
0.0938
0.0933
0.0941
0.0940
0.0937
0.0940
0.0938
0.0935
0.0913
0.0968
0.0969
Date:~ Z--1 1__!}_
TSMITH
Gravimetric
Filter Final
(g)
0.1485
0.1493
0.1499 !
0.1474
0.1477
0.1483
0.1488
0.1496
0.1501
0.1495
0.1508 1
0.1511
0.1507
0.1515
0.1507
0.1501
0.1488
0.1545
0.1538
~ vd'
Technician
Filter Net
(g)
Recovery
0.0551
0.0557
0.0560
0.0540
0.0542
0.0546
0.0554
0.0559
0.0563
0.0562
0.0567
0.0571
0.0570
0.0575
0.0569
0.0566
0.0575
0.0577
0.0569
81.03
81.91
82.35
79.41
79.71
80.29
81.47
82.21
82.79
82.65
83.38
83.97
83.82
84.56
83.68
83.24
84.56
84.85
83.68
Sheet1
TOO
Detector ID Sample ID Alpha Beta Count Time Voltage
B1
1304132-01
3
177
30
1400 5/21/13 14:17
~a
Jl:.,
00
i""'
,-, ..-.
Page 1
rfD.,,-,
~-~
Sheet1

TOD
294
1400 5/21/13 15:46
1304132-10 15
C1
120
159
1400 5/21/13 15:46
1304132-02 23
A1
120
C2
1304132-11
17
384
120
1400 5/21/13 15:46
1400 5/21/13 15:46
1304132-12 11
191
C3
120
146
1400 5/21/13 15:46
1304132-03 15
A2
120
1400 5/21/13 15:46
1304132-04 16
288
120
A3
1304132-13 17
202
1400 5/21/13 15:46
C4
120
1400 5/21/13 15:46
1304132-05
9
240
120
A4
1304132-06 17
342
120
1400 5/21/13 15:46
81
248
1400 5/21/13 15:46
1304132-07
12
120
82
1400 5/21113 15:46
182
1304132-08
120
83
9
192
1400 5/21/13 15:46
1304132-09 16
120
84
)t;:~,
(II)
M
Page 1
<\2-1-\()
v
~-v,\\i
"5 \c.<>
Sheet1

TOD
C1
1304132-14
8
167
120
1400 5/21/13 15:47
1304132-15 22
170
1400 5/21/13 15:47
C2
120
1400
1304132-16
241
5/21113 15:47
C3
21
120
1400
5/21/13
15:47
1304132-17
9
205
120
C4
1400 5/21/13 15:47
1304132-18 19
189
02
120
1400 5/21113 15:47
1304132-19 19
222
120
04
li!'~
~
(!)
Page 1
"'-
Eberllne Analytical
Oak Ridge laboratory
GPC Detector Report
Detector
Bkg CPM
PFW
LCL
Mean
UCL
Alpha
11/18/2007
5/21/2013
3.33E-02
-2.17E+01
2.92E-01
2.23E+01
Alpha
11/18/2007
5/21/2013
3.33E-02
-1.85E+01
2.61E-01
1.90E+01
LB4110A- A3
Alpha
11/18/2007
5/21/2013
O.OOE+OO
-1.80E+01
2.22E-01
1.84E+01
LB4110A - A4
Alpha
11/18/2007
5/21/2013
6.67E-02
-1.91E+01
2.44E-01
1.96E+01
LB4110A- B1
Alpha
5.00E-02
O.OOE+OO
-9.87E-02
-7.93E-02
7.52E-02
Alpha
5/21/2013
5/21/2013
LB4110A- B2
LB4110A- B3
11/18/2007
11/18/2007
7 .27E-02
2.49E-01
2.25E-01
Alpha
11/18/2007
5/21/2013
3.33E-02
-6.38E-02
5.33E-02
1. 70E-01
LB4110A - B4
Alpha
11/18/2007
5/21/2013
8.33E-02
-1.43E-01
7.92E-02
3.01E-01
LB4110A- C1
Alpha
5/21/2013
1.67E-02
-1.52E-01
8.91E-02
3.30E-01
11/18/2007
LB4110A- C2
Alpha
11/18/2007
5/21/2013
3.33E-02
-1.79E-01
8.82E-02
3.56E-01
LB4110A - C3
Alpha
11/18/2007
5/21/2013
1.67E-01
-1.75E-01
1.01E-01
3.78E-01
LB4110A- C4
Alpha
11/18/2007
5/21/2013
5.00E-02
-6.32E-02
6.88E-02
2.01E-01
LB4110A- D1
Alpha
11/18/2007
5/21/2013
1.67E-02
-5.37E-02
8.39E-02
2.21E-01
LB4110A- D2
Alpha
11/18/2007
5/21/2013
1.17E-01
-7 .08E-02
6.07E-02
1.92E-01
5/21/2013
5/21/2013
6.67E-02
p
-----p
-4.78E-02
-5.73E-02
7.17E-02
7.08E-02
1.91E-01
-l.OOE-01
1.01E-01
3.03E-01
Alpha
LB4110A - D4
Alpha
11/18/2007
11/18/2007
LB4110R- A1
Alpha
11/24/2006
5/21/2013
5.00E-02
1.17E-01
LB4110R- A2
Alpha
11/24/2006
5/21/2013
O.OOE+OO
-8.99E-02
7.74E-02
2.45E-01
LB4110R - A3
Alpha
11/24/2006
5/21/2013
1.17E-01
-7.43E-02
7. 71E-02
2.28E-01
LB4110R- A4
LB4110R- B1
Alpha
11/24/2006
11/24/2006
5/21/2013
5/21/2013
5.00E-02
O.OOE+OO
p
p
-5.30E-02
-9.57E-02
7.15E-02
6.19E-02
1.96E-01
2.19E-01
1.67E-02
-6.95E-02
6.41E-02
1.98E-01
Alpha
LB4110R- B2
Alpha
LB4110R- B3
Alpha
LB4110R- B4
------------ - - - - - - - -
---
-----
11/24/2006
5/21/2013
11/24/2006
5/21/2013
1.33E-01
-6.52E-02
7.01E-02
2.05E-01
3.33E-02
P __ ~6.46E-02
7.08E-02
2.06E-01
1---
11/24/2006
5/21/2013
LB4110R- C1
Alpha
11/24/2006
5/21/2013
6.67E-02
-7.78E-02
7.43E-02
2.26E-01
LB4110R - C2
Alpha
11/24/2006
5/21/2013
5.00E-02
-7.54E-02
7.20E-02
2.19E-01
1.33E-01
-8.88E-02
8.47E-02
2.58E-01
Alpha
11/24/2006
5/21/2013
LB4110R- C4
Alpha
11/24/2006
5/21/2013
3.33E-02
-6.21E-02
8.20E-02
2.26E-01
LB4110R - D1
Alpha
11/24/2006
5/21/2013
O.OOE+OO
-9.98E-02
7.26E-02
2.45E-01
2.18E-01
2.23E-01
LB4110R- C3
------- --
LB4110R - D2
Alpha
11/24/2006
5/21/2013
O.OOE+OO
Alpha
11/24/2006
5/21/2013
O.OOE+OO
-7.40E-02
-7.93E-02
7.20E-02
LB4110R- D3
LB4110R- D4
Alpha
11/24/2006
5/21/2013
O.OOE+OO
-7.08E-02
7.67E-02
-1.56E-02
9.58E-02
LB5100 - 1
Alpha
7/10/2006
10/26/2007
--
5.00E-02
7.18E-02
c.-JI'-tt---
1.99E-01
Alpha
--------
!':>.
Count Date
LB4110A- A2
-----
00
Calibration Date
LB4110A- A1
LB4110A- D3
11.":1
Alpha/Beta
------
,,.
Printed: S/21/2013 6:59AM

Page 1 of 1
(ALL Backgrounds)
2.24E-01
2.07E-01
Eberllne Analytical
GPC Detector Report
Detector
Alpha/Beta
Calibration Date
LB4110A- A1
Beta
11/18/2007
LB4110A- A2
Beta
Beta
LB4110A - A3
~'--------,-
LCL
Mean
UCL
5/21/2013
8.3SE+OO
-2.95E+02
7.63E+00
3.10E+02
11/18/2007
5/21/2013
3.42E+OO
3.10E+01
2.55E+OO
3.61E+01
11/18/2007
__5/21/2013
1.42E+OO
-5.12E+01
2.66E+OO
5.65E+01
3.32E+01
3.05E+OO
3.93E+01
__ _____
,
..
11/18/2007
5/21/2013
6.62E+OO
LB4110A- 81
Beta
11/18/2007
5/21/2013
1.40E+OO ,
-1.04E+01
3.25E+OO
1.69E+01
LB4110A 82
Beta
11/18/2007
5/21/2013
1.17E+OO
-7.53E+OO
1.98E+OO
1.15E+01
LB4110A 83
Beta
11/18/2007
5/21/2013
1.20E+OO
1.08E-01
1.36E+OO
2.62E+OO
Beta
11/18/2007
5/21/2013
1.15E+01
Beta
11/18/2007
5/21/2013
7.58E+OO
-5.49E+OO
1.97E+OO
LB4110A C1
1.35E+OO.
1.27E+OO.
2.15E+OO
9.79E+OO
LB4110A C2
Beta
11/18/2007
5/21/2013
1.02E+OO
3.80E-01
1.27E+OO
2.16E+OO
LB4110A- C3
Beta
11/18/2007
5/21/2013
1.48E+OO.
4.71E-01
1.47E+OO
2.46E+OO
LB4110A- C4
Beta
11/18/2007
5/21/2013
-1.77E+00
LB4110A D1
LB4110A D2
Beta
11/18/2007
11/18/2007
5/21/2013
5/21/2013
1.97E+OO
2.13E+OO
2.58E+00
6.04E+00
7.54E+OO
1.75E+OO.
-2.37E+OO
-6. 75E01
1.57E+00
3.81E+OO
11/18/2007
5/21/2013
4.22E+OO
1.23E+00
4.47E+OO
7.71E+00
LB4110A- 84
Beta
- - - - - - ---------
LB4119!<_: [)_~ _ Beta

LB4110A - D4
Beta
11/18/2007
5/21/2013
LB4110R A1
Beta
11/24/2006
5/21/2013
LB4110R- A2
Beta
11/24/2006
5/21/2013
-------- ---
~lE-01.
--
;;-
----------
1.12E+OO.
-4.48E-01
1.37E+OO
3.20E+OO
1.02E+00.
-6.18H01
3.76E+00
6.93E+01
8.33E-Ot
-4.91E+01
2.05E+00
5.32E+01
LB4110R A3
Beta
11/24/2006
5/21/2013
1.32E+OQ
-4.55E+01
2.79E+OO
5.10E+01
LB4110R A4
Beta
11/24/2006
5/21/2013
1.03E+OO
4.54E+01
2.02E+OO
4.94E+01
LB4110R- 81
Beta
11/24/2006
5/21/2013
1.23E+OO.
-4. 78E+01
2.05E+OO
5.18E+01
LB4110R - 82
Beta
11/24/2006
5/21/2013
1.28E+OQ
-4. 77E+01
LB4110R - 83
Beta
2.08E+00
2.70E+OO
5.29E+01
LB4110R - 84
11/24/2006
5/21/2013
- -..------------. -------------Beta
11/24/2006
5/21/2013
LB4110R- C1
Beta
11/24/2006
5/21/2013
LB4110R- C2
Beta
11/24/2006
5/21/2013
p
1.07E+OO
-4. 75E+01
- - - ----- --------
p
l.OOE+O()
-4.78E+01
p
1.47E+OO.
-4.76E+01
p
1.48E+00
-4.76E+01
---------
----------
1.95E+OO
5.17E+01
3.02E+OO
5.37E+01
2.75E+OO
5.31E+01
-4.81E+01
-5.42E+01
2.55E+00
5.32E+01
2.98E+OO
6.02E+01
O.OOE+OO
4.50E+01
5.75E+00
5.65E+01
-4.85E+01
1.94E+OO
5.24E+01
5.19E+01
5.72E+OO
6.33E+01
2.31E+OO
5.28E+01
1.58E+00
3.48E+OO
Beta
Beta
11/24/2006
11/24/2006
5/21/2013
LB4110R C4
5/21/2013
r---1.37E+OO
LB4110R D1
Beta
11/24/2006
5/21/2013
-------------.. --"----------------
5.19E+01
1.37E+OO
LB4110R- C3
... "---- -"'""
LB4110R D2
Beta
11/24/2006
5/21/2013
O.OOE+OO
LB4110R D3
11/24/2006
5/21/2013
O.OOE+OO
LB4110R D4
Beta
Beta
11/24/2006
5/21/2013
O.OOE+OO
LB5100 - 1
Beta
7/10/2006
10/26/2007
4.52E+OO
---
U11
PFW
Count Date
Beta
--------
lJ:>,
(:0
Bkg CPM
'
LB4110A A4
!iil:i
Printed: 5/21/2013 6:59AM

Page 1 of 1
(ALL Backgrounds)
------ _,,_,_ p-. -

F
------
4.82E+01
-3.19E-01
----- -----..
---:---
c...-
rrl'-
Eberline Analytical
GPC Detector Report

(ALL Efficiencies)
Detector
PFW
LCL
Mean
UCL
-0.0180
0.2148
11/18/2007
5/21/2013
0.2407
L84110A- A2
Alpha
-0.0555
0.1728
Alpha
5/21/2013
5/21/2013
0.2090
L84110A- A3
11/18/2007
11/18/2007
0.4477
0.4010
0.2113
-0.0790
0.1617
0.4024
L84110A- A4
Alpha
11/18/2007
5/21/2013
0.2174
-0.0575
0.1806
0.4186
5/21/2013
0.2079
0.1943
0.2246
0.2549
0.1929
0.2217
0.2506
L84110A- 81
Alpha
L84110A- 82
LB4110A- 83
Alpha
Alpha
11/18/2007
11/18/2007
5/21/2013
5/21/2013
0.2133
0.2391
0.1296
0.2326
0.3356
L84110A- 84
Alpha
11/18/2007
5/21/2013
0.2257
0.2090
0.2367
0.2643
5/21/2013
0.2212
0.1974
0.2208
0.2443
5/21/2013
5/21/2013
0.2223
0.2537
0.2506
0.1967
0.2229
0.2252
0.2494
0.2759
0.2231
0.1966
0.2257
0.2549
5/21/2013
0.2207
0.2035
0.2333
0.2632
11/18/2007
5/21/2013
0.2472
0.2277
0.2890
11/18/2007
0.2540
0.1852
p
p
0.2314
0.1649
0.2584
0.2638
11/18/2007
L84110A- C1
Alpha
L84110A- C2
Alpha
11/18/2007
L84110A- C3
Alpha
11/18/2007
LB4110A- 03
Alpha
Alpha
Alpha
Alpha
11/18/2007
11/18/2007
5/21/2013
11/18/2007
0.2963
LB4110A- D4
Alpha
11/18/2007
5/21/2013
5/21/2013
0.1998
0.2346
L84110R- A1
Alpha
11/24/2006
5/21/2013
0.2363
0.2032
0.2389
0.2746
L84110R- A2
Alpha
11/24/2006
5/21/2013
0.2145
0.1899
0.2206
L84110R- A3
LB4110R- A4
Alpha
Alpha
11/24/2006
11/24/2006
5/21/2013
5/21/2013
0.2240
0.2363
p
p
0.1964
0.2160
0.2249
0.2457
0.2513
0.2533
0.2754
LB4110R- 81
Alpha
11/24/2006
5/21/2013
0.2259
0.1878
0.2261
0.2644
L84110R- 82
Alpha
11/24/2006
5/21/2013
0.2119
0.1801
0.2175
0.2549
L84110R- 83
Alpha
11/24/2006
5/21/2013
0.2502
0.2068
0.2440
0.2813
L84110R- 84
Alpha
LB4110R- C1
Alpha
11/24/2006
11/24/2006
L84110R- C2
Alpha
11/24/2006
L84110R- C3
L84110R- C4
Alpha
Alpha
5/21/2013
0.2235
0.1937
0.2319
0.2701
5/21/2013
0.2069
0.1861
0.2153
0.2444
5/21/2013
0.2172
0.1963
0.2248
0.2533
0.2366
0.2064
0.2397
0.2730
0.1858
5/21/2013
11/24/2006
5/21/2013
5/21/2013
0.2077
p
F
0.0333
0.2229
0.2063
0.2599
0.0000
LB4110R- 01
L84110R- 02
Alpha
11/24/2006
11/24/2006
Alpha
11/24/2006
5/21/2013
0.0000
0.0386
0.2346
0.4305
LB4110R- 03
Alpha
11/24/2006
5/21/2013
0.0000
0.0380
0.2304
0.4229
L84110R- 04
Alpha
11/24/2006
5/21/2013
0.0000
0.0290
0.3368
0.3332
0.1857
0.3455
0.3425
LB5100 - 1
Eff
Alpha
L84110A- 02
Count Date
L84110A- A1
L84110A- D1
0,)
Calibration Date
L84110A- C4
Alpha/Beta
Printed: 5/21/2013 6:59AM

Page 1 of 1
Alpha
7/10/2006
10/26/2007
0.3792
0.3578
c...-)fl.,v.--
Eberline Analytical
GPC Detector Report

(ALL Efficiencies)
--
Detector
Alpha/Beta
LB4110A- A1
Beta
11/18/2007
LB4110A- A2
Beta
LB4110A- A3
Beta
Count Date
Eff
PFW
LCL
Mean
UCL
5/21/2013
0.5635
0.2044
0.5628
0.9211
11/18/2007
5/21/2013
0.4916
0.1552
0.4635
0.7717
11/18/2007
5/21/2013
0.4676
0.8316
0.5159
0.0827
0.1351
0.4571
0.4879
0.8408
Beta
11/18/2007
LB4110A- B1
Beta
11/18/2007
5/21/2013
0.4882
0.4637
0.5305
0.5973
LB4110A- B2
Beta
11/18/2007
5/21/2013
0.5089
0.4639
0.5276
0.5912
LB4110A- B3
Beta
11/18/2007
5/21/2013
0.5311
0.3197
0.5321
LB4110A- B4
Beta
11/18/2007
5/21/2013
0.5309
0.5545
LB4110A- C1
Beta
11/18/2007
5/21/2013
0.5021
0.4921
0.4503
0.7445
0.6169
0.5027
0.5551
LB4110A- C2
Beta
11/18/2007
5/21/2013
0.5044
0.4281
0.5011
0.5741
LB4110A- C3
Beta
11/18/2007
5/21/2013
0.6050
0.5279
0.5902
0.6526
0.4569
0.5250
0.5931
0.4797
0.5541
0.6286
5/21/2013
LB4110A- C4
LB4110A- D1
Beta
Beta
11/18/2007
11/18/2007
5/21/2013
5/21/2013
0.5113
0.5316
LB4110A- D2
Beta
11/18/2007
5/21/2013
0.5406
0.4901
0.5885
0.6870
0.6012
0.5369
0.6155
0.6941
0.3861
0.4733
0.4815
0.5604
0.6544
0.5967
LB4110R- A1
LB4110R- A2
LB4110R- A3
Beta
Beta
Beta
Beta
Beta
LB4110R- A4
Beta
LB4110R- B1
Beta
LB4110R- B2
Beta
11/18/2007
5/21/2013
11/18/2007
5/21/2013
11/24/2006
11/24/2006
5/21/2013
0.4371
0.5604
5/21/2013
0.5050
0.4210
0.5679
0.5089
0.5267
0.4581
0.5397
0.6213
0.5102
0.5918
0.6734
0.5427
0.5202
0.6318
11/24/2006
5/21/2013
11/24/2006
5/21/2013
0.5984
11/24/2006
11/24/2006
5/21/2013
0.5258
5/21/2013
0.5117
0.4536
0.4314
0.6090
11/24/2006
5/21/2013
0.6073
0.5018
0.5914
0.6809
Beta
11/24/2006
5/21/2013
0.5306
0.4623
0.5499
0.6375
LB4110R- C1
Beta
11/24/2006
5/21/2013
0.4629
0.4239
0.5031
0.5824
LB4110R- C2
LB4110R- C3
Beta
5/21/2013
5/21/2013
0.5144
0.5572
Beta
11/24/2006
11/24/2006
0.4504
0.4815
0.5292
0.5712
0.6080
0.6610
LB4110R- C4
Beta
11/24/2006
5/21/2013
0.4979
0.4323
0.5264
0.6204
LB4110R- D1
Beta
11/24/2006
5/21/2013
0.0000
0.0787
0.4933
0.9078
LB4110R- D2
LB4110R- D3
LB4110R- D4
Beta
0.0000
0.0000
0.0891
0.0865
0.5543
0.5383
1.0194
0.9901
Beta
11/24/2006
5/21/2013
5/21/2013
5/21/2013
Beta
11/24/2006
11/24/2006
0.0000
0.0678
0.4431
0.8184
LB5100- 1
Beta
7/10/2006
10/26/2007
0.4428
0.4555
0.4731
0.4906
LB4110R- B3
-.j
Calibration Date
LB4110A- A4
LB4110A- D4
I>
():)
Page 1 of 1
--------
LB4110A- D3
!Zl
Printed: S/21/2013 6:59AM
LB4110R- B4
Beta
'
n~
'
'
SECTION XII
BARIUM-133 ANALYTICAL TRACER DATA
VAX/VMS Peak Search Report Generated 15-MAY-2013 07:34:06.78

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
frrc.~
DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_l30413201_GEl BAFIL 191 42.CN

PEAK Vl6.9 PEAKEFF V2.2
SPIKE
15-MAY-2013 00:00:00
1304132-01
FILTER
GEl
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30.84
35.06
61.85
66.02
81.36
92.72
102.16
112.02
116.46
146.79
161.43
191.48
276.70
303.12
307.44
333.94
338.21
356.47
384.20
387.30
3 91.73
414.92
418.35
421.62
437.46
468.21
510.97
584.28
610.89
2253
540
294
128
812
68
23
231
32
23
29
17
90
177
49
89
18
585
168
255
56
37
31
9
114
23
19
14
8
84
58
95
85
157
71
69
37
39
93
49
55
14
22
22
15
21
33
13
9
8
14
12
12
14
5
10
9
4
2
2
5
5
0
0
0
2
2
0
0
0
0
2
2
4
4
0
3
3
3
3
3
3
0
0
0
0
0
c...-
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
l. 51
1.68
1. 99
2.06
l. 92
l. 36
l. 96
l. 81
l. 82
2.84
1. 51
l. 08
l. 37
l. 65
2.01
1.81
2.45
l. 86
2.27
1.65
l. 80
2.29
1.94
l. 90
l. 93
2.02
l. 93
5.49
3.09
31.07
35.29
62.08
66.25
81.59
92.95
102.39
112.25
116.68
147.01
161.66
191.71
276.92
303.33
307.65
334.16
338.42
356.68
384.40
387.51
391.93
415.13
418.56
421.83
437.67
468.41
511.17
584.47
611.08
Left
Pw
27
27
58
58
77
90
100
106
106
145
158
191
273
299
299
329
329
351
381
381
381
409
409
409
432
465
507
580
608
13
13
12
12
10
6
7
16
16
9
6
5
8
15
15
14
14
11
15
15
15
19
19
19
11
6
8
11
7
15-MAY-2013 07:18:51
l.OOOOOE+OO filter
0
BAFIL
0 00:15:00.30 0.0%
4096
10.00000
Cts/Sec %Err
2.50E+00
6.00E-Ol
3.26E-01
l.42E-01
9.03E-Ol
7.54E-02
2.58E-02
2.57E-Ol
3.60E-02
2.59E-02
3.25E-02
l.89E-02
9.98E-02
1.97E-Ol
5.43E-02
9.93E-02
l. 99E- 02
6.50E-Ol
1.87E-01
2.84E-01
6.22E-02
4.07E-02
3.48E-02
l.OlE-02
1.27E-Ol
2.61E-02
2.09E-02
l. 55E-02
8.89E-03
2.2
4.9
7.7
16.0
4.6
23.1
62.6
7.7
36.2
77.2
42.5
69.8
12.8
8.3
20.7
12.7
56.7
4.6
10.3
7.2
17.2
25.4
28.9
89.7
11.3
25.1
37.2
48.5
53.2
Fit
4.49E+Ol
4.70E+00
4.73E+00
6.02E+00
1.96E+00
1.85E+Ol
1.94E+00
Summary of Nuclide Activity

Sample ID : 1304132-01
Acquisition date
Total number of lines in spectrum

Number of unidentified lines
Number of lines tentatively identified by NID
29
25
4
Page :
2
15-MAY-2013 07:18:51
13.79%
Nuclide Type : FISSION

Nuclide
BA-133
Hlife
10.50Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 3.766E+02
Total Activity
3.766E+02
Wtd Mean
Decay Corr
pCi/filter
3.767E+02
Decay Corr
2-Sigma
2-Sigma Error %Error Flags
0.724E+02
19.22
3.767E+02
Nuclide Type : NATURAL

Nuclide
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 3.958E+02
Total Activity
Grand Total Activity :
Flags: "K"
"E"
Wtd Mean
Decay Corr
pCi/filter
3.958E+02
3.958E+02
3.958E+02
7.725E+02
7.725E+02
Keyline not found

Manually edited
"M"
"A"
Decay Corr
2-Sigma
0.639E+02
16.14
Manually accepted
Nuclide specific abn. limit
Nuclide Line Activity Report

Sample ID : 1304132-01
Acquisition date
Page :
3
15-MAY-2013 07:18:51
Nuclide Type: FISSION

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for
Uncorrected Decay Corr 2-Sigma

%Eff
pCi/filter pCi/filter %Error
3.767E+02 19.22
1.963E+01 3.766E+02
6.083E+02 33.65
4.915E+00 6.083E+02
4.204E+02
17.68
6.963E+00 4.204E+02
3 Valid Peaks =
3.767E+02+/- 7.238E+01
Status
OK
OK
OK
19.22%)
Nuclide Type: NATURAL

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag: "*'' = Keyline

%Eff
5.865E+01 3.958E+02
3.958E+02 16.14
1 Valid Peaks =
Status
OK
3.958E+02+/- 6.388E+01 ( 16.14%)
Combined Activity-MDA Report

Sample ID : 1304132-01
Acquisition date
Page :
4
15-MAY-2013 07:18:51
---- Identified Nuclides

Nuclide
BA-133
TH-234
Activity
(pCi/filter)
3.767E+02
3.958E+02
Act error
7.238E+01
6.388E+01
MDA
(pCi/ filter)
2.066E+01
6.030E+01
MDA error
Act/MDA
3. 391E+00
1.932E+00
18.235
6.564
MDA error
Act/MDA
6.191E+00
2.554E+01
3.632E-03
8.271E-02
7.375E+00
1.565E-01
-0.207
-0.178
0.000
3.039
0.713
1.435
Non-Identified Nuclides
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
-4.096E+00
-3.509E+01
O.OOOE+OO
1.337E+01
4.321E+01
9.571E+00
Act error
1.303E+01
1.464E+02
O.OOOE+OO
2.158E+00
3.633E+01
3.399E+00
MDA
(pCi/filter)
1.983E+01
1.974E+02
1.933E-01
4.401E+00
6.058E+01
6.671E+00
Q___

Configvration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
DKAlOO: [GAMMA.SCQSR.ARCHIVE]SMP 130413202 GEl - BAFIL 191544.CN

PEAK V16.9 PEAKEFF V2.2
BLANK
15-MAY-2013 00:00:00
1304132-02
FILTER
GEl
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
27.90
30.91
34.89
52.56
61.96
66.01
81.17
92.27
111.85
116.53
162.06
185.58
277.04
303.02
307.77
334.89
338.53
356.41
376.35
384.09
387.31
391.82
414.90
418.62
421.97
437.55
446.02
468.38
472.90
512.12
727.32
39
2103
596
69
259
139
939
17
182
28
40
15
50
172
38
52
28
594
24
140
215
46
56
35
10
108
6
26
8
19
8
71
3
3
3
0
2
2
0
0
0
0
0
0
0
2
2
0
0
0
0
3
3
0
1
1
1
0
0
3
3
0
0
)trr~
79
86
100
75
69
108
108
107
76
79
78
45
22
29
38
15
23
6
23
37
25
6
5
4
9
3
11
6
11
0
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1. 51
1.40
1.85
2.92
1.61
1.74
1.94
1.56
1.38
3.80
1. 31
1.09
1.45
1.56
2.01
1.71
1.38
1.87
1.59
2.27
1. 72
1.21
1.77
1.90
1. 90
1. 82
2.07
2.33
2.34
2.73
1. 00
28.14
31.15
35.13
52.80
62.19
66.24
81.40
92.50
112.08
116.76
162.28
185.80
277.26
303.24
307.99
335.10
338.74
356.62
376.55
384.29
387.51
392.03
415.10
418.83
422.17
437.76
446.23
468.58
473.11
512.32
727.50
15-MAY-2013 07:37:09
l.OOOOOE+OO filter
0
BAFIL
0 00:15:00.29 0.0%
4096
10.00000
Left
Pw
Cts/Sec %Err
27
27
27
50
58
58
76
90
108
116
159
185
272
300
300
331
338
353
373
381
381
391
411
411
411
434
443
465
465
509
725
13
13
13
8
11
11
10
7
7
5
8
6
9
11
11
7
4
7
7
10
10
5
16
16
16
9
6
15
15
11
6
4.35E-02 32.5
2.34E+00 2.3
6.62E-01 5.9
7.67E-02 27.5
2.88E-01 7.9
1.55E-01 12.5
1.04E+00 3.9
1.94E-02101.0
2.02E-01 12.0
3.09E-02 51.5
4.47E-02 41.2
1.67E-02 96.6
5.57E-02 28.0
1.91E-01 8.2
4.22E-02 24.8
5.77E-02 23.9
3.13E-02 28.9
6.60E-01 4.3
2.64E-02 27.3
1.55E-01 13.0
2.39E-01 8.4
5.06E-02 23.5
6.25E-02 15.3
3.89E-02 24.6
1.09E-02 70.5
1. 20E- 01 11.0
6.54E-03 62.4
2.84E-02 28.0
8.52E-03 79.6
2 .11E-02 40.9
8.89E-03 35.4
Fit
6.94E+01
3.60E+00
2.03E+01
2.49E+01
2.05E+00
1.62E+00

Sample lD : 1304132-02
Acquisition date

Nuclide Type
Nuclide
BA-133
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
4.356E+02
Total Activity
:
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 3.491E+02
Total Activity
=
=
---------
4.356E+02
Wtd Mean
Decay Corr
pCi/filter
4.356E+02
---------
Decay Corr
2-Sigma
0.809E+02
18.58
4.356E+02
NATURAL
Nuclide
Hlife
TH-234 4.47E+09Y
Flags: "K"
"E"
12.90%
FISSlON
Hlife
10.50Y
Nuclide Type
31
27
4
Page :
2
15-MAY-2013 07:37:09
---------
Wtd Mean
Decay Corr
pCi/filter
3.491E+02
---------
3.491E+02
3.491E+02
7.847E+02
7.847E+02
Keyline not found

Manually edited
"M"
"A"
=
=
Decay Corr
2-Sigma
0.583E+02
16.70
Manually accepted

Sample IO : 1304132-02
Acquisition date
Page :
3
15-MAY-2013 07:37:09

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

1. 963E+01 4.356E+02
4.356E+02 18.58
5.912E+02 33.55
4.915E+00 5.912E+02
4.271E+02 17.44
6.963E+00 4.270E+02
%Eff
3 Valid Peaks
Status
OK
OK
OK
4.356E+02+/- 8.092E+01 ( 18.58%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag: "*"
Key line

5.865E+01 3.491E+02
3.491E+02 16.70
%Eff
1 Valid
Peaks~
Status
OK
3.491E+02+/- 5.832E+01 ( 16.70%)

Sample ID : 1304132-02
----
Acquisition date
Page :
4
15-MAY-2013 07:37:09
Identified Nuclides
Nuclide
BA-133
TH-234
Activity
(pCi/filter)
4.356E+02
3.491E+02
Act error
8.092E+01
5.832E+01
MDA
(pCi/filter)
1.752E+01
5.724E+01
MDA error
Act/MDA
2.876E+00
1.834E+00
24.865
6.099
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/ filter) Ided
-3.956E+00
1.407E+01
O.OOOE+OO
8.618E+00
9.374E+00
9.766E+00
Act error
MDA
(pCi/ filter)
MDA error
Act/MDA
1.389E+01
1.558E+02
O.OOOE+OO
1.775E+00
4.031E+01
3.465E+00
2.120E+01
2.205E+02
1.933E-01
3.646E+00
5.861E+01
6.546E+00
6.617E+00
2.853E+01
3.632E-03
6.851E-02
7.136E+00
1. 536E-01
-0.187
0.064
0.000
2.364
0.160
1.492

Configl.lration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
15-MAY-2013 00:00:00
1304132-03
FILTER
GEl
0 00:15:00.00
25
3.00000
No
Energy
Area
Bkgnd
4
4
0
1
1
0
0
0
0
0
0
0
0
3
3
0
2
2
2
1
1
0
0
0
0
30.84
35.15
53.10
61.89
65.63
81.16
92.83
100.22
111.83
132.48
221.68
276.69
303.16
333.95
338.34
356.37
384.10
387.00
391.71
415.97
425.62
437.54
468.31
511.50
617.38
2075
469
119
244
103
792
52
27
177
32
17
56
129
57
33
521
134
231
61
28
9
85
29
23
7
69
56
59
46
52
152
70
82
130
55
58
25
22
18
15
25
12
9
2
2
0
15
6
0
0
13
14
15
16
17
18
19
20
21
22
23
24
25
ftt~
DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP- 130413203 GEl BAFIL- 191548.CN

FB AT PZ-100-KS TOT
Pk I t
1
2
3
4
5
6
7
8
9
10
11
12
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1. 50
1.69
2.68
1. 58
1. 58
1.96
1.50
5.27
1. 45
3.33
2.28
1.27
1.69
1.76
2.23
1. 92
1. 66
2.05
1. 97
1. 90
1. 90
1.98
1. 90
2.47
1.12
31.07
35.38
53.33
62.12
65.86
81.39
93.06
100.45
112.05
132.71
221.90
276.90
303.38
334.16
338.55
356.58
384.31
387.20
391.92
416.17
425.83
437.75
468.51
511.70
617.57
Left
Pw
27
27
50
58
58
77
90
97
108
129
218
273
300
330
330
352
382
382
382
411
411
432
464
508
614
13
13
8
11
11
10
7
8
8
9
8
7
6
14
14
9
20
20
20
19
19
9
11
8
6
15-MAY-2013 08:02:19
l.OOOOOE+OO filter
0
BAFIL
0 00:15:00.28 0.0%
4096
10.00000
Cts/Sec %Err
2.31E+00
5.22E-01
1.32E-Ol
2. 71E-Ol
1.14E-01
8.80E-01
5.78E-02
2.97E-02
1.97E-Ol
3.60E-02
1.87E-02
6.17E-02
1.43E-01
6.32E-02
3.62E-02
5.79E-Ol
1.49E-01
2.57E-01
6.82E-02
3.15E-02
l.OlE-02
9.41E-02
3.17E-02
2.56E-02
7.78E-03
2.2
5.4
14.4
8.1
17.2
4.6
30.1
61.8
13.5
44.5
83.2
20.0
10.5
17.6
33.2
4.7
9.4
8.1
15.2
28.5
53.3
13.7
24.6
20.9
37.8
Fit
3.47E+Ol
7.97E+00
4.21E+00
8.78E+00
5.59E+00

Sample ID : 1304132-03
Acquisition date

Nuclide Type
Nuclide
BA-133
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
3.674E+02
---------
Total Activity
:
3.674E+02
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
3.292E+02
---------
Total Activity
Grand Total Activity
nKn
liE II
=
=
Wtd Mean
Decay Corr
pCi/filter
3.674E+02
---------
Decay Corr
2-Sigma
0.706E+02
19.22
3.674E+02
NATURAL
Nuclide
Hlife
TH-234 4.47E+09Y
Flags:
20.00%
FISSION
Hlife
10.50Y
Nuclide Type
25
20
5
Page :
2
15-MAY-2013 08:02:19
Wtd Mean
Decay Corr
pCi/filter
3.292E+02
---------
3.292E+02
3.292E+02
6.966E+02
6.966E+02
Key line not found

Manually edited
Decay Corr
2-Sigma
0.560E+02
17.01
uM" = Manually accepted
"A"

Sample ID : 1304132-03
Acquisition date
Page :
3
15-MAY-2013 08:02:19

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for
Uncorrected Decay Carr 2-Sigma

%Eff
1.963E+01 3.674E+02
3.674E+02 19.22
4.915E+00 4.424E+02
4.425E+02 36.05
6.963E+00 3.747E+02
3.747E+02 17.84
3 Valid Peaks =
Status
OK
OK
OK
3.674E+02+/- 7.063E+01 ( 19.22%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag: "*'' = Keyline

%Ef
5.865E+01 3.292E+02
3.292E+02 17.01
1 Valid Peaks =
Status
OK
3.292E+02+/- 5.598E+01 ( 17.01%)

Sample ID : 1304132-03
----
Acquisition date
Page :
4
15-MAY-2013 08:02:19
Identified Nuclides
Nuclide
BA-133
TH-234
Activity
(pCi/filter)
Act error
MDA
(pCi/filter)
MDA error
Act/MDA
3.674E+02
3.292E+02
7.063E+01
5.598E+01
1.843E+01
5.051E+01
3.025E+00
1.618E+00
19.935
6.518
MDA error
Act/MDA
6.372E+00
2.727E+Ol
3.632E-03
8.128E-02
7.803E+00
1.459E-01
0.162
-0.145
0.000
2.802
0.383
1. 575
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
3.312E+00
-3.051E+01
O.OOOE+OO
1.212E+Ol
2.457E+01
9.798E+00
Act error
1.141E+01
1.555E+02
O.OOOE+OO
2.142E+00
4.238E+01
3.194E+00
MDA
(pCi/filter)
2.041E+01
2.108E+02
1.933E-01
4.325E+00
6.409E+01
6.221E+00

Configuration
:
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
r;c( n-
DKAlOO: [G~MA.SCUSR.ARCHIVE]SMP_l30413204_GEl_BAFIL_ 9155l.CN

D-14 TOT
15-MAY-2013 00:00:00
1304132-04
FILTER
GEl
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
27.90
30.91
34.95
53.05
61.80
66.07
81.21
92.85
111.89
114.92
160.66
277.00
303.31
334.33
356.38
383.88
386.96
391.62
415.36
418.41
437.65
468.54
511.59
41
1706
442
63
234
89
739
34
145
25
34
22
120
47
517
125
187
37
32
23
80
19
23
49
61
81
84
61
77
110
75
47
51
95
35
29
34
21
13
8
4
14
14
15
11
2
3
3
3
0
2
2
0
0
2
2
0
0
0
0
0
1
1
1
3
3
0
0
0
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
Left
Pw
28.14
31.14
35.18
53.29
62.03
66.30
81.44
93.08
112.11
115.15
160.88
277.21
303.52
334.54
356.59
384.09
387.17
3 91. 83
415.57
418.62
437.86
468.75
511.79
27
27
27
50
58
58
76
89
108
108
156
276
299
331
353
380
380
380
410
410
433
466
508
13
13
13
8
12
12
11
6
13
13
10
6
7
7
7
17
17
17
12
12
10
6
10
1.51
1. 39
1. 85
3.12
1.73
1.74
1. 93
1.11
1. 81
1.65
1.77
1.14
1. 91
1. 29
1. 86
1. 88
1. 88
1.88
2.29
2.30
1. 83
2.17
2.13
15-MAY-2013 08:22:42
1. OOOOOE+OO filter
0
BAFIL
0 00:15:00.26 0.0%
4096
10.00000
Cts/Sec %Err
4.59E-02
1.90E+00
4.91E-01
7.00E-02
2.60E-01
9.86E-02
8.21E-Ol
3.78E-02
1.61E-Ol
2.75E-02
3.78E-02
2.44E-02
1.34E-Ol
5.23E-02
5.74E-Ol
1. 39E-01
2.08E-Ol
4.08E-02
3.55E-02
2.56E-02
8.93E-02
2.07E-02
2.58E-02
27.4
2.5
7.2
28.2
8.4
18.6
4.6
43.7
11.5
59.3
56.8
48.9
11.7
25.1
4.6
10.4
9.7
21.9
30.4
42.9
14.3
36.3
24.1
Fit
4.56E+01
2.01E+00
5.17E+00
2.01E+Ol
7.65E-01

Sample ID : 1304132-04
Acquisition date

Nuclide Type
Nuclide
BA-133
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 3.427E+02
--------~
Total Activity
:
3.427E+02

=
Wtd Mean
Decay Corr
pCi/filter
3.427E+02
---------
Decay Corr
2-Sigma
Q.659E+02
19.23
3.427E+02
NATURAL
Wtd Mean
Uncorrected
Nuclide
Hlife
Decay pCi/filter
TH-234 4.47E+09Y
1. 00
3.159E+02
--------Total Activity
3.159E+02
Flags: "K"
17.39%
FISSION
Hlife
10.50Y
Nuclide Type
23
19
4
Page :
2
15-MAY-2013 08:22:42
6.586E+02
Key line not found
uE" = Manually edited
Wtd Mean
Decay Corr
pCi/filter
3.159E+02
---------
Decay Corr
2-Sigma
0.552E+02
17.47
3.159E+02
6.586E+02
11M II = Manually accepted
"An = Nuclide specific abn.
limit

Sample ID : 1304132-04
Acquisition date
Page :
3
15-MAY-2013 08:22:42

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Ef
1.963E+01 3.427E+02
3.427E+02 19.23
4.915E+00 4.132E+02
4.132E+02 37.44
3.716E+02 17.77
6.963E+00 3.716E+02
3 Valid Peaks
3.427E+02+/- 6.591E+01
Status
OK
OK
OK
19.23%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag: ''*" ; Keyline

%Eff
5.865E+01 3.159E+02
3.159E+02 17.47
1 Valid Peaks;
Status
OK
3.159E+02+/- 5.519E+01 ( 17.47%)

Sample ID : 1304132-04
Acquisition date
Page :
4
15-MAY-2013 08:22:42

Nuclide
BA-133
TH-234
Activity
(pCi/filter)
Act error
3.427E+02
3.159E+02
6.591E+01
5.519E+01
MDA
(pCi/filter)
1.655E+01
6.226E+01
MDA error
Act/MDA
2.717E+00
1.995E+00
20.709
5.074
MDA error
Act/MDA
6.463E+00
2.628E+01
3.632E-03
6.483E-02
7.142E+00
1.496E-01
0.009
-0.086
0.000
2.192
0.046
1.153
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
1. 842E- 01
-1. 754E+01
O.OOOE+OO
7.562E+00
2.705E+00
7.357E+00
Act error
1.293E+01
1. 4 77E+02
O.OOOE+OO
1.678E+00
4.145E+01
3.525E+00
MDA
(pCi/ filter)
2.070E+01
2.032E+02
1.933E-01
3.450E+00
5.866E+01
6.379E+00
c.--
(It(.....-

Configuration
Analyses by
Client ID
Deposition Date
Sample Pate
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
DKA100: [GAMMA.SCUSR.ARCHIVE]SMP 130413205 GE2 - BAFIL 191545.CN

D-14 DIS
15-MAY-2013 00:00:00
1304132-05
FILTER
GE2
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
30.91
35.17
53.23
61.81
65.95
81.01
111.56
143.03
148.74
161.18
276.37
303.26
330.89
338 .11
352.03
356.01
383.87
386.99
391.45
415.67
437.12
467.59
471.90
511.72
826.35
1868
435
62
188
102
768
162
21
21
37
53
132
10
22
10
511
104
175
43
33
97
15
7
20
9
103
122
162
68
63
118
99
40
37
77
28
53
8
13
7
7
7
8
10
18
8
3
1
6
0
3
3
0
2
2
0
0
1
1
0
0
0
3
3
1
1
3
3
3
0
0
4
4
0
0
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1.38
1. 53
1.92
1.60
1.61
1.34
1.34
1. 60
1. 61
2.72
1.92
1.51
1. 65
2.20
1. 83
1.50
2.12
1.86
2.26
1.59
1. 60
2.57
2.12
3.98
3.24
31.02
35.28
53.35
61.92
66.07
81.12
111.68
143.15
148.85
161.29
276.48
303.37
331.00
338.21
352.13
356.12
383.97
387.10
3 91. 56
415.77
437.23
467.70
472.00
511.82
826.44
Left
Pw
26
26
50
58
58
77
108
140
140
158
273
299
329
329
350
350
380
380
380
413
432
464
464
508
823
15
15
8
14
14
8
8
12
12
8
8
8
17
17
13
13
16
16
16
8
10
13
13
11
7
15-MAY-2013 07:37:39
1. OOOOOE+OO filter
0
BAFIL
0 00:15:00.29 0.0%
4096
10.00000
Cts/Sec %Err
2.08E+00
4.84E-01
6.86E-02
2.09E-01
1.13E- 01
8.53E-01
1.80E-01
2.37E-02
2.36E-02
4.12E-02
5.91E-02
1.47E-01
1.06E-02
2.47E-02
1.07E-02
5.68E-01
1.16E-01
1.94E-01
4.75E-02
3.68E-02
1.08E-01
1. 72E-02
7.92E-03
2.17E-02
l.OOE-02
2.4
6.1
38.9
9.9
15.5
4.4
13.2
48.8
49.1
44.0
21.7
12.9
73.4
38.5
43.8
4.4
11.9
9.4
23.5
27.5
11.4
33.6
54.8
32.5
33.3
Fit
4.04E+00
1.92E+00
1.83E+00
6.75E+00
9.16E-01
6.16E+00
6.56E-01
u_s-m-s

Sample ID : 1304132-05
Acquisition date

25
21
4
Page :
2
15-MAY-2013 07:37:39
16.00%

Nuclide
BA-133
Hlife
10.50Y
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00 3.886E+02
Total Activity
3.886E+02
Wtd Mean
Decay Corr
pCi/filter
3.886E+02
Decay Corr
2-Sigma
0.760E+02
19.54
3.886E+02

Nuclide
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00 6. 44 7E+02
Total Activity
Flags: "K"
"E"
=
=
Wtd Mean
Decay Corr
pCi/filter
6.447E+02
6.447E+02
6.447E+02
1.033E+03
1.033E+03
Keyline not found

Manually edited
"M"
"A"
=
=
Decay Corr
2-Sigma
1.409E+02
21.86
Manually accepted

Sample ID : 1304132-05
Acquisition date
Page :
3
15-MAY-2013 07:37:39

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
1.799E+Ol 3.886E+02
3.886E+02 19.54
7.560E+00 2.949E+02
2.949E+02 39.44
7.170E+00 3.566E+02
3.566E+02 17.56
3 Valid Peaks =
Status
OK
OK
OK
3.886E+02+/- 7.595E+Ol ( 19.54%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag:
''*'' = Keyline

%Eff
2.305E+Ol 6.447E+02
6.447E+02 21.86
1 Valid Peaks =
Status
OK
6.447E+02+/- 1.409E+02 ( 21.86%)

Sample ID : 1304132-05
----
Acquisition date
Page :
4
15-MAY-2013 07:37:39
Identified Nuclides
Nuclide
BA-133
TH-234
Activity
(pCi/filter)
Act error
3.886E+02
6.447E+02
7.595E+01
1.409E+02
MDA
(pCi/filter)
1.883E+01
1.269E+02
MDA error
Act/MDA
3.206E+00
1.049E+01
20.636
5.080
MDA error
Act/MDA
1.520E+00
1.947E+01
2.050E-01
6.355E-02
5.863E+00
1.397E+00
0.296
-0.392
2.940
0.944
0.460
1.194
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter) Ided
2.927E+00
-6.646E+01
3.166E+01
2.909E+00
2.389E+01
2.156E+01
Act error
5.359E+00
1.121E+02
5.736E+00
1.695E+00
2.896E+01
9.534E+00
MDA
(pCi/filter)
9.895E+00
1.695E+02
1.077E+01
3.081E+00
5.193E+01
1.806E+01
c.....
54 9
VCAXon/fVMlgusraPetal'oknSearch Report Generated 15-MAY-2013 08:18:19.49_GE _BAFIL_l~l/( ~

.CN
DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_l30413206
~
Analyses by
Client ID
PZ-112-AS TOT
Deposition Date
Sample Date
15-MAY-2013 00:00:00 Acquisition date : 15-MAY-2013 08:02:58
Sample ID
l.OOOOOE+OO filter
1304132-06
Sample Quantity
Sample type
FILTER
Sample Geometry
0
Detector name
GE2
Detector Geometry: BAFIL
Elapsed live time: 0 00:15:00.00
Elapsed real time: 0 00:15:00.30 0.0%
Start channel
End channel
25
4096
Sensitivity
3.00000
Gaussian
10.00000
Critical level
No
Pk It
Energy
Area
Bkgnd
2
2
30.92
35.09
52.20
61.53
65.97
80.92
84.02
91.62
111.83
116.03
161.00
183.20
185.87
276.94
302.77
306.91
312.45
333.71
337.92
356.02
383.72
386.83
391.32
414.53
418.03
424.25
437.10
510.93
1928
431
59
161
91
788
18
26
153
16
42
13
42
121
107
140
140
56
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
0
0
0
1
1
0
1
1
0
2
2
0
3
3
3
2
2
0
22
1
1
23
24
25
26
27
28
0
2
2
0
0
0
66
137
29
12
68
25
501
94
155
34
39
16
8
85
31
55
51
84
64
66
62
20
35
32
9
10
11
18
16
34
22
33
16
5
8
11
6
4
FWHM Channel
1. 32
1.53
2.20
1.28
1. 39
1.50
1. 50
1. 71
1.51
1.56
1.55
1.82
1. 82
1.83
1. 55
2.16
2.17
1.91
2.00
1. 36
1. 86
1.52
1.48
2.07
2.08
1. 47
1.37
2.22
31.04
35.20
52.32
61.65
66.09
81.03
84.14
91.73
111.94
116.14
161.11
183.32
185.98
277.05
302.88
307.02
312.56
333.81
338.03
356.13
383.83
386.94
391.42
414.64
418.14
424.36
437.20
511.03
Left
Pw
26
26
50
58
65
76
76
89
108
108
157
182
182
272
299
299
299
329
329
352
381
381
390
411
411
422
433
507
16
16
8
7
4
11
11
8
12
12
8
9
9
11
28
28
28
12
12
8
9
9
6
10
10
7
8
8
Cts/Sec %Err
2.14E+00
4.79E-Ol
6.52E-02
1. 79E-Ol
1. OlE- 01
8. 76E-Ol
2. 04E-02
2.89E-02
1.70E-Ol
1.77E-02
4.66E-02
1.44E-02
4.66E-02
7.29E-02
1.53E-Ol
3.22E-02
1.38E-02
7.60E-02
2.80E-02
5.57E-Ol
1.04E-Ol
1.72E-01
3.80E-02
4.33E-02
1.78E-02
9.01E-03
9.44E-02
3.44E-02
2.4
6.4
37.8
14.5
16.1
3.8
97.6
64.1
11.2
79.3
36.3
54.3
28.1
20.9
9.1
29.4
56.5
15.8
34.6
4.9
14.8
9.8
27.8
18.7
48.0
81.4
11.9
21.2
Fit
3.22E+00
1.20E+Ol
l.l4E+00
1.41E+00
l.l8E+00
1.31E+00
2.49E+00
3.46E+00

Sample ID : 1304132-06
Acquisition date

Nuclide Type
Nuclide
BA-133
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
3.988E+02
---------
Total Activity
:
3.988E+02
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
5.509E+02
1. 00
5.462E+01
---------
Total Activity
=
Wtd Mean
Decay Corr
pCi/filter
3.988E+02
---------
Decay Corr
2-Sigma
0.760E+02
19.07
3.988E+02
NATURAL
Nuclide
Hlife
TH-234 4.47E+09Y
AM-241
432.20Y
Flags: "K"
14.29%
FISSION
Hlife
10.50Y
Nuclide Type
28
24
4
Page :
2
15-MAY-2013 08:02:58
Wtd Mean
Decay Corr
pCi/filter
5.509E+02
5.462E+01
---------
6.056E+02
6.056E+02
1.004E+03
1.004E+03
Key line not found
"En = Manually edited
"M"
Decay Corr
2-Sigma
1.680E+02
30.50
1.658E+01
30.36
Manually accepted
"A" = Nuclide specific abn.
limit
tll511il

Sample ID : 1304132-06
Acquisition date
Page :
3
15-MAY-2013 08:02:58

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
3.988E+02 19.07
1.799E+01 3.988E+02
7.560E+00 3.064E+02
3.065E+02 35.03
7.170E+00 3.497E+02
3.497E+02 18.04
3 Valid Peaks
3.988E+02+/- 7.604E+01
Status
OK
OK
OK
19. 07%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

AM-241
59.54
Flag:
1 Valid Peaks
35.90*
Final Mean for

%Eff
2.305E+01 5.509E+02
5.509E+02 30.50
2.461E+01
5.509E+02+/- 1.680E+02 ( 30.50%)
5.462E+01
1 Valid Peaks ;
Status
OK
5.462E+01
30.36
OK
5.462E+01+/- 1.658E+01 ( 30.36%)
''*" ; Keyline
m.st t

Sample ID : 1304132-06
Acquisition date
4
Page :
15-MAY-2013 08:02:58

Nuclide
BA-133
TH-234
AM-241
Activity
(pCi/filter)
3.988E+02
5.509E+02
5.462E+01
Act error
MDA
(pCi/filter)
MDA error
Act/MDA
7.604E+01
1.680E+02
1.658E+01
1.915E+01
1.619E+02
1.550E+01
3.261E+00
1.338E+01
1.200E+00
20.824
3.403
3.522
Act error
MDA
(pCi/filter)
MDA error
Act/MDA
5.700E+00
1.129E+02
5.855E+00
1.832E+00
3.292E+01
9.353E+OO
1.668E+02
1.096E+01
3.221E+00
4.907E+01
1.436E+00
1.915E+01
2.087E-01
6.644E-02
5.541E+00
0.047
0.092
2.924
0.726
0.131
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
Key-Line
Activity K.L.
(pCi/filter) Ided
4.361E-01
1. 53 OE+01
3.205E+01
2.337E+00
6.440E+00

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
('
) It('--
DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP 130413207 GE2 - BAFIL_l91552.CN

PZ -112 -AS DIS
15-MAY-2013 00:00:00
1304132-07
FILTER
GE2
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
27.89
30.94
35.04
46.15
53.02
61.70
65.76
71.02
77.17
81.04
111.59
161.10
186.17
238.78
276.52
296.02
302.84
329.97
333.72
355.99
383.72
386.92
391.31
415.56
437.18
465.07
467.72
511.76
552.11
583.65
610.66
746.40
39
2030
512
37
76
154
83
21
29
816
174
21
35
28
57
22
159
2
56
547
86
157
40
36
91
6
11
16
6
7
12
10
152
107
108
156
159
157
50
56
40
50
108
136
62
36
41
17
23
10
17
38
24
33
21
27
10
0
6
10
1
1
7
0
3
3
3
0
0
0
1
1
2
2
0
0
0
0
0
0
0
0
0
0
1
1
0
0
0
1
1
0
0
0
0
0
(._
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1. 66
1. 37
1.68
1.62
2.48
1.24
1.47
1.48
1.64
1.38
1.38
1.48
1.91
2.17
1.72
3.23
1. 37
1. 51
1. 69
1.47
1. 86
1.52
1.74
1.11
1.52
1. 92
1. 93
1. 90
2.87
1.54
2.56
1.45
28.00
31.05
35.16
46.26
53.14
61.81
65.87
71.13
77.28
81.15
111.71
161.21
186.28
238.89
276.63
296.12
302.95
330.08
333.82
356.09
383.83
387.03
391.41
415.67
437.29
465.17
467.82
511.86
552.21
583.75
610.76
746.50
15-MAY-2013 08:23:20
l.OOOOOE+OO filter
0
BAFIL
0 00:15:00.31 0.0%
4096
10.00000
Left
Pw
Cts/Sec %Err
26
26
26
43
50
59
65
65
76
76
108
156
183
235
273
292
300
328
331
351
381
381
390
413
432
464
464
507
550
582
606
743
14
14
14
7
8
6
9
9
10
10
7
10
7
9
9
9
6
4
6
10
9
9
6
7
10
7
7
8
5
5
10
7
4.38E-02 61.7
2.26E+00 2.3
5.69E-Ol 5.6
4.12E-02 58.4
8.48E-02 30.9
1. 71E-01 15.1
9.22E-02 14.3
2.35E-02 59.9
3.21E-02 32.4
9.07E-01 3.7
1.93E-Ol 12.5
2.37E-021Q4.5
3.88E-02 40.9
3 .11E-02 43.0
6.28E-02 24.3
2.44E-02 40.6
1.77E-Ol 9.2
2.41E-03221.3
6.21E-02 17.7
6.08E-01 4.8
9.54E-02 15.9
1. 74E-Ol 9.7
4.48E-02 25.5
3.99E-02 29.1
l.OlE-01 12.3
6.46E-03 33.3
1.17E-02 49.1
1.81E-02 41.6
6.67E-03 48.8
7.99E-03 43.0
1.32E-02 51.5
l.llE-02 31.6
Fit
1.34E+01
2.38E+00
2.69E+00
l.OlE+Ol
1. 62E- 01
iil513

Sample ID : 1304132-07
Acquisition date

Nuclide Type
Nuclide
BA-133
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00 4. 13 OE+02
:
4.130E+02
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00 5.285E+02
~
~
Wtd Mean
Decay Corr
pCi/filter
4.131E+02
---------
Decay Corr
2-Sigma
0.785E+02
19.00
4.131E+02
NATURAL
Nuclide
Hlife
TH-234 4.47E+09Y
Flags: "K"
"E"
12.50%
FISSION
Hlife
10.50Y
Nuclide Type
32
28
4
Page :
2
15-MAY-2013 08:23:20
Wtd Mean
Decay Corr
pCi/filter
5.285E+02
---------
5.285E+02
5.285E+02
9.415E+02
9.416E+02
Keyline not found

Manually edited
"M"
"A"
Decay Corr
2-Sigma
1.670E+02
31.59
Manually accepted
Nuclide specific a.bn. limit
'il.514

Sample ID : 1304132-07
Acquisition date
Page :
3
15-MAY-2013 08:23:20

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
4.131E+02 19.00
1.799E+Ol 4.130E+02
7.560E+00 3.554E+02
3.554E+02 35.13
3.822E+02 17.89
7.170E+00 3.822E+02
3 Valid Peaks
4.131E+02+/- 7.849E+Ol
Status
OK
OK
OK
19.00%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag: "*"

%Eff
2.305E+Ol 5.285E+02
5.285E+02 31.59
1 Valid Peaks
Status
OK
5.285E+02+/- 1.670E+02 ( 31.59%)
Key line
J!l515

Sample ID : 1304132-07
Acquisition date
Page :
4
15-MAY-2013 08:23:20

Nuclide
BA-133
TH-234
Activity
(pCi/filter)
4.131E+02
5.285E+02
Act error
7.849E+01
1.670E+02
MDA
(pCi/filter)
1.915E+01
1.879E+02
MDA error
Act/MDA
3.261E+00
1.552E+01
21.568
2.813
MDA error
Act/MDA
1.478E+00
2.078E+01
1.993E-01
6.878E-02
5.878E+00
1.474E+00
0.004
0.159
2.488
1.028
-0.090
1. 005
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter) Ided
3.882E-02
2.885E+01
2.604E+01
3.428E+00
-4.662E+00
1.915E+01
Act error
5.484E+00
1.077E+02
5.613E+00
1.843E+00
3.251E+01
1.151E+01
MDA
(pCi/filter)
9.625E+00
1.810E+02
1.047E+01
3.335E+00
5.206E+01
1.905E+01
f!l516

Configuration
:
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
/1.--
DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP 130413208 GE3 BAFIL 191 50.CN

PZ-202-SS TOT
15-MAY-2013 00:00:00
1304132-08
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Pk I t
Energy
Area
Bkgnd
1
1
1
1
1
1
0
1
1
0
0
0
0
0
1
1
0
0
1
1
1
3
3
3
0
0
0
30.72
34.81
61.76
65.79
80.82
83.68
92.64
111.72
115.83
134.27
143.44
161.29
276.71
302.97
333.80
337.79
356.14
364.64
383.56
386.87
391.53
414.92
418.27
422.82
436.95
467.47
510.25
1858
415
230
102
740
15
51
178
45
18
25
35
38
120
56
25
484
16
109
187
57
36
32
15
104
31
16
124
83
92
80
86
67
99
56
52
55
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
~l
96
82
42
26
28
16
14
6
9
7
6
11
6
4
14
0
4
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1.37
1.45
1. 51
1.52
1.54
1.41
1.95
1.59
1. 60
1.98
1.41
1.23
1. 29
1. 36
1. 83
1. 83
1. 82
2.83
1.85
1. 87
1.88
2.29
2.01
2.30
1. 94
2.58
2.94
31.04
35.13
62.08
66.11
81.14
84.00
92.96
112.03
116.15
134.59
143.75
161.61
277.01
303.27
334.11
338.10
356.44
364.94
383.86
387.17
391.83
415.23
418.57
423.12
437.25
467.77
510.55
15-MAY-2013 08:03:34
l.OOOOOE+OO filter
0
BAFIL
0 00:15:03.76 0. 4%
4096
10.00000
Left
Pw
Cts/Sec %Err
27
27
58
58
77
77
15
15
16
16
15
15
7
13
13
7
9
7
8
7
11
11
8
6
17
17
17
18
18
18
11
7
7
2.06E+00 2.4
4.61E-Ol 6.2
2.56E-01 9.2
1.13E-01 17.8
8.22E-01 4.2
1.72E-02127.5
5.62E-02 35.1
1.98E-01 10.1
5.02E-02 29.3
2.04E-02 70.8
2.81E-02 72.7
3.90E-02 46.1
4.24E-02 33.5
1. 34E- 01 11.4
6.27E-02 18.9
2.77E-02 36.6
5.37E-Ol 4.8
1.83E-02 33.8
1.21E-01 11.5
2.08E-01 9.3
6.36E-02 16.0
4.04E-02 24.0
3.56E-02 24.2
1.71E-02 42.3
1.16E-01 12.0
3.44E-02 18.0
1.73E-02 32.8
91
108
108
132
140
159
273
300
330
330
354
362
380
380
380
409
409
409
432
464
508
Fit
9.19E+00
4.12E+00
6.88E+00
3.79E+00
4.20E+00
9.57E+00
2.15E+00

Sample ID : 1304132-08
Acquisition date

Nuclide Type
Nuclide
BA-133
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
3.545E+02
---------
Total Activity
:
3.545E+02
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 6.871E+02
---------
Total Activity
"E"
=
=
Wtd Mean
Decay Corr
pCi/filter
3.545E+02
---------
Decay Corr
2-Sigma
0.633E+02
17.86
3.545E+02
NATURAL
Nuclide
Hlife
TH-234 4.47E+09Y
Flags: "K"
14.81%
FISSION
Hlife
10.50Y
Nuclide Type
27
23
4
Page :
2
15-MAY-2013 08:03:34
Wtd Mean
Decay Corr
pCi/filter
6.871E+02
---------
6.871E+02
6.871E+02
1.042E+03
1.042E+03
Key line not found

Manually edited
Decay Corr
2-Sigma
1.344E+02
19.56
"M" =
"Au =
Manually accepted
m-s1s

Sample ID : 1304132-08
Acquisition date
Page :
3
15-MAY-2013 08:03:34

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
3.545E+02 17.86
1.899E+01 3.545E+02
6.222E+00 3.262E+02
3.262E+02 30.76
4.130E+02 16.64
5.860E+00 4.130E+02
3 Valid Peaks =
Status
OK
OK
OK
3.545E+02+/- 6.331E+01 ( 17.86%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

%Eff
2.648E+01 6.871E+02
6.871E+02 19.56
1 Valid Peaks =
Status
OK
6.871E+02+/- 1.344E+02 ( 19.56%)
Flag: "*" = Key line
lll519

Sample ID : 1304132-08
Acquisition date
Page :
4
15-MAY-2013 08:03:34

Nuclide
BA-133
TH-234
Activity
(pCi/filter)
3.545E+02
6.871E+02
Act error
MDA
(pCi/filter)
MDA error
Act/MDA
6.331E+01
1.344E+02
2.051E+01
1.356E+02
3.137E+00
7.284E+00
17.284
5.067
Act error
MDA
(pCi/filter)
MDA error
Act/MDA
1.117E+00
1.488E+01
7.988E-02
4.839E-02
4.438E+00
9.536E-01
0.101
-0.430
1.606
1.104
-0.234
1. 604
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter) Ided
9.883E-01
-7.760E+01
9.020E+00
3.754E+00
-1.287E+01
3.111E+01
5.915E+OO
1.212E+02
2.870E+00
1.804E+00
3.564E+01
9.839E+00
9.774E+00
1.805E+02
5.617E+00
3.402E+00
5.490E+01
1.940E+01

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
(rrr---
DKA100: [GAMMA.SCUSR.ARCHIVE]SMP- 130413209 GE3 - BAFIL 191553.CN

PZ-202-SS DIS
15-MAY-2013 00:00:00
1304132-09
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30.70
34.95
53.40
61.60
65.58
80.82
83.68
111.80
115.91
161.11
242.45
270.32
276.71
302.74
307.26
333.53
337.86
351.53
356.01
364.53
383.83
386.87
390.87
414.96
418.26
422.21
437.14
468.01
511.75
1965
491
49
275
107
775
27
232
83
22
6
12
69
119
31
99
37
13
537
22
109
237
39
50
36
11
105
25
28
75
80
68
81
93
82
61
54
53
72
64
31
30
16
26
6
9
3
9
10
17
15
13
11
11
11
2
9
2
2
2
2
2
2
1
1
3
3
0
0
0
0
3
3
1
1
2
2
0
1
1
1
3
3
3
0
0
0
c..
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
15-MAY-2013 08:23:53
1. OOOOOE+OO filter
0
BAFIL
0 00:15:03.61 0.4%
4096
10.00000
FWHM Channel
Left
Pw
Cts/Sec %Err
31.02
35.27
53.72
61.92
65.90
81.14
84.00
112.11
116.22
161.43
242.76
270.63
277.01
303.05
307.56
333.83
338.17
351.83
356.31
364.84
384.13
387.17
391.17
415.27
418.56
422.51
437.44
468.31
512.04
26
26
49
49
49
76
76
107
107
159
237
266
273
299
299
330
330
351
351
362
381
381
381
412
412
412
434
465
508
14
14
24
24
24
12
12
16
16
7
9
8
10
14
14
16
16
12
12
6
17
17
17
15
15
15
7
8
10
2.18E+00 2.3
5.45E-01 5.3
5.43E-02 33.7
3.06E-01 8.0
1.18E-01 17.8
8.61E-01 4.1
2.96E-02 75.0
2.58E-01 8.1
9.18E-02 20.6
2.47E-02 66.2
6.99E-03234.0
1.36E-02 82.7
7.67E-02 19.1
1.32E-01 10.3
3.41E-02 36.3
1.09E-01 10.8
4.12E-02 21.6
1.46E-02 27.7
5.97E-01 4.3
2.41E-02 31.8
1.21E-01 12.3
2.64E-01 8.1
4.36E-02 31.8
5.57E-02 19.8
4.04E-02 28.7
1.21E-02 64.6
1.17E-01 10.0
2.78E-02 28.3
3.12E-02 21.5
1.40
1. 54
1.64
1. 66
1.67
1.54
1.41
1.64
1.93
2.66
2.00
3.81
1. 96
1. 54
2.19
1.83
1.83
1. 84
1.48
1.88
1. 87
1. 87
1.88
2.29
2.29
2.30
1.86
1.71
3.41
Fit
7.05E+00
3.94E+00
7.97E+00
8.36E-01
2.23E+00
3.59E+00
1.97E+00
3.77E+00
5.77E+00

Sample ID : 1304132-09
Acquisition date

29
25
4
Page :
2
15-MAY-2013 08:23:53
13.79%

Nuclide
BA-133
Hlife
10.50Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 3.712E+02
Total Activity
3.712E+02
Wtd Mean
Decay Corr
pCi/filter
3.712E+02
Decay Corr
2-Sigma
0.660E+02
17.77
3.712E+02

Nuclide
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 8.206E+02
Total Activity
Wtd Mean
Decay Corr
pCi/filter
8.206E+02
8.206E+02
8.206E+02
1.192E+03
1.192E+03
Flags: "K" ; Keyline not found

"E" ; Manually edited
2-Sigma
Decay Corr
1.422E+02
17.33
"M" ; Manually accepted

"A" ; Nuclide specific abn. limit
W522

Sample ID : 1304132-09
Acquisition date
Page :
3
15-MAY-2013 08:23:53

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

3.712E+02 17.77
1.899E+01 3.712E+02
6.222E+00 3.230E+02
3.230E+02 29.12
5.860E+00 4.586E+02
4.587E+02 16.17
%Eff
3 Valid Peaks
Status
OK
OK
OK
3.712E+02+/- 6.596E+01 ( 17. 7n)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag:
.. *"

2.648E+01 8.206E+02
8.206E+02 17.33
%Eff
1 Valid Peaks
Status
OK
8.206E+02+/- 1.422E+02 ( 17.33%)
Key line
-19523

Sample ID : 1304132-09
Acquisition date
Page :
4
15-MAY-2013 08:23:53

Nuclide
BA-133
TH-234
Activity
(pCi/filter)
3.712E+02
8.206E+02
Act error
MDA
(pCi/filter)
MDA error
Act/MDA
6.596E+01
1.422E+02
2.122E+Ol
1.325E+02
3.246E+00
7.114E+00
17.491
6.195
Act error
MDA
(pCi/filter)
MDA error
Act/MDA
1.051E+00
1.572E+Ol
4.842E-02
4.052E-02
4.762E+00
1.007E+00
-0.202
-0.087
0.558
1.397
0. 451
1. 902
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter) Ided
-1.862E+00
-1.657E+01
1.900E+00
3.980E+00
2.658E+01
3.895E+01
5.951E+00
1.207E+02
1.783E+00
1.489E+00
3.408E+01
1.026E+01
9.203E+00
1.906E+02
3.405E+00
2.849E+00
5.890E+01
2.048E+Ol
(.__..VAX/VMS Peak Search Report Generated 15-MAY-2013 08:59:37.92

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
DKA100: [GAMMA.SCUSR.ARCHIVE]SMP_130413210 GE3 BAFIL 191556.CN

DUP07 TOT
15-MAY-2013 00:00:00
1304132-10
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
15-MAY-2013 08:44:17
1.00000E+00 filter
0
BAFIL
0 00:15:03.46 0.4%
4096
10.00000
Pk It
Energy
Area
Bkgnd
FWHM Channel
Left
Pw
Cts/Sec %Err
2
2
0
1
1
1
1
1
1
0
0
1
1
2
2
0
0
3
3
1
1
1
1
1
0
0
0
0
0
30.76
34.96
51.86
61.78
65.63
80.82
83.68
111.66
116.83
160.41
187.48
276.65
281.85
302.98
307.01
334.01
338.10
351.34
356.04
383.53
386.85
414.87
419.70
425.84
436.95
468.44
512.94
610.07
1022.61
1561
380
28
197
64
620
17
156
35
25
24
58
10
98
20
42
30
17
401
87
139
30
16
8
78
20
29
14
6
62
48
119
109
113
78
56
42
27
35
76
12
16
13
14
30
10
2
5
20
51
3
3
3
4
5
0
5
2
1. 38
31.08
1.59
35.28
2.55
52.18
62.10
1. 51
65.95
1. 52
1. 54
81.14
1.41
84.00
1.59 111.98
1.60 117.15
1. 53 160.72
3.01 187.79
1. 78 276.96
1. 78 282.16
1. 82 303.29
1.99 307.31
1.31 334.31
1.26 338.41
2.03 351.65
1.56 356.34
1. 87 383.83
1.87 387.15
1.89 415.17
1. 73 420.00
1. 90 426.14
1.72 437.25
1. 71 468.73
2.75 513.24
1.10 610.36
2.55 1022.88
26
26
50
58
58
76
76
107
107
158
182
274
274
298
298
330
337
351
351
381
381
411
411
411
433
465
509
606
1017
13
13
7
12
12
13
13
14
14
5
10
12
12
28
28
7
5
11
11
10
10
18
18
18
8
6
11
9
8
1.73E+00 2.6
4.22E-01 6.2
3.13E-02 66.2
2.19E-01 10.4
7.15E-02 27.8
6.89E-01 4.6
1.85E-02108.7
1.74E-01 10.4
3.84E-02 33.3
2.78E-02 40.7
2.68E-02 71.1
6.43E-02 15.3
1.07E-02 66.4
1.09E-01 11.9
2.22E-02 49.6
4.70E-02 26.7
3.32E-02 26.4
1.94E-02 21.5
4.46E-01 5.1
9.68E-02 15.8
1.55E-01 12.6
3.31E-02 22.4
1.73E-02 41.3
9.07E-03 55.4
8.67E-02 12.2
2.26E-02 27.7
3.22E-02 18.6
1.51E-02 42.9
6.39E-03 60.2
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
f/![lt--
Fit
4.95E+00
6.73E+00
6.01E+00
3.01E+00
3.14E+00
1.41E+00
3.83E+00
2.83E+01
5.41E+00
1~525

Sample ID : 1304132-10
Acquisition date

Nuclide Type
Nuclide
BA-133
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
2.970E+02
:
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
2.049E+03
1. 00
5.875E+02
Total Activity
=
2.970E+02
Wtd Mean
Decay Carr
pCi/filter
2.971E+02
---------
Decay Carr
2-Sigma
0.544E+02
18.31
2.971E+02
NATURAL
Nuclide
Hlife
PA-231 3.28E+04Y
TH-234 4.47E+09Y
Flags: "K"
"E"
17.24%
FISSION
Hlife
10.50Y
Nuclide Type
29
24
5
Page :
2
15-MAY-2013 08:44:17
---------
Wtd Mean
Decay Carr
pCi/filter
2.049E+03
5.875E+02
---------
2.637E+03
2.637E+03
2.934E+03
2.934E+03
Keyline not found

Manually edited
"M"
"A"
=
=
Decay Carr
2-Sigma
0.610E+03
29.77
1. 28 7E+02
21.91
Manually accepted
til526

Sample ID : 1304132-10
Acquisition date
Page :
3
15-MAY-2013 08:44:17

Nuclide
BA-133
Energy
81.00
302.84
356.01
%-Abn
33.00*
17.80
60.00
Final Mean for

%-Eff
1.899E+01 2.970E+02
2.971E+02 18.31
6.222E+00 2.648E+02
2.648E+02 31.44
5.860E+00 3.429E+02
3.429E+02 16.98
3 Valid Peaks =
Status
OK
OK
OK
2.971E+02+/- 5.440E+01 ( 18.31%-)

Nuclide
PA-231
Energy
9.28
10.11
283.67
302.67
%Abn
42.00*
20.20
1.60
2.30
Final Mean for

TH-234
63.29
Flag: "*" = Keyline
2 Valid Peaks =
3.80*
Final Mean for
Uncorrected
%Eff
pCi/filter
1.000E+02 ----- Line
1.000E+02 ----- Line
6.406E+00 2.831E+02
6.224E+00 2.049E+03
2.648E+01
Status
Absent
Absent
OK
OK
2.049E+03+/- 6.101E+02 ( 29.77%)
5.875E+02
1 Valid Peaks =
Decay Corr 2-Sigma

pCi/filter %Error
Out Of Range ---Out Of Range ---2.831E+02 134.04
2.049E+03 29.77
5.875E+02
21.91
OK
5.875E+02+/- 1.287E+02 ( 21.91%)

Sample ID : 1304132-10
Acquisition date
Page :
4
15-MAY-2013 08:44:17

Nuclide
BA-133
PA-231
TH-234
Activity
(pCi/filter)
Act error
2.971E+02
2.049E+03
5.875E+02
5.440E+01
6.101E+02
1.287E+02
MDA
(pCi/filter)
2.042E+01
3.260E+00
1.508E+02
MDA error
Act/MDA
3.123E+00
4.636E-02
8.098E+00
14.546
628.547
3.897
MDA error
Act/MDA
1.010E+00
1.545E+01
3.454E-02
4.516E+00
8.496E-01
0.123
-0.148
0.988
0.105
0.758
Nuclide
C0-57
CD-109
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter) Ided
1.089E+00
-2.781E+01
2.401E+00
5.877E+00
1.310E+01
Act error
5.253E+00
1.198E+02
1.296E+00
3.420E+01
9.957E+00
MDA
(pCi/filter)
8.843E+00
1.874E+02
2.429E+00
5.586E+01
1.728E+01

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP- 130413211- GEl BAFIL 191554.CN

DUP07 DIS
15-MAY-2013 00:00:00
1304132-11
FILTER
GEl
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
30.82
35.12
51.79
58.77
61.91
65.63
81.30
93.62
111.93
116.09
142.93
146.28
161.38
186.38
276.66
303.19
308.29
312.22
334.14
337.81
345.08
356.38
376.96
383.96
386.96
391.62
414.97
418.77
437.43
468.14
511.46
556.54
610.18
2113
462
44
18
247
92
809
28
237
53
14
23
37
20
65
166
36
12
93
24
11
606
11
105
211
50
37
25
96
33
29
7
7
75
44
94
61
74
88
145
100
33
25
37
54
54
79
36
15
12
8
14
8
12
24
12
10
6
1
20
19
5
6
10
2
5
3
3
0
1
1
1
0
0
2
2
3
3
0
0
0
5
5
5
2
2
0
0
1
1
1
1
1
1
0
0
0
0
0
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1.52
1. 62
2.23
1. 57
1.58
1.58
1.89
1.15
1. 81
1. 81
2.03
2.04
1. 31
1. 08
1. 25
1. 82
2.60
2.43
2.03
2.03
2.23
1. 88
1. 87
1. 88
1. 88
1. 88
1. 89
1.90
1.94
2.52
2.74
2.40
1.36
31.05
35.35
52.02
59.00
62.14
65.86
81.53
93.85
112.16
116.31
143.15
146.51
161.60
186.60
276.88
303.41
308.51
312.44
334.35
338.02
345.29
356.59
377.17
384.17
387.17
3 91. 83
415.17
418.98
437.64
468.34
511.66
556.74
610.37
Left
Pw
27
27
49
57
57
57
77
91
108
108
141
141
159
183
273
299
299
299
331
331
342
351
374
374
374
374
412
412
433
464
507
553
608
13
],.3
8
13
13
13
10
7
14
14
11
11
6
7
8
18
18
18
12
12
7
10
21
21
21
21
12
12
9
11
10
7
6
15-MAY-2013 08:42:25
l.OOOOOE+OO filter
0
BAFIL
0 00:15:00.28 0.0%
4096
10.00000
Cts/Sec %Err
2.35E+00
5.13E-01
4.93E-02
1.97E-02
2.74E-Ol
1.02E-Ol
8.99E-01
3 .11E-02
2.63E-Ol
5.93E-02
1.52E-02
2.60E-02
4.15E-02
2.18E-02
7.27E-02
1.85E-01
4.03E-02
1.29E-02
1.03E-01
2.67E-02
1. 18E- 02
6.73E-01
1. 21E-02
1.17E-01
2.35E-Ol
5.58E-02
4.15E-02
2.80E-02
1.06E-01
3.64E-02
3.22E-02
8.09E-03
7.92E-03
2.2
5.3
40.7
81.7
8.6
20.7
4.5
62.1
7.6
22.3
66.0
57.1
34.9
78.6
20.1
8.3
28.6
71.4
12.0
40.5
62.8
4.3
56.0
11.1
8.6
18.3
24.5
36.8
11.0
22.5
27.6
47.7
60.8
Fit
3.36E+01
6.79E+00
4.49E+00
2.06E+00
3.44E+00
5.16E-01
1.25E+Ol
4.23E+00

Sample ID : 1304132-11
Acquisition date

Nuclide Type
Nuclide
BA-133
Wtd Mean
Uncorrected
Decay pCi/filter
3.752E+02
1. 00
Total Activity
:
15.15%
FISSION
Hlife
10.50Y
Nuclide Type
33
28
5
Page :
2
15-MAY-2013 08:42:25
---------
3.752E+02
Wtd Mean
Decay Corr
pCi/filter
3.753E+02
---------
Decay Corr
2-Sigma
0.719E+02
19.16
3.753E+02
NATURAL
Nuclide
Hlife
TH-234 4.47E+09Y
AM-241
432.20Y
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
3.324E+02
1. 00
1. 848E+00
Total Activity
---------
Wtd Mean
Decay Corr
pCi/filter
3.324E+02
1. 848E+00
---------
3.343E+02
3.343E+02
7.095E+02
7.095E+02

Decay Corr
2-Sigma
0.596E+02
17.94
3.020E+OO
163.42


Sample ID : 1304132-11
Acquisition date
Page :
3
15-MAY-2013 08:42:25

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%-Eff
3.753E+02 19.16
1.963E+01 3.752E+02
5.708E+02 33.57
4.915E+00 5.707E+02
6.963E+00 4.353E+02
4.353E+02 17.47
3 Valid Peaks
Status
OK
OK
OK
3.753E+02+/- 7.189E+01 ( 19. 16%-)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

AM-241
59.54
1 Valid
35.90*
Final Mean for

%Eff
3.324E+02 17.94
5.865E+01 3.324E+02
Peaks~
8.010E+01
1 Valid
3.324E+02+/- 5.964E+01 ( 17.94%)
1.848E+00
Peaks~
Status
OK
1.848E+00 163.42
OK
1.848E+00+/- 3.020E+OO (163.42%-)
Flag: "*" = Keyline
U5.31

Sample ID : 1304132-11
----
Acquisition date
Page :
4
15-MAY-2013 08:42:25
Identified Nuclides
Nuclide
BA-133
TH-234
AM-241
Activity
(pCi/filter)
Act error
3.753E+02
3.324E+02
1.848E+00
7.189E+01
5.964E+01
3.020E+00
MDA
(pCi/filter)
1.813E+01
5.509E+01
4.262E+00
MDA error
Act/MDA
2.976E+00
1.765E+00
9.998E-02
20.697
6.034
0.434
MDA error
Act/MDA
6.115E+00
2.796E+01
3.632E-03
7.327E-02
6.722E+00
0.137
0.397
0.000
2.877
-0.209
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
Key-Line
Activity K.L.
(pCi/filter) Ided
2.676E+00
8.576E+01
O.OOOE+OO
1.122E+01
-1.153E+01
Act error
1.182E+01
1.408E+02
O.OOOE+OO
1.857E+00
4.123E+01
MDA
(pCi/filter)
1.959E+01
2.161E+02
1.933E-01
3.899E+00
5.522E+01
c:_

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_130413212
PZ-106-KS TOT
15-MAY-2013 00:00:00
1304132-12
FILTER
GEl
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30.83
35.06
53.06
61.89
65.76
81.21
93.15
111.98
116.09
161.02
185.11
219.77
276.96
302.95
307.62
324.95
333.96
337.96
356.36
364.75
383.92
387.04
391.56
414.82
418.16
422.16
437.36
467.87
510.89
2058
576
57
262
112
839
22
245
35
24
20
13
62
154
29
13
99
24
567
31
120
270
46
43
29
12
106
32
22
69
67
115
75
86
147
100
54
57
76
69
48
40
18
18
11
6
2
17
10
11
7
4
11
10
9
8
6
2
2
2
0
2
2
0
0
2
2
0
0
0
0
1
1
1
1
1
0
0
3
3
3
2
2
2
0
0
0
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1.48
1. 68
1. 87
1. 73
1.74
1.92
1.41
1. 81
1. 81
1.61
1.39
1.63
1.16
1. 64
1. 82
1. 84
1. 84
1.84
1.90
3.80
2.05
1. 86
2.25
2.08
2.09
2.09
1.89
1.75
1.89
31.06
35.29
53.29
62.12
65.99
81.44
93.38
112.21
116.31
161.25
185.33
219.99
277.18
303.17
307.83
325.17
334.17
338.17
356.57
364.96
384.13
387.25
391.77
415.03
418.36
422.36
437.56
468.07
511.08
Left
Pw
27
27
49
58
58
77
90
107
107
158
182
216
273
299
299
321
321
321
354
362
381
381
381
411
411
411
432
464
507
13
13
9
13
13
10
7
14
14
7
7
7
8
12
12
21
21
21
7
7
17
17
17
15
15
15
10
8
7
GEl_BAFI~~t~~CN
15-MAY-2013 09:01:17
l.QOOOOE+OO filter
0
BAFIL
0 00:15:00.28 0.0%
4096
10.00000
Cts/Sec %Err
2.29E+00
6.40E-Ol
6.38E-02
2.91E-01
1.25E-01
9.33E-01
2.39E-02
2.72E-Ol
3.92E-02
2.65E-02
2.22E-02
1.40E-02
6.89E-02
1. 71E-01
3.19E-02
1. 40E- 02
l.lOE-01
2.70E-02
6.30E-01
3.46E-02
1. 34E-01
2.99E-01
5.11E-02
4.81E-02
3.25E-02
1.33E-02
1.18E-01
3.55E-02
2.39E-02
2.2
4.7
36.1
8.0
16.7
4.4
80.4
8.0
38.4
63.8
72.2
94.9
21.8
9.0
28.3
45.0
10.6
33.5
4.4
24.7
10.2
7.1
28.0
18.7
32.4
59.6
10.9
22.1
23.7
Fit
3.66E+01
4.08E+00
2.65E+00
5.90E+00
3.31E+00
2.51E+01
3.39E+00
:8533

Sample ID : 1304132-12
Acquisition date

Nuclide Type
Nuclide
BA-133
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
3.892E+02
---------
Total Activity
:
3.892E+02
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
3.530E+02
---------
Total Activity
"KH =
"En =
Wtd Mean
Decay Corr
pCi/filter
3.892E+02
---------
2-Sigma
Decay Corr
19.04
0.741E+02
3.892E+02
NATURAL
Nuclide
Hlife
TH-234 4.47E+09Y
Flags:
13.79%
FISSION
Hlife
10.50Y
Nuclide Type
29
25
4
Page :
2
15-MAY-2013 09:01:17
Wtd Mean
Decay Corr
pCi/filter
3.530E+02
---------
3.530E+02
3.530E+02
7.422E+02
7.422E+02
Key line not found

Manually edited
Decay Corr
2-Sigma
0.590E+02
16.72
"Mn = Manually accepted
"A"

Sample ID : 1304132-12
Acquisition date
Page :
3
15-MAY-2013 09:01:17

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
3.892E+02 19.04
1. 963E+01 3.892E+02
4.915E+OO 5.296E+02
5.296E+02 34.39
6.963E+OO 4.079E+02
4.079E+02 17.49
3 Valid Peaks =
Status
OK
OK
OK
3.892E+02+/- 7.409E+01 ( 19.04%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

%Eff
5.865E+01 3.530E+02
3.530E+02 16.72
Vali~
Peaks=
Status
OK
3.530E+02+/- 5.901E+01 ( 16.72%)
lil535

Sample ID : 1304132-12
Page
Acquisition date
15-MAY-2013 09:01:17

Nuclide
BA-133
TH-234
Activity
(pCi/ filter)
3.892E+02
3.530E+02
Act error
7.409E+Ol
5.901E+Ol
MDA
(pCi/filter)
1.752E+Ol
5.509E+01
MDA error
Act/MDA
2.876E+00
1.765E+00
22.218
6.408
MDA error
Act/MDA
6.792E+OO
2.770E+01
3.632E-03
6.935E-02
7.397E+00
1.529E-01
-0.149
-0.265
0.000
2.638
0.102
1.565
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
-3.231E+OO
-5.681E+Ol
O.OOOE+OO
9.735E+00
6.202E+00
1.020E+Ol
Act error
1.415E+Ol
1.622E+02
O.OOOE+OO
1.760E+00
4.253E+Ol
3.406E+00
MDA
(pCi/ filter)
2.176E+Ol
2.141E+02
1.933E-01
3.690E+OO
6.076E+01
6.517E+00

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
..
(ttr--
DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP- 130413213 GEl BAFIL 19156l.CN

PZ-106-KS DIS
15-MAY-2013 00:00:00
1304132-13
FILTER
GEl
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
30.86
35.09
38.31
52.23
61.88
65.84
81.22
92.73
95.64
111.98
116.27
161.23
186.83
276.78
303.05
333.79
338.70
356.31
377.03
384.02
387.15
391.43
414.69
418.02
420.99
437.37
468.04
473.26
511.41
701.52
2045
490
29
72
234
109
841
33
18
214
33
16
25
53
160
103
19
566
16
136
211
48
38
30
10
136
31
8
22
9
63
47
32
101
78
89
135
48
52
58
69
82
52
41
15
26
29
11
12
21
16
18
13
13
10
8
5
3
4
2
4
4
4
0
1
1
0
1
1
3
3
0
0
0
0
0
0
0
0
2
2
2
4
4
4
0
0
0
0
0
(_
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1.42
1. 61
1. 86
2.06
1.58
1. 58
1.92
1. 62
1.62
1. 82
2.00
1.04
1.19
1. 25
1. 63
1.48
1. 26
1.95
2.54
2.06
1.83
2.07
2.08
2.52
2.53
1. 98
2.43
1. 00
2.78
2.50
31.09
35.32
38.54
52.46
62.11
66.07
81.45
92.95
95.87
112.20
116.50
161.46
187.05
277.00
303.27
334.00
338.91
356.52
377.24
384.23
387.36
391.64
414.90
418.23
421.20
437.57
468.25
473.47
511.61
701.70
Left
Pw
27
27
27
49
58
58
77
90
90
108
108
157
184
273
301
330
338
352
375
381
381
381
411
411
411
433
463
472
508
698
14
14
14
8
13
13
9
11
11
12
12
7
6
8
5
7
5
9
5
18
18
18
14
14
14
11
9
5
8
7
15-MAY-2013 09:24:26
l.OOOOOE+OO filter
0
BAFIL
0 00:15:00.28 0.0%
4096
10.00000
Cts/Sec %Err
2.27E+00
5.44E-01
3.19E-02
8.01E-02
2.60E-Ol
1.21E-01
9.35E-01
3.66E-02
1.95E-02
2.38E-01
3.68E-02
1.74E-02
2.80E-02
5.90E-02
1.78E-Ol
1.14E- 01
2.07E-02
6.29E-Ol
1.76E-02
1.52E-01
2.34E-01
5.32E-02
4.18E-02
3.29E-02
1. 16E- 02
1.51E-01
3.39E-02
8.33E-03
2.44E-02
1.04E-02
2.3
5.1
39.6
26.8
9.0
16.4
4.3
37.8
72.6
8.6
44.6
99.5
49.1
25.1
8.6
12.9
51.0
4.3
40.9
10.1
8.0
21.5
22.4
36.1
87.5
9.5
22.0
48.3
26.5
40.2
Fit
1.87E+01
2.67E+00
3.10E-Ol
1.68E+00
6.64E+00
8.28E+00
!'!537

Sample ID : 1304132-13
Acquisition date

Nuclide Type
Nuclide
BA-133
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
3.901E+02
---------
Total Activity
:
3.901E+02
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
3.151E+02
---------
Total Activity
nEn
=
=
Wtd Mean
Decay Corr
pCi/filter
3.901E+02
---------
Decay Corr
2-Sigma
0.738E+02
18.92
3.901E+02
NATURAL
Nuclide
Hlife
TH-234 4.47E+09Y
Flags: "K"
16.67%
FISSION
Hlife
10.50Y
Nuclide Type
30
25
5
Page :
2
15-MAY-2013 09:24:26
Wtd Mean
Decay Corr
pCi/filter
3.151E+02
---------
3.151E+02
3.151E+02
7.051E+02
7.052E+02
Key line not found

Manually edited
Decay Corr
2-Sigma
0.589E+02
18.71
"Mn = Manually accepted

"Au = Nuclide specific abn.
limit
W538

Sample ID : 1304132-13
Acquisition date
Page :
3
15-MAY-2013 09:24:26

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
1.963E+01 3.901E+02
3.901E+02 18.92
4.915E+00 5.508E+02
5.508E+02 33.96
4.067E+02 17.46
6.963E+00 4.067E+02
3 Valid Peaks =
3.901E+02+/- 7.379E+01
Status
OK
OK
OK
18. 92%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag:
"*" = Key line

%Eff
5.865E+01 3. 151E+02.
3.151E+02 18.71
1 Valid Peaks=
Status
OK
3.151E+02+/- 5.895E+01 ( 18.71%)

Sample ID : 1304132-13
Acquisition date
Page :
4
15-MAY-2013 09:24:26
Identified Nuclides
Nuclide
BA-133
TH-234
Activity
(pCi/filter)
3.901E+02
3.151E+02
Act error
7.379E+01
5.895E+01
MDA
(pCi/filter)
1.736E+01
6.226E+01
MDA error
Act/MDA
2.850E+00
1.995E+00
22.471
5.061
MDA error
Act/MDA
7.490E+00
2.533E+01
3.632E-03
6.775E-02
7.129E+00
1.506E-01
0.704
-0.078
0.000
2.259
0.215
1.181
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-I;ine
Activity K.L.
(pCi/filter) Ided
1.688E+01
-1.526E+01
O.OOOE+OO
8.145E+OO
1.261E+01
7.586E+00
Act error
1.402E+01
1.417E+02
O.OOOE+OO
1.765E+00
3.973E+01
3.540E+00
MDA
(pCi/filter)
2.399E+01
1.958E+02
1. 933E-01
3.605E+00
5.856E+01
6.421E+00

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
Pk It
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
2
2
0
2
2
0
0
0
0
0
0
0
0
0
0
0
0
0
3
3
3
0
0
0
0
0
0
0
0
DKA100: [GAMMA.SCUSR.ARCHIVE]SMP_130413214 - GE2 BAFIL 191555.CN

FB AT PZ-100-KS TOT
15-MAY-2013 00:00:00
1304132-14
FILTER
GE2
0 00:15:00.00
25
3.00000
No
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
Energy
Area
Bkgnd
FWHM Channel
Left
Pw
30.86
35.15
52.56
61.88
65.69
81.04
92.75
111.69
116.12
161.76
276.83
302.84
307.34
333.91
339.28
356.02
364.82
377.05
383.83
386.84
390.92
437.17
450.42
468.05
512.11
522.74
595.84
636.99
1062.05
1926
472
73
181
72
687
48
161
44
56
86
148
23
43
29
445
13
14
97
179
38
73
7
23
18
8
7
6
7
109
125
171
76
1.41
30.98
1. 53
35.27
1.62
52.67
1. 60
62.00
1.61
65.80
1. 28
81.15
1. 42
92.87
1.35 111.80
1.59 116.23
2.26 161.87
2.01 276.94
1.33 302.95
1.96 307.45
1. 78 334.02
1. 85 339.38
1. 33 356.12
1. 82 364.92
1.91 377.16
1.60 383.93
1.93 386.94
1.96 391.03
1. 62 437.27
1.15 450.53
1.46 468.16
2.13 512.21
1.27 522.84
1. 24 595.94
2.13
637.09
2.70 1062.14
26
26
49
58
58
77
88
108
115
158
272
300
306
330
337
352
361
374
382
382
382
433
447
464
507
520
592
633
1058
15
15
8
12
12
8
8
7
6
11
10
6
6
7
7
8
7
6
15
15
15
7
6
9
11
7
8
7
7
71
126
81
108
65
66
19
14
21
35
20
26
14
12
16
16
13
15
2
13
10
2
6
5
0
15-MAY-2013 08:43:21
1.00000E+00 filter
0
BAFIL
0 00:15:00.30 0.0%
4096
10.00000
Cts/Sec %Err
2.14E+00
5.25E-01
8.12E-02
2.01E-01
7.99E-02
7.63E-01
5.28E-02
1.79E-01
4.85E-02
6.22E-02
9.52E-02
1.65E-01
2.55E-02
4.80E-02
3.21E-02
4.94E-01
1.44E-02
1.52E-02
1. 08E-01
1.99E-01
4.22E-02
8.10E-02
7.22E-03
2.51E-02
1.98E-02
8.44E-03
8.21E-03
6.67E-03
7.78E-03
Fit
2.4 6.48E+00
5.9
33.4
10.5 1.06E+01
23.3
4.7
36.0
13.3
33.6
31.1
14.5
9.1
37.3
27.3
32.6
5.1
55.2
48.4
13.6 3.11E+00
9.4
26.4
14.7
49.3
36.1
42.9
52.8
67.7
74.9
37.8

Sample ID : 1304132-14
Acquisition date

29
25
4
Page :
2
15-MAY-2013 08:43:21
13.79%

Nuclide
BA-133
Hlife
10.50Y
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
3. 4 77E+02
Total Activity
3.477E+02
Wtd Mean
Decay Corr
pCi/filter
3.477E+02
Decay Corr
2-Sigma
0.692E+02
19.90
3.477E+02

Nuclide
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 6.218E+02
Total Activity
Flags: "K"
"E"
=
=
Wtd Mean
Decay Corr
pCi/filter
6.218E+02
6.218E+02
6.218E+02
9.695E+02
9.695E+02
Keyline not found

Manually edited
"M"
"A"
=
=
Decay Corr
2-Sigma
1.427E+02
22.95
Manually accepted
6542

Sample ID : 1304132-14
Acquisition date
Page :
3
15-MAY-2013 08:43:21

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
1.799E+01 3.477E+02
3.477E+02 19.90
3.312E+02 35.00
7.560E+00 3.312E+02
7.170E+00 3.106E+02
3.106E+02 18.31
3 Valid Peaks =
Status
OK
OK
OK
3.477E+02+/- 6.920E+01 ( 19. 90%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag: "*" = Keyline

%Eff
2.305E+01 6.218E+02
6.218E+02 22.95
1 Valid Peaks =
Status
OK
6.218E+02+/- 1.427E+02 ( 22.95%)

Sample ID : 1304132-14
Acquisition date
Page :
4
15-MAY-2013 08:43:21

Nuclide
BA-133
TH-234
Activity
(pCi/filter)
Act error
3.477E+02
6.218E+02
6.920E+01
1.427E+02
MDA
(pCi/filter)
1.899E+01
1.492E+02
MDA error
Act/MDA
3.234E+00
1.233E+01
18.307
4.168
MDA error
Act/MDA
1.464E+00
1.899E+01
2.032E-01
6.897E-02
5.455E+00
1.469E+00
0.183
-0.295
2.730
1. 280
-0.453
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
1. 739E+00
-4.884E+01
2. 913E+Ol
4.279E+00
-2.186E+01
1.838E+01
Act error
5.646E+00
1.229E+02
5.702E+00
1.795E+00
3.713E+Ol
1. 04 7E+01
MDA
(pCi/filter)
9.531E+00
1.654E+02
1.067E+01
3.344E+00
4.831E+01
1.899E+01
0. 968
c._

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
(ftl~
DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP 130413215 GE2 BAFIL J: 1559.CN

FB AT PZ-100-KS DIS
15-MAY-2013 00:00:00
1304132-15
FILTER
GE2
0 00:15:00.00
25
3.00000
No
Pk I t
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
30.89
35.01
45.52
52.47
61.65
65.93
80.90
91.75
111.88
115.75
185.32
276.56
280.23
283.23
303.01
306.55
333.55
337.92
356.02
383.80
386.84
391.25
414.04
418.48
422.23
433.72
436.95
463.94
468.07
511.08
610.63
699.37
2026
433
40
84
178
81
777
49
181
36
44
67
9
9
184
32
70
38
535
134
146
54
25
30
8
8
94
6
25
36
13
8
119
104
186
143
123
69
110
95
58
48
56
13
9
8
12
17
16
21
23
23
29
16
4
10
9
1
5
4
4
8
5
1
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
1
1
7
7
0
0
0
0
1
1
0
2
2
2
2
2
2
2
0
1
1
0
9
9
9
1
1
1
1
0
0
0
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1. 38
1. 39
2.51
2.55
1. 23
1.28
1. 30
3.13
1.55
1.56
1. 66
1. 93
1. 94
1. 94
1.66
1.97
1.99
1.97
1.41
1. 86
1.54
2.09
2.15
2.70
2.15
1.90
1.66
1. 92
1.93
1. 92
1. 65
1.27
31.01
35.13
45.64
52.59
61.76
66.05
81.01
91.87
112.00
115.86
185.43
276.66
280.34
283.34
303.12
306.66
333.65
338.03
356.13
383.90
386.95
391.36
414.15
418.58
422.33
433.83
437.05
464.05
468.18
511.18
610.73
699.47
Left
Pw
26
26
42
42
59
65
77
88
108
108
182
271
271
271
297
297
328
328
352
372
372
390
409
409
409
433
433
462
462
506
606
697
15
15
16
16
6
4
8
9
15
15
7
20
20
20
14
14
15
15
9
18
18
5
16
16
16
7
7
13
13
11
10
6
15-MAY-2013 09:01:56
l.OOOOOE+OO filter
0
BAFIL
0 00:15:00.31 0.0%
4096
10.00000
Cts/Sec %Err
2.25E+00
4.81E-01
4.47E-02
9.38E-02
1.97E-01
8.98E-02
8.63E-01
5.45E-02
2.01E-Ol
4.05E-02
4.89E-02
7.49E-02
l.OlE-02
1.05E-02
2.04E-Ol
3.58E-02
7.78E-02
4.27E-02
5.95E-01
1.49E-01
1.63E-01
6.01E-02
2.80E-02
3.37E-02
8.76E-03
8.93E-03
1.05E-01
6.27E-03
2.72E-02
4.00E-02
1. 44E- 02
8.77E-03
2.4
6.1
57.7
28.3
12.4
18.6
4.3
38.5
9.7
35.1
32.0
15.6
96.1
71.7
7.7
31.3
15.7
24.8
4.6
10.9
10.1
18.2
25.4
28.9
79.2
32.9
11.3
58.8
24.7
22.7
42.5
42.5
Fit
6.19E+00
1.93E+00
1.34E+00
1.99E+00
7.74E+00
1.29E+00
2.34E+00
3.23E+00
9.44E+00
7.59E-01

Sample ID : 1304132-15
Acquisition date

Nuclide Type
Nuclide
BA-133
Wtd Mean
Uncorrected
Decay pCi/filter
3.931E+02
1. 00
Total Activity
:
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 3.170E+03
1. 00
6.091E+02
Total Activity
=
=
---------
3.931E+02
Wtd Mean
Decay Corr
pCi/filter
3.931E+02
---------
Decay Corr
2-Sigma
0.766E+02
19.47
3.931E+02
NATURAL
Nuclide
Hlife
PA-231 3.28E+04Y
TH-234 4.47E+09Y
Flags: "K"
"E"
15.63%
FISSION
Hlife
10.50Y
Nuclide Type
32
27
5
Page :
2
15-MAY-2013 09:01:56
---------
Wtd Mean
Decay Corr
pCi/filter
3.170E+03
6.091E+02
---------
3.779E+03
3.779E+03
4.173E+03
4.173E+03
Keyline not found

Manually edited
"M"
"A"
=
=
Decay Corr
2-Sigma
32.03
1.015E+03
1.608E+02
26.40
Manually accepted

Sample ID : 1304132-15
Acquisition date
Page :
3
15-MAY-2013 09:01:56

Nuclide
BA-133
Energy
81.00
302.84
356.01
%"Abn
33.00*
17.80
60.00
Final Mean for

%"Eff
3.931E+02 19.47
1.799E+01 3.931E+02
4.098E+02 33.59
7.560E+00 4.097E+02
7.170E+00 3.736E+02
3.736E+02 17.73
3 Valid Peaks =
Status
OK
OK
OK
3.931E+02+/- 7.656E+01 ( 19.47%)

Nuclide
PA-231
Energy
9.28
10.11
283.67
302.67
%Abn
42.00*
20.20
1. 60
2.30
Final Mean for

TH-234
63.29
Flag:
"*" = Keyline
2 Valid Peaks =
3.80*
Final Mean for
Uncorrected
%"Eff
pCi/filter
1.000E+02 ----- Line
l.OOOE+02 ----- Line
7.750E+00 2.291E+02
7.562E+00 3.170E+03
2.305E+01
3.170E+03+/- 1.015E+03
6.091E+02
1 Valid Peaks =
Decay Corr 2-Sigma

pCi/filter %Error
Out Of Range ---Out Of Range ---2.291E+02 145.94
3.170E+03 32.03
6.091E+02
26.40
Status
Absent
Absent
OK
OK
32.03%")
OK
6.091E+02+/- 1.608E+02 ( 26.40%)

Sample ID : 1304132-15
----
Acquisition date
4
Page :
15-MAY-2013 09:01:56
Identified Nuclides
Nuclide
BA-133
PA-231
TH-234
Activity
(pCi/filter)
3.931E+02
3.170E+03
6.091E+02
Act error
7.656E+01
1.015E+03
1.608E+02
MDA
(pCi/filter)
1.800E+01
1.068E+01
1.652E+02
MDA error
Act/MDA
3.065E+00
2.033E-01
1.365E+01
21.838
296. 928
3.688
MDA error
Act/MDA
1.424E+00
1.948E+01
6.676E-02
5.424E+00
1.420E+00
-0.276
-0.154
0.920
-0.230
1.189
Nuclide
C0-57
CD-109
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
-2.561E+00
-2.606E+01
2.979E+00
-1.106E+01
2.183E+01
Act error
6.066E+00
1.222E+02
1.801E+00
3.515E+01
1.060E+01
MDA
(pCi/filter)
9.275E+00
1.697E+02
3.236E+00
4.804E+01
1.835E+01
S548
C..-

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
15-MAY-2013 00:00:00
1304132-16
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30.74
35.01
52.51
56.68
61.59
65.76
70.98
80.82
83.68
92.82
111.73
116.00
160.54
276.77
302.85
307.15
312.99
333.68
338.00
356.03
371.45
383.68
386.94
391.55
414.53
417.87
437.19
468.04
510.89
1889
538
58
20
326
148
28
705
26
54
225
64
61
65
133
39
14
64
23
456
12
74
200
41
38
14
84
19
20
76
81
98
54
74
77
68
66
43
110
56
62
52
47
24
24
20
22
34
19
30
14
3
3
5
5
5
5
0
1
1
0
5
5
0
0
3
3
3
3
3
0
0
6
6
6
1
1
0
0
0
J;/lv-,_..--
DKA100: [GAMMA.SCUSR.ARCHIVE]SMP_130413216 GE3 BAFIL 191: 60 :-(:N

PZ-100-KS TOT
7
12
15
15
10
2
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1. 49
1.60
2.18
1. 36
1. 90
2.22
1.18
1. 54
1. 41
1.87
1. 57
2.34
1. 64
2.05
1.57
2.19
2.19
1. 77
2.22
1.77
2.05
1. 84
1.83
2.01
1. 89
1. 90
1. 71
1. 21
2.19
31.06
35.33
52.83
57.00
61.91
66.08
71.30
81.14
84.00
93.14
112.04
116.31
160.85
277.08
303.16
307.46
313.29
333.99
338.30
356.33
371.75
383.99
387.24
391.86
414.83
418.17
437.49
468.34
511.19
Left
Pw
26
26
49
49
49
49
70
76
76
89
108
108
157
272
297
297
297
329
329
351
366
381
381
381
411
411
434
465
507
15
15
21
21
21
21
5
12
12
9
12
12
8
11
23
23
23
14
14
9
7
17
17
17
13
13
8
7
8
15-MAY-2013 09:02:47
1.00000E+00 filter
0
BAFIL
0 00:15:03.81 0. 4%
4096
10.00000
Cts/Sec %Err
2.10E+00
5.98E-01
6.43E-02
2.18E-02
3.62E-01
1.64E-01
3.11E-02
7.84E-01
2.85E-02
5.95E-02
2.50E-01
7.12E-02
6.74E-02
7.21E-02
1.48E-01
4.29E-02
1.55E-02
7.07E-02
2.50E-02
5.07E-01
1.29E-02
8.18E-02
2.22E-01
4.56E-02
4.19E-02
1.51E-02
9.37E-02
2.16E-02
2.23E-02
2.4
5.0
31.4
59.3
7.0
14.0
47.5
4.4
78.6
37.9
8.3
27.5
24.3
24.3
10.1
32.2
66.5
16.5
46.3
5.0
86.0
17.1
8.8
20.5
21.8
66.9
13.6
34.3
25.4
Fit
1.07E+01
4.34E+00
1.11E+01
7.98E-01
2.79E+00
3.17E+00
6.88E+00
2.21E+00

Sample ID : 1304132-16
Acquisition date

29
25
4
Page :
2
15-MAY-2013 09:02:47
13.79%

Nuclide
BA-133
Hlife
10.50Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 3.380E+02
Total Activity
3.380E+02
Wtd Mean
Decay Corr
pCi/filter
3.380E+02
Decay Corr
2-Sigma
0.612E+02
18.10
3.380E+02

Nuclide
Hlife
TH-234 4.47E+09Y
wto Mean
Uncorrected
Decay pCi/filter
1.00 9.730E+02
Total Activity
Flags: "K"
"E"
=
=
Wtd Mean
Decay Corr
pCi/filter
9.730E+02
9.730E+02
9.730E+02
1.311E+03
1.311E+03
Keyline not found

Manually edited
"M"
"A"
=
=
Decay Corr
2-Sigma
1.505E+02
15.47
Manually accepted

Sample ID : 1304132-16
Acquisition date
Page :
3
15-MAY-2013 09:02:47

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
1.899E+01 3.380E+02
3.380E+02 18.10
6.222E+00 3.600E+02
3.601E+02 28.82
3.897E+02 16.89
5.860E+00 3.897E+02
3 Valid Peaks
3.380E+02+/- 6.117E+01
Status
OK
OK
OK
18. 10%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

%Eff
2.648E+01 9.730E+02
9.730E+02 15.47
1 Valid Peaks =
Status
OK
9.730E+02+/- 1.505E+02 ( 15.47%)
~551

Sample ID : 1304132-16
Acquisition date
Page :
4
15-MAY-2013 09:02:47

Nuclide
BA-133
TH-234
Activity
(pCi/filter)
Act error
3.380E+02
9.730E+02
6.117E+01
1.505E+02
Act error
MDA error
Act/MDA
1.809E+01
1.231E+02
2.767E+00
6.610E+00
18.679
7.906
MDA
(pCi/filter)
MDA error
Act/MDA
1.053E+00
1.447E+01
4.804E-02
3.803E-02
4.228E+00
1.004E+00
-0.199
0.453
0.863
0.965
0.541
2.052
MDA
(pCi/filter)
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
-1. 832E+00
7.956E+01
2.916E+OO
2.581E+00
2.831E+Ol
4.189E+01
5.954E+00
1.103E+02
1.690E+00
1.463E+00
3.229E+01
1.047E+01
9.215E+00
1.755E+02
3.378E+00
2.674E+00
5.230E+01
2.042E+01
~552

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
(ltr~
DKA100: [GAMMA.SCUSR.ARCHIVE)SMP_130413217 GE3 BAFIL 191562.CN

PZ-100-KS DIS
15-MAY-2013 00:00:00
1304132-17
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
27.81
30.77
34.85
53.61
61.56
65.43
80.87
92.20
111.66
116.38
128.48
142.65
166.15
186.44
277.26
302.77
309.46
333.60
338.38
356.11
383.61
386.89
391.24
414.87
418.53
421.87
432.33
437.06
467.88
509.75
512.52
516.67
34
1884
470
42
269
60
838
33
204
36
22
17
26
23
51
127
7
79
24
472
92
218
37
31
25
20
6
89
24
7
14
5
44
76
76
108
149
153
147
67
48
36
42
72
3
3
3
0
0
0
0
0
2
2
0
0
0
0
0
0
0
7
7
0
3
3
3
1
1
1
2
2
0
1
1
1
55
66
38
21
55
18
12
29
12
12
9
10
8
7
0
3
4
1
2
3
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1.43
1.36
1.75
2.51
1. 38
1.42
1. 64
1. 28
1.75
1.76
2.19
1.38
1.49
1.41
1.75
1.52
0.97
2.67
1.98
1. 88
1. 83
1. 92
1.88
1.89
1.90
1.90
2.10
2.10
2.04
1.96
1. 96
1.97
28.13
31.09
35.17
53.93
61.88
65.75
81.19
92.52
111.97
116.69
128.79
142.96
166.46
186.75
277.57
303.07
309.77
333.90
338.68
356.41
383.91
387.19
391.55
415.17
418.83
422.17
432.64
437.36
468.18
510.05
512.82
516.97
15-MAY-2013 09:25:11
1.00000E+00 filter
0
BAFIL
0 00:15:03.76 0.4%
4096
10.00000
Left
Pw
Cts/Sec %Err
27
27
27
50
58
65
76
90
107
107
126
140
164
185
273
300
307
328
328
352
380
380
380
409
409
409
432
432
464
507
507
507
13
13
13
7
7
6
10
6
14
14
6
7
7
6
9
6
7
15
15
10
16
16
16
17
17
17
11
11
7
13
13
13
3.78E-02 26.3
2.09E+00 2.4
5.23E-01 5.3
4.64E-02 44.1
2.99E-01 9.7
6.69E-02 35.2
9.31E-Ol 4.4
3.64E-02 43.3
2.27E-Ol 8.8
4.06E-02 33.5
2.40E-02 52.2
1.84E-02 88.4
2.86E-02 51.5
2.5sE-02 60.0
5.62E-02 26.2
1.42E-01 10.5
8.06E-03174.3
8.81E-02 15.2
2.65E-02 33.8
5.24E-01 5.1
1. 03E-01 12.3
2.42E-01 8.2
4.16E-02 22.5
3.49E-02 24.1
2.79E-02 31.0
2.20E-02 37.2
7.01E-03
0.0
9.94E-02 11.8
2.69E-02 24.2
S.lOE-03 53.6
1.59E-02 34.4
5.25E-03 67.8
Fit
2.21E+01
3.64E+00
4.56E+00
1.04E+01
1.70E+00
1.08E+00
9.39E-01

Sample ID : 1304132-17
Acquisition date

32
28
4
Page :
2
15-MAY-2013 09:25:11
12.50%

Nuclide
BA-133
Hlife
10.50Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 4.015E+02
Total Activity
4.015E+02
Wtd Mean
Decay Corr
pCi/filter
4.015E+02
Decay Corr
2-Sigma
0.726E+02
18.08
4.015E+02

Nuclide
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
8.024E+02
1. 00
Total Activity
Wtd Mean
Decay Corr
pCi/filter
8.024E+02
8.024E+02
8.024E+02
1.204E+03
1.204E+03

2-Sigma
Decay Corr
1.651E+02
20.58


Sample ID : 1304132-17
Acquisition date
Page :
3
15-MAY-2013 09:25:11

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
4.015E+02 18.08
1.899E+01 4.015E+02
3.453E+02 29.44
6.222E+00 3.453E+02
5.860E+00 4.028E+02
4.028E+02 17.02
3 Valid Peaks
Status
OK
OK
OK
4.015E+02+/- 7.261E+01 ( 18. 08%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag: "*"

%Eff
2.64SE+01 8.024E+02
8.024E+02 20.58
1 Valid Peaks
Status
OK
8.024E+02+/- 1.651E+02 ( 20.58%)
Keyline
1i1555

Sample ID : 1304132-17
Acquisition date
Page :
4
15-MAY-2013 09:25:11

Nuclide
BA-133
TH-234
Activity
(pCi/filter)
Act error
4.015E+02
8.024E+02
7.261E+01
1.651E+02
MDA
(pCi/filter)
1.794E+01
1.584E+02
MDA error
Act/MDA
2.743E+00
8.510E+00
22.382
5.064
MDA error
Act/MDA
1.020E+00
1.405E+01
4. 671E-02
3.890E-02
4.204E+00
9.729E-01
-0.071
-0.449
0.994
1.189
0. 304
1.721
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
-6.372E-01
-7.644E+01
3.265E+00
3.252E+00
1.582E+01
3.406E+01
Act error
6.377E+00
1.321E+02
1.600E+00
1.383E+OO
3.415E+01
1.130E+01
MDA
(pCi/filter)
8.928E+00
1.704E+02
3.284E+00
2.735E+00
5.201E+01
1.979E+01
c__

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
[GAMMA.SCUSR.ARCHIVE]SMP_l30413218_GEl_BAFIL_l9I5'f~~
PEAKEFF V2.2
DKAlOO:
PEAK Vl6.9
S-53 TOT
15-MAY-2013 00:00:00
1304132-18
FILTER
GEl
0 00:15:00.00
25
3.00000
No
Pk I t
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
47.22
63.13
93.00
186.02
225.45
240.48
264.89
382.67
409.04
511.67
545.57
20
41
57
21
12
9
17
8
12
28
6
17
19
22
14
3
14
13
3
0
6
2
0
0
0
0
0
0
0
0
0
0
0
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
Left
Pw
47.45
63.36
93.23
186.24
225.67
240.69
265.10
382.87
409.25
511.87
545.77
44
60
90
182
223
235
260
380
406
506
543
6
8
7
7
6
7
12
6
8
12
5
1. 62
1.47
1. 24
1. 20
2.21
2.01
4.62
2.83
2.11
2.67
1. 70
15-MAY-2013 09:40:44
l.OOOOOE+OO filter
0
BAFIL
0 00:15:00.10 0.0%
4096
10.00000
Cts/Sec %Err
2.23E-02
4.57E-02
6.32E-02
2.33E-02
1.33E-02
1.02E-02
1.89E-02
8.89E-03
1.33E-02
3.10E-02
6.53E-03
Fit
39.9
23.8
19.2
36.7
36.8
75.3
47.7
49.2
28.9
25.8
56.8
:111557

Sample ID : 1304132-18
Acquisition date

Page :
2
15-MAY-2013 09:40:44
11
10
1
9.09%

Nuclide
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 5.548E+01
Total Activity
Flags: "K"
"E"
=
=
Wtd Mean
Decay Corr
pCi/filter
5.548E+01
5.54BE+01
5.548E+01
5.548E+01
5.548E+01
Keyline not found

Manually edited
"M"
"A"
=
=
Decay Corr
2-Sigma
2.656E+01
47.87
Manually accepted

Sample ID : 1304132-18
Acquisition date
Page :
3
15-MAY-2013 09:40:44

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

%Eff
5.865E+01 5.548E+01
5.548E+01 47.87
1 Valid Peaks =
Status
OK
5.548E+01+/- 2.656E+01 ( 47.87%")
Flag: "*" = Keyline
ll!55S

Sample ID : 1304132-18
Acquisition date
Page :
4
15-MAY-2013 09:40:44

Nuclide
TH-234
Activity
(pCi/filter)
5.548E+01
Act error
2.656E+01
MDA
(pCi/ filter)
2.796E+01
MDA error
Act/MDA
8.959E-01
1.984
MDA error
Act/MDA
3.721E+00
1.631E+01
1.958E+00
3.632E-03
4.869E-02
4.773E+00
5.458E-02
-0.217
-0.242
-0.280
0.000
1.800
0.348
0.090
Nuclide
C0-57
CD-109
BA-133
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
-2.588E+00
-3.046E+01
-3.346E+00
O.OOOE+OO
4.664E+00
1.363E+01
2.092E-01
Act error
7.020E+00
8.145E+01
7.160E+00
O.OOOE+OO
1.198E+00
2.092E+01
1.324E+00
MDA
(pCi/filter)
1.192E+01
1.261E+02
1.193E+01
1.933E-01
2.591E+OO
3.920E+01
2.327E+00

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
rtrr..___
DKAlOO: [GAMMA.SCUSR.ARCHIVE)SMP_130413219 GE3 BAFIL- 19 566.CN

S-53 DIS
15-MAY-2013 00:00:00
1304132-19
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Pk I t
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30.74
34.94
52.63
61.62
65.75
69.97
80.96
83.68
91.96
111.75
115.99
238.88
276.14
303.27
333.76
338.10
356.05
376.67
383.59
386.91
391.40
414.66
417.87
422.53
437.13
467.63
510.61
574.81
610.05
2079
482
112
236
128
17
840
15
36
227
45
14
67
104
58
34
483
21
85
204
51
27
21
11
75
36
11
10
7
89
123
64
68
69
78
57
90
44
26
38
21
56
14
15
19
16
13
7
1
13
10
7
15
4
0
0
1
2
2
0
2
2
2
2
2
0
2
2
0
0
0
3
3
0
0
4
4
4
1
1
1
0
0
0
0
0
C-
96
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1.41
1.58
2.16
1. 66
1.67
1.68
1.70
1.41
3.19
1. 75
1. 76
1. 74
1.62
1. 36
1.76
2.22
1.83
1. 66
1. 87
1. 93
2.09
1. 89
1.90
1.90
1. 86
1. 36
2.11
2.32
1.39
31.06
35.26
52.95
61.94
66.07
70.29
81.27
84.00
92.28
112.06
116.30
239.19
276.45
303.57
334.07
338.40
356.35
376.98
383.89
387.21
391.70
414.96
418.17
422.83
437.43
467.93
510.91
575.10
610.34
15-MAY-2013 09:41:18
l.OOOOOE+OO filter
0
BAFIL
0 00:15:03.64 0.4%
4096
10.00000
Left
Pw
Cts/Sec %Err
26
26
48
58
58
58
78
78
90
107
107
234
273
300
329
329
352
373
381
381
381
412
412
412
433
464
508
572
607
15
15
10
17
17
17
9
9
8
13
13
7
6
7
14
14
8
8
14
14
14
17
17
17
7
7
7
7
6
2.31E+00 2.3
5.35E-01 5.5
1. 25E- 01 20.7
2.62E-Ol 8.6
1.42E-01 13.3
1. 94E- 02 76.5
9.34E-01 3.7
1.64E-02138.4
4.05E-02 47.6
2.52E-01 8.0
4. 96E-02 25.9
1.57E-02 77.2
7.43E-02 16.3
1.16E-01 15.3
6.45E-02 16.5
3.78E-02 28.1
5.37E-Ol 4.8
2.32E-02 39.9
9.40E-02 14.6
2.27E-Ol 8.6
5.69E-02 16.6
2.99E-02 27.7
2.29E-02 41.1
1.20E-02 57.6
8.34E-02 14.3
3.94E-02 18.9
1. 22E- 02 30.2
1.11E-02 31.6
7.29E-03 48.8
Fit
9.77E+00
3.95E+00
1.70E+01
2.97E+00
4.16E+00
5.35E+00
2.39E+00
l!l561

Sample ID : 1304132-19
Acquisition date

29
25
4
Page :
2
15-MAY-2013 09:41:18
13.79%

Nuclide
BA-133
Hlife
10.50Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 4.028E+02
Total Activity
4.028E+02
Wtd Mean
Decay Corr
pCi/filter
4.028E+02
Decay Corr
2-Sigma
0.704E+02
17.48
4.028E+02

Nuclide
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 7.039E+02
Total Activity
Flags: "K"
"E"
7.039E+02
7.039E+02
1.107E+03
1.107E+03
Keyline not founO.

edited
= Manually
Wtd Mean
Decay Corr
pCi/filter
7.039E+02
"M"
"A"
=
=
2-Sigma
Decay Corr
1.293E+02
18.37
Manually accepted
tli562

Sample ID : 1304132-19
Acquisition date
Page :
3
15-MAY-2013 09:41:18

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
1.899E+01 4.028E+02
4.028E+02 17.48
6.222E+00 2.832E+02
2.832E+02 36.86
5.860E+00 4.128E+02
4.128E+02 16.68
3 Valid Peaks =
4.028E+02+/- 7.042E+01
Status
OK
OK
OK
17.48%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag:
"*" = Keyline
Uncorrected l)ecay Corr 2-Sigma

%Eff
2.648E+Ol 7.039E+02
7.039E+02 18.37
1 Valid Peaks=
Status
OK
7.039E+02+/- 1.293E+02 ( 18.37%)

Sample ID : 1304132-19
Acquisition date
Page :
4
15-MAY-2013 09:41:18

Nuclide
BA-133
TH-234
Activity
(pCi/filter)
4.028E+02
7.039E+02
Act error
7.042E+01
1.293E+02
MDA
(pCi/filter)
2.042E+01
1.207E+02
MDA error
Act/MDA
3.123E+00
6.485E+00
19.726
5.829
MDA error
Act/MDA
1.065E+00
1.433E+01
4.449E-02
3.820E-02
4.251E+00
9.166E-01
0.249
-0.378
0.934
1.160
0.008
1. 719
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
2.321E+00
-6.569E+01
2.922E+00
3.116E+00
4.262E-01
3.204E+01
Act error
5.396E+OO
1.328E+02
1.520E+00
1.430E+00
3.707E+01
9.650E+00
MDA
(pCi/filter)
9.319E+00
1.738E+02
3.128E+00
2.686E+00
5.259E+01
1.864E+01

Engineering Management Support, Inc.: West Lake OU-1

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ENGINEERING MANAGEMENT SUPPORT, INC.

West Lake OU-1

EBERLINE ANALYTICAL/OAK RIDGE LABORATORY

Chain of Custody & pH Check Sheet

Analytical Results Summary

Quality Control Sample Results Summary

Laboratory Technician's Notes

Analytical Data (Isotopic Uranium)

Analytical Data (Isotopic Thorium)

Analytical Data (Radium-226)

Analytical Data (Radium-228)

Barium-133 Analytical Tracer Data

Last Page Number

STANDARD OPERATING PROCEDURE

Eberline Services -Oak Ridge Laboratory

Eberline Services Work Order # _ _ _ _ _

First Technical Data Review

Second Technical Data Review

Data Entry/Electronic Deliverable

Electronic Deliverable Proof

Sample>l\AJ"'Iyzed within Holding Time

Client in Possession of Data

Technical/Clerical Corrections, Signatures Needed, Problems, Etc

Date package approved by:

REC'D APR 18 2.013

Chain of Custody Record

Send Report To:~J

(865) 481-0683 Phone (865) 4834621 Fax

-:Jdvv \:) ~.\0

14/J:>/13]0!;0 I&~ I 1 I )()11\J IY: I/ll X1 1>1

p2- goo -:Y5

Sampler (Print Name):

I I I XJI XJ I~ I~ I"Xl I.XJ

--l--~-eCeived by: (Signature)

- ------ --- sE Rv ,-c E: s

_____ -------- --------- -

Location circle one)

_________,_ ------ -------- ---- ------

------- ------------- ---- ---------"'""""" -------------------------..- -...---------------------------------

Printed: 4/18/2013 2:30PM

Oak Ridge Laboratory

Original Lab Deadline: 05/16/13

Location circle one)

l\u6 ~,Dj ((; '(3

(ffi., (l::t-t" '

Printed: 5/10/2013 9:23 AM

Oak Ridge Laboratory

Location circle one

-- ---- ----- -- ------ Relinquished by

---- --- --------- ----

Ptinted: 4/18/2013 2:30 PM -

Oak Ridge Laboratory

Location circle one)

------ ---- -------

Printed: 4/18/2013 2:30 PM

Location circle one)

Printed: 4118/2013 2:30 PM

Printed: 4/18/2013 1:00 PM

Internal Work Order

(Volumes, pH, & CPM)

Sample Receiving Report

I Rec Vol Ttl ~ M"v

06T PZ-112-AS TOT/