Spectral data for Compound A, problem II.

H NMR at 500 MHz

CHCl3

Expansion of
H NMR

Expansion of H NMR

Broad band decoupled C NMR, with couplings indicated

d
d
CDCl3
t
d
t

Infrared spectrum of A.

UV: max 258 nm ( 5500)

Mass spec: Parent ion at m/z = 148. M+1 = 11.3% M+2 = <1%