.Metrohm 701 KF Titrino Ton analysis A compact instrument with outstanding performance CAMBDAMED Kez, Laboratriumi miszerek és est Kereskedelem, seri 6 kalibilis 1026 Budapest, Hix 7. Tel: (6) THAIS, 200-419, Fa 3942879 E-mail lambda medelender hu£.Metrohm on analysis sic configuration The basic set-up of the KF Titrino comprises the fol- lowing components: + 701 KF Tino, the intol- ligent titrator that re quires minimum bench: space. + 703 Titration Stand compact auxiliary unit holds the tration vessel and sists contents; as- pirates spent solution and adds solvent, bath atthe push of a button. + Exchange Unit, avail able wih POTFEIPTFE: or ceramic stopcock and with burete volumes of 1,5, 10, 20 and 50 mL, with one burette tip each {or trating and dosing + Reagents: all commer. Cally available reagonts {or volumetric KF titra lion can be used. Use of the 703 Titration Standis recommended be- ‘cause itis compact and fa iltates iquic handling, However, the 701 KF Tirino can 9 courae also be used together withthe 728 Magnotic Expansion possibilities It you wish to connect a PC to the 70% KF Titvno, the ‘optional Metrodata menu programme is a great heip. allons the comprehensive remote contol of the instru ment and gives access to all its functions and status conditions. Furthermore, methods, instument settings, tivation data and results can be saved in the PC and transferred from there to other storage media of 1o a LIMS. Curves can be plotted in realtime or reproduced trom the stored tration data For comprehensive documentation of your analysis and for result reporis, printer can be connected; a balance makes possible the automatic transfer of sample weights ‘pon recorder can be used to record the fllowing types of curves: + volume vs, time + dit vs. time + measured voltage vs. time, Gaui Flexible approach ‘The 768 KF Drying Oven js available for those cases whore the water content of insoluble solids isto be de- termined and these cannat be introduced into the tra: tion vessel, e.g, because they react withthe reagents. ‘The integrated pump of the 768 KF Drying Oven deliv fer a constant flow of dry air that transports the water ‘given off by the sample heated in the oven tothe tia: tion vessel. The new «drift stop» endpoint criterion makes the oven method both more precise and fastr. ‘The oven method can iso be performed more economi cally using the 688 KF Drying Oven together with the (661 Pump UnitEasy operation, wide-ranging possibilities Routine operation ‘The separate keypad gives access to all the 701 KF ‘Titrino's functions. For routine operation, the Keypad can be aisconnected and the instrument operated via the keys ‘on its front pane +The START key gets the tration going + The STOP key stops the titration should this be nec- essary. + The DOS key allows the manually controlled dosing of reagent, e.g. when priming the Exchange Uni. |p normal routine operation, the START key is all you require... need we say anything more concerning ease. of operation? Yes, the 701 KF Tiina talks to you in your preferred language, be it English, Spanish, French or German, 701 KF Titrino am Progress in KF methodology ‘The 701 KF Titator combines extremely easy routine ‘operation with flexibility, thus allowing you to adapt the instrument configuration to your special requirements: + Apply bi-vottametic or bi-amperometric endpoint in- ication with freely selectable polarising current or voltage. *+ Choose between two stop criteria, namely the con: ventional «delay time» orthe novel «rit stop», which, combined withthe high rocolution of tho burete vole lume (10 000 inerements), yields fest yet highly pre- ‘ise results, + Define a start volume to further speed up the deter- mminations, + Take advantage of the «live keyboards to change pa- ramotors while titration isin progress. + Work with or without solution concitioning between determinations, with or without an automatic request for sample size and sample identification. + Inthe «conditioning» mode, get the current ct value without delay atthe push of a button, + Have diift taken into account for result calculation Os Metrohm lon analysis During tivation, the display shows the volume of rea- ‘gent used togetner with an analogue endpoint proximity indieator. This keeps you informed on the progress of the titration, required, the 701 KF Titrino will add up the reagent consumption in order to keap you from running out of Feagent or from unknowingly exhausting the butfer ca- pacity of the solvent when working with a two-compo- ont reagent. ORGThe 701 ina nutshell Dialogue languages English, Spanish, French or German are selectable Display Backlit LCD, 5 mm high, two lines of 24 charactors each Keypad Gives access toallthe functions ofthe 701 KF Tin ‘can be cisconnected for routine operation Tiation modes Kar Fischer tation Titer determination with water or methanolwater stangare Tutor dotorination with socium tartrate (NaQOC{CHOH),COONa » 2 H,0), Blank determination Statistics Mean value Absolute and relative standard deviation Delete a givon result and recalculate statistios Dat vate Can be callod up at any time inthe conditioning mace ‘and s displayed witnout delay Enopoint incication Bivaltametic or bi-amperomettic ‘Start volume 0.99.99 mL; addad at the start ofa titration in order to save time ‘Stop enteria 1. Dit siop Titration stops as soan as the end- Point voltage (current) and a preset ft value are reached 2. Delay time Titration stops as soon as the end point voltage (curent) has been thin the prescribed range for the olay time given Formula for result calculation (VB) TXE: esutt = ———— sxD where = dispensed KFR volume B= blank volume T= tive F = factor S = sample size D = divisor O.Metrohm Dit-compensated results Determinations can be caried outwith or without the dhift value boing taken into account for result calcula tion Units available forthe resuit °%, ppm, mail. g. mg, mL. malpe (mg per piece) ‘Reagent consumption adder Cumulative reagont consumption can be evaluates: 2 warming ie displayed whan tho olacted limi fe reached “Analogue output “The following curves can be obtained on an optional ‘en recorder: volume vs. ime, dit vs. time or meas: lured voltage vs. time Connection possbitis via QVC output 708 Tiration Stand or 728 (imax. 200 mA) Magnetic Stier RS 292C interface Printor and balance OR. ‘computer (PC) ‘Analogue output Pen recorder Conventional remote Control unit for KF Sample contol (JO lines) Changer or fora laboratory robat (each in conjunction ‘ath aPC) ‘Dimensions (including Exchange Unit) ‘wietn 150 mm Height 450 mm Depth 275 mm Weigh, inctuding accessories 66kgO.Metrohm Ordering information, options Recommended instrument combination 2.701.0010 701 KF Titrino Compact KF Tirator for fast and precise water determinations. Titration stop either by means of delay time or by drit criterion. Sofware-controlled polarisr for bivotametric or bi-amperometic indication. Easy operation thanks to dialogue in English, French, Spanish or German. Equipped with RS 232C ‘serial interface and remote control (JO lines). Including accessories. 2.703.010 703 Titration Stand (option) ‘Compact tiation stand with magnetic ster and integrated pump for adding rinsing solution or solvent and for aspirating the tation vessel contents. Including accessories, Options Stirrer 2.728.040 728 Magnetic Stirer including base plate, stand rod and electrode holder without power adapter, with {xed cable for attachment to the 701 KF Titrino ‘eco semimicro titration equipment 165618,000 Semimicro tiation equipment consisting of tiation vessel plus lid, adsorption tube, screw nipples for ‘electrodes, burette tips or spray nozzles; blind stoppers, septum stopper, spray nozzles, rinsing dis- ‘nibutor, tubing connections, aspiration ti and magnetic string bar Exchange Units with glass cylinder and flat PCTFE/PTFE stopcock 69014.113 Exchange Unit 1 mL with 1 tip each for tration and dosing, 1 L reagent bottle made of brown glass 63014.159 Exchange Unit 5 ml with 1 tip each for tation and dosing, 1 L reagent bottle made of brown glass 63014213 Exchange Unit 10 mL with 1 tip each for tivation and dosing, 1 L reagent bottio mado of brown glass 6.304223 Exchange Unit 20 mL with 1 ip each for tivation and dosing, 1 L reagent bottie made of brown glass 6.014.253 Exchange Unit 50 mL with 1 tp each for tivation and dosing, 1 L reagent botle mado of Brown glass The bottle attachments of the above Exchange Unis alow direct reagent dispensing rom botles with GLAS glass threads, i.e. 1 reagent bottles from Baker and Fiedel-ce Haén. For other typos of bottles, the folowing adapters are available: 16.1802.110 Siphon for Merck reagent battles with $40 thraad 8.1618.000 Adapter 32 mm/GL45 for Fluka reagent bottles and 500 mL. reagent bottles trom Riedel-de Haén 8.1618.010 Adapter 28 mm/GL45 for Fisher reagent bates Connecting cables for printers, balances and PC 6.2126.020 Connecting cable for Seiko thermal printer OPU 411-20 Type I 6.2125.050 Connecting cable for Gizen iDP 56X RS or Epson FX, LX, LO printers 5.2125.040 Connecting cable for Epson printer EX 800/.0 850 (DIN plug) 6.2125.030 Stackable plug for connecting printer and balance at the same time {6.2125.020 Connecting cable for Metter balances AE 011/012 and for AND balances (use Mottlor cable ME 23995 {or Meier balances AM, AT, PM and Meter interface LC-RS25 for Mettler balances AB, AG) 62125070 Cable for Sartorius balances MPB and MC1 (RS 232C) 6.2125.080 Cable for Procisa balancas {82125.060 Connecting cable for ISM” PUIX!/A and compatibles 6.2125.010 Adapter cable RS 292C 25 pin ~9 pin for IBM” AT and compatibies fited with a9 pin connector Metrodata PC programmes {6.6007.100 Menu programme (IBM-DOS) for the 701 KF Titrino 6.600800 VESUY 3.0 for Windows™ 95 or Windows™ NT, allows connection of 2 or more instruments (depend: ing on the version, includes haréware dongle ‘768 KF Drying Oven 2.768.0010 Oven for civing off moisture of solid and quid samples containing interfering or insoluble compounds. May be used with any volumetric or coulometric KF tater. Automatic motor-driven sample transfer, builtin air pump and two gas drying bottles, external gas connection (e.g. N,), inc. accessories, IGA Ga)