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Objectives of mixing
1.Simple physical mixture: simply the production of a blend of two
or more miscible liquids or two or more uniformly divided solids.
degree of mixing must commonly be of a high order, as many
such mixtures are dilutions of a potent substance (e.g. small
amount of steroid mixed in large amount of inert diluents)
correct dosage must be ensured
TYPES OF MIXTURES
Positive mixtures: are formed from materials such as
gases and miscible liquids, where irreversible mixing would
take place, by diffusion, without the expenditure of energy
provided time is unlimited.
such materials do not present any problems in mixing.
Negative mixtures: Suspensions of solids in liquids are
examples of negative mixtures
require work for their formation, and the components of
which will separate unless work is continually expended on
them.
Negative mixtures are more difficult to form and a higher
degree of mixing efficiency is required.
2. Shear mixing
In this type, forces of attraction are broken down so that
each particle moves on its own between regions of
different components and parallel to their surface
When shear occurs between regions of different
composition and parallel to their interface, it reduces the
scale of segregation by thinning the dissimilar layers.
Shear occur in a direction normal to the interface of such
layers is also effective since it too reduces the scale of
segregation.
using agitator arm or a blast of air.
3. Diffusive mixing
Mixing by diffusion is said to occur when random
motion of particles within a particle bed causes them to
change position relative to one another.
Such as exchange of positions by single particles result
in reduction of the intensity of segregation.
Diffusive mixing occurs at the interfaces of dissimilar
regions that are undergoing shear and therefore results
from shear mixing.
Micromixing
Classification of mixers :
a) Batch Type mixers
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Tumblers
V-cone blender or twin shell blender
Double cone blender
Tumbling blender with agitator mixing blade
Ribbon blender
Sigma blade mixer
Planetary mixer
Fluidized mixer
BATCH MIXERS
Agitator mixers
Agitator mixer for powders can take a similar form to
paddle mixers for liquids, but their efficiency is low.
Planetary motion mixers are effective, but special design
are to be preferred.
This type of mixers employs a stationary container to
hold the material and brings about mixing by means of
moving screws, paddles or blades.
Use: Since the mixers do not depend entirely on gravity
as do the tumblers, it is useful in mixing wet solids,
sticky pastes etc.
The high shear force effectively break up lumps or
aggregates.
MECHANISM-MIXING OF FLUIDS
1. Bulk transport the movement of a relatively large portion of
the material being mixed from one location in the system to
another constitutes bulk transport.
accomplished by means of paddles, revolving blades
2. Turbulent Mixing--the phenomenon of turbulent mixing is a
direct result of turbulent fluid flow, which is characterized by a
random fluctuation of the fluid velocity at any given point with in
the system.
fluid velocity at a given instant may be expressed as the vector
sum of its components in the x, y, and z directions.
Paddles
Propeller
Turbine
Characteristics:
For liquids of low viscosity simple flat paddles are used
and the emphasis is on radial and tangential
movements.
Paddles for more viscous liquids generally have a
number of blades, often shaped to fit closely to the
surface of the vessel, avoiding dead spot and
deposited solids.
An alternative design for the more viscous range of
liquids is the planetary motion mixer, which has a
smaller paddle that rotates on its own axis, but travels
also, in circular path round the mixing vessel.
Shaker Mixers
Mixers in this category cause the container material to be
agitated, either in an oscillatory or a rotatory movement.
Oscillatory movement: applied to small scale
rotatory movement: applied to large vessels