1.

Explain the application of UV - Spectroscopy

2. Explain the application of NMR - Spectroscopy
3. State Beers Law
4. State the application of visible spectroscopy.
5. State the application of Colorimetry.
6. State the difference between Single and Double Beam
spectrometers.
7. Give classification diagram for different chromatographic
techniques.
8. State the various methods of expressing precision and accuracy
of a result withrelevant relationships.
9. Write on (i) Determine and indeterminate errors.
(ii) Coupled vibrations and fermi resonance.
10. State (i) Normal distribution curves in error analysis.
(ii) Rejection criteria.
PART B Answer Five of the following questions :- (5 x 16 = 80)
11.A (i)With a neat sketch explain principle, working method and
application of visiblespectrometry. (10)
(ii)Explain application of colorimetry (6)
OR
B.Explain in detail about instrumentation ,operation,principle of
mass spectroscopy(16)
12.A(i) With necessary sketch explain principle, working method of
Infra red spectroscopy.(8)
ii) Give a note on Hooks law. (4)
iii) Discuss application of single and double beam spectrometers. (4)
OR
12.B(i) Explain with neat sketch and suitable example, the
application and theory of Massspectroscopy. (10)
ii) Explain the difference between Raman Spectra and IR Spectra. (6)
13.Ai) Explain in detail the merits and demerits of different types of
conductometrictitrationss. (8)
ii) Define the two important laws of conductance. (4)
iii) Give a note on Ion Selective electrodes. (4)
OR
13.Bi) Explain types of potentiometer titrations and also discuss the
advantages. (8)
ii) Explain thermometric titrations and their applications. (8)
14.A(i) Explain with neat sketch, working principle and method of
paper chromatography. (8)
ii) Discuss in detail on Gas chromatography. (6)
iii) What is chromatographic technique. (2)
OR
14.B(i) Discuss in detail about theory and application of thin layer
chromatography. (6)
ii) Explain in detail about Gel permeation chromatography. (6)

iii) Discuss the application of high performance liquid

chromatography. (4)
15.A(i) How the different spectrophotometers are prcised? (6)
(ii) Discuss in detail about errors in pH meters. (6)
(iii) What are the type errors occurred in visible spectrometry. (4)
OR
15.B(i) Give details how to get accuracy in Gas chromatography. (6)
(ii) Discuss in detail about errors in mass spectroscopy. (6)
iii) List out the methods of expressing the accuracy in NMR
spectroscopy. (4)