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SUPPLY, DELTVER, INSTALL AND COMMISSIONING ONE UNIT OF GAS

CHROMATOGRAPH-MASS SPECTROMETER SYSTEM WITH ACCESSORIES


General

The GCMS should be PC based software driven Quadruple system.


All gas flow including septum purge should be Electronic / digital controlled.
Display of all Gas Chromatograph and Autosapmler control should be at the GC or Data
system
The system comes with all sorts of accessories.

Gas Chromatograph (GC) System

The Gas Chromatographic performance should have retention time repeatability


<0.008% or < 0.0008 min,
Area repeatability should have <1% RSD
The system should comprise of the following modules:
Column Oven

Should be reliable, leak-free in-oven connections technology for analyzing complex


matrices, as well as providing gains in productivity and data integrity.
Column Oven technology should be provides direct rapid heating and cooling of capillary
columns for extremely fast analytical cycle times and higher productivity.
Should be capable of temperature programming.
Oven temperature controllable from Ambient temperature +4 C to 450 C with
Liquid N2 cryogenic cooling: 80 to 450 C and with
CO2 cryogenic cooling: 40 to 450 C.
Temperature setpoint resolution: 0.1 C.
Temperature accuracy: +- 1% of the set temperature.
Number of programming ramps/hold should be: 20 to 21 with Negative ramps.
Maximum achievable temperature ramp rate: 120 C/min
Maximum run time: 999.99 min
Cool down rate should be 450o C to 50o C in 4 minutes.
Ambient rejection: < 0.01 C per 1 C.

System should have capability to use Ultra Inert Column of conventional size and Ultra Inert inlet
liner.
Recommended maximum sustained column flow to MS should be 50mL/min
One unit of Split/Split less Sample Injection System with EPC:

Injection system should have gas saver mode to reduce gas consumption without
compromising performance.
System should have Electronic flow control to eliminate ghost peaks.
Split/splitless inlet should be change liners quickly and easily without special tools.
Split ratios range should be up to 7,500:1 to avoid column overload.
Pressure Range: 0 to 680 kPa.
Maximum operating temperature: 400C
Suited for diameter of columns should be 0.200 mm in 0 to 100psig pressure &
< 0.200 mm in 0 to 150 psig pressure.
Total flow setting range should be:
0 to 200 mL/min N2
0 to 1,250 mL/min H2 or He

Electronic Pneumatics Control (EPC) will be include:


Pressure set points adjusted by increments of 0.001 psi, with typical control 0.001 for
the range 0.000 to 99.999 psi; 0.01 psi for the range 100.00 psi to 150.00 psi
Inlet modules Pressure sensors: Accuracy: < 2% full scale, Repeatability:< 0.05 psi,
Temperature coefficient:< 0.01 psi/C, Drift: < 0.1 psi/6 months.
Flow sensors: Accuracy: < 5% depending on carrier gas, Repeatability: < 0.35% of
setpoint, Temperature Coefficient < 0.20 mL/min per C for He or H2; < 0.05 mL/min
NTP per C for N2.
Mass Spectrometer (MS):
The system should have Trace Ion Detection capability to reductions electric noise of scan MS
data to improve the quality of mass spectrum
It should have a mass range of 1.6 to 1050 u
System Scan rate should be capable up to 20,000 u/sec
Mass filter should be Monolithic hyperbolic quadrupole & The Mass Filter and Detector
should be placed on the same plate as Ion Source for better accessibility
Mass axis stability must be better than 0.10 u/48 h
Detector should be Triple Axis Detector with high energy dynode and long life electron
multiplier
Ion source temperature should be 150350 C
Quadrupole temperature should be 106200 C
It must should have Electron Ionization (EI), Positive Chemical ionization (PCI) and
Negative Chemical (NCI) ionization modes
Pumping system should have high vacuum pump to utilize an air-cooled high vacuum
turbo pump with minimum pumping speed of: 255 L/s turbo pump with 2.5 m3/hr
mechanical pump
Maximum analytical gas flow should be 1.5 mL/min (diffusion)
mL/min 4 mL/min (standard turbo)
Line voltage requirement: 220240 V 5%, 50/60 Hz

Instrument detection limit:


GCMS Instrument detection limit by High Efficiency Source 1.5 fg
Extractor for EI/CI source: 10 fg
Inert Plus EI: 10 fg Extractor
EI 24 fg Stainless steel source
Performance Specification:
-GCMS High Efficiency Source, EI Scan S/N:300:1, Sample concentration 0.1 pg/L OFN, using
Turbo molecular pump
-Extractor for EI,CI source for CI, EI Scan S/N:1,500:1, Sample concentration 1 pg/L OFN PCI
scan S/N: 1,200:1, NCI scan S/N: 2,000:1 using Turbo molecular pump
-Inert Plus EI, Extractor source, EI scan S/N: 1,500:1, Sample concentration:1 pg/L OFN using
Turbo molecular pump
-EI Stainless steel, EI scan S/N: 550:1, sample concentration:1 pg/L OFN using Turbo molecular
pump or diffusion
Data Communications should be:
LAN
Two analog output channels as standard
Remote start/stop
Keyboard control of the automatic liquid sampler.
Storage of 10 methods
Storage of five automatic liquid sampler sequences
Binary-coded decimal input for a stream selection valve

Auto Injection System for Liquid samples:

Fast injections are performed in less than 100 ms.


Support of 250- and 500-L syringes with optional Enhanced Sample Handling
Syringe Carriage
Variable sampling depth 2 to +30 mm above default
Minimum sample injection should be10 nL (with 1 L syringe)
Multiple injection mode 199 injections of specified volume
Post-injection dwell time 01 minute
Vial handling should be for 16 samples with injection tower and standalone turret
Sample solvent capacity should be
4 mL solvent vials
2 4 mL for injector tower with standalone turret
10 4 mL for injector tower with transfer turret.

Flame ionization detector(FID) with advanced electronic control modules, for packed &
capillary column
-Flame ionization detector (FID) which will responds to most organic compounds.
-Detector should have minimum detectable level (for tridecane): < 1.4 pg C/s
-Linear dynamic range: >107 ( 10%).
-Data rates up to 500 Hz accommodate peaks as narrow as 10 msec at half height.
-advanced electronic control modules for three gases:
- Air: 0 to 800 mL/min
- H2 : 0 to 100 mL/min
- Makeup gas (N2 or He): 0 to 100 mL/min
- will be available in two versions: capillary column optimized or adaptable for either packed or
capillary columns.
- Should be flameout detection and automatic reignition
-Capable for 450 C maximum operating temperature
Software:

The Data Processing software should file be automatic conversions on the MS Data
Analysis.
Long file name drag and drop function can be fully utilized.
System start-stop should be fully automated and controlled via the software. Reporting
format functions must be flexible format is based in users design. Like MS-words,
complete flexible function introduces ease and rapidness for making report and tidying up
the analysis result.
This software must be fully GLP/GMP and access software.
Strong security function, validation function for hardware &software and audit trial
function for data Instability are built in as a standard.
Reproducibility and recovery of concentration can be calculated and judgment of pass or
fail can be given. It is also possible to stop the run schedule based judgment.
Qualitative tools provide deconvolution and library searching across a wide selection of
general and application-specific libraries.
Quantitation capabilities to shorten path to results
Qualitative tools to extract the important information from your samples
The library search mode should be either by similarly search or index search Automatic
calculation of Retention Index for target compounds.
Should have Retention Time-Locking software, where retention time repeatability
will be <0.008% or < 0.0008 min
Should have sleep/wake mode(GC/MS) option for power saving
Outlier flagging and integration metrics help focus on problem compounds
Additionally Automatic adjustment of Retention Time in the analysis.

6. Environmental Conditions/Safety and Regulatory Certifications:

The instrument should be designed and manufactured under a quality system registered to ISO
9001. The instrument complies with international regulatory, safety, and electromagnetic
compatibility requirements.
Ambient operating temperature: 15 C to 35 C
Ambient operating humidity: 5% to 95%
Storage extremes: 40 C to 70 C
Line voltage requirements: 10% of nominal
Guaranteed support for the system shall have minimum ten year: value guarantee such that
vendor shall have ten years guaranteed parts and comprehensive service available or give
residual value credit for replacement
Standard: Instrument should be ISO & CE Certified.
Computer: Local or supply from manufacturer:
Intel Pentium IV Processor, Corei5
Original Intel Motherboard with Network Card
Operating System Windows7.
MS Office Original Licensed version
Printer: Laser Printer, Canon or HP
Gas & gas regulator: Required He gas with regulator should be supply by supplier.
UPS:

True On-Line UPS, Capacity 6 KVA


Input Voltage 1l8V AC - 300 V AC; Output:220 V AC,
Frequency Range: 46-54 Hz
Phase: Single Phase with ground
Power Factor :> 0.95
Back up time 120 min. (Full Load) and 180 min (Half Load)
Input voltage 118-300VAC
Output voltage: 220VAC. Frequency: 46-54 Hz
Output Wave form : Pure Sine wave

Accessories: Minimum required for 1 years trouble free operation.