Professional Documents
Culture Documents
Table of Contents
Chapter 1..........................................................................................................................................4
INTRODUCTION...........................................................................................................................4
1.1.
1.2.
Selection of Materials.......................................................................................................6
1.2.1.
Cement.......................................................................................................................6
1.2.2.
Fine aggregate............................................................................................................6
1.2.3.
Coarse aggregate........................................................................................................7
1.2.4.
Water..........................................................................................................................7
1.2.5.
Chemical Admixtures................................................................................................7
1.2.6.
Mineral admixtures....................................................................................................8
1.2.7.
Metakaolin.................................................................................................................8
1.2.8.
Flyash.........................................................................................................................9
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Chapter 1
INTRODUCTION
Concrete is a widely used structural material consisting essentially of a binder and mineral filler.
Department of Civil Engineering
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Concrete Strength
20 - 50Mpa
50 100Mpa
100-150Mpa
>150Mpa
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Selection of suitable ingredients for concrete having the desired rheological properties,
strength etc
Cement
Physical and chemical characteristics of cement play a vital role in developing
strength and controlling rheology of fresh concrete. Fineness affects water requirements for
consistency. When looking for cement to be used in High strength concrete one should choose
cement containing as little C3A as possible because the lower amount of C 3A, the easier to
control the rheology and lesser the problems of cement-super plasticizer compatibility. Finally
from strength point of view, this cement should be finally ground and contain a fair amount of
C3S.
1.2.2.
Fine aggregate
Both river sand and crushed stones may be used. Coarser sand may be preferred as
finer sand increases the water demand of concrete and very fine sand may not be essential in
High strength concrete as it usually has larger content of fine particles in the form of cement and
mineral admixtures such as fly ash, etc. The sand particles should also pack to give minimum
void ratio as the test results show that higher void content leads to requirement of more mixing
water.
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1.2.3.
Coarse aggregate
The coarse aggregate is the strongest and least porous component of concrete.
Coarse aggregate in cement concrete contributes to the heterogeneity of the cement concrete and
there is weak interface between cement matrix and aggregate surface in cement concrete. This
results in lower strength of cement concrete by restricting the maximum size of aggregate and
also by making the transition zone stronger. By usage of mineral admixtures, the cement concrete
becomes more homogeneous and there is marked enhancement in the strength properties as well
as durability characteristics of concrete. The strength of High strength concrete may be
controlled by the strength of the coarse aggregate, which is not normally the case with the
conventional cement concrete. Hence, the selection of coarse aggregate would be an important
step in High strength concrete design mix.
1.2.4.
Water
Water is an important ingredient of concrete as it actively participates in the
chemical reactions with cement. The strength of cement concrete comes mainly from the binding
action of the hydrated cement gel. The requirement of water should be reduced to that required
for chemical reaction of unhydrated cement as the excess water would end up in only formation
of undesirable voids in the hardened cement paste in concrete. From High strength concrete mix
design considerations, it is important to have the compatibility between the given cement and the
chemical/mineral admixtures along with the water used for mixing.
1.2.5.
Chemical Admixtures
Chemical admixtures are the essential ingredients in the concrete mix, as they
increase the efficiency of cement paste by improving workability of the mix and there by
resulting in considerable decrease of water requirement.
Different types of chemical admixtures are
Plasticizers
Super plasticizers
Retarders
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1.2.6.
Mineral admixtures
The major difference between conventional cement concrete and High strength
concrete is essentially the use of mineral admixtures in the latter. Some of the mineral admixtures
are
Fly ash
Metakaolin
Silica fumes
Mineral admixtures like Fly Ash, Metakaolin and Silica fume act as pozzolonic
materials as well as fine fillers, thereby the microstructure of the hardened cement
matrix becomes denser and stronger. The use of silica fume fills the space between
cement particles and between aggregate and cement particles. It is worth while noting
that addition of silica fume to the concrete mix does not impart any strength to it, but
acts as a rapid catalyst to gain the early age strength.
1.2.7.
Metakaolin
Metakaolin is refined kaolin clay that is fired (calcined) under carefully controlled conditions to
create an amorphous aluminosilicate that is reactive in concrete. Like other pozzolans (fly ash
and silica fume are two common pozzolans), metakaolin reacts with the calcium hydroxide
(lime) byproducts produced during cement hydration.
Calcium hydroxide accounts for up to 25% of the Ordinary Portland cement, and calcium
hydroxide does not contribute to the concretes strength or durability. Metakaolin combines with
the calcium hydroxide to produce additional cementing compounds, the material responsible for
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1.2.8.
Flyash
Most Flyash is pozzolanic, which means its a siliceous or siliceous-and-aluminous material that
reacts with calcium hydroxide to form a cement. When Portland cement reacts with water, it
produces a hydrated calcium silicate (CSH) and lime. The hydrated silicate develops strength and
the lime fills the voids. Properly selected fly ash reacts with the lime to form CSHthe same
cementing product as in Portland cement. This reaction of fly ash with lime in concrete improves
strength.. Special care must be taken in selecting fly ash to ensure improved properties in
concrete.
The most important benefit is reduced permeability to water and aggressive
chemicals. Properly cured concrete made with fly ash creates a denser
product because the sizes of the pores are reduced. This increases strength
and reduces permeability. Flyash also benefits precast concrete by reducing
permeability, which is the leading cause of premature failure, better
workability,
pumpability,
cohesiveness,
finish,
ultimate
strength,
and
durability. The fine particles in fly ash help to reduce bleeding and
segregation and improve pumpability and finishing, especially in lean mixes.
The main need of this hour is to develop high strength concrete, as economical as
possible and in an eco friendly manner.
The usage of supplementary materials like fly ash, silica fume, which are also a
byproduct of manufacturing industries, need a thorough understanding before dealing
them in the concrete mix.
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The usage of the superplasticizer in the current situation has to be dealt with utmost
importance.
The development of high strength concrete has to take care of the practical conditions
at the site, such as workability with increase in more complex structures.
HSC offers many advantages over conventional concrete. The higher compressive
strength of concrete results reduction in sizes of columns and increases available floor
space.
Admixtures are chemical substances which are added in small amounts just before or
during the mixing, and which helps to achieve higher strength by decreasing w/c ratio
at the same workability.
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1.4. Summary:
HSC has notorious advantages such as, high resistance to frost and deicer scaling
damage, ease of replacement, high toughness and impact resistance, ease of
compaction without segregation .
HSC works out to be economical, even though its initial cost is higher than that of
conventional concrete.
The use of HSC in construction enhances the service life of the structures and the
structures suffer less damage which would reduce the overall cost.
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Chapter 2
LITERATURE SURVEY
Literature review is a background studies that aims to review the critical points of recent
information. All of information gained via internet, journals, conference papers and books is
gathered to get a better idea and inspiration on this project.
In this chapter, the similar previous projects that developed by others is reviewed and discussed
to give critical review and also to choose the suitable equipment and method before starting the
project implementation.
Caijun Shi, Jianfan Xiao, Dehui Wang, Zhengyu Huang and Zhi Fang et.al[1], proposed A
review on high strength concrete: Raw materials and mixture design, high strength
concrete (HSC) refers to cement-based materials exhibiting compressive strength higher than 50
MPa, high ductility, and excellent durability. This paper reviews the theoretical principles, raw
materials, mixture design methods, and preparation techniques for HSC. Reduction in porosity,
improvement in microstructure, enhancement in homogeneity, and increase in toughness are four
basic principles for HSC design. Raw materials, preparation technique, and curing regimes have
significant influence on properties of HSC. The use of widely available supplementary
cementitious materials, such as fly ash, Metakaolin and slag for partial/complete
addition/replacement of cement, could significantly reduce the materials cost without sacrifice of
strength. The use of high temperature curing results in denser microstructure and better
performance than room temperature curing does, but obviously limits its applications of HSC.
Thus, preparation of HSC using widely available raw materials, common technology, such as
conventional casting and room temperature curing, are trends for production of HSC.
The main principles for HSC design are reduction in porosity, improvement in
microstructure, enhancement in homogeneity, and increase in toughness. Raw materials,
preparation technique and curing regimes have significant influence on properties of HSC. At the
same time, HSC with proper amount of those supplementary cementitious materials could
achieve compressive strength of 50100 MPa after normal curing regime.
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Nikhil K. Kulkarni et.al [2], proposed Strength of Plain Cement Concrete with Partial
addition of Cement by Metakaolin and replacement of Fly Ash in terms of improved
performance on compressive strength and flexural strengths, Experimental work was
carried out to investigate the effect of Metakaolin and Fly ash by partial addition and replacing
cement repectively and keeping same water cement ratio to ordinary concrete & Metakaolin and
fly ash. In this program 48 cube samples of size 150mmx150mmx150mm for different
percentages of addition of Metakaolin and Fly ash with partial replacement of cement were
casted and tested. The concrete mixes had 0%, 5%,10%,15% of Fly ash and Meta Kaolin,
replacing cement partially, so as to determine the best proportion, which would give maximum
compressive strength. Beam specimens were casted and tested for their flexural strength. The
dimensions of each beam were 750mmx150mmx150mm.The beams were tested on universal
testing machine to verify their flexural strength after 7days, 28 days of curing with single point
load. The results are compared with the beams of varying flexural strength of
Plain Cement Concrete, Plain Cement Concrete with Metakaolin & Fly ash.
Plain concrete is a brittle material and fails suddenly. Addition of Metakaolin & partial
replacement of Fly ash to concrete changes its brittle mode of failure into a more ductile one and
improves the concrete ductility. The compressive strength and flexural strength of concrete
increases with Metakaolin & fly ash content. It is true up to 12% replacement if we replace
cement by more than 12% strength starts reducing. Therefore it always preferable to use
Metakaolin & Fly ash with 10% replacement of cement and it gives us better result.
Martin Cyr, Minh Trinh et.al [3],
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Experimental work was carried out to investigate the effect of Fly Ash on Properties of Concrete.
In the study. Use of fly ash in concrete imparts several environmental benefits and thus it is
ecofriendly. It saves the requirement for the same strength thus saving of raw materials such as
limestone, coal etc required for manufacture of cement. Fly ash is pozzolanic material & it
improving the properties of concrete like compressive strength & Durability. The results obtained
are discussed and compared with the available literature.
It has been found that Slump loss of concrete increases with increase in w/c ratio of
concrete. For w/c ratio 0.35 without any admixtures, initial slump cannot be measured by slump
cone test as it is very less. Ultimate compressive strength of concrete goes on decreasing with
increase in w/c ratio of concrete. Slump loss of concrete goes on increasing with increase of
quantity of fly ash. Concrete with 7%, 9%, 12% replacement of cement with fly ash shows good
compressive strength for 28 days than normal concrete for 0.35 w/c ratio. But in the case of 20%
replacement of cement with fly ash ultimate compressive strength of concrete decreases.
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2.1. Summary
High strength concrete can be produced using conventional raw materials. Reduction in
porosity, improvement in microstructure, enhancement in homogeneity, and increase in
toughness are four basic principles for HSC design. Raw materials, preparation
technique, and curing regimes have significant influence on properties of HSC. The use
of widely available Supplementary cementitious materials, such as Flyash, Metakaolin
and Blast furnance slag for partial addition/replacement of cement, could significantly
distribution shifts towards finer pores and therefore the permeability of the paste reduces.
Fly ash is Pozzolanic material & it improving the properties of concrete like compressive
strength & Durability. Slump loss of concrete increases with increase in w/c ratio of
concrete. Ultimate compressive strength of concrete goes on decreasing with increase in
w/c ratio of concrete. Slump loss of concrete goes on increasing with increase of quantity
of fly ash. Partial replacement up to 12% increases the 28days compressive strength
whereas replacement above 15 20% reduces the 28 days compressive strength.
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Type
OPC
MK
Sio2
21.8
52.3
Al2O3
4.8
44.9
Fe2O3
3.8
0.4
CaO
63.3
0.5
SO3 MgO
Na2O
K2O
2.2
0.9
0.21 Development
0.46
of High Strength
Concrete
<0.1
0.2 using
0.12 Metakaolin
0.02
FAs
h
9.91
20.8
49.0
1.92
0.21
<0.01
4.11
<0.01
Chapter 3
MATERIAL AND TESTING
3.1. Materials
The following are the materials that were used in this investigation. The chemical composition of
ordinary Portland Cement (OPC), Metakaolin (MK) and Fly Ash are presented in Table 1.
Ordinary Portland Cement (OPC), 53 Grade conforming to BIS: 12269 1987 (specific
gravity: 3.15).
Metakaolin as mineral admixture in dry densified form was obtained from Chennai
conforming to ASTM C 1240 (specific gravity: 2.54).
FlyAsh as mineral admixture in dry densified form was obtained from RMC plant,
Tatuguni, Bengaluru conforming to ASTM C 1241 (specific gravity: 2.06).
Superplasticizer (chemical admixture) based on Polycarboxy ethylene PC 20 was
obtained from Bengaluru conforming to BIS: 9103 1999 and ASTM C-494.
Locally available quarried and crushed granite stones confirming to graded aggregate of
nominal size 12.5 mm as per table 2 of BIS: 383 1970 (specific gravity: 2.82) as Coarse
aggregates (CA).
Locally available river sand confirming to grading zone II of table 4 BIS: 383-1970
(specific gravity: 2.60, fineness modulus: 2.964) as fine aggregates (FA).
Table1. Chemical Composition of OPC, MK and FlyAsh
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Cement
FAsh
MK (g)
(g)
(g)
325.5
24.5
32.55
322.0
28.0
32.20
318.5
31.5
31.85
325.5
24.5
35.81
322.0
28.0
35.42
318.5
31.5
35.04
Cement (g)
FAsh (g)
325.5
24.5
39.06
322.0
28.0
38.64
325.5
24.5
318.5
31.5
38.22
322.0
28.0
318.5
31.5
325.5
24.5
322.0
28.0
318.5
31.5
325.5
24.5
322.0
28.0
318.5
31.5
Water
w/c ratio
Penetration
Initial setting
final setting
(ml)
( mm)
time (min)
time (min)
Development
126.24
0.33
6
37 of High Strength
750
Concrete
using Metakaolin
133.77
0.35
7
32
720
133.64
0.35
5
34
745
138.90
0.36
6
39
776
145.24
0.38
7
41
810
146.31
0.38
7
45
845
MK (g)
Water (ml)
w/c ratio
Penetration
Normal
132.28
0.34
7
39
768
consistency
139.92
0.36
6
36( mm)
754
32.55
126.24
0.33
6
0.33
139.78
0.36
6
40
806
32.20
133.77
0.35
7
0.35
31.85
133.64
0.35
5
0.35
35.81
138.90
0.36
6
0.36
35.42
145.24
0.38
7
0.38
35.04
146.31
0.38
7
0.38
39.06
132.28
0.34
7
0.34
38.64
139.92
0.36
6
0.36
38.22
139.78
0.36
6
0.36
3.2. Testing
3.2.1. Normal consistency
Normal consistency on binder materials i.e. Cement, Metakaolin, Flyash were carried out as
per BIS: 269 1989 and IS: 4031 1988 ( Part 4) by adding metakaoin by 10, 11, 12 percent
and replacing Flyash by 7, 8 ,9 percent. The details of the mix proportions and normal
consistency are given in table2 and detailed procedure is given in Appendix B.1.
Table2. Details of mix proportion for normal consistency
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FAsh
(g)
24.5
28.0
31.5
24.5
28.0
31.5
24.5
28.0
31.5
MK
(g)
32.55
32.20
31.85
35.81
35.42
35.04
39.06
38.64
38.22
Water
(ml)
126.24
133.77
133.64
138.90
145.24
146.31
132.28
139.92
139.78
w/c
ratio
0.33
0.35
0.35
0.36
0.38
0.38
0.34
0.36
0.36
Weight
(g)
701
722
730
734
724
732
738
750
722
Load
(KN)
50
85
85
80
85
80
100
120
70
Compressive
strength (N/mm2)
8.89
15.11
15.11
14.22
15.11
14.22
17.78
21.33
12.44
Aggregate crushing value of coarse aggregates was carried out as per BIS:2386- 1963(Part 4) on
aggregates passing through 12.5 mm and retaining on 6.3 mm. Test results showed low crushing
values under a uniform loading of 4 tonne per minute until the total loading of 40 tonne. The
details of the aggregate crushing value procedure are given in Appendix B.5.
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200
150
100
50
0
1.1000000000000001 2
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3.3. summary
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Chapter 4
METHODOLOGY
Conventional design that comprise of beams, columns, brick/block in fills and plastering have
inherent inefficiencies during construction.
So, Apart from using more intensive man power and longer construction duration, there are some
inherent difficulties in achieving high quality.
structures.
To build the superstructure of long span bridges and to enhance the durability of bridge
decks.
To satisfy the specific needs of special applications such as durability ,modulus of
elasticity and flexural strength.
Thus the challenges and difficulties involved in the construction push us into improvising the
concrete mix to achieve high strength concrete with new supplementary materials in the most
Eco-friendly manner.
So along these lines the research work was conducted as follows;
Literature Review
The first step in our research work was to gather and review relevant literature, mix design,
specifications, materials, new or existing products, research findings and current practice used to
produce high strength concrete.
The information gathered from papers, journals, on material properties, mix proportions and
other factors have been used in the understanding the development on high strength concrete.
The group members designed M60 mix. This mix was used to verify the resulting concrete
properties produced by the inclusion of different supplementary cementitious materials and
concrete admixtures.
Metakaolin was found to reduce permeability, increase early compressive strength, reduce
bleeding.
Fly ash was found to increased workability, reduce heat of hydration and increase ultimate
compressive strength of concrete.
Department of Civil Engineering
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Superplasticisers increased workability and decreased water demand for concrete mixes.
After all these we started casting of moulds as per the following schedule
We used 150x150mm size moulds for casting and compacted well by using vibrator and hand
compaction .Then moulds were filled and kept and after 24hours it was de moulded and kept for
curing in a tank of size 1.5x1m at optimum temperature of 27degree Celsius. This is done to
protect concrete from loss of moisture. Good curing can help mitigate the appearance of un
planned cracking.
Testing moulds was removed and testing was done under compressive testing machine to obtain
a required compressive strength .This process was carried out on 28th day from moulding.
Our aim was to develop High Compressive Strength hence casted only 150x150mm moulds. To
know the relation between compressive strength and tensile strength one can cast cylindrical
moulds for further study.
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MK
%
550
MK10
600
MK10
550
MK11
600
MK11
550
MK12
FAsh
%
W/C
ratio
Ceme
nt (kg)
FAsh
(g)
7%
0.29
2.25
172.0
225.0
Fine aggregates
(FA) kg
2.36mm
down
3.4
7%
0.32
2.25
172.0
225.0
3.4
1.74
2.86
8%
0.29
2.23
195.0
223.0
3.4
1.74
2.86
8%
0.32
2.23
195.0
223.0
3.4
1.74
2.86
9%
9%
7%
0.29
0.32
0.29
2.20
2.20
2.49
218.4
218.4
184.6
220.0
220.0
249.0
3.4
3.4
3.4
1.74
1.74
1.74
2.86
2.86
2.86
7%
0.32
2.49
184.6
249.0
3.4
1.74
2.86
8%
8%
9%
0.29
0.32
0.29
2.46
2.46
2.43
210.6
210.6
239.0
246.0
246.0
243.0
3.4
3.4
3.4
1.74
1.74
1.74
2.86
2.86
2.86
9%
0.32
2.43
239.0
243.0
3.4
1.74
2.86
7%
7%
8%
8%
9%
9%
7%
0.29
0.32
0.29
0.32
0.29
0.32
0.29
2.08
2.08
2.06
2.06
2.04
2.04
2.44
156.8
156.8
179.2
179.2
201.6
201.6
229.5
229.5
226.4
226.4
224.2
224.2
269.0
3.4
3.4
3.4
3.4
3.4
3.4
3.4
1.74
1.74
1.74
1.74
1.74
1.74
1.74
2.86
2.86
2.86
2.86
2.86
2.86
2.86
7%
0.32
2.44
269.0
3.4
1.74
2.86
184.
1
184.
1
MK
(g)
Coarse aggregates
(CA) kg
16mm 12.5mm
down
down
1.74
2.86
8%
8%
9%
0.29
0.32
0.29
2.42
2.42
2.39
210.2
210.2
236.4
266.1
266.1
263.2
3.4
3.4
3.4
1.74
1.74
1.74
2.86
2.86
2.86
9%
0.32
2.39
236.4
263.2
3.4
1.74
2.86
7%
0.29
249.
9
1.74
2.86
2.08
156.
8
3.4
2015-2016
SP
Water
(ml)
PC-20
(g)
33.7
5
33.7
5
33.4
5
33.4
5
33
33
37.3
5
37.3
5
36.9
36.9
36.4
5
36.4
5
31.2
31.2
30.9
30.9
30.6
30.6
787
36.6
840
36.6
36.3
36.3
35.8
5
35.8
5
927
839
926
31.2
722
Page 30
852
768
847
765
844
848
936
846
933
845
932
718
790
715
789
714
788
839
925
0.32
4.3. Summary
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790
715
789
714
788
851
931
843
930
842
929
Chapter 5
RESULTS AND ANALYSIS
5.1. Tests on fresh concrete
The variation in slump of different % replacement of FlyAsh in high strength concrete is given in
graph (a), (b) ,(c), (d), (e), (f) While observing the characteristic of fresh concrete of different
mixes, it was noted that, the concrete matrix when replaced by different proportion of MK and
FAsh, the workability increases with increasing quantity of FAsh. As a result, good workability
will be achieved. The increase in the percentage of replacement of FAsh results in more paste
volume, which also contributes to a reduction in bleeding. It is to be noted that all the mixtures
used in this work exhibited slumps less than 50 mm which is considered as very low.
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90
80
70
60
50
Slump in mm
Slump in mm 40
30
20
10
90
80
70
60
50
40
30
20
10
0
0
Fash7% Fash8% Fash9%
(a)
(b)
120
90
100
80
70
80
Slump in mm
60
60
50
40
Slump in mm 40
30
20
20
10
0
Fash7% Fash8% Fash9%
(c)
(d)
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80
80
70
70
60
60
50
50
Slump in mm 40
Slump in mm 40
30
30
20
20
10
10
0
Fash7%Fash8%Fash9%
(e)
0
Fash7% Fash8% Fash9%
(f)
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MK10%
MK11%
MK12%
100
90
80
70
60
28 Days Compressive Strength (N/mm2)
50
40
30
20
10
0
INFERENCE : 550 Kg/m3 cement for all percent of Flyash gives less strength compared to
600kg/m^3 cement content
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COMPARISION OF DIFFERENT MK %
(a)
(b)
For all percent of MK at varying percent 7,8,9 % FLYASH STRENGTH INCREASES TILL 8%
And thereafter starts increasing at a diminishing rate.
(c)
Department of Civil Engineering
(d)
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MK10%
MK11%
W/C - 0.29
W/C - 0.29
W/C - 0.32
W/C - 0.32
decreases drastically
MK12%
W/C - 0.29
W/C - 0.32
28 Days Co mpressive Strength (N/mm2)
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CONCLUSION
Based on the investigation carried out on the ternary blended HSC mixes, the following
conclusions are drawn.
A simplified mix design procedure for HSC using MK-Fash blend and superplasticizer is
formulated by combining BIS & ACI code methods of mix design and available
literatures on HSC
The optimum percentage of cement replacement by MK,Fash are 11%, 8% at W/C ratio
0.29
The BIS: 456-2000 code underestimates the flexural strength for HSC.
Use of MK & Fash in concrete reduces the workability in terms of slump.
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FUTURE SCOPE
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fck + 6.9
20.5 - 34.5
fck + 8.3
fck + 9.7
Less than 62
20-25
10-12.5
A.3. Estimation of
free water content
The water content to obtain the desired workability depends upon the amount of water and
amount of superplasticizer and its characteristics. However, the saturation point of the
superplasticizer is known, and then the water dosage is obtained based on table 3. If the
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0.6
0.8
1.0
1.2
1.4
(%)
Water dosage
(l/m3)
120 to 125
125 to 135
135 to 145
145 to 155
155 to 165
volume of concrete
10
12.5
20
2.5
2.0
1.5
25
1.0
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Cubic
Rounded
1050-1100
1100-1150
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The fine aggregate content per unit volume of concrete is obtained by multiplying the absolute
volume of fine aggregate and the specific gravity of the fine aggregate.
A.11. Moisture adjustments
The actual quantities of CA, FA and water content are calculated after allowing necessary
corrections for water absorption and free (surface) moisture content of aggregates. The volume
of water included in the liquid superplasticizer is calculated and subtracted from the initial
mixing water.
A.12. Unit mass of concrete
The mass of concrete per unit volume is calculated by adding the masses of the concrete
ingredients.
Standard consistency of cement is that consistency which will permit the vicat plunger to
penetrate to a point 5 to 7 mm from the bottom of the vicat mould.
PROCEDURE
1. Prepare paste of weighed quantity of Cement, Metakaolin, Fly Ash with a weighted
quantity of water.
2. Take care that the time of gauging is not less than 3 minutes, not more than 5minutes
and the gauging shall be completed before setting occurs.
3. Fill the vicat mould with this paste, the mould resting upon a non- porous plate.
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Setting time is the time interval for which the cement products remain in plastic
condition.
Initial setting time is regarded as the time elapsed between the moment that the water is
added to the cement to the time that the paste starts losing its plasticity.
Final setting time is the time elapsed between the moment the water is added to the e
time when the paste has completely lost its plasticity and has attained sufficient firmness
to resist certain pressure.
PROCEDURE
1. Prepare a neat cement paste by gauging 300gms of cement with 0.85 times the water
required to give a paste of standard consistency.
2. Take care that the time of gauging is not less than 3 minutes, not more than 5minutes
and the gauging shall be completed before setting occurs.
3. Start a stop- watch at the instant when water is added to the cement.
4. Fill the mould with the cement paste gauged as above the mould resting on a nonporous .
5. Fill the mould completely and smooth off the surface of the paste making it level with
the top of the mould. The cement block thus prepared in the mould is the test block
Determination of initial setting time:
1. Place the test blocks confined in the mould and rest it on the non-porous plate, under
the rod bearing initial setting needle, lower the needle gently in contact with the
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Specific gravity is the ratio between weights of a given volume of material and weight of
an equal volume of water.
PROCEDURE
1. Clean and dry the specific gravity bottle and weigh it with the stopper (W1).
2. Fill the specific gravity bottle with cement sample at least half of the bottle and weigh
with stopper(W2).
3. Fill the specific gravity bottle containing the cement, with kerosene ( free from water)
placing the stopper and weigh it (W3).
4. After weighing the bottle, the bottle shall be cleaned and dried again.
5. Ten fill it with fresh kerosene and weigh it with stopper (W4).
6. Remove the kerosene from the bottle and fill it with full of water and weigh it with
stopper (W5).
7. Calculate specific gravity using the formula
Specific gravity of cement , Sc=
(W 2W 1 )(W 4W 1)
( ( W 4W 1 ) ( W 3W 2 ) )(W 5W 1)
PROCEDURE
Take 200gm of cement and 600gm in the proportion 1:3 by weight in a pan.
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Crushing value of aggregates is a measure which relatively gives an idea of its resistance
to crushing under a compressive load applied gradually.
PROCEDURE
Coarse aggregate passing 12.5mm IS sieve and retained on a10mm. IS sieve and heated at 100 to
110C for 4 hours and cooled to room temperature.
1. Put the cylinder in position on the base plate and weigh it (W)
2. Put the sample in 3 layers, each layer being subjected to 25 strokes using the tamping rod,
and weigh it (W1)
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W 2 X 100
W 1W
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PROCEDURE
1.
2. Immediately after immersion the entrapped air is removed from the sample by lifting the
basket containing it 25 mm above the base of the tank and allowing it to drop at the rate
of about one drop per second. The basket and aggregate should remain completely
immersed in water for a period of 24 hour afterwards.
3. The basket and the sample are weighed while suspended in water at a temperature of 22
32C. The weight while suspended in water is noted (W1g).
4. The basket and aggregates are removed from water and allowed to drain for a few
minutes, after which the aggregates are transferred to the dry absorbent clothes. The
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W3
(W 3( W 1W 2 ))
1. The sample should be thoroughly washed to remove finer particles and dust, drained and
then placed in the wire basket and immersed in distilled water at a temperature between
22 and 32oC.
2. After immersion, the entrapped air should be removed by lifting the basket and allowing
it to drop 25 times in 25 seconds. The basket and sample should remain immersed for a
period of 24 + hrs afterwards.
3. The basket and aggregates should then be removed from the water, allowed to drain for a
few minutes, after which the aggregates should be gently emptied from the basket on to
one of the dry clothes and gently surface-dried with the cloth, transferring it to a second
dry cloth when the first would remove no further moisture. The aggregates should be
spread on the second cloth and exposed to the atmosphere away from direct sunlight till it
appears to be completely surface-dry. The aggregates should be weighed (Weight A).
4. The aggregates should then be placed in an oven at a temperature of 100 to 110 oC for
24hrs. It should then be removed from the oven, cooled and weighed (Weight B).
Water absorption = [(A B)/B] x 100%.
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Aggregate impact value is a measure of resistance to sudden impact or shock, which may
differ from its resistance to gradually applied compressive load.
PROCEDURE
2. The sample should be oven-dried for 4hrs. at a temperature of 100 to 110oC and cooled.
3. The measure should be about one-third full with the prepared aggregates and tamped with
25 strokes of the tamping rod.
4. Add two more layer in similar manner, so that the cylinder is full.
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6. The net weight of the aggregates in the measure should be determined to the nearest gram
(W ).
7. The cup of the impact testing machine should be fixed firmly in position on the base of
the machine and the whole of the test sample placed in it and compacted by 25 strokes of
the tamping rod.
8. The hammer should be raised to 380mm above the upper surface of the aggregates in the
cup and allowed to fall freely onto the aggregates. The test sample should be subjected to
a total of 15 such blows, each being delivered at an interval of not less than one second.
9. Remove the crushed aggregates from the cup and sieve it through 2.36mm IS sieve until
no further significant amount passes in one minute. Weigh the fraction passing the sieve
to an accuracy of 1gm. Also, weigh the fraction retained in the sieve.
10. Compute the aggregate impact value using formula,
Aggregate impact value=
W2
X 100
W1
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to ASTM C 1240)
Specific gravity is the ratio between weights of a given volume of material and weight of
an equal volume of water.
PROCEDURE
1. Clean and dry the specific gravity bottle and weigh it with the stopper (W1).
2. Fill the specific gravity bottle with cement sample at least half of the bottle and weigh
with stopper(W2).
3. Fill the specific gravity bottle containing the metakaolin, with kerosene ( free from water)
placing the stopper and weigh it (W3).
4. After weighing the bottle, the bottle shall be cleaned and dried again.
5. Ten fill it with fresh kerosene and weigh it with stopper (W4).
6. Remove the kerosene from the bottle and fill it with full of water and weigh it with
stopper (W5).
7. Calculate specific gravity using the formula
Specific gravity of cement , Sc=
(W 2W 1 )(W 4W 1)
( ( W 4W 1 ) ( W 3W 2 ) )(W 5W 1)
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to ASTM C 1240)
Specific gravity is the ratio between weights of a given volume of material and weight of
an equal volume of water.
PROCEDURE
1. Clean and dry the specific gravity bottle and weigh it with the stopper (W1).
2. Fill the specific gravity bottle with cement sample at least half of the bottle and weigh
with stopper(W2).
3. Fill the specific gravity bottle containing the flyash, with kerosene ( free from water)
placing the stopper and weigh it (W3).
4. After weighing the bottle, the bottle shall be cleaned and dried again.
5. Ten fill it with fresh kerosene and weigh it with stopper (W4).
6. Remove the kerosene from the bottle and fill it with full of water and weigh it with
stopper (W5).
7. Calculate specific gravity using the formula
Specific gravity of cement , Sc=
(W 2W 1 )(W 4W 1)
( ( W 4W 1 ) ( W 3W 2 ) )(W 5W 1)
Slump test is carried out to determine the workability of that concrete mix.
PROCEDURE
1. Mix the dry constituents thoroughly to get a uniform colour and then add water.
2. The internal surface of the mould is to be thoroughly cleaned and placed on a smooth,
horizontal, rigid and non-absorbent surface.
3. Place the mixed concrete in the cleaned slump cone in 4 layers each. Approximately in
height of the mould. Tamp each layer 25 times with tamping rod.
4. Remove the cone immediately, rising it slowly and carefully in the vertical direction.
5. As soon as the concrete settlement comes to a stop, measure the subsistence of the
concrete in cms, which gives the slump.
Appendix D: Test on hardened concrete
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The test specimens are stored in moist air for 24hours and after this period the specimens are
marked and removed from the moulds and kept submerged in clear fresh water until taken out
prior to test.
PROCEDURE
1. Remove the specimen from water after specified curing time and wipe out excess water
from the surface.
2. Take the dimension of the specimen to the nearest 0.2m.
3. Clean the bearing surface of the testing machine.
4. Place the specimen in the machine in such a manner that the load shall be applied to the
opposite sides of the cube cast.
5. Align the specimen centrally on the base plate of the machine.
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Rotate the movable portion gently by hand so that it touches the top surface of the
specimen.
7. Apply the load gradually without shock and continuously at the rate of
140kg/cm2/minute till the specimen fails.
8. Record the maximum load.
9. Calculate compressive strength of cement concrete using formula,
compressive strength=
Load
Area
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