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34]
M eth No. 5506 5515 5506 5515 2018 2538 2539 3507 1603 3506 2558 1300 2549 3800 2555 2506 1606 1003 2003 1019 7903 1606 2501 2539 1604 0801 5603 5602 9200 9201 2539 5601 5502 7401 1402 1405 1000 Flow Ra te ( L /m i n ) 2.0 2.0 2.0 2.0 0.1 - 1.5 0.01 - 0.05 0.01 - 0.05 0.1 - 0.5 0.01 - 0.1 0.2 - 1.0 0.01 - 0.2 0.01 - 0.2 0.01 - 0.05 0.1 - 2.0 0.01 - 0.2 0.2 0.01 - 0.2 0.01 - 0.2 0.2 - 1.0 0.01 - 0.2 0.2 - 0.5 0.01 - 0.2 0.01 - 0.1 0.01 - 0.05 0.01 - 0.2 28.3 1 0.2 - 1 NA NA 0.01 - 0.05 0.1 - 1 0.2 - 1.0 1-4 0.01 - 0.2 0.01 - 0.2 0.01 - 1.0 Vol. (L) min max Acenaphthene Acenaphthene Acenaphthylene Acenaphthylene A c e talde hyde A c e talde hyde A c e talde hyde A c e talde hyde Ac etic ac id A c e tic anhydride Ac eto in Acetone Acetone Acetone Acetone Ac eto ne cy an oh yd rin Ac eto nitr ile A c e tyle ne dic hlor ide A c e tyle ne te trabr o m ide A c e tyle ne te trac hlo r ide Ac ids , ino rg an ic ACN Ac ro lein Ac ro lein Ac rylo nitr ile Ae ro bic ba cte ria Alach lor A l ac hlo r A l ac hlo r A lac hlo r Aldehydes, screening Aldicarb Ald rin Alka line du sts A llyl alc oho l A llyl alc oho l A llyl c hlor ide PO LYN UC LEA R A RO M ATIC HYDR OC ARBO NS by H PLC PO LYN UC LEA R A RO M ATIC HYDROCARBONS PO LYN UC LEA R A RO M ATIC HYDR OC ARBO NS by H PLC PO LYN UC LEA R A RO M ATIC HYDROCARBONS ALIPHATIC ALDEHYDES A C E T AL D E HY D E A L D EH Y D E S, SC R E E N IN G A C E T AL D E HY D E AC ETIC AC ID A C E T IC A N H Y D R ID E AC ETO IN KETONES I V O L A TI LE O R G A N IC C P D S (Screen in g) ORG ANIC AND INORGAN IC GASES BY EXTR ACTIV E FTIR SPEC T R O MET R Y KETONES I AC ETO NE CY AN O HY DR IN AC ETON ITRILE H Y D R O C A R B O N S , H A L O G E N A TE D 1,1,2,2 !T E TR A B R O M O E T H AN E 1,1,2,2 !T E TR A C H L O R O E TH A N E AC IDS , INO RG AN IC AC ETON ITRILE AC RO LEIN A L D EH Y D E S, SC R E E N IN G AC RYLO NITRILE A ER O BIC B AC TE RIA by G C -F AM E ALA C HLO R in AIR CHLORINATED ORG ANONITROGEN H ER BIC ID ES (A IR SA M PL IN G ) CHLORINATED ORG ANONITROGEN HER BICIDES (HAND WAS H) CHLORINATED ORG ANONITROGEN HE RBIC IDES (DER M AL P ATC H)) A L D EH Y D E S, SC R E E N IN G ORG ANONITROGEN PESTICIDES A L D R IN & L IN D A N E ALKA LINE DU STS ALC O HO LS III ALCOHO LS COM BINED A L LY L C H LO R I D E 200 - 1000 200 - 1000 200 - 1000 200 ! 1000 1 - 15 1 ! 12 5-5 6 - 60 20 - 300 25 - 100 1 - 10 0.5 - 3 1-6 Inst r. D ep . 0.5 - 3.0 0.3 - 12 1 - 25 0.2 - 5 50 - 100 3.0 - 30 3.0 - 100 1 - 25 1.5 - 48 5-5 3.5 - 20 50 - 300 70 - 1750 12 - 480 NA NA 5-5 var-480 18 - 240 70 - 1000 1 - 10 2 - 10 16 - 100 ac eto nitr ile va r ies ac eto nitr ile va r ies ACN t ol t ol r ea g formic a r ea g Ac et-M eth C S2 t h erma l NA C S2 Et Ac M e C l/M e O H C S2 T HF C S2 H C O 3 /C O 3
2-
E x tr a c ti o n
Chemical
M e th od Na m e
A n a ly t ic a l T e c h n iq u e HPLC !FL/U V G C !FID HPLC !FL/U V G C !FID HP LC /UV G C !F ID G C !F ID /M S HPLC !U V G C !FID VIS G C -FID G C !FID TD /G C !M S FTIR G C -FID G C !NPD G C !FID G C !FID G C !FID G C !FID IC G C !FID G C !NPD G C !F ID /M S G C !FID G C -FID ELISA G C /E C D G C - EC D G C - EC D G C !F ID /M S HP LC - U V G C !E C N T it ra t ion G C !FID G C -FID G C !FID
Sampler P T F E & X A D !2 P T F E & X A D !2 P T F E & X A D !2 P T F E & X A D !2 SG-DNPH X A D !2 /H M P X AD -2 /H M P BuB CCT BuB A -C M S CCT TD Di r. R e a d A -C M S P or Q S CCT CCT SG PCT SG(washed) C C T lg X A D !2 /H M P X A D !2 /H M P CCT i m p a c to r SPE disk OV S-2 polyethylene bag PUF pad X A D !2 OV S-2 GFF & BuB PTFE CCT CCT CCT
M e C l/M e O H t ol t ol a c et/C S 2 hex/MTBE met h a nol reagent NA IPA/diazomethane t ol reagent isooct HCl IP A/C S 2 IP A -C S 2 bz
3/15/2003
MF!1
Chemical Al lyl glyc idyl ethe r A l lyl tric hlo r ide Alumina A l um inum A l um inum A l um inum A l um inum Am ine s, a liph atic Am ine s, a ro m atic Aminobenzene Aminobenzene 2 !A m ino e thano l 2 !A m ino e thano l 2-aminotoluene p !Am ino ph en yla rso nic ac id 2 !Aminotoluene Am m on ia Am m on ia n ! and s e c !Am yl ac etate n-Am yl ac etate Am yl ac etate iso-A my lace tate Aniline Aniline Aniline Anisidine Anthracene Anthracene Antimony Antimony p !Ar sa nilic ac id Ar se nic Ar se nic Ar se nic Ar se nic Ar se nic A r senic trio xide
M eth No. 2545 1003 0500 7300 7303 7301 7013 2010 2002 2002 2017 2007 3509 2017 5022 2002 6015 6016 1450 1450 2549 1450 2002 2017 8317 2514 5506 5515 7303 7301 5022 7900 7300 9102 7303 7301 7901
M e th od Na m e ALLYL GLYCIDYL ETHER HYDROC ARBONS, HALOG ENATED PARTICU LATES N.O.R . E LE M E NT S b y IC P E LE M EN TS by IC P (H O T B L O C K /H C l /H N O 3 D IG E S T IO N ) ELE M EN TS b y IC P (A Q UA RE G IA A SH IN G ) ALUMINUM & CPDS, as Al AM INE S, A LIPH ATIC AM INE S, A RO M ATIC AM INE S, A RO M ATIC A N IL IN E , o - TO L U ID I NE , A N D N I TR O B E N Z EN E AMINOETHANO L COM POUNDS I AM INO ETH AN O L C O M PO UN DS II A N IL IN E , o - TO L U ID I NE , A N D N I TR O B E N Z EN E A R S E N IC , O R G A N O ! AM INE S, A RO M ATIC AM M O NIA by VIS AM M O NIA by IC ESTERS I ESTERS I V O L A TI LE O R G A N IC C P D S (Screen in g) ESTERS I AM INE S, A RO M ATIC ANILINE , O -TOLU IDINE, & N I TR O B E N Z EN E ANALINE an d @ -TOLUIDINE in urine A N IS ID I NE PO LYN UC LEA R A RO M ATIC HYDR OC ARBO NS by H PLC PO LYN UC LEA R A RO M ATIC HYDROCARBONS E LE M EN TS by IC P (H O T B L O C K /H C l /H N O 3 D IG E S T IO N ) ELE M EN TS b y IC P (A Q UA RE G IA A SH IN G ) ARSENIC, organo! AR SENIC & compoun ds , a s As E LE M E NT S b y IC P ELEMENTS on WIPES E LE M EN TS by IC P (H O T B L O C K /H C l /H N O 3 D IG E S T IO N ) ELE M EN TS b y IC P (A Q UA RE G IA A SH IN G ) AR SENIC TR IOX IDE, as A s
Flow Ra te ( L /m i n ) 0.01 - 0.2 0.01 - 0.2 1-2 1-4 1-4 1-4 1-3 0.01 - 1.0 0.2 - 1.0 0.2 - 1.0 0.2 0.01 - 0.2 0.5 - 1.0 0.2 1-3 0.02 - 1.0 0.1 - 0.2 0.1 - 0.5 0.01 - 0.2 0.01 - 2 0.01 - 0.05 0.01 - 2 0.02 - 0.2 0.2 NA 0.5 - 1.0 2.0 2.0 1-4 1-4 1-3 1-3 1-4 NA 1-4 1-4 1-3
Vol. (L) min max 1.5 - 8 2 - 60 7 - 133 5 - 100 Se e Ta ble 5 - 100 10 - 400 3 - 30 30 - 150 30 - 150 5 - 50 4 - 24 5 - 300 5 - 50 50 - 1000 10 - 150 0.1 - 90 0.1 - 96 1 - 10 1 - 10 1-6 1 - 10 5 - 30 5 - 50 NA 24 - 320 200 - 1000 200 - 1000 Se e Ta ble 50 - 2000 50 - 1000 30 - 1000 5 - 2000 NA Se e Ta ble 5 - 2000 30 - 1000
E x tr a c ti o n
A n a ly t ic a l T e c h n iq u e G C !FID G C !FID Grav IC P !AES ICP-AES ICP-AES FAAS G C !FID G C !FID G C !FID G C -FID G C !FID IC G C -FID IC !HYAAS G C !FID VIS !Au to IC G C !FID G C -FID TD /G C !M S G C -FID G C !FID G C -FID H P LC /E C D HPLC !U V HPLC !FL/U V G C !FID ICP-AES ICP-AES IC !HYAAS HYAAS IC P !AES ICP-AES ICP-AES ICP-AES G FAAS
Sampler Tenax CCT P VC , ta re d MC EF MC EF MC EF MC EF SG SG SG GFF + SG SG IM P GFF + SG PTFE SG S G + H 2SO 4 S G + H 2SO 4 CCT CCT TD CCT SG GFF+SG NA X A D !2 P T F E & X A D !2 P T F E & X A D !2 MC EF MC EF PTFE MC EF MC EF Wipe MC EF MC EF MC EF
d ieth y l et h er CS2
!
H N O 3/HC lO 4 H C l /H N O 3 H C l /H N O 3 HNO3 H 2SO 4/a q M e O H Et h a nol Et h a nol Et h a nol M eO H/H 2O HSA et h a nol b u ffer Et h a nol H 2O H 2O C S2 C S2 t h erma l C S2 Et h a nol et h a nol Alk MeOH ac eto nitr ile va r ies H C l /H N O 3 H C l /H N O 3 b u ffer H N O 3/H 2SO 4/HC lO 4 H N O 3/HC lO 4 NA H C l /H N O 3 H C l /H N O 3 H N O 3/H 2O 2
3/15/2003
MF!2
Chemical Arsine A sbe sto s A sbe sto s A sbe sto s A sbe sto s A sp arta m e A sp ha lt fu m e Atrazine Atrazine Atrazine Atrazine Az ela ic a cid Azinphos methyl Ba cte ria B[a]P B[a]P Bar ium Bar ium Bar ium Bar ium Benomyl Be nzalde hyde Benz[a]anthracene Benz(a)anthracene Benzene Benzene Benzene Benzene Benzene Be nzene so lubles 1, 3-be nze ne diol Be nzidine D ye s Benzidine Benzo[a]pyrene Benzo(a)pyrene
M eth No. 6001 7400 7402 9000 9002 5031 5042 5602 8315 9200 9201 5019 5600 0801 5506 5515 7056 9102 7303 7301 5601 2549 5506 5515 2549 3700 1501 1500 3800 5042 5701 5013 5509 5506 5515 A R S IN E
M e th od Na m e
Flow Ra te ( L /m i n ) 0.01 - 0.2 0.5 - 16 0.5 - 16 NA NA 1-3 1-4 0.2 - 1 NA NA NA 1-3 0.2 - 1.0 28.3 2.0 2.0 1-4 NA 1-4 1-4 0.1 - 1 0.01 - 0.05 2.0 2.0 0.01 - 0.05 > 0.02 0.01 - 0.2 0.01 - 0.2 0.1 - 2.0 1-4 0.2 - 1 1-3 0.2 2.0 2.0
Vol. (L) min max 0.1 - 10 400 - va r 400 - va r NA NA 70 - 1200 28 - 400 12 - 480 NA NA NA 200 - 1000 12 - 240 50 - 300 200 - 1000 200 - 1000 50 - 2000 NA Se e Ta ble 50 - 2000 var - 480 1-6 200 - 1000 200 - 1000 1-6 80% vol 5 - 30 2 - 30 Inst r. D ep . 28 5 - 160 150 - 500 20 - 100 200 - 1000 200 - 1000
E x tr a c ti o n
A n a ly t ic a l T e c h n iq u e G FAAS PCM TEM XR D PLM HPLC !U V G RA VIM ETR IC G C /E C D GC-M SD G C - EC D G C - EC D G C !FID G C !FPD G C -FID HPLC !FL/U V G C !FID FAAS ICP-AES ICP-AES ICP-AES HP LC - U V TD /G C !M S HPLC !FL/U V G C !FID TD /G C !M S GC G C !FID G C !FID FTIR Grav G C -FID HPLC !U V HPLC !U V HPLC !FL/U V G C !FID
Sampler CCT MCEF open MCEF open bu lk bu lk PTFE Tared PTFE OV S-2 Urine polyethylene bag PUF pad P VC O VS !2 i m p a c to r P T F E & X A D !2 P T F E & X A D !2 MC EF Wipe MC EF MC EF OV S-2 TD P T F E & X A D !2 P T F E & X A D !2 TD air bag CCT CCT Di r. R e a d Tared PTFE OV S-7 PTFE GFF P T F E & X A D !2 P T F E & X A D !2
HNO3 NA NA NA NA eluent benzene reagent NA NA IP A/ diazomethane Et h a nol t ol/a cet hex/MTBE ac eto nitr ile va r ies H 2O NA H C l /H N O 3 H C l /H N O 3 reagent t h erma l ac eto nitr ile va r ies t h erma l NA C S2 C S2 NA benzene met h a nol H 2O triethyl amine /M e O H ac eto nitr ile va r ies
A S BE ST O S F IB ER S b y PC M ASBESTOS FIBERS by TEM ASBESTOS, CHRYSOTILE b y XR D ASBES TOS (bulk) by PLM A SP AR TA M E B E N Z EN E S O LU B LE F R AC T IO N A N D TOTAL PARTICULATE (ASPHALT FUME) CHLORINATED ORG ANONITROGEN H ER BIC ID ES (A IR SA M PL IN G ) TR IAZ INE HE RB IC IDE S a nd the ir METABOLITES CHLORINATED ORG ANONITROGEN HER BICIDES (HAND WAS H) CHLORINATED ORG ANONITROGEN HE RBIC IDES (DER M AL P ATC H)) AZ ELA IC A C ID ORG ANOPHO SPHORUS PESTICIDES A ER O BIC B AC TE RIA by G C -F AM E PO LYN UC LEA R A RO M ATIC HYDR OC ARBO NS by H PLC PO LYN UC LEA R A RO M ATIC HYDROCARBONS B A R IU M , S O LU B LE C O M P O U N D S ELEMENTS on WIPES E LE M EN TS by IC P (H O T B L O C K /H C l /H N O 3 D IG E S T IO N ) ELE M EN TS b y IC P (A Q UA RE G IA A SH IN G ) ORG ANONITROGEN PESTICIDES V O L A TI LE O R G A N IC C P D S (Screen in g) PO LYN UC LEA R A RO M ATIC HYDR OC ARBO NS by H PLC PO LYN UC LEA R A RO M ATIC HYDROCARBONS V O L A TI LE O R G A N IC C P D S (Screen in g) B EN ZE NE by po rta ble G C HY DR O C AR BO NS , AR O M ATIC HYDROC ARBONS, BP 36 !216 C ORG ANIC and INORGANIC G ASES by EX TR ACTIV E FTIR SPE C T R O MET R Y B E N Z EN E S O LU B LE F R AC T IO N A N D TOTAL PARTICULATE (ASPHALT FUME) R ES O RC IN O L DYES BENZIDINE and 3,3'!DICHLORO !B E N Z ID I NE PO LYN UC LEA R A RO M ATIC HYDR OC ARBO NS by H PLC PO LYN UC LEA R A RO M ATIC HYDROCARBONS
3/15/2003
MF!3
Chemical Benzo[a]fluoranthene Benzo(b)fluoranthene Benzo[e]pyrene Benzo(e)pyrene Benzo[k]fluoranthene Benzo(k)fluoranthene Benzo[ghi]perylene Benzo(ghi)perylene Be nzo su lfon az ole Be nzo thia zo le Be nzoyl pe r o xide Be nzyl c hlo ride Be r yllium Be r yllium Be r yllium Be r yllium Be r yllium & c o m po und s Bio ae r o so l Biphenyl Bism uth B itu m en fu m e Bo r o n Bo r o n c ar bide Bo r o n o xide Brom oform Bromine 1-Bromopropane 2-Bromopropane Brom oform Bromotrifluoromethane Bro m ox yn il Brom oxy nil octa noa te 1,3 !Butadiene 2 !Butanone 2 !Butanone 2-Butanone
M eth No. 5506 5515 5506 5515 5506 5515 5506 5515 2550 2550 5009 1003 7300 9102 7303 7301 7102 0800 2530 7303 5042 7303 7506 0500 1003 6011 1025 1003 1017 5010 5010 1024 2500 2549 3800
M e th od Na m e PO LYN UC LEA R A RO M ATIC HYDR OC ARBO NS by H PLC PO LYN UC LEA R A RO M ATIC HYDROCARBONS PO LYN UC LEA R A RO M ATIC HYDR OC ARBO NS by H PLC PO LYN UC LEA R A RO M ATIC HYDROCARBONS PO LYN UC LEA R A RO M ATIC HYDR OC ARBO NS by H PLC PO LYN UC LEA R A RO M ATIC HYDROCARBONS PO LYN UC LEA R A RO M ATIC HYDR OC ARBO NS by H PLC PO LYN UC LEA R A RO M ATIC HYDROCARBONS B EN ZO TH IA ZO LE IN AS PH A LT F UM E B EN ZO TH IA ZO LE IN AS PH A LT F UM E B E N Z O Y L P E R O X ID E HYDROC ARBONS, HALOG ENATED E LE M E NT S b y IC P ELEMENTS on WIPES E LE M EN TS by IC P (H O T B L O C K /H C l /H N O 3 D IG E S T IO N ) ELE M EN TS b y IC P (A Q UA RE G IA A SH IN G ) BERYLLIUM and cpds, as Be BIOA ERO SO L SAM PLING (Indoor A ir) DIPHENYL E LE M EN TS by IC P (H O T B L O C K /H C l /H N O 3 D IG E S T IO N ) B E N Z EN E S O LU B LE F R AC T IO N A N D TOTAL PARTICULATE (ASPHALT FUME) E LE M EN TS by IC P (H O T B L O C K /H C l /H N O 3 D IG E S T IO N ) B O R O N C A R B ID E PARTICU LATES N.O.R . HYDROC ARBONS, HALOG ENATED C H L O R IN E a n d B R O M I N E 1 - a n d 2 -B R O M O P R O P A N E HYDROC ARBONS, HALOG ENATED T R IF L UO R O B R O M O M E T HA N E BRO MO XYN IL and B 'OC TANO ATE BRO MO XYN IL and B 'OC TANO ATE 1,3 !B U TA D IE N E M E T H YL E TH Y L K E TO N E V O L A TI LE O R G A N IC C P D S (Screen in g) ORG ANIC and INORGANIC G ASES by EX TR ACTIV E FTIR SPE C T R O MET R Y
Flow Ra te ( L /m i n ) 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 1.0 - 2.0 1.0 - 2.0 1-3 0.01 - 0.2 1- 4 NA 1-4 1-4 1-4 28.3 0.01 - 0.5 1-4 1-4 1-4 1.7 or 2 .2 1.5 - 2.0 0.01 - 0.2 0.3 - 1.0 0.01 - 0.2 0.01 - 0.2 0.01 - 0.05 1-3 1-3 0.01 - 0.5 0.01 - 0.2 0.01 - 0.05 0.1 - 2.0
Vol. (L) min max 200 - 1000 200 - 1000 200 - 1000 200 - 1000 200 - 1000 200 - 1000 200 - 1000 200 - 1000 480 - 960 480 - 960 40 - 400 6 - 50 1250-2000 NA Se e Ta ble 1250-2000 25 - 2000 va r ies 15 - 30 Se e Ta ble 28 - 400 Se e Ta ble 100 - 1000 25 - 133 4 - 70 8 - 360 0.1 - 12 4 - 70 0.3 - 1.0 2 - 400 90 - 400 5 - 25 1 - 12 1-6 Inst r. D ep .
E x tr a c ti o n
A n a ly t ic a l T e c h n iq u e HPLC !FL/U V G C !FID HPLC !FL/U V G C !ID HPLC !FL/U V G C !ID HPLC !FL/U V G C !ID G C - SC D G C - SC D HPLC !U V G C !FID IC P !AES ICP-AES ICP-AES ICP-AES G FAAS va r ies G C !FID ICP-AES Grav ICP-AES XR D Grav G C -FID IC G C -FID G C !FID G C !FID HPLC !U V HPLC !U V G C !FID G C !FID TD /G C !M S FTIR
Sampler P T F E & X A D !2 P T F E & X A D !2 P T F E & X A D !2 P T F E & X A D !2 P T F E & X A D !2 P T F E & X A D !2 P T F E & X A D !2 P T F E & X A D !2 PTFE + X D-2 PTFE + X D-2 MC EF CCT MC EF Wipe MC EF MC EF MC EF I m p a c to r Te na x G C MC EF Tared PTFE MC EF C Y C & P VC P VC CCT Ag F CCT CCT 2 C C T (lg + sm ) PTFE PTFE CCT C a rb o n b e a d s TD Di r. R e a d
ac eto nitr ile va r ies ac eto nitr ile va r ies ac eto nitr ile va r ies ac eto nitr ile va r ies hexane hexane d ieth y l et h er C S2 H N O 3/HC lO 4 NA H C l /H N O 3 H C l /H N O 3 H N O 3/H 2SO 4 NA C C l4 H C l /H N O 3 benzene H C l /H N O 3 ash NA C S2 N a 2S 2O 3 C S2 C S2 C H 2C l2 C H 3C N C H 3C N C H 2C l2 C S2 t h erma l NA
3/15/2003
MF!4
Chemical Bu tox ya ce tic a cid 2 !Buto xye thyano l 2 !Buto xye thano l n !, s ec !, & t!Buty l ace tate Buty l ace tate iso-Bu tyl ac etate 1-Bu tyl ac etate Butyl alc o ho l tert !Butyl alc o ho l n ! & s e c !Butyl alc o hol n- Butyl alc oho l se c -Butyl alc o ho l n !Butylamine Butyl cellosolve Butyl cellosolve 1,3 !Butyle ne glygo l Butyl glyc idyl e the r n !Butyl me rc aptan n !Butyl me rc aptan p !tert !Butyltoluene Butyr alde hyde C a dm ium C a dm ium C a dm ium C a dm ium C a dm ium & c o m po un ds C a lc ium C a lc ium C a lc ium C a lc ium & c o m po und s C a m pho r C a m pho r C ap sa icin C a ptan C a ptan C a ptan Carbaryl Carbaryl (Sevin)
M eth No. 8316 2549 1403 1450 2549 1450 1450 2549 1400 1401 1405 1405 2012 2549 1403 5523 1616 2525 2542 1501 2539 7300 9102 7303 7301 7048 7300 7303 7301 7020 1301 2553 5041 5601 9205 9202 5601 5006
M e th od Na m e BUTOXYACETIC ACID in urine V O L A TI LE O R G A N IC C P D S (Screen in g) ALC O HO LS IV ESTERS I V O L A TI LE O R G A N IC C P D S (Screen in g) ESTERS I ESTERS I V O L A TI LE O R G A N IC C P D S (Screen in g) ALCOHO LS I ALC O HO LS II ALCOHO LS COM BINED ALCOHO LS COM BINED n !B U TY L AM I N E V O L A TI LE O R G A N IC C P D S (Screen in g) ALC O HO LS IV GLYC OLS BUTYL GLYCIDYL ETHER n !BU TYL MER CAPTAN M E R C A P TA N S HY DR O C AR BO NS , AR O M ATIC A L D EH Y D E S, SC R E E N IN G E LE M E NT S b y IC P ELEMENTS on WIPES E LE M EN TS by IC P (H O T B L O C K /H C l /H N O 3 D IG E S T IO N ) ELE M EN TS b y IC P (A Q UA RE G IA A SH IN G ) C A D M IU M a nd c pd s, as C d E LE M E NT S b y IC P E LE M EN TS by IC P (H O T B L O C K /H C l /H N O 3 D IG E S T IO N ) ELE M EN TS b y IC P (A Q UA RE G IA A SH IN G ) C A LC IU M a nd c pd s a s C a KE TO NE S II KE TO NE S II C AP SA ICIN an d D IHY DR O C AP SA ICIN ORG ANONITROGEN PESTICIDES CAPTAN and THIOPHENATE-METHYL o n D E RM A L P A TC H CAPTAN and THIOPHENATE-METHYL in Handrinse ORG ANONITROGEN PESTICIDES CARBARYL
Flow Ra te ( L /m i n ) NA 0.01 - 0.05 0.01 - 0.05 0.01 - 0.2 0.01 - 0.05 0.01 - 2 0.01 - 2 0.01 - 0.05 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 1.0 0.01 - 0.05 0.01 - 0.05 0.5 - 2 0.01 - 0.2 0.01 - 0.05 0.1 - 0.2 0.01 - 0.2 0.05 1-4 NA 1-4 1-4 1-3 1-4 1-4 1-4 1-3 0.01 - 0.2 0.01 - 0.2 1-3 0.1 - 1 NA NA 0.1 - 1 1-3
Vol. (L) min max NA 1-6 2 - 10 1 - 10 1-6 1 - 10 1 - 10 1-6 1 - 10 2 - 10 2 - 10 2 - 10 2 - 100 1-6 1 - 10 5 - 60 15 - 30 1-4 10 - 150 1 - 29 5-5 13 - 2000 NA Se e Ta ble 13 - 2000 25 - 1500 5 - 200 Se e Ta ble 5 - 200 20 - 400 1 - 25 1 - 25 5 - 1000 var-480 NA NA var-480 20 - 400
E x tr a c ti o n
A n a ly t ic a l T e c h n iq u e G C - EC D TD /G C !M S G C !FID G C !FID TD /G C !M S G C -FID G C -FID TD /G C !M S G C !FID G C !FID G C -FID G C -FID G C !FID TD /G C !M S G C !FID G C !FID G C !FID G C !FPD G C !FPD G C !FID G C !F ID /M S IC P !AES ICP-AES ICP-AES ICP-AES FAAS IC P !AES ICP-AES ICP-AES FAAS G C !FID G C -FID HPLC !FL HP LC - UV HP LC - U V HP LC - U V HP LC - UV VIS NA TD
Sampler
NA t h erma l C H 2C l2/M e O H C S2 t h erma l C S2 C S2 t h erma l C S2 C S2 IP A -C S 2 IP A -C S 2 MeOH t h erma l C H 2C l2/M e O H MeOH C S2 a cet H C l/D C E C S2 t ol H N O 3/HC lO 4 NA H C l /H N O 3 H C l /H N O 3 H N O 3/H C l H N O 3/HC lO 4 H C l /H N O 3 H C l /H N O 3 H N O 3/HC lO 4 M e O H /C S 2 IP A -C S 2 C H 3C N reagent IP A /A C N NA reagent reagent
CCT CCT TD CCT CCT TD CCT CCT CCT CCT S G + H 2SO 4 TD CCT O VS !7 CCT Chrom 104 GFF/HgAc CCT X A D !2 /H M P MC EF Wipe MC EF MC EF MC EF MC EF MC EF MC EF MC EF CCT A -C M S GFF OV S-2 Patch Hand wa sh OV S-2 GFF
3/15/2003
MF!5
Chemical C ar be nd az im C a r bito l C a r bo fur an C a r bo n blac k C a r bo n, e le m e ntal C a r bo n dio xide C a r bo n disulfide C a r bo n m o no xide C a r bo n te trac hlo r ide
M eth No. 5601 2549 5601 5000 5040 6603 1600 6604 1003 1552 7404 5510 5039 5025 5014 6011 2015 2008 1003 1026 1003 1003 1018 5503 2513 1003 2005 2014 1002 5601 5600 7600 7604 7024 7300 7301 7303 9102 7600 7604
M e th od Na m e ORG ANONITROGEN PESTICIDES V O L A TI LE O R G A N IC C P D S (Screen in g) ORG ANONITROGEN PESTICIDES C A R BO N B LA C K ELEM ENTA L CA RBO N (DIES EL PA RT.) C A R B O N D IO X I D E C A R B O N D IS U LF ID E CARBON MONOXIDE HYDROC ARBONS, HALOG ENATED TERPENES C E LL UL OS E IN SU LA TIO N CHLORDANE C H L O R IN A T ED C A M P H E N E C H L O R IN A T ED D IP H E N YL O X ID E CH LORINA TED TERPH ENYL C H L O R IN E a n d B R O M I N E C H L O R O A C E T AL D E HY D E C HLO RO AC ETIC AC ID HYDROC ARBONS, HALOG ENATED p - C H LO R O B E N Z O T RI FL U O R ID E HYDROC ARBONS, HALOG ENATED HYDROC ARBONS, HALOG ENATED D I C H LO R O D I F LU O R O M E T H A N E POLY CH LORO BIPHENY LS ETH YLE NE CH LO RO HY DR IN HYDROC ARBONS, HALOG ENATED N I TR O A R O M A T IC C O M P O U N D S p !C H L O RO P H EN O L
Flow Ra te ( L /m i n ) 0.1 - 1 0.01 - 0.05 0.1 - 1 1-2 2-4 0.02 - 0.1 0.01 -0 .2 NA 0.01 - 0.2 0.01 - 0.02 1 0.5 - 1.0 0.2 - 1 0.5 - 1.5 1-3 0.3 - 1.0 0.05 - 0.2 0.05 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.05 0.05 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 1.0 0.05 - 0.2 0.01 - 0.1 0.1 - 1 0.2 - 1.0 1-4 1-4 1-3 1-4 1-4 1-4 NA 1-4 1-4
Vol. (L) min max var - 480 1-6 var-480 30 - 570 142-19000 80% vol 2 - 25 NA 3 - 150 2 - 30 NA 10 - 200 2 - 30 8 - 200 100 - 1500 2 - 90 3 - 16 1 - 100 1.5 - 40 0.1 - 10 0.5 - 60 0.5 - 8 1-4 1 - 50 2 - 35 1 - 50 1 - 150 1.5 - 40 1.5 - 8 var-480 12 - 240 8 - 400 100 - 1000 10 - 1000 5 - 1000 5 - 1000 Se e Ta ble NA 8 - 400 100 - 1000
E x tr a c ti o n
A n a ly t ic a l T e c h n iq u e HP LC - U V TD /G C !M S HP LC - U V Grav E G A/TO A G C !T C D G C !FPD Sens or G C !FID G C !FID SEM G C !E C D G C !E C D G C !E C N G C !E C D IC G C !E C D IC G C !FID G C -FID G C -FID G C !FID G C !FID G C !E C D G C !FID G C !FID G C !FID HPLC !U V G C !FID HP LC , U V G C !FPD VIS IC FAAS IC P !AES ICP-AES ICP-AES ICP-AES VIS IC
Sampler OV S-2 TD OV S-2 P VC QFF air bag CC T & d ry tu b e Port In str CCT CCT ACF M C E F & Ch ro m 102 MC EF MC EF GFF Ag F SG SG CCT CCT CCT CCT 2 C C T (lg + sm ) G FF & F lor isil PCT CCT SG SG CCT OV S-2 O VS !2 P VC P VC MC EF MC EF MC EF MC EF Wipe P VC P VC
reagent t h erma l reagent NA t h erma l NA toluene NA C S2 C S2 NA t ol p et eth er isooctane isooctane N a 2S 2O 3 MeOH H 2O C S2 C S 2/M e O H C S2 C S2 C H 2C l2 hexane IP A /C S 2 C S2 MeOH C H 3C N C S2 reagent t ol/a cet reagent N a O H / N a2 C O 3 H C l /H N O 3 H N O 3/HC lO 4 H C l /H N O 3 H C l /H N O 3 NA reagent N a O H / N a2 C O 3
* -3-Carene
Cellulose Chlordane Chlorinated camphene C hlo rinate d diphe nyl ox ide Chlorinated terphenyl Chlorine C hlo ro ac e talde hyde C hlo ro ac etic ac id Chlorobenzene p -Chlo r o be nzo tr ifluo r id e Chlorobromomethane Chlorobromomethane Chlorodifluoromethane Chlorodiphenyl (42 & 54% C I) 2 !Chlo ro e thano l Ch loroform 4 !Chloronitrobenzene p !Chlo ro phe no l Chloroprene C hlo rpr o pham C hlo rpyr ifo s C hr om ic a cid C hr om ic a cid C hr o m ium C hr o m ium C hr o m ium C hr o m ium C hr o m ium Chromium, hexavalent Chromium, hexavalent
$!C H L O R O P R E N E
ORG ANONITROGEN PESTICIDES ORG ANOPHO SPHORUS PESTICIDES C H R O M I U M , HE X A V A LE N T C H R O M I U M , HE X A V A LE N T C H R O M IU M a nd c pd s, as C r E LE M E NT S b y IC P ELE M EN TS b y IC P (A Q UA RE G IA A SH IN G ) E LE M EN TS by IC P (H O T B L O C K /H C l /H N O 3 D IG E S T IO N ) ELEMENTS on WIPES C H R O M I U M , HE X A V A LE N T C H R O M I U M , HE X A V A LE N T
3/15/2003
MF!6
Chemical Chromium, hexavalent Chromium, hexavalent Chromium, hexavalent Chrysene Chrysene C oal tar naphtha C oal tar pitc h vo latile s C ob alt C ob alt C ob alt C ob alt C obalt & c o m po unds C oppe r Co ppe r Co ppe r Co ppe r Co ppe r (dust & fum e ) Cr e so l
M eth No. 7605 7703 9101 5506 5515 1550 5042 7300 9102 7301 7303 7027 7300 7301 9102 7303 7029 2549
M e th od Na m e C H RO M IU M HE XA VA LE NT b y IO N CHROM ATOGRAPHY CHROM IUM, HEXAV ALENT b y Field Portab le Spe ctroph otom etry CHROM IUM, HEXAV ALENT in s ett led dust PO LYN UC LEA R A RO M ATIC HYDR OC ARBO NS by H PLC PO LYN UC LEA R A RO M ATIC HYDROC ARBONS NAPHTHAS B E N Z EN E S O LU B LE F R AC T IO N A N D TOTAL PARTICULATE (ASPHALT FUME) E LE M E NT S b y IC P ELEMENTS on WIPES ELE M EN TS b y IC P (A Q UA RE G IA A SH IN G ) E LE M EN TS by IC P (H O T B L O C K /H C l /H N O 3 D IG E S T IO N ) C O B A LT an d c p ds , a s C o E LE M E NT S b y IC P ELE M EN TS b y IC P (A Q UA RE G IA A SH IN G ) ELEMENTS on WIPES E LE M EN TS by IC P (H O T B L O C K /H C l /H N O 3 D IG E S T IO N ) CO PPER (dust & fumes) V O L A TI LE O R G A N IC C P D S (Screen in g) C R ES O LS an d P HE NO L A L D EH Y D E S, SC R E E N IN G C R O T O N A L D EH Y D E DICHLORODIFLUORO METHANE, 1,2 !DICHLOROTETR AFLU O R O ! ETHA NE, & C H L O R O D IF L UO R O M E T H A N E HY DR O C AR BO NS , AR O M ATIC CYANIDES, aerosol an d g a s H Y D R O G E N C Y A N ID E C YA NU RIC AC ID CHLORINATED ORG ANONITROGEN H ER BIC ID ES (A IR SA M PL IN G ) TR IAZ INE HE RB IC IDE S a nd the ir METABOLITES CHLORINATED ORG ANONITROGEN HER BICIDES (HAND WAS H) CHLORINATED ORG ANONITROGEN HE RBIC IDES (DER M AL P ATC H)) HYDROC ARBONS, BP 36 !216 C ALC O HO LS III ALCOHO LS COM BINED
Flow Ra te ( L /m i n ) 0.1 - 4 1-4 NA 2.0 2.0 0.01 - 0.2 1-4 1-4 NA 1-4 1-4 1-3 1-4 1-4 NA 1-4 1-3 0.01 - 0.05
Vol. (L) min max 1 - 400 10 - 1200 NA 200 - 1000 200 - 1000 1.3 - 20 28 - 400 25 - 2000 NA 25 - 2000 Se e Ta ble 30 - 1500 5 - 1000 5 - 1000 NA Se e Ta ble 50 - 1500 1-6
E x tr a c ti o n
A n a ly t ic a l T e c h n iq u e IC VIS Sp ot HPLC !FL/U V G C !FID G C !FID Grav IC P !AES ICP-AES ICP-AES ICP-AES FAAS IC P !AES ICP-AES ICP-AES ICP-AES FAAS TD /G C !M S P VC
Sampler
N a O H - N a2C O 3 ( N H4) 2SO 4/ N H4O H NA ac eto nitr ile va r ies C S2 benzene H N O 3/HC lO 4 NA H C l /H N O 3 H C l /H N O 3 a q re g /H N O 3 H N O 3/HC lO 4 H C l /H N O 3 NA H C l /H N O 3 H N O 3/H C l t h erma l
PVC, MCE, PTFE Te st s trip P T F E & X A D !2 P T F E & X A D !2 CCT tared PTFE MC EF Wipe MC EF MC EF MC EF MC EF MC EF Wipe MC EF MC EF TD
1 - 24 5-5 1 - 49 1-4
MeOH t ol b u ffer C H 2C l2
X A D !7 X A D !2 /H M P BuB 2 CCT
Cyanazine
8315
NA
NA
NA
GS-MSD
Urine
Cyanazine
9200
NA
NA
NA
G C - EC D
Cyanazine
9201
NA
NA
IPA/diazomethane
G C - EC D
2.5 - 5 1 - 10 2 - 10
C S2 IP A /C S 2 IP A -C S 2
3/15/2003
MF!7
Chemical Cyclohexanone
E x tr a c ti o n
A n a ly t ic a l T e c h n iq u e TD /G C !M S TD
Sampler
t h erma l
1 - 10 1 - 10 5-7 1-5
C S2 C S2 C S2 Et Ac
2,4 !D 2,4-D a cid; 2,4-D,2 -ethylhe xyl ester; 2, 4-D , 2-buto xye thyl ester 2,4-D a cid; 2,4-D,2 -ethylhe xyl ester; 2, 4-D , 2-buto xye thyl ester 2,4-D a cid; 2,4-D,2 -ethylhe xyl ester; 2, 4-D , 2-buto xye thyl ester D ec abr o mo diphe nyl Ox i de n !Decane
5001 5602
1-3 0.2 - 1
15 - 200 12 - 480
MeOH reagent
HPLC !U V G C - EC D
9200
NA
NA
NA
G C - EC D
polyethylene bag
9201
NA
NA
IPA/diazomethane
G C - EC D
PUF pad
2559 2549
D E C A B R O M O D I PH E N Y L O X I D E V O L A TI LE O R G A N IC C P D S (Screen in g)
o HYDROC ARBONS, BP 36 o-216 C
48 - 960 1-6
T ol t h erma l
G C /N C D TD /G C !M S
GFF TD
NA 0.2 - 1.0 NA
NA 30 - 500 NA
C S2 toluene NA
D EM E TO N TR IAZ INE HE RB IC IDE S a nd the ir METABOLITES TR IAZ INE HE RB IC IDE S a nd the ir METABOLITES ALC O HO LS III ALCOHO LS COM BINED DIACETYL DYES SILICA, AMOR PHOUS ORG ANOPHO SPHORUS PESTICIDES D I AZ O M E T H A N E PO LYN UC LEA R A RO M ATIC HYDR OC ARBO NS by H PLC PO LYN UC LEA R A RO M ATIC HYDROCARBONS D I BO R A N E
Desisopropylatrazine
8315
NA
NA
NA
GC-M SD
Urine
D i ac eto ne alc oho l D i ac eto ne alc oho l Diacetyl o !Dianisidine Diato ma ce ou s ea rth D i azino n Diazomethane Dibenz[a,h]anthracene
0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 1-3 1-3 0.2 - 1 0.2 2.0
Dibenz(a,h) anthracene
5515
2.0
200 - 1000
va r ies
G C !FID
P T F E & X A D !2
Diborane
6006
0.5 - 1.0
60 - 260
H 2O 2
PES
Dibromodifluoromethane 2 !D ibutylam ino e thanol Dibu tyl ph osp ha te Dibu tyl ph tha late
D I FL U O R O D IB R O M O M E T H A N E A M I N O E TH A N O L C O M P O U N D S DIBUTY L PHO SPH ATE D I BU T YL P HT H A LA T E & DI(2 !ETHY LHEX YL) PHTH ALATE O R G A N O T IN C O M P O U N D S
IPA M eO H/H 2O C H 3C N C S2
5504
1 - 1.5
50 - 500
A c etic a /C H 3C N
HP LC /G FAAS
G F F + X A D !2
2549
0.01 - 0.05
1-6
va r ies
TD /G C !M S
TD
o-Dichlorobenzene
1003
0.01 - 0.2
1 - 10
C S2
G C -FID
CCT
3/15/2003
MF!8
M e th od Na m e HYDROC ARBONS, HALOG ENATED HYDROC ARBONS, HALOG ENATED BENZIDINE an d 3,3'!D I C H LO R O B E N Z ID I NE DICHLORODIFLUORO METHANE, 1,2 !DICHLOROTETR AFLUO R O ! ETHANE & C H L O R O D IF L UO R O M E T H A N E HYDROC ARBONS, HALOG ENATED HYDROC ARBONS, HALOG ENATED DICHLOROETHYL ETHER HYDROC ARBONS, HALOG ENATED D I C H LO R O F L U O R O M E T HA N E M E T H YL E N E C H L O R ID E V O L A TI LE O R G A N IC C P D S (Screen in g) 1,1 !DICHLORO !1 !N I TR O E T H AN E P R O P Y LE N E D IC H L O R ID E DIC HLO RO DIFLUO RO ME THAN E, 1,2 !DICHLOROTETR AFLUO R O ! ETHANE & C H L O R O D IF L UO R O M E T H A N E ORG ANOPHO SPHORUS PESTICIDES ELEM ENTA L CA RBO N (DIES EL PA RT.) AM INO ETH AN O L C O M PO UN DS II AM INE S, A LIPH ATIC AMINOETHANO L COM POUNDS I GLYC OLS V O L A TI LE O R G A N IC C P D S (Screen in g) ETHYLENEDIAMINE, DIETHY LENE TRIAM INE, & T R IE T HY L EN E TE T RA M I N E DIBUTYL PHTHALATE an d DI(2 !ETHY LHEX YL) PHTH ALATE D I FL U O R O D IB R O M O M E T H A N E DIC HLO RO DIFLUO RO ME THAN E, 1,2 !DICHLOROTETR AFLU O R O !ET HAN E & C H L O R O D IF L UO R O M E T H A N E C AP SA ICIN an d D IHY DR O C AP SA ICIN KETONES I KETONES I DIMETHYLACETAMIDE and D I M E TH Y L FO R M A M I D E AM INE S, A LIPH ATIC 2 -(D IM E TH YL AM IN O )E TH A NO L 1 -D IM E TH YL AM IN O -2 -P RO P AN O L AM INE S, A RO M ATIC A R S E N IC , O R G A N O !
E x tr a c ti o n
C S2 C S2 TE A/M e O H
Dichlorodifluoromethane
1018
0.01 - 0.05
1-4
C H 2C l2
G C !FID
2 CCT (lg + sm )
1,1 !Dichloroethane 1,2 !Dichloroethane D i c hlo r o e thyl e the r 1,2 !Dichloroethylene Dichlorofluoromethane Dichloromethane Dichloromethane
0.01 - 0.2 0.01 - 0.2 0.01 - 1.0 0.01 - 0.2 0.01 - 0.05 0.01 - 0.2 0.01 - 0.05
C S2 C S2 C S2 C S2 C S2 C S2 t h erma l
C S2 Acet/cyclohexane C H 2C l2
G C !FID G C !E C N G C !FID
D i c ro to pho s Diesel exhaust Diethanolamine Diethylamine 2 !D ie thylam ino e thanol D i e thyle ne glyc o l D i e thyle ne glyc o l e ther
0.2 - 1 1-4 0.5 - 1.0 0.01 - 1.0 0.01 - 0.2 0.5 - 2 0.01 - 0.05
O VS !2 QFF IM P SG SG O VS !7 TD
Diethylenetriamine
2540
0.01 - 0.1
1 - 20
DMF
HPLC !U V
X A D !2 w/10 % N ITC
5020
1-3
10 - 200
C S2
G C !FID
MC EF
1012 1018
2.5 - 10 1-4
IPA C H 2C l2
G C !FID G C !FID
2 CCT 2 CCT
7 - 1000 1 - 10 1 - 10 15 - 80
C H 3C N C S2 C S2 MeOH
GFF CCT A -C M S SG
Dimethylamine 2-(D im e thylam ino )e thanol 1-D im e thylam ino -2-propan ol N,N !Dimethylaniline Dim eth yla rsin ic a cid
2010 2561
3 - 30 10 - 24
G C !FID G C -FID
SG XAD
2002 5022
3 - 30 50 - 1000
Et h a nol b u ffer
G C !FID IC !HYAAS
SG PTFE
3/15/2003
MF!9
M e th od Na m e DIMETHYLACETAMIDE & D I M E TH Y L FO R M A M I D E 1,1 !D I M E TH Y L HY D R A Z IN E AM INE S, A RO M ATIC DIM ETHY L SULFA TE D I O X AN E DIPHENYL GLYCOL ETHER S
E x tr a c ti o n
A n a ly t ic a l T e c h n iq u e G C !FID SG
Sampler
MeOH
1,1 !Dimethylhydrazine N,N !Dimethyl!p !toluidine Dim ethy l sulfate Dioxane Diphenyl D i pro pyle ne glyc o l mo no m e thyl e the r D i sulfo to n D i uro n n-Dodecane D y e s ! benzidine !, o !tolidine !, o !dianisidine ! E le me ntal c ar bo n Elem ents Elem ents
0.2 - 1.0 0.02 - 1.0 0.01 - 0.2 0.01 - 0.2 0.01 - 0.5 0.1 - 0.2
ORG ANOPHO SPHORUS PESTICIDES ORG ANONITROGEN PESTICIDES HYDROC ARBONS, BP 36 -216 C D Y E S , B E N ZI D IN E !, o ! T O LI D IN E !, o ! D IA N IS ID I NE ELEM ENTA L CA RBO N (DIES EL PA RT.) E LE M E NT S b y IC P ELEMENTS by ICP (Aqu a R eg ion Ashin g) E LE M EN TS by IC P (H O T B L O C K /H C l /H N O 3 D IG E S T IO N ) EN DR IN
o o
t h erma l H N O 3/HC lO 4 Aq R eg
QFF MC EF MC EF PVCF MC EF
Elem ents
7303
1-4
Se e Ta ble
H C l /H N O 3
ICP-AES
En dr in
5519
0.5 - 1.0
12 - 400
t ol
G C !E C D
MCEF & Chrom 102 CCT GFF CCT PTFE PTFE PTFE TD
EP ICH LO RO HY DR IN EPN P R O P Y LE N E O X ID E E S TR O G E N I C C O M P O U N D S E S TR O G E N I C C O M P O U N D S E S TR O G E N I C C O M P O U N D S V O L A TI LE O R G A N IC C P D S (Screen in g) ALCOHO LS I AMINOETHANO L COM POUNDS I ORG ANOPHO SPHORUS PESTICIDES ORG ANOPHO SPHORUS PESTICIDES ALC O HO LS IV ESTERS I V O L A TI LE O R G A N IC C P D S (Screen in g) ETHY L AC ETATE ESTERS I KE TO NE S II HY DR O C AR BO NS , AR O M ATIC E T HY L BR O M I D E KE TO NE S II E T HY L C H LO R I D E ETH YLE NE CH LO RO HY DR IN
$ -Estradiol
Estrone
E thano l Ethanolamine E thio n E tho pr o p 2 !Etho xye thano l 2 !Etho xye thyl a ce tate Ethy l ace tate
0.01 - 0.05 0.01 - 0.2 0.2 - 1 0.2 - 1 0.01 - 0.05 0.01 - 0.2 0.01 - 0.05
Ethy l ace tate Ethy l acry late Ethyl amyl ketone Ethylbenzene E thyl bro m ide Ethyl butyl ketone E thyl c hlo ride Eth yle ne ch lor oh yd rin 3/15/2003
0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.02 - 0.05 0.01 - 0.2 MF!10
C S2 C S2 M e O H /C S 2 C S2 IPA M e O H /C S 2 C S2 IP A /C S 2
Chemical Ethylenediamine
M e th od Na m e ETHY LENE DIAM INE, DIETHY LENE TRIAM INE, & T R IE T HY L EN E TE T RA M I N E E T HY L EN E D IB R O M I D E HYDROC ARBONS, HALOG ENATED GLYC OLS N ITR O G LY C ER IN & ETH YL EN E G LY C O L DINITRA TE E T HY L EN E O X ID E E TH YL EN E O X ID E b y p orta ble G C ORG ANIC and INORGANIC G ASES by EX TR ACTIV E FTIR SPE C T R O MET R Y ETHYLENE THIOUREA E T HY L EN I M IN E ETHYL ETHER ETHYL ETHER ETHY L FO RM ATE M E R C A P TA N S ME THYL a nd ETH YL M ETHA CR YLATE ORG ANOPHO SPHORUS PESTICIDES A S BE ST O S & o th e r F IB ER S b y PC M PO LYN UC LEA R A RO M ATIC HYDR OC ARBO NS by H PLC PO LYN UC LEA R A RO M ATIC HYDROCARBONS PO LYN UC LEA R A RO M ATIC HYDR OC ARBO NS by H PLC PO LYN UC LEA R A RO M ATIC HYDROCARBONS FLUORIDES, aerosol & ga s
E x tr a c ti o n
A n a ly t ic a l T e c h n iq u e HPLC !U V
DMF
E thyle ne dibr o m ide E thyle ne dic hlor ide E thyle ne glyc o l Ethy lene glyc ol dinitra te
0.1 - 25 1 - 50 5 - 60 3 - 100
G C !E C D G C !FID G C !FID G C !E C D
CCT CCT O VS !7 Te na x G C
DMF NA NA
G C !E C D G C !PID FTIR
E thyle ne thio ur e a Ethylenimine E thyl ethe r E thyl ethe r Ethy l form ate E thyl m e rc aptan Ethy l me tha cryta te F e nam ipho s Fibrous glass Fluoranthene
5011 3514 1610 1610 1452 2542 2537 5600 7400 5506
1-3 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.1 - 0.2 0.01 - 0.05 0.2 - 1 0.5 - 16 2.0
200 - 800 1 - 48 0.25 - 3 0.25 - 3 0.3 - 10 10 - 150 1-8 12 - 240 400 !va r ies 200 - 1000
VIS HPLC !U V G C -FID G C !FID G C !FID G C !FPD G C -FID G C !FPD PCM HPLC !FL/U V
!
ac eto nitr ile
Fluoranthene
5515
2.0
200 - 1000
va r ies
G C !FID
P T F E & X A D !2
Fluorene
5506
2.0
200 - 1000
HPLC !FL/U V
P T F E & X A D !2
Fluorene
5515
2.0
200 - 1000
va r ies
G C !FID
P T F E & X A D !2
F luo r ide s
7902
1-2
12 - 800
N a OH
ISE
F luo r ide s
7906
FLU O RID ES by IC
1-2
N a OH
IC
Fluorotrichloromethane F o no fo s F o r malde hyde F o r malde hyde F o r malde hyde F o r malde hyde F o r malde hyde
F L UO R O T R IC H L O R O M E T H A NE ORG ANOPHO SPHORUS PESTICIDES F O R M A L D E HY D E F O R M A L D E HY D E F O R M A L D E HY D E A L D EH Y D E S, SC R E E N IN G ORG ANIC and INORGANIC G ASES by EX TR ACTIV E FTIR SPE C T R O MET R Y FORM ALDEHYDE on dust ORG ANONITROGEN PESTICIDES FO RM IC A C ID
0.01 - 0.05 0.2 - 1.0 0.1 - 1.5 0.01 - 0.1 0.2 - 1.0 0.01 - 0.05 0.1 - 2.0
H 2O /D N PH /C H 3C N reagent H 2O
HPLC !U V HP LC , U V IC
F ur fur al F ur fur al
2529 2539
FU R FU R AL A L D EH Y D E S, SC R E E N IN G
1 - 12 5-5
t ol t ol
G C !FID G C !F ID /M S
3/15/2003
MF!11
M e th od Na m e F UR FU RY L A LC O H O L E LE M EN TS by IC P (H O T B L O C K /H C l /H N O 3 D IG E S T IO N ) G L U TA R A LD E H Y D E PARTICU LATES N.O.R . G LY C ID O L GLYC OLS E LE M EN TS by IC P (H O T B L O C K /H C l /H N O 3 D IG E S T IO N ) A L D EH Y D E S, SC R E E N IN G V O L A TI LE O R G A N IC C P D S (Screen in g) HYDROC ARBONS, BP 36 !216 C KE TO NE S II KE TO NE S II CHLORINATED ORG ANONITROGEN H ER BIC ID ES (A IR SA M PL IN G ) CHLORINATED ORG ANONITROGEN HER BICIDES (HAND WAS H) CHLORINATED ORG ANONITROGEN HE RBIC IDES (DER M AL P ATC H)) H E X A C H LO R O B U T A D IE N E HEXACHLOR O !1,3 !CY CLO PEN TA D I EN E HYDROC ARBONS, HALOG ENATED ISOCYANATES
E x tr a c ti o n
A n a ly t ic a l T e c h n iq u e G C !FID ICP-AES
Sampler Por Q MC EF
a cet H C l /H N O 3
G lutar alde hyde Glycerin mist G lyc ido l G lyc ols G old
C H 3C N NA T HF MeOH H C l /H N O 3
SG/DNPH P VC CCT O VS !7 MC EF
H eptanal n !Heptane
2539 2549
5-5 1-6
t ol t h erma l
G C !F ID /M S TD /G C !M S
X A D !2 /H M P TD
NA 1 - 25 1 - 25 12 - 480
C S2 IP A -C S 2 IP A -C S 2 reagent
CCT A -C M S A -C M S OV S-2
H er bic ides
9200
NA
NA
NA
G C - EC D
H er bic ides
9201
NA
NA
IPA/diazomethane
G C - EC D
Hexachlorobutadiene Hexa chloro !1,3 !cy clo pentadiene Hexachloroethane Hexamethylene! diisoc ya nate 1,6-Hexamethylene ! diisoc ya nate 1,6-Hexamethylene diiso cy an ate (HD I) H exanal H exanal
2543 2518
1 - 100 0.25 - 90
hexane hexane
G C !E C D G C !E C D
X A D !2 2 Por T
1003 5522
3 - 70 15 - 360
C S2 tryptamine/DMSO
CCT IM P
5521
ISO C YA NA TES , M O NO M ER IC
1.0
5 - 500
rea ge nts
HPLC !EC HD
IM P
5525
1-2
1 - 500
MAP
HP LC /UV
G F F, IM P
2539 2549
A L D EH Y D E S, SC R E E N IN G V O L A TI LE O R G A N IC C P D S (Screen in g) V O L A TI LE O R G A N IC C P D S (Screen in g) HYDROC ARBONS, BP 36 !216 C ORG ANIC and INORGANIC G ASES by EX TR ACTIV E FTIR SPE C T R O MET R Y KETONES I KETONES I HIP PU RIC an d M ETH YL H IPP UR IC ACID in urine H Y D R A ZI N E AC IDS , INO RG AN IC AC IDS , INO RG AN IC H Y D R O G E N C Y A N ID E H Y D R O G E N C Y A N ID E
5-5 1-6
t ol t h erma l
G C !F ID /M S TD /G C !M S
X A D !2 /H M P TD
n !Hexane
2549
0.01 - 0.05
1-6
t h erma l
TD /G C !M S
TD
n !Hexane n-Hexane
1500 3800
4-4 Inst r. d ep .
C S2 NA
G C !FID FTIR
CCT Di r. R e a d
1 - 10 1 - 10 NA
C S2 C S2 Et a c
G C !FID G C -FID HP LC - U V
CCT A -C M S NA
VIS IC IC VIS IC -D C Am p
BuB SG SG s od a lim e SL
2-
3/15/2003
MF!12
E x tr a c ti o n
A n a ly t ic a l T e c h n iq u e ISE
KOH H C O 3 /C O 3 N a OH
2-
IC ISE
H y dr o ge n flo ur ide
7906
FLU O RID ES by IC
1-2
1 - 800
N a OH
IC
H y dr o ge n sulfide
6013
H Y D R O G E N S UL F ID E (withdrawn) H Y D R O Q U IN O N E PO LYN UC LEA R A RO M ATIC HYDR OC ARBO NS by H PLC PO LYN UC LEA R A RO M ATIC HYDROCARBONS I O D IN E E LE M EN TS by IC P (H O T B L O C K /H C l /H N O 3 D IG E S T IO N ) ELEMENTS on WIPES ELE M EN TS b y IC P (A Q UA RE G IA A SH IN G ) E LE M EN TS by IC P (H O T B L O C K /H C l /H N O 3 D IG E S T IO N ) E LE M E NT S b y IC P ESTERS I ALC O HO LS III ALCOHO LS COM BINED ESTERS I ALC O HO LS II ALCOHO LS COM BINED A L D EH Y D E S, SC R E E N IN G ISO C YA NA TES , M O NO M ER IC ISOCYANATES I SO P H O R O N E I SO P H O R O N E ISOCYANATES, TOTAL (MAP)
0.1 - 1.5
1.2 - 40
N H 4OH /H 2O 2
IC
Hydroquinone Indeno[1,2,3-cd]pyrene
5004 5506
1-4 2.0
5515
2.0
200 - 1000
va r ies
G C !FID
P T F E & X A D !2
Iodine I ndium
6005 7303
15 - 225 Se e Ta ble
N a 2C O 3 H C l /H N O 3
IC ICP-AES
C C T w /alk ali MC EF
I ron I ron
9102 7301
NA 1-4
NA 5 - 100
NA H C l /H N O 3
ICP-AES ICP-AES
Wipe MC EF
I ron
7303
1-4
Se e Ta ble
H C l /H N O 3
ICP-AES
MC EF
I ron Isoa my l ace tate I soam yl alc o ho l I soam yl alc o ho l Isob utyl a ce tate I sobutyl alco ho l I sobutyl alco ho l I sobutyraldehyde I soc yanate s I soc yanate s Isophorone Isophorone Isop ho rone diisoc ya nate (IPD I) Isop rop yl ac etate Isop rop yl ac etate I sopr o pyl alco ho l
7300 1450 1402 1405 1450 1401 1405 2539 5521 5522 2508 2556 5525
1-4 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.05 1.0 1-2 0.01 - 1.0 0.01 - 1 1-2
IC P !AES G C !FID G C !FID G C -FID G C !FID G C !FID G C -FID G C !F ID /M S HPLC !EC HD HPLC !FL/EC HD G C !FID G C -FID HP LC /UV
ISOP RO PYL A CE TATE ISOP RO PYL A CE TATE V O L A TI LE O R G A N IC C P D S (Screen in g) ALCOHO LS I ISOPROPYL ETHER ISOPROPYL GLYCIDYL ETHER ALIPHATIC ALDEHYDES A L D EH Y D E S, SC R E E N IN G KEPONE NAPHTHAS
G C !FID G C -FID TD /G C !M S
CCT CCT TD
I sopr o pyl alco ho l I sopr o pyl e the r I sopr o pyl glyc idyl ether I sovale r alde hyde I sovale r alde hyde Kepone Kerosene
0.01 - 0.2 0.01 - 0.05 0.01 - 0.2 0.1 - 1.5 0.01 - 0.05 0.5 - 1.0 0.01 - 0.2
2 -b u ta n on e /C S 2 C S2 C S2 ACN t ol b z/M e O H C S2
3/15/2003
MF!13
Chemical Lanthanum
M e th od Na m e ELE M EN TS b y IC P (A Q UA RE G IA A SH IN G ) ELEMENTS on WIPES LEAD by FAAS LEAD BY FIELD POR TABLE XRF LEAD by GFAAS LEAD BY ULTRASOUND /ASV E LE M E NT S b y IC P LEAD in Air by Che mical Spot Test LEAD in Surface Wipe Sa mp les ELE M EN TS b y IC P (A Q UA RE G IA A SH IN G ) ELEMENTS on WIPES E LE M EN TS by IC P (H O T B L O C K /H C l /H N O 3 D IG E S T IO N ) LEAD in DUST WIPES by C h emica l Spot Test L E AD S U LF ID E TERPENES V O L A TI LE O R G A N IC C P D S (Screen in g) A L D R IN a n d LI N DA N E E LE M E NT S b y IC P ELE M EN TS b y IC P (A Q UA RE G IA A SH IN G ) ALKA LINE DU STS E LE M E NT S b y IC P ELE M EN TS b y IC P (A Q UA RE G IA A SH IN G ) E LE M EN TS by IC P (H O T B L O C K /H C l /H N O 3 D IG E S T IO N ) ORG ANOPHO SPHORUS PESTICIDES M A L E IC A N H Y D R ID E MANEB MANEB E LE M E NT S b y IC P ELEMENTS on WIPES ELE M EN TS b y IC P (A Q UA RE G IA A SH IN G ) E LE M EN TS by IC P (H O T B L O C K /H C l /H N O 3 D IG E S T IO N ) KETONES I ISO C YA NA TES , M O NO M ER IC
Flow Ra te ( L /m i n ) 1-4
E x tr a c ti o n
A n a ly t ic a l T e c h n iq u e ICP-AES
Sampler MC EF
H C l /H N O 3
NA 200 - 1500 570 - 1900 1 - 1500 20 - 1500 1250 -2000 10 - 240 NA 50 - 2000
Wipe MC EF MC EF MC EF MC EF MC EF MC EF Wipes MC EF
!
H N O 3/HC lO 4 H C l /H N O 3
Lead Lead
9102 7303
NA 1-4
NA Se e Ta ble
NA H C l /H N O 3
ICP-AES ICP-AES
Wipe MC EF
Lead
9105
NA
NA
NA
Sp ot
Wipe
T HF C S2 t h erma l
XR D G C !FID TD /G C !M S
C Y C & P VC CCT TD
isooctane H N O 3/HC lO 4 H C l /H N O 3
G C !E C N IC P !AES ICP-AES
70 - 1000 5 - 67 5 - 67
HCl H N O 3/HC lO 4 H C l /H N O 3
PTFE MC EF MC EF
M agne sium
7303
1-4
Se e Ta ble
H C l /H N O 3
ICP-AES
MC EF
M alathio n M ale ic A nhydride M ane b M ane b Mang anese Mang anese Mang anese
Mang anese
7303
1-4
Se e Ta ble
H C l /H N O 3
ICP-AES
MC EF
MBK MDI (4,4'!methylene ! b isphe nyl iso c yanate ) MDI (4,4'!methylene ! b isphe nyl iso c yanate ) Me rcury
1300 5521
1 - 10 5 - 500
C S2 rea ge nts
CCT IM P
5522
ISOCYANATES
1-2
15 - 360
tryptamine
HPLC !FL/EC HD
IM P
6009
MER CURY
0.15 - 0.25
2 - 100
H N O 3/H C l
AAS !cold va p
Ho pc alite
3/15/2003
MF!14
Chemical Mercaptans M e sityl o xide M e sityl o xide M eta ls in air M e talwo r k ing F luids
M e th od Na m e M E R C A P TA N S KE TO NE S II KE TO NE S II E LE M E NT S b y IC P META LWO RKING FLUIDS (MW F) ALL CATEGO RIES F O R M A L D E HY D E ORG ANOPHO SPHORUS PESTICIDES M E TH A NO L V O L A TI LE O R G A N IC C P D S (Screen in g) ORG ANIC and INORGANIC G ASES by EX TR ACTIV E FTIR SPE C T R O MET R Y ORG ANONITROGEN PESTICIDES ORG ANONITROGEN PESTICIDES CHLORINATED ORG ANONITROGEN H ER BIC ID ES (A IR SA M PL IN G ) CHLORINATED ORG ANONITROGEN HER BICIDES (HAND WAS H) CHLORINATED ORG ANONITROGEN HE RBIC IDES (DER M AL P ATC H)) ME THYL C ELLO SO LVE A CE TATE ALC O HO LS IV ME THYL A CE TATE ME THYL A CR YLATE ME THYL A CR YLATE M E TH A NO L METHYLAL p -TO LUE NE SU LFO NIC AC ID
Flow Ra te ( L /m i n ) 0.1 - 0.2 0.01 - 0.2 0.01 - 0.2 1-4 1.6 - 2.0
E x tr a c ti o n
H C l/D C E M e O H /C S 2 IP A -C S 2 H N O 3/HC lO 4 D C M/MeO H/T ol MeOH ac eto nitr ile t ol/a cet H 2O/IPA t h erma l
HP LC - U V G C !FPD G C -FID TD /G C !M S
SG/DNPH O VS !2 SG TD
M e thano l
3800
0.1 - 20
Inst r. d ep .
NA
FTIR
Di r. R e a d
HP LC - U V HP LC - U V G C /E C D
M e to lac hlo r
9200
NA
NA
NA
G C - EC D
M e to lac hlo r
9201
NA
NA
IPA/diazomethane
G C - EC D
2 !M etho xye thyl a ce tate 2 !M e tho xye thano l M ethy l ace tate M ethy l acry late M ethy l acry late M e thyl alco ho l M e thylal 4-M eth ylb en ze ne su lfon ic ac id N -Methyl-y-butyrolactone Methyl !(n !am yl) !ketone M eth yla rso nic ac id M e thyl br o m ide Methyl cellosolve M ethy l celloso lve a ce tate M e thyl c hlo r ide Me thyl chloro form Me thyl chloro form
0.01 - 0.2 0.01 - 0.05 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.02 - 0.2 0.01 - 0.2 1-3
N - M E TH Y L -2 - PY R R O L ID I NO N E KE TO NE S II A R S E N IC , O R G A N O ! M E T H YL B RO M I D E ALC O HO LS IV ME THYL C ELLO SO LVE A CE TATE M E T H YL C H LO R I D E HYDROC ARBONS, HALOG ENATED V O L A TI LE O R G A N IC C P D S (Screen in g) AC ETON ITRILE HYDROC ARBONS, BP 36 !216 C M E TH YL CY C LO H EX AN O L M E T H YL C Y C LO H E X A N O N E ISOCYANATES, TOTAL (MAP)
0.05 - 0.2 0.01 - 0.2 1-3 0.01 - 0.1 0.01 - 0.05 0.01 - 0.2 0.01 - 0.1 0.01 - 0.2 0.01 - 0.05
M e thyl c yanide Methyl cyclohexane M e thylc yc lo he xano l Methylcyclohexanone 4,4 '-M eth yle ne -b is (c yc lo he xyl iso cy an ate ) (HM DI)
3/15/2003
MF!15
Chemical 4,4-Methylene-bis (phenyl isoc ya na te) (M DI) M e thyle ne c hlo r ide M e thyle ne c hlo r ide
Flow Ra te ( L /m i n ) 1-2
E x tr a c ti o n
A n a ly t ic a l T e c h n iq u e HP LC /UV
Sampler G F F, IM P
MAP
1005 2549
M E T H YL E N E C H L O R ID E V O L A TI LE O R G A N IC C P D S (Screen in g) ORG ANIC and INORGANIC G ASES by EX TR ACTIV E FTIR SPE C T R O MET R Y 4,4'!M E T H YL E N ED I AN I LI N E ISOCYANATES
C S2 t h erma l
G C -FID TD /G C !M S
2 CCT TD
3800
0.1 - 20
Inst r. d ep .
NA
FTIR
Di r. R e a d
5029 5522
1-2 1-2
10 - 1000 15 - 360
K O H/M e O H tryptamine
GF F/H 2SO 4 IM P
2549
V O L A TI LE O R G A N IC C P D S (Screen in g) M E T H YL E TH Y L K E TO N E KETONES I M E T H YL E TH Y L K E TO N E P E R O X ID E
0.01 - 0.05
1-6
t h erma l
TD /G C !M S
TD
Methyl ethyl ketone Methyl ethyl ketone Methyl ethyl ketone p er o xide 5 !Methyl !3 !heptanone 5-Methyl-3-heptanone M eth yl h ipp ur ic a cid
0.25 - 12 1 - 10 52 - 520
C S2 C S2 reagent
Carbon be ads A -C M S IM P
KE TO NE S II KE TO NE S II HIP PU RIC an d M ETH YL H IPP UR IC ACID in urine M E T H YL IO D I D E ESTERS I ALC O HO LS III ALCOHO LS COM BINED V O L A TI LE O R G A N IC C P D S (Screen in g) KETONES I KETONES I M E R C A P TA N S ME THYL a nd ETH YL M ETHA CR YLATE ORG ANOPHO SPHORUS PESTICIDES V O L A TI LE O R G A N IC C P D S (Screen in g) N - M E TH Y L -2 - PY R R O L ID I NO N E HY DR O C AR BO NS , AR O M ATIC HY DR O C AR BO NS , AR O M ATIC METH YL tert !BUTYL ETHER METHYLTIN CHLORIDES ORG ANOPHO SPHORUS PESTICIDES NAPHTHAS E LE M E NT S b y IC P EL EM EN TS b y IC P (A qu a R eg ia Ashin g) EL EM EN TS b y IC P (H ot B loc k/H C l/ H N O 3 Digestion) ELEMENTS on WIPES ORG ANOPHO SPHORUS PESTICIDES
1 - 25 1 - 25 NA
M e O H /C S 2 IP A -C S 2 Et a c
G C !FID G C -FID HP LC - U V
CCT A -C M S NA
M e thyl io dide M ethy l isoam yl ac etate M e thyl iso butyl c ar binol M e thyl iso butyl c ar binol Methyl isobutyl ketone
0.01 - 1.0 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.05
15 - 50 1 - 10 1 - 10 1 - 10 1-6
t ol C S2 IP A /C S 2 IP A -C S 2 t h erma l
Methyl isobutyl ketone Methyl isobutyl ketone M e thyl me r c aptan M ethy l me tha cryla te M e thyl par athio n M e thyl phe no l
0.01 - 0.2 0.01 - 0.2 0.1 - 0.2 0.01 - 0.05 0.2 - 1 0.01 - 0.05
N -methyl-2-pyrrolidinone
0.05 - 0.2 0.01 - 0.2 0.01 - 0.2 0.1 - 0.2 0.25 - 1 0.2 - 1.0 0.01 - 0.2 1-4 1-4
G C -NP D o r FID G C !FID G C -FID G C !FID GC-FPD G C !FPD G C !FID IC P !AES ICP-AES
M o lybde num
7303
1-4
Se e Ta ble
H C l /H N O 3
ICP-AES
MC EF
9102 5600
NA 0.2 - 1
NA 12 - 240
NA t ol/a cet
ICP-AES G C !FPD
Wipe O VS !2
3/15/2003
MF!16
Chemical Monom ethylaniline Monom ethylhydrazine M yc o bac te rium Nap htha (coal tar) Naphthalene Naphthalene
M e th od Na m e M O N O M E T HY L AN I LI N E M O N O M E T HY L H YD R A Z IN E M YC O BA C TER IUM TUB ER C ULO SIS NAPHTHAS HY DR O C AR BO NS , AR O M ATIC PO LYN UC LEA R A RO M ATIC HYDR OC ARBO NS by H PLC PO LYN UC LEA R A RO M ATIC HYDROC ARBONS ISOCYANATES, TOTAL (MAP)
Vol. (L) min max 11 - 100 3 - 20 va r ies 1.3 - 20 100 - 200 200 - 1000
E x tr a c ti o n
$4
0.01 - 0.2 0.01 - 1.0 2.0
Naphthalene
5515
2.0
200 - 1000
va r ies
G C -FID
P T F E & X A D !2
5525
1-2
1 - 500
MAP
HP LC - U V
G F F, IM P
5518 7303
NAPHTHYLAMINES EL EM EN TS b y IC P (H ot B loc k/H C l/ H N O 3 Digestion) E LE M E NT S b y IC P EL EM EN TS b y IC P (A qu a R eg ia Ashin g) EL EM EN TS b y IC P (H ot B loc k/H C l/ H N O 3 Digestion) ELEMENTS on WIPES NICKEL CARBONYL N I C O TI N E N I C O TI N E AC IDS , INO RG AN IC N I TR IC O X I D E & N IT R O G E N D IO X I D E
30 - 100 Se e Ta ble
acetic a /IPA H C l /H N O 3
G C !FID ICP-AES
GFF & SG MC EF
N i c ke l N i c ke l
7300 7301
1 !4 1-4
25 - 1000 5 - 1000
H N O 3/HC lO 4 H C l /H N O 3
IC P !AES ICP-AES
MC EF MC EF
N i c ke l
7303
1-4
Se e Ta ble
H C l /H N O 3
ICP-AES
MC EF
p !N I TR O A N IL IN E N I TR O A R O M A T IC C O M P O U N D S A N IL IN E , o - TO L U ID I NE , A N D N I TR O B E N Z EN E A N IL IN E , o - TO L U ID I NE , A N D N I TR O B E N Z EN E N I TR O A R O M A T IC C O M P O U N D S N I TR O E T H AN E N I TR IC O X I D E & N IT R O G E N D IO X I D E N I TR O G E N D IO X I D E N I TR O G E N D IO X I D E N ITR O G LY C ER IN & ETH YL EN E G LY C O L DINITRA TE N I TR O M E T H A N E 2 !N I TR O P R O P A N E 1-NITROPYRENE in DIESEL PARTICULATES NITROSAMINES N I TR O A R O M A T IC C O M P O U N D S ORG ANIC and INORGANIC G ASES by EX TR ACTIV E FTIR SPE C T R O MET R Y
20 10 - 150 5 - 50
N i tr o be nzo l
2017
0.2
5 - 50
et h a nol
G C -FID
GFF + SG
p !Nitrochlorobenzene Nitroethane N i tr o ge n dio xide N i tr o ge n dio xide N i tr o ge n pe r o xide Nit ro gly ce rin
Et Ac Et Ac T ol
G C !FPD G C !FID G C /N C D
15 - 1000 1 - 30 Inst r. d ep .
M e O H /C H 2C l2 MeOH NA
T D tu b e SG Di r. R e a d
3/15/2003
MF!17
M e th od Na m e N I TR O U S O X ID E HYDROC ARBONS, BP 36-216 oC N-Methyl-2-Pyrrolidinone PARTICU LATES N.O.R . V O L A TI LE O R G A N IC C P D S (Screen in g) HYDROC ARBONS, BP 36 !216 C V O L A TI LE O R G A N IC C P D S (Screen in g) 1 !O C TA N ETH IO L OIL MIST, MINER AL ORG ANONITROGEN PESTICIDES ORG ANOPHO SPHORUS PESTICIDES
Vol. (L) min max 80% vol 4-4 0.5 - 125 7 - 133 1-6
E x tr a c ti o n
A n a ly t ic a l T e c h n iq u e IR G C -FID GC-FID/NPD G R AV TD /G C !M S
NA C S2 C H 2C l2/M e O H NA t h erma l
n !Octane Oc tam ethylcy clotetra ! siloxane 1 !Oc tane thio l O il m ist (m ine ra l) O r gano nitro ge n pe sticides O r gano pho spho r us Pestic ide s Oxamyl O xyge n PA C
1500 2549
4-4 1-6
C S2 t h erma l
G C !FID TD /G C !M S
CCT TD
G C !FPD IR HP LC - U V G C !FPD
ORG ANONITROGEN PESTICIDES OXYG EN POLY AROM ATIC COMPO UNDS, TOTAL (PACs) EL EM EN TS b y IC P (H ot B loc k/H C l/ H N O 3 Digestion) PARAQUAT ORG ANOPHO SPHORUS PESTICIDES PARTICU LATES N.O.R ., TO T AL PARTICU LATES, N.O .R, RESPIRAB LE
0.1 - 1 NA 1-2
reagent NA hexane
HP LC , U V Sens or FI-FL
Palladium
7303
1-4
Se e Ta ble
H C l /H N O 3
ICP-AES
MC EF
Par aquat Par athio n Par tic ulate s N . O. R. Par tic ulate s N . O. R.
1-4 0.2 - 1.0 1-2 1.7, 2.2, 2.5 0.01 - 0.2 0.01 - 0.2 0.5 - 1.0 1-2 0.01 - 0.05
H 2O t ol/a cet NA NA
PTFE O VS !2 P VC C Y C & P VC
POLYCHLORO BENZENES P E N TA C H L O R O E TH A N E P EN TA C HL OR O PH EN O L PEN TAM IDINE ISETH ION ATE V O L A TI LE O R G A N IC C P D S (Screen in g) HYDROC ARBONS, BP 36 !216 C KETONES I KETONES I PE RC HL O RO ETH YL EN E (p or t G C ) in exha led bre ath a nd a ir V O L A TI LE O R G A N IC C P D S (Screen in g) ORG ANOPHO SPHORUS PESTICIDES ORG ANONITROGEN PESTICIDES NAPHTHAS PO LYN UC LEA R A RO M ATIC HYDR OC ARBO NS by H PLC PO LYN UC LEA R A RO M ATIC HYDROC ARBONS V O L A TI LE O R G A N IC C P D S (Screen in g)
G C !E C D G C !E C D HPLC !U V HPLC/FL TD /G C !M S
C S2 C S2 C S2 NA
Perchloroethylene
2549
0.01 - 0.05
1-6
t h erma l
TD /G C !M S
TD
Phenanthrene
5515
2.0
200 - 1000
va r ies
G C -FID
P T F E & X A D !2
Phe no l
2549
0.01 - 0.05
1-6
t h erma l
TD /G C !M S
TD
3/15/2003
MF!18
Chemical Phe no l Phe nyl e the r Phe nyl e the r!diphenyl mixture Phe nyl glyc idyl ethe r Phenylhydrazine Pho rate Phosdrin (mevinphos) Phosphine Ph os ph or ic a cid Pho spho rus Pho spho rus Pho spho rus
E x tr a c ti o n
Sampler X A D !7 CCT SG
MeOH C S2 bz
PHENYL GLYCIDYL ETHER P H E N YL H Y DR A Z IN E ORG ANOPHO SPHORUS PESTICIDES ORG ANOPHO SPHORUS PESTICIDES P H O S P H IN E AC IDS , INO RG AN IC E LE M E NT S b y IC P PHOSPHOR U S EL EM EN TS b y IC P (A qu a R eg ia Ashin g) EL EM EN TS b y IC P (H ot B loc k/H C l/ H N O 3 Digestion) ELEMENTS on WIPES P H O S P H O R U S T R IC H L O R ID E TERPENES V O L A TI LE O R G A N IC C P D S (Screen in g) E LE M E NT S b y IC P PO LYN UC LEA R A RO M ATIC HYDROC ARBONS SUPER ABSORBENT POLYMER PO LYC YC LIC AR O M ATIC COM POU NDS, TOTAL EL EM EN TS b y IC P (H ot B loc k/H C l/ H N O 3 Digestion) POLY CH LORO BIPHENY LS
0.01 - 1 0.2 - 1.0 0.2 - 1 0.2 - 1 0.01 - 0.2 0.2 - 0.5 1-4 0.01 - 0.2 1-4
CCT B u B/H C l O VS !2 O VS !2 S G / H g( C N )2 S G ( w a s h ed ) MC EF Te na x G C MC EF
H N O 3/HC lO 4 xylene H C l /H N O 3
7303
1-4
Se e Ta ble
H C l /H N O 3
ICP-AES
MC EF
Pho spho rus Pho spho rus tr ic hlor ide Pinene Pinene
NA 11 - 100 2 - 30 1-6
Pla tinum PA H
7300 5506
1-4 2.0
H N O 3/HC lO 4 va r ies
MC EF P T F E & X A D !2
5035 5800
1-2 1-2
50 - 1500 5 - 1000
C u (Ac)2 hexane
IC P or AAS FI-FL
P VC
Platinum
7303
1-4
Se e Ta ble
H C l /H N O 3
ICP-AES
MC EF
5503
0.05 - 0.2
1 - 50
hexane
G C !E C D
7301
EL EM EN TS b y IC P (A qu a R eg ia Ashin g) EL EM EN TS b y IC P (H ot B loc k/H C l/ H N O 3 Digestion) ALKA LINE DU STS E S TR O G E N I C C O M P O U N D S TR IAZ INE HE RB IC IDE S a nd the ir METABOLITES ORG ANONITROGEN PESTICIDES A L D EH Y D E S, SC R E E N IN G ALIPHATIC ALDEHYDES ORG ANONITROGEN PESTICIDES ESTERS I ALC O HO LS II ALCOHO LS COM BINED P R O P Y LE N E D IC H L O R ID E
1-4
5 - 1000
H C l /H N O 3
ICP-AES
MC EF
Po tassium
7303
1-4
Se e Ta ble
H C l /H N O 3
ICP-AES
MC EF
1-4 1 NA
HCl M eth NA
t it ra t ion HP LC - U V GC-M SD
Pr o pham Pr o pio nalde hyde Pr o pio nalde hyde Pr o po xur n !Prop yl ac etate n !Pr o pyl alc o ho l n- Pro pyl alco ho l Pr o pyle ne dic hlor ide
0.1 - 1 0.01 - 0.05 0.1 - 1.5 0.1 - 1 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2
3/15/2003
MF!19
Chemical Pro pyle ne glyc o l Pr o pyle ne glyc o l m o no m e thyl e the r Pr o pyle ne glyc o l mo nom ethy l ethe r ac etate Pr o pyle ne o xide Pyrene
M e th od Na m e
E x tr a c ti o n
A n a ly t ic a l T e c h n iq u e G C !FID G C -FID
Sampler O VS !7 A-747
MeOH M e C l2/Me th
GLYCOL ETHER S
2554
GLYCOL ETHERS
0.1 - 0.2
3 - 25
M e C l2/Me th
G C -FID
A-747
1612 5506
P R O P Y LE N E O X ID E PO LYN UC LEA R A RO M ATIC HYDR OC ARBO NS by H PLC PO LYN UC LEA R A RO M ATIC HYDROCARBONS PYRETHUM P Y R ID I NE R ES O RC IN O L RIB AV IRIN ORG ANOPHO SPHORUS PESTICIDES ROTENONE NAPHTHAS E LE M E NT S b y IC P EL EM EN TS b y IC P (A qu a R eg ia Ashin g) EL EM EN TS b y IC P (H ot B loc k/H C l/ H N O 3 Digestion) ELEMENTS on WIPES SILICA, AMOR PHOUS
CCT P T F E & X A D !2
Pyrene
5515
2.0
200 - 1000
va r ies
G C !FID
P T F E & X A D !2
Pyr e thr um Pyridine R eso rc ino l Rib av irin R onne l Rotenone Rubber solvent S e le nium S e le nium
1-4 0.01 - 1.0 0.2 - 1 1-4 0.2 - 1 1-4 0.01 - 0.2 1-4 1-4
S e le nium
7303
1-4
Se e Ta ble
H C l /H N O 3
ICP-AES
MC EF
9102 7501
NA 1.7 or 2 .2
NA 50 - 400
NA ash
ICP-AES XR D
Silica, crystalline
7500
SILICA, CRYSTALLINE, by XR D
1.7, 2.2, 2.5 1.7, 2.2, 2.5 1.7, 2.2, 2.5 1.7, 2.2, 2.5 1.7, 2.2, 2.5 1-4 1-4
400 - 1000
a s h or T HF
XR D
Silica, crystalline
7601
S IL IC A , C R Y ST A LL IN E
400 - 800
H 3PO 4/HF
VIS
Silica, crystalline
7602
400 - 800
ash
IR
7500
S IL IC A , C R Y ST A LL IN E , b y X R D.
400 - 1000
a s h or T HF
XR D
7603
300 - 1000
ash
IR
C Y C & P VC
S ilve r S ilve r
7300 7301
E LE M E NT S b y IC P EL EM EN TS b y IC P (A qu a R eg ia Ashin g) ELEMENTS on WIPES CHLORINATED ORG ANONITROGEN H ER BIC ID ES (A IR SA M PL IN G ) CHLORINATED ORG ANONITROGEN HER BICIDES (HAND WAS H) CHLORINATED ORG ANONITROGEN HE RBIC IDES (DER M AL P ATC H)) EL EM EN TS b y IC P (H ot B loc k/H C l/ H N O 3 Digestion) FLUORIDES, aerosol & ga s
H N O 3+ H C l /H N O 3
IC P !AES ICP-AES
MC EF MC EF
S ilve r Simazine
9102 5602
NA 0.2 - 1
NA 12 - 480
NA reagent
ICP-AES G C /E C D
Wipe OV S-2
Simazine
9200
NA
NA
NA
G C - EC D
Simazine
9201
NA
NA
IPA/diazomethane
G C - EC D
S o dium
7303
1-4
Se e Ta ble
H C l /H N O 3
ICP-AES
MC EF
7902
1-2
12 - 800
N a OH
ISE
3/15/2003
MF!20
Chemical S odium hexa fluoro !alum inate S o dium hydr o xide Stibine Stoddard solvent S t ro ntium
M e th od Na m e FLU O RID ES by IC
Flow Ra te ( L /m i n ) 1-2
E x tr a c ti o n
A n a ly t ic a l T e c h n iq u e IC
N a OH
ALKA LINE DU STS S T IB IN E NAPHTHAS EL EM EN TS b y IC P (A qu a R eg ia Ashin g) EL EM EN TS b y IC P (H ot B loc k/H C l/ H N O 3 Digestion) ELEMENTS on WIPES S T RY C H N IN E HY DR O C AR BO NS , AR O M ATIC ORG ANIC and INORGANIC G ASES by EX TR ACTIV E FTIR SPE C T R O MET R Y S U LF U R D IO X I D E
HCl HCl C S2 H C l /H N O 3
S t ro ntium
7303
1-4
Se e Ta ble
H C l /H N O 3
ICP-AES
MC EF
NA 70 - 1000 1 - 14 Inst r. D ep .
NA rea ge nts C S2 NA
S ulfur dioxide
6004
0.5 - 1.5
4 - 200
H C O 3-/C O 32-
IC
S ulfur he xafluo ride Su lfur ic a cid S ulfuryl fluo r ide S ulpr o fo s S upe r abso rbe nt po lymer Simazine
S U LF U R H EX A F LU O R ID E AC IDS , INO RG AN IC S U LF U R Y L F L UO R I D E ORG ANOPHO SPHORUS PESTICIDES SUPER ABSORBENT POLYMER TR IAZ INE HE RB IC IDE S a nd the ir METABOLITES 2,4 !D an d 2,4,5 !T MYCO BACTERIUM TUBERCULOSIS, A IR B O R N E E LE M E NT S b y IC P EL EM EN TS b y IC P (A qu a R eg ia Ashin g) EL EM EN TS b y IC P (H ot B loc k/H C l/ H N O 3 Digestion) ELEMENTS on WIPES ORG ANOPHO SPHORUS PESTICIDES TERPENES o !TERPHENYL 1,1,2,2 !T E TR A B R O M O E T H AN E
2,4,5 !T TB
5001 0900
1-3
15 - 200 va r ies
MeOH reagent
HPLC !U V PCR
GFF PTFE
$4
1-4 1-4
T ellurium T ellurium
7300 7301
25 - 2000 25 - 2000
HNO3 H C l /H N O 3
IC P !AES ICP-AES
MC EF MC EF
T ellurium
7303
1-4
Se e Ta ble
H C l /H N O 3
ICP-AES
MC EF
T ellurium T erbufo s T erpe ne s o !Terphenyl 1,1,2,2 !Te tra bro m o ethane Te tra bu tylt in 1,2,4,5 !Tetrachlorobenzene 1,1,2,2 !Tetrach loro ! 2,2-difluoroethane
NA 12 - 240 2 - 30 2 - 30 50 - 100
NA t ol/a cet C S2 C S2 T HF
O R G A N O T IN C O M P O U N D S POLYCHLORO BENZENES 1,1,2,2 !TETRACHLORO !2,2 ! DIFLUOROETHANE & 1,1,2,2 !TETR ACHLOR O !1,2 ! D I FL U O R O E TH A N E 1,1,2,2 !TETRACHLORO !2,2 ! DIFLUOROETHANE & 1,1,2,2 !TETR ACHLOR O !1,2 ! D I FL U O R O E TH A N E 1,1,2,2 !T E TR A C H L O R O E TH A N E 1 , 1, 2 ,2 - TE T RA C H L O R O E TH A N E
50 - 500 3 - 12 0.5 - 2
aaa hexane C S2
HP LC /G FAAS G C !E C D G C !FID
1016
0.01 -0.035
0.5 - 2
C S2
G C !FID
CCT
1019 2562
3 - 30 3 - 30
C S2 C S2
G C !FID G C -FID
PCT A -C M S
3/15/2003
MF!21
M e th od Na m e HYDROC ARBONS, HALOG ENATED PE RC HL O RO ETH YL EN E (p or t G C ) in exha led bre ath a nd a ir GLYC OLS TETR AETHYL LEAD (as Pb ) TETRA ETHY L PYRO PHO SPH ATE ORG ANIC and INORGANIC G ASES by EX TR ACTIV E FTIR SPE C T R O MET R Y TETR AHYDR OFU R AN ORG ANIC and INORGANIC G ASES by EX TR ACTIV E FTIR SPE C T R O MET R Y TETRKIS(HYDR OX YM ETHYL) P H O S P H O N IU M C H L O R ID E TETRAMETHYL LEAD (as P b ) TETRAMETHYL THIOUREA T E TR A N IT R O M E TH A N E E LE M E NT S b y IC P EL EM EN TS b y IC P (A qu a R eg ia Ashin g) EL EM EN TS b y IC P (H ot B loc k/H C l/ H N O 3 Digestion) ORG ANONITROGEN PESTICIDES CAPTAN and THIOPHENATE-METHYL o n D E RM A L P A TC H CAPTAN and THIOPHENATE-METHYL in Hand Rinse THIO PH EN ATE -M ETH YL in AIR THIRAM EL EM EN TS b y IC P (A qu a R eg ia Ashin g) EL EM EN TS b y IC P (H ot B loc k/H C l/ H N O 3 Digestion) ORG ANOTIN CPDS. (as Sn) E LE M E NT S b y IC P EL EM EN TS b y IC P (A qu a R eg ia Ashin g) EL EM EN TS b y IC P (H ot B loc k/H C l/ H N O 3 Digestion) V O L A TI LE O R G A N IC C P D S (Screen in g) TOLU ENE (Diffusive sam pler) HYDROC ARBONS, BP 36 !216 C HY DR O C AR BO NS , AR O M ATIC ORG ANIC and INORGANIC G ASES by EX TR ACTIV E FTIR SPE C T R O MET R Y 2,4 ! & 2,6 !T O L UE N E D IA M I N E T O L UE N E !2,4 !DIISO CY ANA TE ISO C YA NA TES , M O NO M ER IC
E x tr a c ti o n
A n a ly t ic a l T e c h n iq u e G C -FID Po rt G C -PID
C S2 NA
T etr ae thyle ne glyc o l T etr ae thyl lead Tetra ethy l pyro ph osp ha te Tetrafluoroethylene
5 - 60 30 - 200 20 - 48 Inst r. d ep .
O VS !7 X A D !2 2 Chrom 102 Di r. R e a d
1609 3800
1-9 Inst r. d ep .
C S2 NA
G C !FID FTIR
CCT Di r. R e a d
Te tra kis (hy dr ox ym eth yl) p ho spho nium c hlo ride T etr am e thyl lead T etr am e thyl thio ur e a Tetranitromethane T hallium T hallium
5046
1 - 1.7
1 - 400
ACN
HP LC - U V
GFF
X A D !2 IMP /H 2O I M P /E t A c MC EF MC EF
!
H N O 3/HC lO 4 H C l /H N O 3
T hallium
7303
1-4
Se e Ta ble
H C l /H N O 3
ICP-AES
MC EF
5601 9205
0.1 - 1 NA
var - 480 NA
reagent IP A /A C N
HP LC , U V HP LC - U V
OV S-2 Patch
Thiophenate-methyl
9202
NA
NA
NA
HP LC - U V
Hand wa sh
IP A /A C N C H 3C N H C l /H N O 3
HP LC - U V HPLC !U V ICP-AES
QFF/SST PTFE MC EF
Tin
7303
1-4
Se e Ta ble
H C l /H N O 3
ICP-AES
MC EF
a c etic a /C H 3C N H N O 3/HC lO 4 H C l /H N O 3
G F F & X A D !2 MC EF MC EF
T itanium
7303
1-4
Se e Ta ble
H C l /H N O 3
ICP-AES
MC EF
Toluene
2549
0.01 - 0.05
1-6
t h erma l
TD /G C !M S
TD
C S2 C S2 C S2 NA
2,4 & 2,6 !Toluenediamine Toluene !2,4 !diisoc ya nate Toluene !2,4 !diisoc ya nate
a ce ty la te /M e O H MeOH a ce ty la te /M e O H
IM P GW coated IM P
3/15/2003
MF!22
Chemical Toluene !2,4 !diisoc ya nate Tolue ne 2 ,4-d issoc ya nate (2,4 -TD I) Toluene !2,6 !diisoc ya nate Toluene !2,6 !diisoc ya nate Tolue ne-2 ,6-d iisocy ana te (2,6 -TD I) p -To lue ne su lfon ic a cid o !Toluidine o !Toluidine
E x tr a c ti o n
A n a ly t ic a l T e c h n iq u e HPLC !FL/EC HD HP LC - U V IM P
Sampler
tryptamine/DMSO MAP
G F F, IM P
tryptamine/DMSO a ce ty la te /M e O H MAP
IM P IM P G F F, IM P
P-TO LUE NE SU LFO NIC AC ID AM INE S, A RO M ATIC A N IL IN E , o - TO L U ID I NE , A N D N I TR O B E N Z EN E DYES ANALINE an d o-TOLUIDINE in urine ANALINE an d o-TOLUIDINE in urine HYDROC ARBONS, HALOG ENATED TRIBUTY L PHO SPH ATE O R G A N O T IN C O M P O U N D S POLYCHLORO BENZENES HYDROC ARBONS, HALOG ENATED HYDROC ARBONS, HALOG ENATED V O L A TI LE O R G A N IC C P D S (Screen in g) HYDROC ARBONS, HALOG ENATED T R IC H L O R O E TH Y L EN E TR IC H LO R O ETH YL EN E b y p ort G C ORG ANIC and INORGANIC G ASES by EX TR ACTIV E FTIR SPE C T R O MET R Y F L UO R O T R IC H L O R O M E T H A NE HYDROC ARBONS, HALOG ENATED HYDROC ARBONS, HALOG ENATED O R G A N O T IN C O M P O U N D S 1,1,2 !TRICHLOR O !1,2,2 ! T R IF L UO R O E T H A N E V O L A TI LE O R G A N IC C P D S (Screen in g) AM INO ETH AN O L C O M PO UN DS II GLYC OLS ETHYLENEDIAMINE, DIETHY LENE TRIAM INE, & T R IE T HY L EN E TE T RA M I N E T R IF L UO R O B R O M O M E T HA N E T R IM E L LI TI C A N HY D R ID E 2,4,7 !TRINITR O !FLUOREN !9 !O N E TRIOR THO CR ESYL P HO SPH ATE TRIPHE NYL P HO SPH ATE T R IP H E N YL TI N C H L O R ID E
10 - 1000 10 - 150 5 - 50
HP LC - U V G C !FID G C -FID
GFF SG GFF + SG
o !Toluidine o !Toluidine o-Toluidine Tribromomethane Tributy l pho sph ate T ri butyltin c hlo r ide 1,2,4 !Trichlorobenzene 1,1,2 !Trichloroethane 1,1,1 !Trichloroethane 1,1,1 !Trichloroethane
5013 8317 8313 1003 5034 5504 5517 1003 1003 2549
1-3 NA NA 0.01 - 0.2 1-3 1 - 1.5 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.05
C S2 C S2 NA NA
Trichlorofluoromethane Trichloromethane 1,2,3 !Trichloropropane T ri c hcylohe xyltin hydrox ide 1,1,2 !Tric hlo r o 1,2,2 !trifluoroethane 1,1,2 !Tric hlo r o 1,2,2 !trifluoroethane Triethanolamine T ri e thyle ne glyc o l Triethylenetetramine
C S2 C S2 C S2 a c etic a /C H 3C N C S2
2549
0.01 - 0.05
1-6
t h erma l
TD /G C -M S
TD
5 - 300 5 - 60 1 - 20
IC G C -FID HP LC - U V
Trifluorobromomethane T ri m e llitic anhydride 2,4,7 !Trin it ro flu o re n !9!o n e Triortho cre syl ph osp ha te Triphe nyl p ho sph ate T ri phenyltin c hlo r ide
2 C C T(lg + sm ) P VC PTFE MC EF MC EF P VC
3/15/2003
MF!23
M e th od Na m e M YC O BA C TER IUM TUB ER C ULO SIS EL EM EN TS b y IC P (A qu a R eg ia Ashin g) TU NGSTEN (sol ubl e/i nso lu b le) T U RP E N TI N E V O L A TI LE O R G A N IC C P D S (Screen in g) HYDROC ARBONS, BP 36-216 oC ALIPHATIC ALDEHYDES V A L ER A L D EH Y D E A L D EH Y D E S, SC R E E N IN G E LE M E NT S b y IC P EL EM EN TS b y IC P (A qu a R eg ia Ashin g) EL EM EN TS b y IC P (H ot B loc k/H C l/ H N O 3 Digestion) ELEMENTS on WIPES VANADIUM OX IDES VINYL A CE TATE HY DR O C AR BO NS , AR O M ATIC V IN Y L B R O M I D E V IN Y L C H L O R ID E V IN Y L ID E N E C H LO R I D E ORG ANIC and INORGANIC G ASES by EX TR ACTIV E FTIR SPE C T R O MET R Y HY DR O C AR BO NS , AR O M ATIC NAPHTHAS V O L A TI LE O R G A N IC C P D S (Screen in g) W AR FA RIN M E TH A NO L V O L A TI LE O R G A N IC C P D S (Screen in g) HY DR O C AR BO NS , AR O M ATIC ORG ANIC and INORGANIC G ASES by EX TR ACTIV E FTIR SPE C T R O MET R Y ORG ANIC and INORGANIC G ASES by EX TR ACTIV E FTIR SPE C T R O MET R Y ORG ANIC and INORGANIC G ASES by EX TR ACTIV E FTIR SPE C T R O MET R Y AM INE S, A RO M ATIC E LE M E NT S b y IC P EL EM EN TS b y IC P (A qu a R eg ia Ashin g) EL EM EN TS b y IC P (H ot B loc k/H C l/ H N O 3 Digestion) ELEMENTS on WIPES
Flow Ra te ( L /m i n )
E x tr a c ti o n
A n a ly t ic a l T e c h n iq u e PCR ICP-AES
Sampler PTFE MC EF
$4
1-4
va r ies 50 - 1000
reagent H C l /H N O 3
H F /H N O 3 C S2 t h erma l
FAAS G C -FID TD /G C -M S
MC EF CCT TD
n-Undecane V a ler alde hyde V a ler alde hyde V a ler alde hyde V a nadium V a nadium
0.01 - 0.05 0.1 - 1.5 0.01 - 0.04 0.01 - 0.05 1-4 1-4
CCT SG-DNPH X AD -2 /H M P X AD -2 /H M P MC EF MC EF
V a nadium
7303
1-4
Se e Ta ble
H C l /H N O 3
ICP-AES
MC EF
V a nadium V a nadium o xide s Viny l ace tate Vinyl benzene V i nyl br o m ide V i nyl c hlor ide V i nylide ne c hlo r ide V i nylide ne F luo r ide
NA 1.7 or 2 .2 0.1 - 0.2 .01 - 1 0.01 - 0.2 0.05 0.01 - 0.2 0.1 - 20
NA T HF C H 2C l2/M e O H C S2 Et h a nol C S2 C S2 NA
1 - 24 1.3 - 20 1-6
C S2 C S2 t h erma l
G C !FID G C !FID TD /G C !M S
CCT CCT TD
HPLC !U V G C !FID TD /G C !M S
PTFE SG TD
1501 3800
2 - 23 Inst r. d ep .
C S2 NA
G C !FID FTIR
CCT Di r. R e a d
m -Xylene
3800
0.1 - 20
Inst r. d ep .
NA
FTIR
Di r. R e a d
o-Xylene
3800
0.1 - 20
Inst r. d ep .
NA
FTIR
Di r. R e a d
3 - 20 5 - 1000 5 - 1000
Et h a nol H N O 3/HC lO 4 H C l /H N O 3
SG MC EF MC EF
Y ttr ium
7303
1-4
Se e Ta ble
H C l /H N O 3
ICP-AES
MC EF
Y ttr ium
9102
NA
NA
NA
ICP-AES
Wipe
3/15/2003
MF!24
M e th od Na m e ZINC and compounds, as Zn E LE M E NT S b y IC P EL EM EN TS b y IC P (A qu a R eg ia Ashin g) EL EM EN TS b y IC P (H ot B loc k/H C l/ H N O 3 Digestion) ELEMENTS on WIPES Z IN C O X I D E E LE M E NT S b y IC P EL EM EN TS b y IC P (A qu a R eg ia Ashin g) ELEMENTS on WIPES
E x tr a c ti o n
Sampler MC EF MC EF MC EF
HNO3 H N O 3/HC lO 4 H C l /H N O 3
Zinc
7303
1-4
Se e Ta ble
H C l /H N O 3
ICP-AES
MC EF
NA -H N O 3/HC lO 4 H C l /H N O 3
Wipe P VC MC EF MC EF
9102
NA
NA
NA
ICP-AES
Wipe
0500 0600 0800 0801 0900 1000 1001 1002 1003 1004 1005 1006 1007 1008 1009 1010 1011 1012 1013 1014 1015 1016
PARTICU LATES N.O.R . PARTICULATES, N.O.R, RESP. B IO A E R O S O L SA M P L IN G A ER O BIC B AC TE RIA - G C -F AM E MYCO BACTERIUM TUBERCULOSIS A L LY L C H LO R I D E M E T H YL C H LO R I D E
1-2 1.7, 2.2 ,2.5 28.3 28.3 4 0.01 - 1.0 0.01 - 0.1 0.01 - 0.1 0.01 - 0.2 0.01 - 1.0 0.01 - 0.2 0.01 - 0.05 0.05 0.02 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 1.0 0.01 - 0.2 0.01 -0.035
7 - 133 20 - 400 va r ies 50 - 300 va r ies 16 - 100 0.4 - 3 1.5 - 8 3 - 70 2 - 15 0.5 - 2.5 0.3 - 7 0.7 - 5 0.1 - 25 2 - 10 2 - 30 0.5 - 4 2.5 - 10 0.1 - 3.5 15 - 50 2.5 - 7 0.5 - 2
G R AV Grav. va r ies G C -FID PCR G C !FID G C !FID G C !FID G C !FID G C !FID G C !FID G C !FID G C !FID G C !E C D G C !FID G C !FID G C !FID G C !FID G C !E C N G C !FID G C !FID G C !FID
P VC CY C & P VC i m p a c to r I m p a c to r PTFE CCT 2 C C T (lg + sm ) CCT CCT CCT 2 CCT C CT ( lg ) 2 CCT CCT C CT ( lg ) CCT CCT 2 CCT PCT CCT CCT CCT
$!C H L O R O P R E N E
HYDROC ARBONS, HALOG ENATED DICHLOROETHYL ETHER M E T H YL E N E C H L O R ID E F L UO R O T R IC H L O R O M E T H A NE V IN Y L C H L O R ID E E T HY L EN E D IB R O M I D E V IN Y L B R O M I D E EP ICH LO RO HY DR IN E T HY L BR O M I D E D I FL U O R O D IB R O M O M E T H A N E P R O P Y LE N E D IC H L O R ID E M E T H YL IO D I D E V IN Y L ID E N E C H LO R I D E 1,1,2,2 !TETRACHLORO !2,2 ! DIFLUOROETHANE & 1,1,2,2 !TETR ACHLOR O !1,2 ! D I FL U O R O E TH A N E T R IF L UO R O B R O M O M E T HA N E DICHLORODIFLUORO METHANE, 1,2 !DICHLOROTETR AFLU O R O ! ETHANE& C H L O R O D IF L UO R O M E T H A N E 1,1,2,2 !T E TR A C H L O R O E TH A N E 1,1,2 !TRICHLOR O !1,2,2 ! T R IF L UO R O E T H A N E T R IC H L O R O E TH Y L EN E
1017 1018
0.1 - 1 1-4
C H 2C l2 C H 2C l2
G C -FID G C !FID
1019 1020
3 - 30 0.1 - 3
C S2 C S2
G C !FID G C -FID
PCT CCT
1022 3/15/2003
1 - 30
C S2
G C -FID
CCT
Chemical
M eth No. 1024 1025 1026 1300 1301 1302 1400 1401 1402 1403 1404 1405 1450 1451 1452 1453 1454 1457 1458 1459 1460 1500 1501 1550 1551 1552 1600 1601 1602 1603 1604 1606 1608 1609 1610 1611 1612 1613 1614 1615 1616 1617
M e th od Na m e 1,3 !B U TA D IE N E 1 - a n d 2 -B R O M O P R O P A N E P- C H LO R O B E N Z O T RI FL U O R ID E KETONES I KE TO NE S II N - M E TH Y L -2 - PY R R O L ID I NO N E ALCOHO LS I ALC O HO LS II ALC O HO LS III ALC O HO LS IV M E TH YL CY C LO H EX AN O L ALCOHO LS COM BINED ESTERS I ME THYL C ELLO SO LVE A CE TATE ETHY L FO RM ATE VINYL A CE TATE ISOP RO PYL A CE TATE ETHY L AC ETATE ME THYL A CE TATE ME THYL A CR YLATE ISOP RO PYL A CE TATE HYDROC ARBONS, BP 36 !216 C HY DR O C AR BO NS , AR O M ATIC NAPHTHAS T U RP E N TI N E TERPENES C A R B O N D IS U LF ID E 1,1 !DICHLORO !1 !N I TR O E T H AN E D I O X AN E AC ETIC AC ID AC RYLO NITRILE AC ETON ITRILE G LY C ID O L TETR AHYDR OFU R AN ETHYL ETHER METHYLAL P R O P Y LE N E O X ID E P Y R ID I NE E T HY L EN E O X ID E METH YL tert !BUTYL ETHER BUTYL GLYCIDYL ETHER PHENYL ETHER
Flow Ra te ( L /m i n ) 0.01 - 0.5 0.01 - 0.2 0.01 - 0.2 0.01 - 2.0 0.01 - 0.2 0.05 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.05 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.1 - 0.2 0.02 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.02 - 0.2 0.01 - 0.2 0.01 - 1.0 0.01 - 0.2 0.01 - 0.2 0.01 - 2 0.01 - 0.2 0.01 - 1.0 0.01 - 0.2 0.01 - 0.1 0.01 - 0.2 0.01 - 0.2 0.01 - 1.0 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 1.0 0.05 - 0.15 0.1 - 0.2 0.01 - 0.2 0.01 - 0.2
Vol. (L) min max 5 - 25 0.1 - 12 0.1 - 10 1 - 10 1 - 25 0.5 - 125 1 - 10 2 - 10 1 - 10 6 - 50 1 - 15 2 - 10 1 - 10 0.2 - 20 0.3 - 10 0.75 - 24 0.1 - 9 0.1 - 10 0.2 - 10 1-5 0.1 - 9 2-7 1 - 30 1.3 - 20 1 - 10 2 - 30 2 - 25 1.5 - 15 0.5 - 15 20 - 300 3.5 - 20 1 - 25 5 - 100 1-9 0.25 - 3 1-3 0.5 - 5 18 - 150 1 - 24 2 - 96 15 - 30 1 - 50
E x tr a c ti o n
A n a ly t ic a l T e c h n iq u e G C !FID G C -FID G C -FID G C !FID G C !FID GC-FID/NPD G C !FID G C !FID C G !FID G C !FID G C !FID G C -FID G C !FID G C !FID G C !FID G C -FID G C !FID G C !FID G C !FID G C !FID G C -FID G C !FID G C !FID G C !FID G C -FID G C !FID G C !FPD G C !FID G C !FID G C !FID G C !FID G C !FID G C !FID G C !FID G C !FID G C !FID G C !FID G C !FID G C !E C D G C !FID G C !FID G C !FID
Sampler CCT CCT CCT CCT CCT CCT CCT CCT CCT CCT CCT CCT CCT CCT CCT MS(carbon) CCT CCT CCT CCT CCT CCT CCT CCT CCT CCT C CT & d ry tu b e PCT CCT CCT CCT CCT CCT CCT CCT CCT CCT CCT PC T w/HB r 2 CC T ( lg ) CCT CCT
3/15/2003
MF!26
Chemical
M e th od Na m e ISOPROPYL ETHER PHENYL GLYCIDYL ETHER ISOPROPYL GLYCIDYL ETHER M E TH A NO L AM INE S, A RO M ATIC 1,1,2,2 !T E TR A B R O M O E T H AN E DIMETHYLACETAMIDE and D I M E TH Y L FO R M A M I D E N I TR O A R O M A T IC C O M P O U N D S AMINOETHANO L COM POUNDS I C HLO RO AC ETIC AC ID AM INE S, A LIPH ATIC FO RM IC A C ID
Flow Ra te ( L /m i n ) 0.01 - 0.05 0.01 - 1 0.01 - 0.2 0.02 - 0.2 0.2 - 1.0 0.2 - 1.0 0.01 - 1.0
E x tr a c ti o n
1 - 150 4 - 24 1 - 100 3 - 30 1 - 24
SG SG SG SG P T FE & S G ( w a s h ed ) S G + H 2SO 4 SG SG SG SG/DNPH GFF + SG w/H 2SO 4 SG-DNPH Carbon be ads X A D !2 /H M P 2 Chrom 102 Por Q P or Q S T e n a x!G C
n !B U TY L AM I N E PHENYL ETHER !DIPHENYL MIXT U R E p !C H L O RO P H EN O L C H L O R O A C E T AL D E HY D E F O R M A L D E HY D E A N IL IN E , o - TO L U ID I NE , A N D N I TR O B E N Z EN E ALIPHATIC ALDEHYDES M E T H YL E TH Y L K E TO N E AC RO LEIN TETRA ETHY L PYRO PHO SPH ATE F UR FU RY L A LC O H O L AC ETO NE CY AN O HY DR IN N ITR O G LY C ER IN & ETH YL EN E G LY C O L DINITRA TE I SO P H O R O N E 1 !O C TA N ETH IO L ETH YLE NE CH LO RO HY DR IN A N IS ID I NE D I AZ O M E T H A N E D I C H LO R O F L U O R O M E T HA N E P E N TA C H L O R O E TH A N E HEXACHLOR O !1,3 !CYC LO P EN T AD I EN E E T HY L C H LO R I D E M E T H YL B RO M I D E
0.01 - 1.0 0.01 - 0.2 0.05 - 0.2 0.05 - 0.2 0.03 - 1.5 0.2
2 - 100 1 - 40 1.5 - 40 3 - 16 1 - 15 5 - 50
0.1 - 1.5 0.01 - 0.2 0.01 - 0.1 0.01 - 0.2 0.01 - 0.05 0.2 0.2 - 1.0
0.01 - 1.0 0.01 - 0.2 0.01 - 0.2 0.5 - 1.0 0.2 0.01 - 0.05 0.01 - 0.2 0.01 - 0.2
2519 2520
0.3 - 3 1-5
C S2 C S2
G C !FID G C !AED
2 CC T ( lg ) PC T(2)+d ry tube Por Q The rma loso rb/N Chrom104/ ma leic anh .
M E T H YL C Y C LO H E X A N O N E NITROSAMINES 1,3 !C Y C L O P E N TA D IE N E
a cet M e O H /C H 2C l2 Et Ac
3/15/2003
MF!27
Chemical
M eth No. 2524 2525 2526 2527 2528 2529 2530 2532 2533 2534 2535 2536 2537 2538 2539 2540
M e th od Na m e DIM ETHY L SULFA TE n !BU TYL MER CAPTAN N I TR O E T H AN E N I TR O M E T H A N E 2 !N I TR O P R O P A N E FU R FU R AL DIPHENYL G L U TA R A LD E H Y D E TETR AETHYL LEAD (as Pb ) TETR AMETHYL LEAD (as P b ) T O L UE N E !2,4 !DIISO CY ANA TE V A L ER A L D EH Y D E ME THYL a nd ETH YL M ETHA CR YLATE A C E T AL D E HY D E A L D EH Y D E S, SC R E E N IN G ETHY LENE DIAM INE, DIETHY LENE TRIAM INE, & T R IE T HY L EN E TE T RA M I N E F O R M A L D E HY D E M E R C A P TA N S H E X A C H LO R O B U T A D IE N E N I C O TI N E ALLYL GLYCIDYL ETHER V O L A TI LE O R G A N IC C P D S (Screen in g) B EN ZO TH IA ZO LE IN AS PH A LT F UM E N I C O TI N E ME THYL A CR YLATE KE TO NE S II GLYCOL ETHER S KETONES I
Flow Ra te ( L /m i n ) 0.01 - 0.2 0.01 - 0.05 0.01 - 0.05 0.01 - 0.05 0.01 - 0.05 0.01 - 0.05 0.01 - 0.5 0.01 - 0.08 0.01 - 1.0 0.01 - 0.2 0.2 - 1.0 0.01 - 0.04 0.01 - 0.05 0.01 - 0.05 0.01 - 0.05 0.01 - 0.1
Vol. (L) min max 0.25 - 12 1-4 1.5 - 3 1.2 - 3 0.1 - 2 1 - 12 15 - 30 4 - 39 30 - 200 15 - 100 2 - 170 0.5 - 10 1-8 1 - 12 5-5 1 - 20
E x tr a c ti o n
A n a ly t ic a l T e c h n iq u e G C !E C N G C !FPD G C !FID G C !FPD G C !FID G C !FID G C !FID HPLC !U V G C !PID G C !PID HPLC !U V G C -FID G C !FID G C !F ID G C !F ID /M S HPLC !U V
Sampler Por P Chrom 104 2 X A D !2 Chrom 106 Chrom 106 X A D !2 /H M P Te na x G C SG/DNPH X A D !2 X A D !2 GW coated X AD -2 /H M P X A D !2 X A D !2 /H M P X A D !2 X A D !2 w/10 % N ITC
0.01 - 0.1 0.1 - 0.2 0.05 - 0.2 1.0 0.01 - 0.2 0.01 - 0.05
X A D !2 /H M P GFF/HgAc X A D !2 X A D !2 Tenax TD
1.0 - 2.0 0.1 - 1.0 0.01 - 0.2 0.01 - 0.2 0.1 - 0.2 0.01 - 0.2
480 - 960 0.5 - 600 1-5 1 - 25 3 - 25 0.5 - 3.0 1 - 10 2 - 25 1 - 10 1 - 10 48 - 960 480 - 960
2561
0.02 - 1
10 - 24
MeOH
G C -FID
XAD
0.01 - 0.2 0.2 - 1.0 0.2 - 1.0 0.2 - 1.0 0.2 - 1.0
3/15/2003
MF!28
Chemical
M eth No. 3507 3508 3509 3510 3511 3512 3513 3514 3515 3516 3518 3600 3601 3700 3701 3702 3704
M e th od Na m e A C E T AL D E HY D E M E T H YL E TH Y L K E TO N E P E R O X ID E AM INO ETH AN O L C O M PO UN DS II M O N O M E T HY L H YD R A Z IN E M O N O M E T HY L AN I LI N E M A L E IC A N H Y D R ID E T E TR A N IT R O M E TH A N E E T HY L EN I M IN E 1,1 !D I M E TH Y L HY D R A Z IN E C R O T O N A L D EH Y D E P H E N YL H Y DR A Z IN E MANEB MANEB B EN ZE NE by po rta ble G C TR IC H LO R O ETH YL EN E b y p ort G C E TH YL EN E O X ID E b y p orta ble G C P ER C H LO R O E TH Y LE N E (p o rta b le G C ) in e xh ale d b rea th a nd air ORG ANIC and INORGANIC G ASES by EX TR ACTIV E FTIR SPE C T R O MET R Y TOLU ENE (Diffusive sam pler) C A R BO N B LA C K 2,4 !D an d 2,4,5 !T W AR FA RIN PARAQUAT H Y D R O Q U IN O N E THIRAM CARBARYL ROTENONE PYRETHUM B E N Z O Y L P E R O X ID E BRO MO XYN IL and B 'OC TANO ATE ETHYLENE THIOUREA EPN DYES CH LORINA TED TERPH ENYL S T RY C H N IN E DIBUTY L PHO SPH ATE 2,4,7 !TRINITR O !FLUOREN !9 !O N E AZ ELA IC A C ID D I BU T YL P HT H A LA T E & DI(2 !ETHY LHEX YL) PHTH ALATE o !TERPHENYL ARSENIC, organo!
Flow Ra te ( L /m i n ) 0.1 - 0.5 0.5 - 0.2 0.5 - 1.0 0.5 - 1.5 0.2 - 1.0 0.2 - 1.5 0.5 - 1.0 0.2 0.2 - 1.0 0.1 - 0.2 0.2 - 1.0 NA NA > 0.02 > 0.02 > 0.02 0.1 - 1
Vol. (L) min max 6 - 60 52 - 520 5 - 300 3 - 20 11 - 100 40 - 500 20 - 250 1 - 48 2 - 100 1 - 49 25 - 120 NA NA 80% vol 80% vol 80% vol 8 0% V O L
E x tr a c ti o n
A n a ly t ic a l T e c h n iq u e HPLC !U V VIS IC VIS G C !FID HPLC !U V G C !FID HPLC !U V VIS DPP VIS HP LC - U V HP LC - U V GC GC -port G C !PID Po rt G C -PID BuB IM P IM P
Sampler
B u B/H C l BuB /H 2SO 4 BuB /H 2O I M P /E t A c BuB Bu B (. 1 M HC l) BuB B u B/H C l Patch Hand wa sh air bag air bag air bag air bag
3800
0.1 - 20
Inst r. d ep .
NA
FTIR
Di r. R e a d
4000 5000 5001 5002 5003 5004 5005 5006 5007 5008 5009 5010 5011 5012 5013 5014 5016 5017 5018 5019 5020
NA 1-2 1-3 1-4 1-4 1-4 1-4 1-3 1-4 1-4 1-3 1-3 1-3 1-2 1-3 1-3 1-3 1-3 1-3 1-3 1-3
15 min-8h 30 - 570 15 - 200 200 - 1000 40 - 1000 30 - 180 10 - 400 20 - 400 8 - 400 20 - 400 40 - 400 2 - 400 200 - 800 15 - 700 150 - 500 100 - 1500 70 - 1000 50 - 250 100 - 500 200 - 1000 6 - 200
C S2 NA MeOH MeOH H 2O ac etic ac id C H 3C N reagent C H 3C N C H 3C N d ieth y l et h er C H 3C N H 2O isooctane H 2O isooctane rea ge nts C H 3C N toluene Et h a nol C S2
G C !FID Grav HPLC !U V HPLC !U V HPLC !U V HPLC !U V HPLC !U V VIS HPLC !U V HPLC !U V HPLC !U V HPLC !U V VIS G C !FPD HPLC !U V G C !E C D HPLC !U V G C !FPD HP LC - U V G C !FID G C !FID
Diffusive P VC GFF PTFE PTFE MC EF PTFE GFF PTFE GFF MC EF PTFE PVC or MCEF GFF PTFE GFF GFF PTFE PTFE P VC MC EF
2 - 30 50 - 1000
C S2 b u ffer
G C !FID IC !HYAAS
PTFE PTFE
Chemical
M eth No. 5025 5026 5027 5029 5030 5031 5032 5033 5034 5035 5036 5037 5038 5039 5040
M e th od Na m e C H L O R IN A T ED D IP H E N YL O X ID E OIL MIST, MINER AL RIB AV IRIN 4,4'!M E T H YL E N ED I AN I LI N E C YA NU RIC AC ID A SP AR TA M E PEN TAM IDINE ISETH ION ATE p !N I TR O A N IL IN E TRIBUTY L PHO SPH ATE SUPER ABSORBENT POLYMER T R IM E L LI TI C A N HY D R ID E TRIOR THO CR ESYL P HO SPH ATE TRIPHE NYL P HO SPH ATE C H L O R IN A T ED C A M P H E N E ELEMENTAL CARBON (DIESEL PARTICULATE) C AP SA ICIN an d D IHY DR O C AP SA ICIN B E N Z EN E S O LU B LE F R AC T IO N A N D TOTAL PARTICULATE (ASPHALT FUME) p -TO LUE NE SU LFO NIC AC ID E S TR O G E N I C C O M P O U N D S TETRAKIS (HYD RO XYM ETHYL) P H O S P H O N IU M C H L O R ID E A L D R IN & L IN D A N E POLY CH LORO BIPHENY LS O R G A N O T IN C O M P O U N D S PO LYN UC LEA R A RO M ATIC HYDROC ARBONS KEPONE BENZIDINE and 3,3'!DICHLORO !B E N Z ID I NE CHLORDANE
Flow Ra te ( L /m i n ) 0.5 - 1.5 1-3 1-4 1-2 1-3 1-3 1-2 1-3 1-3 1-3 1.5 - 2 1-3 1-3 0.2 - 1 2-4
Vol. (L) min max 8 - 200 20 - 500 5 - 1000 10 - 1000 10 - 1000 70 - 1200 50 - 1500 20 2 - 100 50 - 1500 400 - 1000 2 - 100 10 - 400 2 - 30 142 -19000
E x tr a c ti o n
A n a ly t ic a l T e c h n iq u e G C !E C N IR HPLC !U V HPLC !U V HPLC !U V HPLC !U V HPLC/FL HPLC !U V G C !FPD IC P or AAS G C -FID GC-FPD GC-FPD G C !E C D E G A/TO A
isooctane C C l4 H 2SO 4 K O H/M e O H rea ge nts eluent rea ge nts IPA d ieth y l et h er C u (Ac)2 MeOH d ieth y l et h er d ieth y l et h er p et eth er t h erma l
5041 5042
1-3 1 -4
5 - 1000 28 - 400
C H 3C N benzene
1-3 1 1 - 1.7
HP LC - U V HP LC - U V HP LC - U V
5508 5509
50 - 600 20 - 100
G C !E C D HPLC !U V
M C E F & IM P GFF
5510
0.5 - 1.0
10 - 200
G C !E C D
P EN TA C HL OR O PH EN O L D EM E TO N PO LYN UC LEA R A RO M ATIC HYDROC ARBONS 2,4 ! & 2,6 !T O L UE N E D IA M I N E POLYCHLORO BENZENES NAPHTHYLAMINES EN DR IN
MeOH t ol va r ies
HPLC !U V G C !E C D G C !FID G C !E C D
5 - 500 15 - 360 5 - 60
3/15/2003
MF!30
Chemical
M e th od Na m e META LWO RKING FLUIDS (MW F) ALL CATEGO RIES ISOCYANATES, TOTAL (MAP) METHYLTIN CHLORIDES T R IP H E N YL TI N C H L O R ID E ORG ANOPHO SPHORUS PESTICIDES ORG ANONITROGEN PESTICIDES CHLORINATED ORG ANONITROGEN H ER BIC ID ES (A IR SA M PL IN G ) ALA C HLO R in AIR THIO PH EN ATE -M ETH YL in AIR FORM ALDEHYDE on dust R ES O RC IN O L P O L Y AR O M A T IC C O M P O U N D S (PACs) A R S IN E P H O S P H IN E S U LF U R D IO X I D E
E x tr a c ti o n
A n a ly t ic a l T e c h n iq u e Grav
Sampler PTFE/CYC
HP LC - U V GC-FPD H P LC - IC P G C !FPD HP LC - U V G C /E C D
G F F, IM P O VS P VC O VS !2 OV S-2 OV S-2
SPE disk QFF/SST I O M / P VC OV S-7 PTFE + XA D-2 CCT S G / H g( C N )2 M CE F & p a d w / N a2C O 3 C C T w /alk ali P TF E & C C T w / o xi d iz e r C C T (lo w N i) S G w /H g C l2 Ho pc alite s od a lim e Ag F C CT ( lg ) P T FE & C CT ( lg ) M S w / T EA & o x id i ze r S G + H 2SO 4 S G + H 2SO 4 SL BuB /H 2O air bag po rta ble air bag air bag Port In str Diffusive MC EF MC EF MC EF
0.1 - 10 1 - 16 4 - 200
HNO3 reagent H C O 3 /C O 3
2-
G FAAS VIS IC
6005 6006
I O D IN E D I BO R A N E
15 - 225 60 - 260
N a 2C O 3 H 2O 2
IC PES
0.05 - 0.2 0.01 - 0.2 0.15 - 0.25 0.05 - 0.2 0.3 - 1.0 0.05 - 0.1 0.1 - 1.5
6014
0.025
1.5 - 6
reagent
VIS
6015 6016 6017 6402 6600 6601 6602 6603 6604 6700 7013 7020 7024
AM M O NIA by VIS AM M O NIA by IC H Y D R O G E N C Y A N ID E P H O S P H O R U S T R IC H L O R ID E N I TR O U S O X ID E OXYG EN S U LF U R H EX A F LU O R ID E C A R B O N D IO X I D E CARBON MONOXIDE NITR OGEN DIOX IDE (Di ffu sive) ALUMINUM & CPDS, as Al C A LC IU M a nd c pd s a s C a C H R O M IU M a nd c pd s, as C r
0.1 - 0.2 0.1 - 0.5 0.05 - 2 0.05 - 0.2 NA NA 0.01 - 0.05 0.02 - 0.1 NA NA 1-3 1-3 1-3
0.1 - 90 0.1 - 96 2 - 90 11 - 100 80% vol 1 - NA 80% vol 80% vol NA NA 10 - 400 20 - 400 10 - 1000
3/15/2003
MF!31
Chemical
M eth No. 7027 7029 7030 7048 7056 7074 7082 7102 7105 7300 7301
M e th od Na m e C O B A LT an d c p ds , a s C o CO PPER (dust & fumes) ZINC and compounds, as Zn C A D M IU M a nd c pd s, as C d B A R IU M , S O LU B LE C O M P O U N D S TU NGSTEN (sol ubl e/i nso lu b le) LEAD by FAAS BERYLLIUM and cpds, as Be LEAD by GFAAS E LE M E NT S b y IC P E LE M E NT S b y IC P (A Q UA RE G IA AS HIN G ) E LE M E NT S b y IC P (A Q UA RE G IA AS HIN G ) EL EM EN TS b y IC P (H ot B loc k/H C l/ H N O 3 Digestion) A S BE ST O S F IB ER S b y PC M ALKA LINE DU STS ASBESTOS FIBERS by TEM C E LL UL OS E IN SU LA TIO N S IL IC A , C R Y ST A LL IN E , b y X R D. SILICA, AMOR PHOUS
Flow Ra te ( L /m i n ) 1-3 1-3 1-3 1-3 1-4 1-4 1-4 1-4 1-4 1-4 1-4
Vol. (L) min max 30 - 1500 50 - 1500 2 - 400 25 - 1500 50 - 2000 200 - 1000 200 - 1500 25 - 2000 1 - 1500 V a r ies V a r ies
E x tr a c ti o n
A n a ly t ic a l T e c h n iq u e FAAS FAAS FAAS FAAS FAAS FAAS FAAS G FAAS G FAAS IC P !AES ICP-AES
Sampler MC EF MC EF MC EF MC EF MC EF MC EF MC EF MC EF MC EF MC EF MC EF PVCF MC EF
7301
1-4
V a r ies
H C l /H N O 3
ICP-AES
7303
1-4
Se e Ta ble
H C l /H N O 3
ICP-AES
MC EF
NA HCl NA NA a s h or T HF ash
MCEF open PTFE MCEF open ACF C Y C + P VC PVC (total) PVC&C YC P VC C Y C & P VC C Y C & P VC C Y C & P VC P VC CYC & MC E or P VC CYC & MC E or P VC C Y C & P VC P VC P VC
Z IN C O X I D E VANADIUM OX IDES L E AD S U LF ID E B O R O N C A R B ID E C H R O M I U M , HE X A V A LE N T S IL IC A , C R Y ST A LL IN E
1-3 1.7, 2.2 ,2.5 1.7, 2.2 ,2.5 1.7, 2.2 ,2.5 1-4 1.7, 2.2 ,2.5
10 - 400 200 - 1000 600 - 1000 100 - 1000 8 - 400 400 - 800
XR D XR D XR D XR D VIS VIS
7602
400 - 800
ash
IR
SILICA in coal mine dust C H R O M I U M , HE X A V A LE N T CHROM IUM, HEXAV ALEN T b y IONCHROMATOG RAPHY LEAD in Air by Che mical Spot Test LEAD BY ULTRASOUND /ASV LEAD by Fi eld Portabl e XR F CHROM IUM, HEXAV ALEN T b y Field Portab le Spe ctroph otom etry AR SENIC & compoun ds , a s As AR SENIC TR IOX IDE, as A s FLUORIDES, aerosol & ga s
ash N a O H / N a2 C O 3 N a O H - N a2C O 3
IR IC IC
7903
AC IDS , INO RG AN IC
0.2 - 0.5
3.0 - 100
IC
3/15/2003
MF!32
Chemical
E x tr a c ti o n
A n a ly t ic a l T e c h n iq u e ISE G C !FPD IC
KOH xylene N a OH
8301
HIP PU RIC an d M ETH YL H IPP UR IC A C I D in U R IN E TR IAZ INE HE RB IC IDE S a nd the ir METABOLITES B U TO X Y A C E TI C A C ID in U R IN E ANALINE and o-TOLUIDINE in urine ASBESTOS, CHRYSOTILE b y XR D ASBES TOS (bulk) by PLM LEAD in Surface Wipe Sa mp les CHROM IUM, HEXAV ALENT in s ett led dust ELEMENTS on WIPES LEAD in DUST WIPES by C h emica l Spot Test CHLORINATED ORG ANONITROGEN HER BICIDES (HAND WAS H) CHLORINATED ORG ANONITROGEN HE RBIC IDES (DER M AL P ATC H)) C AP TA N a nd TH IO PH EN AT EM ETH YL in Handrinse CAPTAN and THIOPHENATEMETHYL on Dermal Patch
NA
Et a c
HP LC - U V
8315
NA
NA
NA
SC-MSD
Urine
NA NA NA NA NA NA
NA NA NA NA NA NA
NA ALK NA NA H N O 3/H 2O 2 NA
G C - EC D H P LC - EC D XR D PLM A A S; IC P Sp ot
NA NA bu lk bu lk Wipes Te st s trip
9102 9105
NA NA
NA NA
NA NA
ICP-AES Sp ot
Wipe Wipe
9200
NA
NA
NA
G C - EC D
9201
NA
NA
IPA/diazomethane
G C - EC D
9202
NA
NA
NA
HP LC - U V
Hand wa sh
9205
NA
NA
IP A -A C N
HP LC - U V
Patch
3/15/2003
MF!33
Analytical Techniques AAS Atomic absorption spectrophotometry AMP Amperometric detector ASV Anodic stripping voltammetry CD Conductivity detector DPP Differential Pulse Polargraphy ECD Electron capture detector ECHD Electrochemical detector ECN Electrolytic conductivity detector EG Evolved gas analysis FAAS Flame AAS FI Flow injection FID Flame ionization detector FL Fluorescence detector FPD Flame photometric detector GC Gas chromatography Grav Gravimetric (filter weight) GFAAS Graphite furnace AAS HPLC High performance liquid chromatography HYAAS Hydride generation AAS IC Ion chromatography ICP! AES Inductively coupled plasma! atomic emission spectroscopy IR Infrared spoectrophotometry ISE Ion specific electrode MS Mass spectrometry NPD Nitrogen phosphorus detector PCM Phase contrast microscopy PES Plasma emission spectrometry PID Photoionization detector PLM Polarized light microscopy SCD Sulfur chemiluminescence detector SEM Scanning electron microscopy Spot Spot test TCD Thermalalal conductivity detector TEM Transmission electron microscopy TOA Thermal optical analyzer UV Ultraviolet VIS Visible absorption spectrophotometry XRD X! ray diffraction XRF X! ray fluorescence Other cap i NA port s var