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M ETHO D FINDER (Ke y on p a g e M F!

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M eth No. 5506 5515 5506 5515 2018 2538 2539 3507 1603 3506 2558 1300 2549 3800 2555 2506 1606 1003 2003 1019 7903 1606 2501 2539 1604 0801 5603 5602 9200 9201 2539 5601 5502 7401 1402 1405 1000 Flow Ra te ( L /m i n ) 2.0 2.0 2.0 2.0 0.1 - 1.5 0.01 - 0.05 0.01 - 0.05 0.1 - 0.5 0.01 - 0.1 0.2 - 1.0 0.01 - 0.2 0.01 - 0.2 0.01 - 0.05 0.1 - 2.0 0.01 - 0.2 0.2 0.01 - 0.2 0.01 - 0.2 0.2 - 1.0 0.01 - 0.2 0.2 - 0.5 0.01 - 0.2 0.01 - 0.1 0.01 - 0.05 0.01 - 0.2 28.3 1 0.2 - 1 NA NA 0.01 - 0.05 0.1 - 1 0.2 - 1.0 1-4 0.01 - 0.2 0.01 - 0.2 0.01 - 1.0 Vol. (L) min max Acenaphthene Acenaphthene Acenaphthylene Acenaphthylene A c e talde hyde A c e talde hyde A c e talde hyde A c e talde hyde Ac etic ac id A c e tic anhydride Ac eto in Acetone Acetone Acetone Acetone Ac eto ne cy an oh yd rin Ac eto nitr ile A c e tyle ne dic hlor ide A c e tyle ne te trabr o m ide A c e tyle ne te trac hlo r ide Ac ids , ino rg an ic ACN Ac ro lein Ac ro lein Ac rylo nitr ile Ae ro bic ba cte ria Alach lor A l ac hlo r A l ac hlo r A lac hlo r Aldehydes, screening Aldicarb Ald rin Alka line du sts A llyl alc oho l A llyl alc oho l A llyl c hlor ide PO LYN UC LEA R A RO M ATIC HYDR OC ARBO NS by H PLC PO LYN UC LEA R A RO M ATIC HYDROCARBONS PO LYN UC LEA R A RO M ATIC HYDR OC ARBO NS by H PLC PO LYN UC LEA R A RO M ATIC HYDROCARBONS ALIPHATIC ALDEHYDES A C E T AL D E HY D E A L D EH Y D E S, SC R E E N IN G A C E T AL D E HY D E AC ETIC AC ID A C E T IC A N H Y D R ID E AC ETO IN KETONES I V O L A TI LE O R G A N IC C P D S (Screen in g) ORG ANIC AND INORGAN IC GASES BY EXTR ACTIV E FTIR SPEC T R O MET R Y KETONES I AC ETO NE CY AN O HY DR IN AC ETON ITRILE H Y D R O C A R B O N S , H A L O G E N A TE D 1,1,2,2 !T E TR A B R O M O E T H AN E 1,1,2,2 !T E TR A C H L O R O E TH A N E AC IDS , INO RG AN IC AC ETON ITRILE AC RO LEIN A L D EH Y D E S, SC R E E N IN G AC RYLO NITRILE A ER O BIC B AC TE RIA by G C -F AM E ALA C HLO R in AIR CHLORINATED ORG ANONITROGEN H ER BIC ID ES (A IR SA M PL IN G ) CHLORINATED ORG ANONITROGEN HER BICIDES (HAND WAS H) CHLORINATED ORG ANONITROGEN HE RBIC IDES (DER M AL P ATC H)) A L D EH Y D E S, SC R E E N IN G ORG ANONITROGEN PESTICIDES A L D R IN & L IN D A N E ALKA LINE DU STS ALC O HO LS III ALCOHO LS COM BINED A L LY L C H LO R I D E 200 - 1000 200 - 1000 200 - 1000 200 ! 1000 1 - 15 1 ! 12 5-5 6 - 60 20 - 300 25 - 100 1 - 10 0.5 - 3 1-6 Inst r. D ep . 0.5 - 3.0 0.3 - 12 1 - 25 0.2 - 5 50 - 100 3.0 - 30 3.0 - 100 1 - 25 1.5 - 48 5-5 3.5 - 20 50 - 300 70 - 1750 12 - 480 NA NA 5-5 var-480 18 - 240 70 - 1000 1 - 10 2 - 10 16 - 100 ac eto nitr ile va r ies ac eto nitr ile va r ies ACN t ol t ol r ea g formic a r ea g Ac et-M eth C S2 t h erma l NA C S2 Et Ac M e C l/M e O H C S2 T HF C S2 H C O 3 /C O 3
2-

E x tr a c ti o n

Chemical

M e th od Na m e

A n a ly t ic a l T e c h n iq u e HPLC !FL/U V G C !FID HPLC !FL/U V G C !FID HP LC /UV G C !F ID G C !F ID /M S HPLC !U V G C !FID VIS G C -FID G C !FID TD /G C !M S FTIR G C -FID G C !NPD G C !FID G C !FID G C !FID G C !FID IC G C !FID G C !NPD G C !F ID /M S G C !FID G C -FID ELISA G C /E C D G C - EC D G C - EC D G C !F ID /M S HP LC - U V G C !E C N T it ra t ion G C !FID G C -FID G C !FID

Sampler P T F E & X A D !2 P T F E & X A D !2 P T F E & X A D !2 P T F E & X A D !2 SG-DNPH X A D !2 /H M P X AD -2 /H M P BuB CCT BuB A -C M S CCT TD Di r. R e a d A -C M S P or Q S CCT CCT SG PCT SG(washed) C C T lg X A D !2 /H M P X A D !2 /H M P CCT i m p a c to r SPE disk OV S-2 polyethylene bag PUF pad X A D !2 OV S-2 GFF & BuB PTFE CCT CCT CCT

M e C l/M e O H t ol t ol a c et/C S 2 hex/MTBE met h a nol reagent NA IPA/diazomethane t ol reagent isooct HCl IP A/C S 2 IP A -C S 2 bz

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MF!1

NIOSH Manual of Analytical Methods

Chemical Al lyl glyc idyl ethe r A l lyl tric hlo r ide Alumina A l um inum A l um inum A l um inum A l um inum Am ine s, a liph atic Am ine s, a ro m atic Aminobenzene Aminobenzene 2 !A m ino e thano l 2 !A m ino e thano l 2-aminotoluene p !Am ino ph en yla rso nic ac id 2 !Aminotoluene Am m on ia Am m on ia n ! and s e c !Am yl ac etate n-Am yl ac etate Am yl ac etate iso-A my lace tate Aniline Aniline Aniline Anisidine Anthracene Anthracene Antimony Antimony p !Ar sa nilic ac id Ar se nic Ar se nic Ar se nic Ar se nic Ar se nic A r senic trio xide

M eth No. 2545 1003 0500 7300 7303 7301 7013 2010 2002 2002 2017 2007 3509 2017 5022 2002 6015 6016 1450 1450 2549 1450 2002 2017 8317 2514 5506 5515 7303 7301 5022 7900 7300 9102 7303 7301 7901

M e th od Na m e ALLYL GLYCIDYL ETHER HYDROC ARBONS, HALOG ENATED PARTICU LATES N.O.R . E LE M E NT S b y IC P E LE M EN TS by IC P (H O T B L O C K /H C l /H N O 3 D IG E S T IO N ) ELE M EN TS b y IC P (A Q UA RE G IA A SH IN G ) ALUMINUM & CPDS, as Al AM INE S, A LIPH ATIC AM INE S, A RO M ATIC AM INE S, A RO M ATIC A N IL IN E , o - TO L U ID I NE , A N D N I TR O B E N Z EN E AMINOETHANO L COM POUNDS I AM INO ETH AN O L C O M PO UN DS II A N IL IN E , o - TO L U ID I NE , A N D N I TR O B E N Z EN E A R S E N IC , O R G A N O ! AM INE S, A RO M ATIC AM M O NIA by VIS AM M O NIA by IC ESTERS I ESTERS I V O L A TI LE O R G A N IC C P D S (Screen in g) ESTERS I AM INE S, A RO M ATIC ANILINE , O -TOLU IDINE, & N I TR O B E N Z EN E ANALINE an d @ -TOLUIDINE in urine A N IS ID I NE PO LYN UC LEA R A RO M ATIC HYDR OC ARBO NS by H PLC PO LYN UC LEA R A RO M ATIC HYDROCARBONS E LE M EN TS by IC P (H O T B L O C K /H C l /H N O 3 D IG E S T IO N ) ELE M EN TS b y IC P (A Q UA RE G IA A SH IN G ) ARSENIC, organo! AR SENIC & compoun ds , a s As E LE M E NT S b y IC P ELEMENTS on WIPES E LE M EN TS by IC P (H O T B L O C K /H C l /H N O 3 D IG E S T IO N ) ELE M EN TS b y IC P (A Q UA RE G IA A SH IN G ) AR SENIC TR IOX IDE, as A s

Flow Ra te ( L /m i n ) 0.01 - 0.2 0.01 - 0.2 1-2 1-4 1-4 1-4 1-3 0.01 - 1.0 0.2 - 1.0 0.2 - 1.0 0.2 0.01 - 0.2 0.5 - 1.0 0.2 1-3 0.02 - 1.0 0.1 - 0.2 0.1 - 0.5 0.01 - 0.2 0.01 - 2 0.01 - 0.05 0.01 - 2 0.02 - 0.2 0.2 NA 0.5 - 1.0 2.0 2.0 1-4 1-4 1-3 1-3 1-4 NA 1-4 1-4 1-3

Vol. (L) min max 1.5 - 8 2 - 60 7 - 133 5 - 100 Se e Ta ble 5 - 100 10 - 400 3 - 30 30 - 150 30 - 150 5 - 50 4 - 24 5 - 300 5 - 50 50 - 1000 10 - 150 0.1 - 90 0.1 - 96 1 - 10 1 - 10 1-6 1 - 10 5 - 30 5 - 50 NA 24 - 320 200 - 1000 200 - 1000 Se e Ta ble 50 - 2000 50 - 1000 30 - 1000 5 - 2000 NA Se e Ta ble 5 - 2000 30 - 1000

E x tr a c ti o n

A n a ly t ic a l T e c h n iq u e G C !FID G C !FID Grav IC P !AES ICP-AES ICP-AES FAAS G C !FID G C !FID G C !FID G C -FID G C !FID IC G C -FID IC !HYAAS G C !FID VIS !Au to IC G C !FID G C -FID TD /G C !M S G C -FID G C !FID G C -FID H P LC /E C D HPLC !U V HPLC !FL/U V G C !FID ICP-AES ICP-AES IC !HYAAS HYAAS IC P !AES ICP-AES ICP-AES ICP-AES G FAAS

Sampler Tenax CCT P VC , ta re d MC EF MC EF MC EF MC EF SG SG SG GFF + SG SG IM P GFF + SG PTFE SG S G + H 2SO 4 S G + H 2SO 4 CCT CCT TD CCT SG GFF+SG NA X A D !2 P T F E & X A D !2 P T F E & X A D !2 MC EF MC EF PTFE MC EF MC EF Wipe MC EF MC EF MC EF

d ieth y l et h er CS2

!
H N O 3/HC lO 4 H C l /H N O 3 H C l /H N O 3 HNO3 H 2SO 4/a q M e O H Et h a nol Et h a nol Et h a nol M eO H/H 2O HSA et h a nol b u ffer Et h a nol H 2O H 2O C S2 C S2 t h erma l C S2 Et h a nol et h a nol Alk MeOH ac eto nitr ile va r ies H C l /H N O 3 H C l /H N O 3 b u ffer H N O 3/H 2SO 4/HC lO 4 H N O 3/HC lO 4 NA H C l /H N O 3 H C l /H N O 3 H N O 3/H 2O 2

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MF!2

NIOSH Manual of Analytical Methods

Chemical Arsine A sbe sto s A sbe sto s A sbe sto s A sbe sto s A sp arta m e A sp ha lt fu m e Atrazine Atrazine Atrazine Atrazine Az ela ic a cid Azinphos methyl Ba cte ria B[a]P B[a]P Bar ium Bar ium Bar ium Bar ium Benomyl Be nzalde hyde Benz[a]anthracene Benz(a)anthracene Benzene Benzene Benzene Benzene Benzene Be nzene so lubles 1, 3-be nze ne diol Be nzidine D ye s Benzidine Benzo[a]pyrene Benzo(a)pyrene

M eth No. 6001 7400 7402 9000 9002 5031 5042 5602 8315 9200 9201 5019 5600 0801 5506 5515 7056 9102 7303 7301 5601 2549 5506 5515 2549 3700 1501 1500 3800 5042 5701 5013 5509 5506 5515 A R S IN E

M e th od Na m e

Flow Ra te ( L /m i n ) 0.01 - 0.2 0.5 - 16 0.5 - 16 NA NA 1-3 1-4 0.2 - 1 NA NA NA 1-3 0.2 - 1.0 28.3 2.0 2.0 1-4 NA 1-4 1-4 0.1 - 1 0.01 - 0.05 2.0 2.0 0.01 - 0.05 > 0.02 0.01 - 0.2 0.01 - 0.2 0.1 - 2.0 1-4 0.2 - 1 1-3 0.2 2.0 2.0

Vol. (L) min max 0.1 - 10 400 - va r 400 - va r NA NA 70 - 1200 28 - 400 12 - 480 NA NA NA 200 - 1000 12 - 240 50 - 300 200 - 1000 200 - 1000 50 - 2000 NA Se e Ta ble 50 - 2000 var - 480 1-6 200 - 1000 200 - 1000 1-6 80% vol 5 - 30 2 - 30 Inst r. D ep . 28 5 - 160 150 - 500 20 - 100 200 - 1000 200 - 1000

E x tr a c ti o n

A n a ly t ic a l T e c h n iq u e G FAAS PCM TEM XR D PLM HPLC !U V G RA VIM ETR IC G C /E C D GC-M SD G C - EC D G C - EC D G C !FID G C !FPD G C -FID HPLC !FL/U V G C !FID FAAS ICP-AES ICP-AES ICP-AES HP LC - U V TD /G C !M S HPLC !FL/U V G C !FID TD /G C !M S GC G C !FID G C !FID FTIR Grav G C -FID HPLC !U V HPLC !U V HPLC !FL/U V G C !FID

Sampler CCT MCEF open MCEF open bu lk bu lk PTFE Tared PTFE OV S-2 Urine polyethylene bag PUF pad P VC O VS !2 i m p a c to r P T F E & X A D !2 P T F E & X A D !2 MC EF Wipe MC EF MC EF OV S-2 TD P T F E & X A D !2 P T F E & X A D !2 TD air bag CCT CCT Di r. R e a d Tared PTFE OV S-7 PTFE GFF P T F E & X A D !2 P T F E & X A D !2

HNO3 NA NA NA NA eluent benzene reagent NA NA IP A/ diazomethane Et h a nol t ol/a cet hex/MTBE ac eto nitr ile va r ies H 2O NA H C l /H N O 3 H C l /H N O 3 reagent t h erma l ac eto nitr ile va r ies t h erma l NA C S2 C S2 NA benzene met h a nol H 2O triethyl amine /M e O H ac eto nitr ile va r ies

A S BE ST O S F IB ER S b y PC M ASBESTOS FIBERS by TEM ASBESTOS, CHRYSOTILE b y XR D ASBES TOS (bulk) by PLM A SP AR TA M E B E N Z EN E S O LU B LE F R AC T IO N A N D TOTAL PARTICULATE (ASPHALT FUME) CHLORINATED ORG ANONITROGEN H ER BIC ID ES (A IR SA M PL IN G ) TR IAZ INE HE RB IC IDE S a nd the ir METABOLITES CHLORINATED ORG ANONITROGEN HER BICIDES (HAND WAS H) CHLORINATED ORG ANONITROGEN HE RBIC IDES (DER M AL P ATC H)) AZ ELA IC A C ID ORG ANOPHO SPHORUS PESTICIDES A ER O BIC B AC TE RIA by G C -F AM E PO LYN UC LEA R A RO M ATIC HYDR OC ARBO NS by H PLC PO LYN UC LEA R A RO M ATIC HYDROCARBONS B A R IU M , S O LU B LE C O M P O U N D S ELEMENTS on WIPES E LE M EN TS by IC P (H O T B L O C K /H C l /H N O 3 D IG E S T IO N ) ELE M EN TS b y IC P (A Q UA RE G IA A SH IN G ) ORG ANONITROGEN PESTICIDES V O L A TI LE O R G A N IC C P D S (Screen in g) PO LYN UC LEA R A RO M ATIC HYDR OC ARBO NS by H PLC PO LYN UC LEA R A RO M ATIC HYDROCARBONS V O L A TI LE O R G A N IC C P D S (Screen in g) B EN ZE NE by po rta ble G C HY DR O C AR BO NS , AR O M ATIC HYDROC ARBONS, BP 36 !216 C ORG ANIC and INORGANIC G ASES by EX TR ACTIV E FTIR SPE C T R O MET R Y B E N Z EN E S O LU B LE F R AC T IO N A N D TOTAL PARTICULATE (ASPHALT FUME) R ES O RC IN O L DYES BENZIDINE and 3,3'!DICHLORO !B E N Z ID I NE PO LYN UC LEA R A RO M ATIC HYDR OC ARBO NS by H PLC PO LYN UC LEA R A RO M ATIC HYDROCARBONS

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NIOSH Manual of Analytical Methods

Chemical Benzo[a]fluoranthene Benzo(b)fluoranthene Benzo[e]pyrene Benzo(e)pyrene Benzo[k]fluoranthene Benzo(k)fluoranthene Benzo[ghi]perylene Benzo(ghi)perylene Be nzo su lfon az ole Be nzo thia zo le Be nzoyl pe r o xide Be nzyl c hlo ride Be r yllium Be r yllium Be r yllium Be r yllium Be r yllium & c o m po und s Bio ae r o so l Biphenyl Bism uth B itu m en fu m e Bo r o n Bo r o n c ar bide Bo r o n o xide Brom oform Bromine 1-Bromopropane 2-Bromopropane Brom oform Bromotrifluoromethane Bro m ox yn il Brom oxy nil octa noa te 1,3 !Butadiene 2 !Butanone 2 !Butanone 2-Butanone

M eth No. 5506 5515 5506 5515 5506 5515 5506 5515 2550 2550 5009 1003 7300 9102 7303 7301 7102 0800 2530 7303 5042 7303 7506 0500 1003 6011 1025 1003 1017 5010 5010 1024 2500 2549 3800

M e th od Na m e PO LYN UC LEA R A RO M ATIC HYDR OC ARBO NS by H PLC PO LYN UC LEA R A RO M ATIC HYDROCARBONS PO LYN UC LEA R A RO M ATIC HYDR OC ARBO NS by H PLC PO LYN UC LEA R A RO M ATIC HYDROCARBONS PO LYN UC LEA R A RO M ATIC HYDR OC ARBO NS by H PLC PO LYN UC LEA R A RO M ATIC HYDROCARBONS PO LYN UC LEA R A RO M ATIC HYDR OC ARBO NS by H PLC PO LYN UC LEA R A RO M ATIC HYDROCARBONS B EN ZO TH IA ZO LE IN AS PH A LT F UM E B EN ZO TH IA ZO LE IN AS PH A LT F UM E B E N Z O Y L P E R O X ID E HYDROC ARBONS, HALOG ENATED E LE M E NT S b y IC P ELEMENTS on WIPES E LE M EN TS by IC P (H O T B L O C K /H C l /H N O 3 D IG E S T IO N ) ELE M EN TS b y IC P (A Q UA RE G IA A SH IN G ) BERYLLIUM and cpds, as Be BIOA ERO SO L SAM PLING (Indoor A ir) DIPHENYL E LE M EN TS by IC P (H O T B L O C K /H C l /H N O 3 D IG E S T IO N ) B E N Z EN E S O LU B LE F R AC T IO N A N D TOTAL PARTICULATE (ASPHALT FUME) E LE M EN TS by IC P (H O T B L O C K /H C l /H N O 3 D IG E S T IO N ) B O R O N C A R B ID E PARTICU LATES N.O.R . HYDROC ARBONS, HALOG ENATED C H L O R IN E a n d B R O M I N E 1 - a n d 2 -B R O M O P R O P A N E HYDROC ARBONS, HALOG ENATED T R IF L UO R O B R O M O M E T HA N E BRO MO XYN IL and B 'OC TANO ATE BRO MO XYN IL and B 'OC TANO ATE 1,3 !B U TA D IE N E M E T H YL E TH Y L K E TO N E V O L A TI LE O R G A N IC C P D S (Screen in g) ORG ANIC and INORGANIC G ASES by EX TR ACTIV E FTIR SPE C T R O MET R Y

Flow Ra te ( L /m i n ) 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 1.0 - 2.0 1.0 - 2.0 1-3 0.01 - 0.2 1- 4 NA 1-4 1-4 1-4 28.3 0.01 - 0.5 1-4 1-4 1-4 1.7 or 2 .2 1.5 - 2.0 0.01 - 0.2 0.3 - 1.0 0.01 - 0.2 0.01 - 0.2 0.01 - 0.05 1-3 1-3 0.01 - 0.5 0.01 - 0.2 0.01 - 0.05 0.1 - 2.0

Vol. (L) min max 200 - 1000 200 - 1000 200 - 1000 200 - 1000 200 - 1000 200 - 1000 200 - 1000 200 - 1000 480 - 960 480 - 960 40 - 400 6 - 50 1250-2000 NA Se e Ta ble 1250-2000 25 - 2000 va r ies 15 - 30 Se e Ta ble 28 - 400 Se e Ta ble 100 - 1000 25 - 133 4 - 70 8 - 360 0.1 - 12 4 - 70 0.3 - 1.0 2 - 400 90 - 400 5 - 25 1 - 12 1-6 Inst r. D ep .

E x tr a c ti o n

A n a ly t ic a l T e c h n iq u e HPLC !FL/U V G C !FID HPLC !FL/U V G C !ID HPLC !FL/U V G C !ID HPLC !FL/U V G C !ID G C - SC D G C - SC D HPLC !U V G C !FID IC P !AES ICP-AES ICP-AES ICP-AES G FAAS va r ies G C !FID ICP-AES Grav ICP-AES XR D Grav G C -FID IC G C -FID G C !FID G C !FID HPLC !U V HPLC !U V G C !FID G C !FID TD /G C !M S FTIR

Sampler P T F E & X A D !2 P T F E & X A D !2 P T F E & X A D !2 P T F E & X A D !2 P T F E & X A D !2 P T F E & X A D !2 P T F E & X A D !2 P T F E & X A D !2 PTFE + X D-2 PTFE + X D-2 MC EF CCT MC EF Wipe MC EF MC EF MC EF I m p a c to r Te na x G C MC EF Tared PTFE MC EF C Y C & P VC P VC CCT Ag F CCT CCT 2 C C T (lg + sm ) PTFE PTFE CCT C a rb o n b e a d s TD Di r. R e a d

ac eto nitr ile va r ies ac eto nitr ile va r ies ac eto nitr ile va r ies ac eto nitr ile va r ies hexane hexane d ieth y l et h er C S2 H N O 3/HC lO 4 NA H C l /H N O 3 H C l /H N O 3 H N O 3/H 2SO 4 NA C C l4 H C l /H N O 3 benzene H C l /H N O 3 ash NA C S2 N a 2S 2O 3 C S2 C S2 C H 2C l2 C H 3C N C H 3C N C H 2C l2 C S2 t h erma l NA

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MF!4

NIOSH Manual of Analytical Methods

Chemical Bu tox ya ce tic a cid 2 !Buto xye thyano l 2 !Buto xye thano l n !, s ec !, & t!Buty l ace tate Buty l ace tate iso-Bu tyl ac etate 1-Bu tyl ac etate Butyl alc o ho l tert !Butyl alc o ho l n ! & s e c !Butyl alc o hol n- Butyl alc oho l se c -Butyl alc o ho l n !Butylamine Butyl cellosolve Butyl cellosolve 1,3 !Butyle ne glygo l Butyl glyc idyl e the r n !Butyl me rc aptan n !Butyl me rc aptan p !tert !Butyltoluene Butyr alde hyde C a dm ium C a dm ium C a dm ium C a dm ium C a dm ium & c o m po un ds C a lc ium C a lc ium C a lc ium C a lc ium & c o m po und s C a m pho r C a m pho r C ap sa icin C a ptan C a ptan C a ptan Carbaryl Carbaryl (Sevin)

M eth No. 8316 2549 1403 1450 2549 1450 1450 2549 1400 1401 1405 1405 2012 2549 1403 5523 1616 2525 2542 1501 2539 7300 9102 7303 7301 7048 7300 7303 7301 7020 1301 2553 5041 5601 9205 9202 5601 5006

M e th od Na m e BUTOXYACETIC ACID in urine V O L A TI LE O R G A N IC C P D S (Screen in g) ALC O HO LS IV ESTERS I V O L A TI LE O R G A N IC C P D S (Screen in g) ESTERS I ESTERS I V O L A TI LE O R G A N IC C P D S (Screen in g) ALCOHO LS I ALC O HO LS II ALCOHO LS COM BINED ALCOHO LS COM BINED n !B U TY L AM I N E V O L A TI LE O R G A N IC C P D S (Screen in g) ALC O HO LS IV GLYC OLS BUTYL GLYCIDYL ETHER n !BU TYL MER CAPTAN M E R C A P TA N S HY DR O C AR BO NS , AR O M ATIC A L D EH Y D E S, SC R E E N IN G E LE M E NT S b y IC P ELEMENTS on WIPES E LE M EN TS by IC P (H O T B L O C K /H C l /H N O 3 D IG E S T IO N ) ELE M EN TS b y IC P (A Q UA RE G IA A SH IN G ) C A D M IU M a nd c pd s, as C d E LE M E NT S b y IC P E LE M EN TS by IC P (H O T B L O C K /H C l /H N O 3 D IG E S T IO N ) ELE M EN TS b y IC P (A Q UA RE G IA A SH IN G ) C A LC IU M a nd c pd s a s C a KE TO NE S II KE TO NE S II C AP SA ICIN an d D IHY DR O C AP SA ICIN ORG ANONITROGEN PESTICIDES CAPTAN and THIOPHENATE-METHYL o n D E RM A L P A TC H CAPTAN and THIOPHENATE-METHYL in Handrinse ORG ANONITROGEN PESTICIDES CARBARYL

Flow Ra te ( L /m i n ) NA 0.01 - 0.05 0.01 - 0.05 0.01 - 0.2 0.01 - 0.05 0.01 - 2 0.01 - 2 0.01 - 0.05 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 1.0 0.01 - 0.05 0.01 - 0.05 0.5 - 2 0.01 - 0.2 0.01 - 0.05 0.1 - 0.2 0.01 - 0.2 0.05 1-4 NA 1-4 1-4 1-3 1-4 1-4 1-4 1-3 0.01 - 0.2 0.01 - 0.2 1-3 0.1 - 1 NA NA 0.1 - 1 1-3

Vol. (L) min max NA 1-6 2 - 10 1 - 10 1-6 1 - 10 1 - 10 1-6 1 - 10 2 - 10 2 - 10 2 - 10 2 - 100 1-6 1 - 10 5 - 60 15 - 30 1-4 10 - 150 1 - 29 5-5 13 - 2000 NA Se e Ta ble 13 - 2000 25 - 1500 5 - 200 Se e Ta ble 5 - 200 20 - 400 1 - 25 1 - 25 5 - 1000 var-480 NA NA var-480 20 - 400

E x tr a c ti o n

A n a ly t ic a l T e c h n iq u e G C - EC D TD /G C !M S G C !FID G C !FID TD /G C !M S G C -FID G C -FID TD /G C !M S G C !FID G C !FID G C -FID G C -FID G C !FID TD /G C !M S G C !FID G C !FID G C !FID G C !FPD G C !FPD G C !FID G C !F ID /M S IC P !AES ICP-AES ICP-AES ICP-AES FAAS IC P !AES ICP-AES ICP-AES FAAS G C !FID G C -FID HPLC !FL HP LC - UV HP LC - U V HP LC - U V HP LC - UV VIS NA TD

Sampler

NA t h erma l C H 2C l2/M e O H C S2 t h erma l C S2 C S2 t h erma l C S2 C S2 IP A -C S 2 IP A -C S 2 MeOH t h erma l C H 2C l2/M e O H MeOH C S2 a cet H C l/D C E C S2 t ol H N O 3/HC lO 4 NA H C l /H N O 3 H C l /H N O 3 H N O 3/H C l H N O 3/HC lO 4 H C l /H N O 3 H C l /H N O 3 H N O 3/HC lO 4 M e O H /C S 2 IP A -C S 2 C H 3C N reagent IP A /A C N NA reagent reagent

CCT CCT TD CCT CCT TD CCT CCT CCT CCT S G + H 2SO 4 TD CCT O VS !7 CCT Chrom 104 GFF/HgAc CCT X A D !2 /H M P MC EF Wipe MC EF MC EF MC EF MC EF MC EF MC EF MC EF CCT A -C M S GFF OV S-2 Patch Hand wa sh OV S-2 GFF

3/15/2003

MF!5

NIOSH Manual of Analytical Methods

Chemical C ar be nd az im C a r bito l C a r bo fur an C a r bo n blac k C a r bo n, e le m e ntal C a r bo n dio xide C a r bo n disulfide C a r bo n m o no xide C a r bo n te trac hlo r ide

M eth No. 5601 2549 5601 5000 5040 6603 1600 6604 1003 1552 7404 5510 5039 5025 5014 6011 2015 2008 1003 1026 1003 1003 1018 5503 2513 1003 2005 2014 1002 5601 5600 7600 7604 7024 7300 7301 7303 9102 7600 7604

M e th od Na m e ORG ANONITROGEN PESTICIDES V O L A TI LE O R G A N IC C P D S (Screen in g) ORG ANONITROGEN PESTICIDES C A R BO N B LA C K ELEM ENTA L CA RBO N (DIES EL PA RT.) C A R B O N D IO X I D E C A R B O N D IS U LF ID E CARBON MONOXIDE HYDROC ARBONS, HALOG ENATED TERPENES C E LL UL OS E IN SU LA TIO N CHLORDANE C H L O R IN A T ED C A M P H E N E C H L O R IN A T ED D IP H E N YL O X ID E CH LORINA TED TERPH ENYL C H L O R IN E a n d B R O M I N E C H L O R O A C E T AL D E HY D E C HLO RO AC ETIC AC ID HYDROC ARBONS, HALOG ENATED p - C H LO R O B E N Z O T RI FL U O R ID E HYDROC ARBONS, HALOG ENATED HYDROC ARBONS, HALOG ENATED D I C H LO R O D I F LU O R O M E T H A N E POLY CH LORO BIPHENY LS ETH YLE NE CH LO RO HY DR IN HYDROC ARBONS, HALOG ENATED N I TR O A R O M A T IC C O M P O U N D S p !C H L O RO P H EN O L

Flow Ra te ( L /m i n ) 0.1 - 1 0.01 - 0.05 0.1 - 1 1-2 2-4 0.02 - 0.1 0.01 -0 .2 NA 0.01 - 0.2 0.01 - 0.02 1 0.5 - 1.0 0.2 - 1 0.5 - 1.5 1-3 0.3 - 1.0 0.05 - 0.2 0.05 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.05 0.05 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 1.0 0.05 - 0.2 0.01 - 0.1 0.1 - 1 0.2 - 1.0 1-4 1-4 1-3 1-4 1-4 1-4 NA 1-4 1-4

Vol. (L) min max var - 480 1-6 var-480 30 - 570 142-19000 80% vol 2 - 25 NA 3 - 150 2 - 30 NA 10 - 200 2 - 30 8 - 200 100 - 1500 2 - 90 3 - 16 1 - 100 1.5 - 40 0.1 - 10 0.5 - 60 0.5 - 8 1-4 1 - 50 2 - 35 1 - 50 1 - 150 1.5 - 40 1.5 - 8 var-480 12 - 240 8 - 400 100 - 1000 10 - 1000 5 - 1000 5 - 1000 Se e Ta ble NA 8 - 400 100 - 1000

E x tr a c ti o n

A n a ly t ic a l T e c h n iq u e HP LC - U V TD /G C !M S HP LC - U V Grav E G A/TO A G C !T C D G C !FPD Sens or G C !FID G C !FID SEM G C !E C D G C !E C D G C !E C N G C !E C D IC G C !E C D IC G C !FID G C -FID G C -FID G C !FID G C !FID G C !E C D G C !FID G C !FID G C !FID HPLC !U V G C !FID HP LC , U V G C !FPD VIS IC FAAS IC P !AES ICP-AES ICP-AES ICP-AES VIS IC

Sampler OV S-2 TD OV S-2 P VC QFF air bag CC T & d ry tu b e Port In str CCT CCT ACF M C E F & Ch ro m 102 MC EF MC EF GFF Ag F SG SG CCT CCT CCT CCT 2 C C T (lg + sm ) G FF & F lor isil PCT CCT SG SG CCT OV S-2 O VS !2 P VC P VC MC EF MC EF MC EF MC EF Wipe P VC P VC

reagent t h erma l reagent NA t h erma l NA toluene NA C S2 C S2 NA t ol p et eth er isooctane isooctane N a 2S 2O 3 MeOH H 2O C S2 C S 2/M e O H C S2 C S2 C H 2C l2 hexane IP A /C S 2 C S2 MeOH C H 3C N C S2 reagent t ol/a cet reagent N a O H / N a2 C O 3 H C l /H N O 3 H N O 3/HC lO 4 H C l /H N O 3 H C l /H N O 3 NA reagent N a O H / N a2 C O 3

* -3-Carene
Cellulose Chlordane Chlorinated camphene C hlo rinate d diphe nyl ox ide Chlorinated terphenyl Chlorine C hlo ro ac e talde hyde C hlo ro ac etic ac id Chlorobenzene p -Chlo r o be nzo tr ifluo r id e Chlorobromomethane Chlorobromomethane Chlorodifluoromethane Chlorodiphenyl (42 & 54% C I) 2 !Chlo ro e thano l Ch loroform 4 !Chloronitrobenzene p !Chlo ro phe no l Chloroprene C hlo rpr o pham C hlo rpyr ifo s C hr om ic a cid C hr om ic a cid C hr o m ium C hr o m ium C hr o m ium C hr o m ium C hr o m ium Chromium, hexavalent Chromium, hexavalent

$!C H L O R O P R E N E
ORG ANONITROGEN PESTICIDES ORG ANOPHO SPHORUS PESTICIDES C H R O M I U M , HE X A V A LE N T C H R O M I U M , HE X A V A LE N T C H R O M IU M a nd c pd s, as C r E LE M E NT S b y IC P ELE M EN TS b y IC P (A Q UA RE G IA A SH IN G ) E LE M EN TS by IC P (H O T B L O C K /H C l /H N O 3 D IG E S T IO N ) ELEMENTS on WIPES C H R O M I U M , HE X A V A LE N T C H R O M I U M , HE X A V A LE N T

3/15/2003

MF!6

NIOSH Manual of Analytical Methods

Chemical Chromium, hexavalent Chromium, hexavalent Chromium, hexavalent Chrysene Chrysene C oal tar naphtha C oal tar pitc h vo latile s C ob alt C ob alt C ob alt C ob alt C obalt & c o m po unds C oppe r Co ppe r Co ppe r Co ppe r Co ppe r (dust & fum e ) Cr e so l

M eth No. 7605 7703 9101 5506 5515 1550 5042 7300 9102 7301 7303 7027 7300 7301 9102 7303 7029 2549

M e th od Na m e C H RO M IU M HE XA VA LE NT b y IO N CHROM ATOGRAPHY CHROM IUM, HEXAV ALENT b y Field Portab le Spe ctroph otom etry CHROM IUM, HEXAV ALENT in s ett led dust PO LYN UC LEA R A RO M ATIC HYDR OC ARBO NS by H PLC PO LYN UC LEA R A RO M ATIC HYDROC ARBONS NAPHTHAS B E N Z EN E S O LU B LE F R AC T IO N A N D TOTAL PARTICULATE (ASPHALT FUME) E LE M E NT S b y IC P ELEMENTS on WIPES ELE M EN TS b y IC P (A Q UA RE G IA A SH IN G ) E LE M EN TS by IC P (H O T B L O C K /H C l /H N O 3 D IG E S T IO N ) C O B A LT an d c p ds , a s C o E LE M E NT S b y IC P ELE M EN TS b y IC P (A Q UA RE G IA A SH IN G ) ELEMENTS on WIPES E LE M EN TS by IC P (H O T B L O C K /H C l /H N O 3 D IG E S T IO N ) CO PPER (dust & fumes) V O L A TI LE O R G A N IC C P D S (Screen in g) C R ES O LS an d P HE NO L A L D EH Y D E S, SC R E E N IN G C R O T O N A L D EH Y D E DICHLORODIFLUORO METHANE, 1,2 !DICHLOROTETR AFLU O R O ! ETHA NE, & C H L O R O D IF L UO R O M E T H A N E HY DR O C AR BO NS , AR O M ATIC CYANIDES, aerosol an d g a s H Y D R O G E N C Y A N ID E C YA NU RIC AC ID CHLORINATED ORG ANONITROGEN H ER BIC ID ES (A IR SA M PL IN G ) TR IAZ INE HE RB IC IDE S a nd the ir METABOLITES CHLORINATED ORG ANONITROGEN HER BICIDES (HAND WAS H) CHLORINATED ORG ANONITROGEN HE RBIC IDES (DER M AL P ATC H)) HYDROC ARBONS, BP 36 !216 C ALC O HO LS III ALCOHO LS COM BINED

Flow Ra te ( L /m i n ) 0.1 - 4 1-4 NA 2.0 2.0 0.01 - 0.2 1-4 1-4 NA 1-4 1-4 1-3 1-4 1-4 NA 1-4 1-3 0.01 - 0.05

Vol. (L) min max 1 - 400 10 - 1200 NA 200 - 1000 200 - 1000 1.3 - 20 28 - 400 25 - 2000 NA 25 - 2000 Se e Ta ble 30 - 1500 5 - 1000 5 - 1000 NA Se e Ta ble 50 - 1500 1-6

E x tr a c ti o n

A n a ly t ic a l T e c h n iq u e IC VIS Sp ot HPLC !FL/U V G C !FID G C !FID Grav IC P !AES ICP-AES ICP-AES ICP-AES FAAS IC P !AES ICP-AES ICP-AES ICP-AES FAAS TD /G C !M S P VC

Sampler

N a O H - N a2C O 3 ( N H4) 2SO 4/ N H4O H NA ac eto nitr ile va r ies C S2 benzene H N O 3/HC lO 4 NA H C l /H N O 3 H C l /H N O 3 a q re g /H N O 3 H N O 3/HC lO 4 H C l /H N O 3 NA H C l /H N O 3 H N O 3/H C l t h erma l

PVC, MCE, PTFE Te st s trip P T F E & X A D !2 P T F E & X A D !2 CCT tared PTFE MC EF Wipe MC EF MC EF MC EF MC EF MC EF Wipe MC EF MC EF TD

Cre sol, all isome rs Cr o tonalde hyde Cr o tonalde hyde Cryofluorane

2546 2539 3516 1018

0.01 - 0.1 0.01 - 0.05 0.1 - 0.2 0.01 - 0.05

1 - 24 5-5 1 - 49 1-4

MeOH t ol b u ffer C H 2C l2

G C !FID G C !F ID /M S DPP G C !FID

X A D !7 X A D !2 /H M P BuB 2 CCT

Cum ene Cyanides Cyanides C ya nu ric ac id Cyanazine

1501 7904 6010 5030 5602

0.01 - 0.2 0.5 - 1.0 0.05 - 0.2 1-3 0.2 - 1

1 - 30 10 - 180 0.6 - 90 10 - 1000 12 - 480

C S2 KOH H 2O rea ge nts reagent

G C !FID ISE VIS HPLC !U V G C /E C D

CCT MCEF & BuB s od a lim e P VC OV S-2

Cyanazine

8315

NA

NA

NA

GS-MSD

Urine

Cyanazine

9200

NA

NA

NA

G C - EC D

polyethylene bag PUF pad

Cyanazine

9201

NA

NA

IPA/diazomethane

G C - EC D

Cyclohexane Cyc lo he xano l Cyc lo he xano l

1500 1402 1405

0.01 - 0.2 0.01 - 0.2 0.01 - 0.2

2.5 - 5 1 - 10 2 - 10

C S2 IP A /C S 2 IP A -C S 2

G C !FID C G !FID G C -FID

CCT CCT CCT

3/15/2003

MF!7

NIOSH Manual of Analytical Methods

Chemical Cyclohexanone

M eth No. 2549

M e th od Na m e V O L A TI LE O R G A N IC C P D S (Screen in g) KETONES I KETONES I HYDROC ARBONS, BP 36 !216 C 1,3 !C Y C L O P E N TA D IE N E

Flow Ra te ( L /m i n ) 0.01 - 0.05

Vol. (L) min max 1-6

E x tr a c ti o n

A n a ly t ic a l T e c h n iq u e TD /G C !M S TD

Sampler

t h erma l

Cyclohexanone Cyclohexanone Cyclohexene 1,3 !Cyclopentadiene

2555 1300 1500 2523

0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.05

1 - 10 1 - 10 5-7 1-5

C S2 C S2 C S2 Et Ac

G C -FID C G !FID C G !FID G C !FID

A -C M S CCT CCT Chrom104/ maleic anhy GFF OV S-2

2,4 !D 2,4-D a cid; 2,4-D,2 -ethylhe xyl ester; 2, 4-D , 2-buto xye thyl ester 2,4-D a cid; 2,4-D,2 -ethylhe xyl ester; 2, 4-D , 2-buto xye thyl ester 2,4-D a cid; 2,4-D,2 -ethylhe xyl ester; 2, 4-D , 2-buto xye thyl ester D ec abr o mo diphe nyl Ox i de n !Decane

5001 5602

2,4 !D an d 2,4,5 !T CHLORINATED ORG ANONITROGEN H ER BIC ID ES (A IR SA M PL IN G )

1-3 0.2 - 1

15 - 200 12 - 480

MeOH reagent

HPLC !U V G C - EC D

9200

CHLORINATED ORG ANONITROGEN HER BICIDES (HAND WAS H)

NA

NA

NA

G C - EC D

polyethylene bag

9201

CHLORINATED ORG ANONITROGEN HE RBIC IDES (DER M AL P ATC H))

NA

NA

IPA/diazomethane

G C - EC D

PUF pad

2559 2549

D E C A B R O M O D I PH E N Y L O X I D E V O L A TI LE O R G A N IC C P D S (Screen in g)
o HYDROC ARBONS, BP 36 o-216 C

2.0 0.01 - 0.05

48 - 960 1-6

T ol t h erma l

G C /N C D TD /G C !M S

GFF TD

n-Decane D eme to n Desethylatrazine

1500 5514 8315

NA 0.2 - 1.0 NA

NA 30 - 500 NA

C S2 toluene NA

G C -FID G C !FPD GC-M SD

CCT M CE F & X A D !2 Urine

D EM E TO N TR IAZ INE HE RB IC IDE S a nd the ir METABOLITES TR IAZ INE HE RB IC IDE S a nd the ir METABOLITES ALC O HO LS III ALCOHO LS COM BINED DIACETYL DYES SILICA, AMOR PHOUS ORG ANOPHO SPHORUS PESTICIDES D I AZ O M E T H A N E PO LYN UC LEA R A RO M ATIC HYDR OC ARBO NS by H PLC PO LYN UC LEA R A RO M ATIC HYDROCARBONS D I BO R A N E

Desisopropylatrazine

8315

NA

NA

NA

GC-M SD

Urine

D i ac eto ne alc oho l D i ac eto ne alc oho l Diacetyl o !Dianisidine Diato ma ce ou s ea rth D i azino n Diazomethane Dibenz[a,h]anthracene

1402 1405 2557 5013 7501 5600 2515 5506

0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 1-3 1-3 0.2 - 1 0.2 2.0

1 - 10 1 - 10 1 - 10 150 - 500 50 - 400 12 - 240 6 - 30 200 - 1000

IP A /C S 2 IP A -C S 2 Ac et-M eth H 2O ash toluene/acetone C S2 ac eto nitr ile

G C !FID G C -FID G C -FID HPLC !U V XR D G C !FPD G C !FID HPLC !FL/U V

CCT CCT A -C M S PTFE PVC/CYC O VS !2 X A D !2 ( c o at e d ) P T F E & X A D !2

Dibenz(a,h) anthracene

5515

2.0

200 - 1000

va r ies

G C !FID

P T F E & X A D !2

Diborane

6006

0.5 - 1.0

60 - 260

H 2O 2

PES

P TF E & C C T w / o xi d iz e r 2 CCT SG PTFE MC EF

Dibromodifluoromethane 2 !D ibutylam ino e thanol Dibu tyl ph osp ha te Dibu tyl ph tha late

1012 2007 5017 5020

D I FL U O R O D IB R O M O M E T H A N E A M I N O E TH A N O L C O M P O U N D S DIBUTY L PHO SPH ATE D I BU T YL P HT H A LA T E & DI(2 !ETHY LHEX YL) PHTH ALATE O R G A N O T IN C O M P O U N D S

0.01 - 0.2 0.01 - 0.2 1-3 1-3

2.5 - 10 4 - 24 50 - 250 6 - 200

IPA M eO H/H 2O C H 3C N C S2

G C !FID G C !FID G C !FPD G C !FID

Dibutyltin bis(isooctyl m e r c apto ac e tate ) o !, p !Dichlorobenzene

5504

1 - 1.5

50 - 500

A c etic a /C H 3C N

HP LC /G FAAS

G F F + X A D !2

2549

V O L A TI LE O R G A N IC C P D S (Screen in g) HYDROC ARBONS, HALOG ENATED

0.01 - 0.05

1-6

va r ies

TD /G C !M S

TD

o-Dichlorobenzene

1003

0.01 - 0.2

1 - 10

C S2

G C -FID

CCT

3/15/2003

MF!8

NIOSH Manual of Analytical Methods

Chemical p-Dichlorobenzene p !Dichlorobenzene 3,3'!Dichlorobenzidine

M eth No. 1003 1003 5509

M e th od Na m e HYDROC ARBONS, HALOG ENATED HYDROC ARBONS, HALOG ENATED BENZIDINE an d 3,3'!D I C H LO R O B E N Z ID I NE DICHLORODIFLUORO METHANE, 1,2 !DICHLOROTETR AFLUO R O ! ETHANE & C H L O R O D IF L UO R O M E T H A N E HYDROC ARBONS, HALOG ENATED HYDROC ARBONS, HALOG ENATED DICHLOROETHYL ETHER HYDROC ARBONS, HALOG ENATED D I C H LO R O F L U O R O M E T HA N E M E T H YL E N E C H L O R ID E V O L A TI LE O R G A N IC C P D S (Screen in g) 1,1 !DICHLORO !1 !N I TR O E T H AN E P R O P Y LE N E D IC H L O R ID E DIC HLO RO DIFLUO RO ME THAN E, 1,2 !DICHLOROTETR AFLUO R O ! ETHANE & C H L O R O D IF L UO R O M E T H A N E ORG ANOPHO SPHORUS PESTICIDES ELEM ENTA L CA RBO N (DIES EL PA RT.) AM INO ETH AN O L C O M PO UN DS II AM INE S, A LIPH ATIC AMINOETHANO L COM POUNDS I GLYC OLS V O L A TI LE O R G A N IC C P D S (Screen in g) ETHYLENEDIAMINE, DIETHY LENE TRIAM INE, & T R IE T HY L EN E TE T RA M I N E DIBUTYL PHTHALATE an d DI(2 !ETHY LHEX YL) PHTH ALATE D I FL U O R O D IB R O M O M E T H A N E DIC HLO RO DIFLUO RO ME THAN E, 1,2 !DICHLOROTETR AFLU O R O !ET HAN E & C H L O R O D IF L UO R O M E T H A N E C AP SA ICIN an d D IHY DR O C AP SA ICIN KETONES I KETONES I DIMETHYLACETAMIDE and D I M E TH Y L FO R M A M I D E AM INE S, A LIPH ATIC 2 -(D IM E TH YL AM IN O )E TH A NO L 1 -D IM E TH YL AM IN O -2 -P RO P AN O L AM INE S, A RO M ATIC A R S E N IC , O R G A N O !

Flow Ra te ( L /m i n ) 0.01 - 0.2 0.01 - 0.2 0.2

Vol. (L) min max 1-8 1 - 10 20 - 100

E x tr a c ti o n

A n a ly t ic a l T e c h n iq u e G C -FID G C !FID HPLC !U V

Sampler CCT CCT GFF

C S2 C S2 TE A/M e O H

Dichlorodifluoromethane

1018

0.01 - 0.05

1-4

C H 2C l2

G C !FID

2 CCT (lg + sm )

1,1 !Dichloroethane 1,2 !Dichloroethane D i c hlo r o e thyl e the r 1,2 !Dichloroethylene Dichlorofluoromethane Dichloromethane Dichloromethane

1003 1003 1004 1003 2516 1005 2549

0.01 - 0.2 0.01 - 0.2 0.01 - 1.0 0.01 - 0.2 0.01 - 0.05 0.01 - 0.2 0.01 - 0.05

0.5 - 15 0.5 - 50 2 - 15 0.2 - 5 0.25 - 3 0.5 - 2.5 1-6

C S2 C S2 C S2 C S2 C S2 C S2 t h erma l

G C !FID G C !FID G C !FID G C !FID G C !FID G C !FID TD /G C !M S

CCT CCT CCT CCT 2 C CT ( lg ) 2 CCT TD

1,1 !Dichlo ro !1 !nitroethane 1,2 !Dichloropropane 1,2 !D ic hlo r o te trafluoroethane

1601 1013 1018

0.01 - 1.0 0.01 - 0.2 0.01 - 0.05

1.5 - 15 0.1 - 3.5 1-4

C S2 Acet/cyclohexane C H 2C l2

G C !FID G C !E C N G C !FID

PCT PCT 2 CCT (lg + sm )

D i c ro to pho s Diesel exhaust Diethanolamine Diethylamine 2 !D ie thylam ino e thanol D i e thyle ne glyc o l D i e thyle ne glyc o l e ther

5600 5040 3509 2010 2007 5523 2549

0.2 - 1 1-4 0.5 - 1.0 0.01 - 1.0 0.01 - 0.2 0.5 - 2 0.01 - 0.05

12 - 240 142 -19000 5 - 300 3 - 30 4 - 24 5 - 60 1-6

t ol/a cet t h erma l HSA H 2SO 4/M e O H M eO H/H 2O MeOH t h erma l

G C !FPD E G A/TO A IC G C !FID G C !FID G C !FID TD /G C !M S

O VS !2 QFF IM P SG SG O VS !7 TD

Diethylenetriamine

2540

0.01 - 0.1

1 - 20

DMF

HPLC !U V

X A D !2 w/10 % N ITC

D i!(2 !ethy lhexy l) phth alate

5020

1-3

10 - 200

C S2

G C !FID

MC EF

Difluorodibromom ethane Difluorodichloromethane

1012 1018

0.01 - 0.2 0.01 - 0.05

2.5 - 10 1-4

IPA C H 2C l2

G C !FID G C !FID

2 CCT 2 CCT

Dih yd ro ca ps aic in Diisobutyl ketone Diisobutyl ketone D i m e thylac e tam ide

5041 1300 2555 2004

1-3 0.01 - 0.2 0.01 - 0.2 0.01 - 1.0

7 - 1000 1 - 10 1 - 10 15 - 80

C H 3C N C S2 C S2 MeOH

HPLC !FL G C !FID G C -FID G C !FID

GFF CCT A -C M S SG

Dimethylamine 2-(D im e thylam ino )e thanol 1-D im e thylam ino -2-propan ol N,N !Dimethylaniline Dim eth yla rsin ic a cid

2010 2561

0.01 - 1.0 0.02 - 0.1

3 - 30 10 - 24

H 2SO 4/M e O H MeOH

G C !FID G C -FID

SG XAD

2002 5022

0.02 - 1.0 1-3

3 - 30 50 - 1000

Et h a nol b u ffer

G C !FID IC !HYAAS

SG PTFE

3/15/2003

MF!9

NIOSH Manual of Analytical Methods

Chemical Dim e thylfo rmamide

M eth No. 2004

M e th od Na m e DIMETHYLACETAMIDE & D I M E TH Y L FO R M A M I D E 1,1 !D I M E TH Y L HY D R A Z IN E AM INE S, A RO M ATIC DIM ETHY L SULFA TE D I O X AN E DIPHENYL GLYCOL ETHER S

Flow Ra te ( L /m i n ) 0.01 - 1.0

Vol. (L) min max 15 - 80

E x tr a c ti o n

A n a ly t ic a l T e c h n iq u e G C !FID SG

Sampler

MeOH

1,1 !Dimethylhydrazine N,N !Dimethyl!p !toluidine Dim ethy l sulfate Dioxane Diphenyl D i pro pyle ne glyc o l mo no m e thyl e the r D i sulfo to n D i uro n n-Dodecane D y e s ! benzidine !, o !tolidine !, o !dianisidine ! E le me ntal c ar bo n Elem ents Elem ents

3515 2002 2524 1602 2530 2554

0.2 - 1.0 0.02 - 1.0 0.01 - 0.2 0.01 - 0.2 0.01 - 0.5 0.1 - 0.2

2 - 100 20 - 100 0.25 - 12 0.5 - 15 15 - 30 3 - 25

reagent Et h a nol d iEt eth er C S2 C C l4 M e C l2/Me th

VIS G C !FID G C !E C N G C !FID G C !FID G C -FID

BuB (0.1 M HC l) SG Por P CCT Te na x G C A-747

5600 5601 1500 5013

ORG ANOPHO SPHORUS PESTICIDES ORG ANONITROGEN PESTICIDES HYDROC ARBONS, BP 36 -216 C D Y E S , B E N ZI D IN E !, o ! T O LI D IN E !, o ! D IA N IS ID I NE ELEM ENTA L CA RBO N (DIES EL PA RT.) E LE M E NT S b y IC P ELEMENTS by ICP (Aqu a R eg ion Ashin g) E LE M EN TS by IC P (H O T B L O C K /H C l /H N O 3 D IG E S T IO N ) EN DR IN
o o

0.2 - 1 0.1 - 1 NA 1-3

12 - 240 var-480 NA 150 - 500

t ol/a cet reagent C S2 H 2O

G C !FPD HP LC , U V G C -FID HPLC !U V

O VS !2 OV S-2 CCT PTFE

5040 7300 7301

2-4 1-4 1-4

142 -19000 V a r ies V a r ies

t h erma l H N O 3/HC lO 4 Aq R eg

E G A-TO A IC P !AES ICP-AES

QFF MC EF MC EF PVCF MC EF

Elem ents

7303

1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

En dr in

5519

0.5 - 1.0

12 - 400

t ol

G C !E C D

MCEF & Chrom 102 CCT GFF CCT PTFE PTFE PTFE TD

Ep ich lor oh yd rin EPN 1,2 !Epoxypropane

1010 5012 1612 5044 5044 5044 2549

EP ICH LO RO HY DR IN EPN P R O P Y LE N E O X ID E E S TR O G E N I C C O M P O U N D S E S TR O G E N I C C O M P O U N D S E S TR O G E N I C C O M P O U N D S V O L A TI LE O R G A N IC C P D S (Screen in g) ALCOHO LS I AMINOETHANO L COM POUNDS I ORG ANOPHO SPHORUS PESTICIDES ORG ANOPHO SPHORUS PESTICIDES ALC O HO LS IV ESTERS I V O L A TI LE O R G A N IC C P D S (Screen in g) ETHY L AC ETATE ESTERS I KE TO NE S II HY DR O C AR BO NS , AR O M ATIC E T HY L BR O M I D E KE TO NE S II E T HY L C H LO R I D E ETH YLE NE CH LO RO HY DR IN

0.01 - 0.2 1-2 0.01 - 0.2 1 1 1 0.01 - 0.05

2 - 30 15 - 700 0.5 - 5 150 - 1000 150 - 1000 150 - 1000 1-6

C S2 isooctane C S2 M eth M eth M eth t h erma l

G C !FID G C !FPD G C !FID HP LC - U V HP LC - U V HP LC - U V TD /G C !M S

$ -Estradiol
Estrone

$ -Estro diol-3 -Ben zoa te


E thano l

E thano l Ethanolamine E thio n E tho pr o p 2 !Etho xye thano l 2 !Etho xye thyl a ce tate Ethy l ace tate

1400 2007 5600 5600 1403 1450 2549

0.01 - 0.05 0.01 - 0.2 0.2 - 1 0.2 - 1 0.01 - 0.05 0.01 - 0.2 0.01 - 0.05

0.1 - 1 4 - 24 12 - 240 12 - 240 1-6 1 - 10 1-6

2 -b u ta n ol/C S 2 5600 t ol/a cet t ol/a cet MeOH C S2 t h erma l

G C !FID G C !FID G C !FPD G C !FPD G C !FID G C !FID TD /G C !M S

CCT SG O VS !2 O VS !2 CCT CCT TD

Ethy l ace tate Ethy l acry late Ethyl amyl ketone Ethylbenzene E thyl bro m ide Ethyl butyl ketone E thyl c hlo ride Eth yle ne ch lor oh yd rin 3/15/2003

1457 1450 1301 1501 1011 1301 2519 2513

0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.02 - 0.05 0.01 - 0.2 MF!10

0.1 - 10 1 - 10 1 - 25 1 - 24 0.5 - 4 1 - 25 0.3 - 3 2 - 35

C S2 C S2 M e O H /C S 2 C S2 IPA M e O H /C S 2 C S2 IP A /C S 2

G C !FID G C !FID G C !FID G C !FID G C !FID G C !FID G C !FID G C !FID

CCT CCT CCT CCT CCT CCT 2 CC T ( lg ) PCT

NIOSH Manual of Analytical Methods

Chemical Ethylenediamine

M eth No. 2540

M e th od Na m e ETHY LENE DIAM INE, DIETHY LENE TRIAM INE, & T R IE T HY L EN E TE T RA M I N E E T HY L EN E D IB R O M I D E HYDROC ARBONS, HALOG ENATED GLYC OLS N ITR O G LY C ER IN & ETH YL EN E G LY C O L DINITRA TE E T HY L EN E O X ID E E TH YL EN E O X ID E b y p orta ble G C ORG ANIC and INORGANIC G ASES by EX TR ACTIV E FTIR SPE C T R O MET R Y ETHYLENE THIOUREA E T HY L EN I M IN E ETHYL ETHER ETHYL ETHER ETHY L FO RM ATE M E R C A P TA N S ME THYL a nd ETH YL M ETHA CR YLATE ORG ANOPHO SPHORUS PESTICIDES A S BE ST O S & o th e r F IB ER S b y PC M PO LYN UC LEA R A RO M ATIC HYDR OC ARBO NS by H PLC PO LYN UC LEA R A RO M ATIC HYDROCARBONS PO LYN UC LEA R A RO M ATIC HYDR OC ARBO NS by H PLC PO LYN UC LEA R A RO M ATIC HYDROCARBONS FLUORIDES, aerosol & ga s

Flow Ra te ( L /m i n ) 0.01 - 0.1

Vol. (L) min max 1 - 20

E x tr a c ti o n

A n a ly t ic a l T e c h n iq u e HPLC !U V

Sampler X A D !2 w/10 % N ITC

DMF

E thyle ne dibr o m ide E thyle ne dic hlor ide E thyle ne glyc o l Ethy lene glyc ol dinitra te

1008 1003 5523 2507

0.02 - 0.2 0.01 - 0.2 0.5 - 2 0.2 - 1.0

0.1 - 25 1 - 50 5 - 60 3 - 100

b z/M e O H C S2 MeOH Et h a nol

G C !E C D G C !FID G C !FID G C !E C D

CCT CCT O VS !7 Te na x G C

E thyle ne o xide E thyle ne o xide E thyle ne o xide

1614 3702 3800

0.05 - 0.15 > 0.02 0.1 - 2.0

1 - 24 80% vol Inst r. d ep .

DMF NA NA

G C !E C D G C !PID FTIR

PC T w/HB r air bag Di r. R e a d

E thyle ne thio ur e a Ethylenimine E thyl ethe r E thyl ethe r Ethy l form ate E thyl m e rc aptan Ethy l me tha cryta te F e nam ipho s Fibrous glass Fluoranthene

5011 3514 1610 1610 1452 2542 2537 5600 7400 5506

1-3 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.1 - 0.2 0.01 - 0.05 0.2 - 1 0.5 - 16 2.0

200 - 800 1 - 48 0.25 - 3 0.25 - 3 0.3 - 10 10 - 150 1-8 12 - 240 400 !va r ies 200 - 1000

H 2O C H C l3 C S2 Et Ac C S2 H C l/D C E C S2 t ol/a cet

VIS HPLC !U V G C -FID G C !FID G C !FID G C !FPD G C -FID G C !FPD PCM HPLC !FL/U V

PVC or MCEF BuB CCT CCT CCT GFF/HgAc XAD O VS !2 MC EF P T F E & X A D !2

!
ac eto nitr ile

Fluoranthene

5515

2.0

200 - 1000

va r ies

G C !FID

P T F E & X A D !2

Fluorene

5506

2.0

200 - 1000

ac eto nitr ile

HPLC !FL/U V

P T F E & X A D !2

Fluorene

5515

2.0

200 - 1000

va r ies

G C !FID

P T F E & X A D !2

F luo r ide s

7902

1-2

12 - 800

N a OH

ISE

MCEF & pad w / N a2 C O 3 MCEF & pad w/ N a 2C O 3 C CT ( lg ) O VS !2 SG/DNPH X A D !2 /H M P P TF E & 2 IM P X A D !2 /H M P Di r. R e a d

F luo r ide s

7906

FLU O RID ES by IC

1-2

s 1 - 800 i 120 - 800 0.3 - 7 12 - 240 1 - 15 1 - 36 1 - 100 5-5 Inst r. d ep .

N a OH

IC

Fluorotrichloromethane F o no fo s F o r malde hyde F o r malde hyde F o r malde hyde F o r malde hyde F o r malde hyde

1006 5600 2016 2541 3500 2539 3800

F L UO R O T R IC H L O R O M E T H A NE ORG ANOPHO SPHORUS PESTICIDES F O R M A L D E HY D E F O R M A L D E HY D E F O R M A L D E HY D E A L D EH Y D E S, SC R E E N IN G ORG ANIC and INORGANIC G ASES by EX TR ACTIV E FTIR SPE C T R O MET R Y FORM ALDEHYDE on dust ORG ANONITROGEN PESTICIDES FO RM IC A C ID

0.01 - 0.05 0.2 - 1.0 0.1 - 1.5 0.01 - 0.1 0.2 - 1.0 0.01 - 0.05 0.1 - 2.0

C S2 t ol/a cet ac eto nitr ile t ol NaHSO 3 t ol NA

G C !FID G C !FPD HP LC - U V G C !FID VIS G C !F ID /M S FTIR

F o r malde hyde F o rm e ta n ate .H C I Fo rm ic a cid

5700 5601 2011

2 0.1 - 1 0.05 - 0.2

240 - 1050 var-480 1 - 24

H 2O /D N PH /C H 3C N reagent H 2O

HPLC !U V HP LC , U V IC

I O M / P VC OV S-2 PTFE & SG ( w a sh e d ) X A D !2 /H M P X A D !2 /H M P

F ur fur al F ur fur al

2529 2539

FU R FU R AL A L D EH Y D E S, SC R E E N IN G

0.01 - 0.05 0.05

1 - 12 5-5

t ol t ol

G C !FID G C !F ID /M S

3/15/2003

MF!11

NIOSH Manual of Analytical Methods

Chemical F u r fur yl alco ho l G allium

M eth No. 2505 7303

M e th od Na m e F UR FU RY L A LC O H O L E LE M EN TS by IC P (H O T B L O C K /H C l /H N O 3 D IG E S T IO N ) G L U TA R A LD E H Y D E PARTICU LATES N.O.R . G LY C ID O L GLYC OLS E LE M EN TS by IC P (H O T B L O C K /H C l /H N O 3 D IG E S T IO N ) A L D EH Y D E S, SC R E E N IN G V O L A TI LE O R G A N IC C P D S (Screen in g) HYDROC ARBONS, BP 36 !216 C KE TO NE S II KE TO NE S II CHLORINATED ORG ANONITROGEN H ER BIC ID ES (A IR SA M PL IN G ) CHLORINATED ORG ANONITROGEN HER BICIDES (HAND WAS H) CHLORINATED ORG ANONITROGEN HE RBIC IDES (DER M AL P ATC H)) H E X A C H LO R O B U T A D IE N E HEXACHLOR O !1,3 !CY CLO PEN TA D I EN E HYDROC ARBONS, HALOG ENATED ISOCYANATES

Flow Ra te ( L /m i n ) 0.01 - 0.05 1-4

Vol. (L) min max 3 - 25 Se e Ta ble

E x tr a c ti o n

A n a ly t ic a l T e c h n iq u e G C !FID ICP-AES

Sampler Por Q MC EF

a cet H C l /H N O 3

G lutar alde hyde Glycerin mist G lyc ido l G lyc ols G old

2532 0500 1608 5523 7303

0.01 - 0.08 1-2 0.01 - 1.0 0.5 - 2 1-4

4 - 39 7 - 133 5 - 100 5 - 60 Se e Ta ble

C H 3C N NA T HF MeOH H C l /H N O 3

HPLC !U V Grav G C !FID G C !FID ICP-AES

SG/DNPH P VC CCT O VS !7 MC EF

H eptanal n !Heptane

2539 2549

0.01 - 0.05 0.01 - 0.05

5-5 1-6

t ol t h erma l

G C !F ID /M S TD /G C !M S

X A D !2 /H M P TD

n !Heptane 2-Heptanone 3-Heptanone H er bic ides

1500 2553 2553 5602

0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.2 - 1

NA 1 - 25 1 - 25 12 - 480

C S2 IP A -C S 2 IP A -C S 2 reagent

G C !FID G C -FID G C -FID G C /E C D

CCT A -C M S A -C M S OV S-2

H er bic ides

9200

NA

NA

NA

G C - EC D

polyethylene bag PUF pad

H er bic ides

9201

NA

NA

IPA/diazomethane

G C - EC D

Hexachlorobutadiene Hexa chloro !1,3 !cy clo pentadiene Hexachloroethane Hexamethylene! diisoc ya nate 1,6-Hexamethylene ! diisoc ya nate 1,6-Hexamethylene diiso cy an ate (HD I) H exanal H exanal

2543 2518

0.05 - 0.2 0.01 - 0.2

1 - 100 0.25 - 90

hexane hexane

G C !E C D G C !E C D

X A D !2 2 Por T

1003 5522

0.01 - 0.2 1-2

3 - 70 15 - 360

C S2 tryptamine/DMSO

G C !FID HPLC !FL

CCT IM P

5521

ISO C YA NA TES , M O NO M ER IC

1.0

5 - 500

rea ge nts

HPLC !EC HD

IM P

5525

ISOCYANATES, TOTAL (MAP)

1-2

1 - 500

MAP

HP LC /UV

G F F, IM P

2539 2549

A L D EH Y D E S, SC R E E N IN G V O L A TI LE O R G A N IC C P D S (Screen in g) V O L A TI LE O R G A N IC C P D S (Screen in g) HYDROC ARBONS, BP 36 !216 C ORG ANIC and INORGANIC G ASES by EX TR ACTIV E FTIR SPE C T R O MET R Y KETONES I KETONES I HIP PU RIC an d M ETH YL H IPP UR IC ACID in urine H Y D R A ZI N E AC IDS , INO RG AN IC AC IDS , INO RG AN IC H Y D R O G E N C Y A N ID E H Y D R O G E N C Y A N ID E

0.01 - 0.05 0.01 - 0.05

5-5 1-6

t ol t h erma l

G C !F ID /M S TD /G C !M S

X A D !2 /H M P TD

n !Hexane

2549

0.01 - 0.05

1-6

t h erma l

TD /G C !M S

TD

n !Hexane n-Hexane

1500 3800

0.01 - 0.2 0.1 - 2.0

4-4 Inst r. d ep .

C S2 NA

G C !FID FTIR

CCT Di r. R e a d

2 !Hexanone 2-Hexanone Hip pu ric ac id

1300 2555 8301

0.01 - 1.0 0.01 - 0.2 NA

1 - 10 1 - 10 NA

C S2 C S2 Et a c

G C !FID G C -FID HP LC - U V

CCT A -C M S NA

Hydrazine H y dr o ge n br o mide H y dr o ge n c hlo r ide H y dr o ge n c yanide H y dr o ge n c yanide

3503 7903 7903 6010 6017

0.2 - 1.0 0.2 - 0.5 0.2 - 0.5 0.05 - 0.2 0.05 - 2

7 - 100 3 - 100 3 - 100 2 - 90 2 - 90

rea ge nts H C O 3 /C O 3 H C O 3-/C O 3 H 2O H 2O


2-

VIS IC IC VIS IC -D C Am p

BuB SG SG s od a lim e SL

2-

3/15/2003

MF!12

NIOSH Manual of Analytical Methods

Chemical H ydr o ge n c yanide H y dr o ge n flo ur ide H y dr o ge n flo ur ide

M eth No. 7904 7903 7902

M e th od Na m e CYANIDES, AEROSOL & G AS AC IDS , INO RG AN IC FLUORIDES, AEROSOL & G AS

Flow Ra te ( L /m i n ) 0.5 - 1.0 0.2 - 0.5 1-2

Vol. (L) min max 7 - 100 3 - 100 12 - 800

E x tr a c ti o n

A n a ly t ic a l T e c h n iq u e ISE

Sampler MC EF SG M CE F & p a d w / N a2C O 3 M CE F & p a d w / N a2C O 3 P T FE & C CT ( lg ) MC EF P T F E & X A D !2

KOH H C O 3 /C O 3 N a OH
2-

IC ISE

H y dr o ge n flo ur ide

7906

FLU O RID ES by IC

1-2

1 - 800

N a OH

IC

H y dr o ge n sulfide

6013

H Y D R O G E N S UL F ID E (withdrawn) H Y D R O Q U IN O N E PO LYN UC LEA R A RO M ATIC HYDR OC ARBO NS by H PLC PO LYN UC LEA R A RO M ATIC HYDROCARBONS I O D IN E E LE M EN TS by IC P (H O T B L O C K /H C l /H N O 3 D IG E S T IO N ) ELEMENTS on WIPES ELE M EN TS b y IC P (A Q UA RE G IA A SH IN G ) E LE M EN TS by IC P (H O T B L O C K /H C l /H N O 3 D IG E S T IO N ) E LE M E NT S b y IC P ESTERS I ALC O HO LS III ALCOHO LS COM BINED ESTERS I ALC O HO LS II ALCOHO LS COM BINED A L D EH Y D E S, SC R E E N IN G ISO C YA NA TES , M O NO M ER IC ISOCYANATES I SO P H O R O N E I SO P H O R O N E ISOCYANATES, TOTAL (MAP)

0.1 - 1.5

1.2 - 40

N H 4OH /H 2O 2

IC

Hydroquinone Indeno[1,2,3-cd]pyrene

5004 5506

1-4 2.0

30 - 180 200 - 1000

ac etic ac id ac eto nitr ile

HPLC !U V HPLC !FL/U V

Inden o [1,2,3 !cd] pyrene

5515

2.0

200 - 1000

va r ies

G C !FID

P T F E & X A D !2

Iodine I ndium

6005 7303

0.5 - 1.0 1-4

15 - 225 Se e Ta ble

N a 2C O 3 H C l /H N O 3

IC ICP-AES

C C T w /alk ali MC EF

I ron I ron

9102 7301

NA 1-4

NA 5 - 100

NA H C l /H N O 3

ICP-AES ICP-AES

Wipe MC EF

I ron

7303

1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

I ron Isoa my l ace tate I soam yl alc o ho l I soam yl alc o ho l Isob utyl a ce tate I sobutyl alco ho l I sobutyl alco ho l I sobutyraldehyde I soc yanate s I soc yanate s Isophorone Isophorone Isop ho rone diisoc ya nate (IPD I) Isop rop yl ac etate Isop rop yl ac etate I sopr o pyl alco ho l

7300 1450 1402 1405 1450 1401 1405 2539 5521 5522 2508 2556 5525

1-4 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.05 1.0 1-2 0.01 - 1.0 0.01 - 1 1-2

5 - 100 1 - 10 1 - 10 1 - 10 1 - 10 2 - 10 2 - 10 5-5 5 - 500 15 - 360 2 - 25 2 - 25 1 - 500

H N O 3/HC lO 4 C S2 IP A /C S 2 IP A -C S 2 C S2 IP A /C S 2 IP A -C S 2 t ol rea ge nts tryptamine/DMSO C S2 DEE MAP

IC P !AES G C !FID G C !FID G C -FID G C !FID G C !FID G C -FID G C !F ID /M S HPLC !EC HD HPLC !FL/EC HD G C !FID G C -FID HP LC /UV

MC EF CCT CCT CCT CCT CCT CCT X A D !2 /H M P IM P IM P PCT XAD G F F, IM P

1454 1460 2549

ISOP RO PYL A CE TATE ISOP RO PYL A CE TATE V O L A TI LE O R G A N IC C P D S (Screen in g) ALCOHO LS I ISOPROPYL ETHER ISOPROPYL GLYCIDYL ETHER ALIPHATIC ALDEHYDES A L D EH Y D E S, SC R E E N IN G KEPONE NAPHTHAS

0.02 - 0.2 0.02 - 0.2 0.01 - 0.05

0.1 - 9 0.1 - 9 1-6

C S2 C S 2-M eth t h erma l

G C !FID G C -FID TD /G C !M S

CCT CCT TD

I sopr o pyl alco ho l I sopr o pyl e the r I sopr o pyl glyc idyl ether I sovale r alde hyde I sovale r alde hyde Kepone Kerosene

1400 1618 1620 2018 2539 5508 1550

0.01 - 0.2 0.01 - 0.05 0.01 - 0.2 0.1 - 1.5 0.01 - 0.05 0.5 - 1.0 0.01 - 0.2

0.2 - 3 0.1 - 3 1 - 30 1 - 15 5-5 50 - 600 1.3 - 20

2 -b u ta n on e /C S 2 C S2 C S2 ACN t ol b z/M e O H C S2

G C !FID G C !FID G C !FID HP LC /UV G C !F ID /M S G C !E C D G C !FID

CCT CCT CCT SG-DNPH X A D !2 /H M P M C E F & IM P CCT

3/15/2003

MF!13

NIOSH Manual of Analytical Methods

Chemical Lanthanum

M eth No. 7301

M e th od Na m e ELE M EN TS b y IC P (A Q UA RE G IA A SH IN G ) ELEMENTS on WIPES LEAD by FAAS LEAD BY FIELD POR TABLE XRF LEAD by GFAAS LEAD BY ULTRASOUND /ASV E LE M E NT S b y IC P LEAD in Air by Che mical Spot Test LEAD in Surface Wipe Sa mp les ELE M EN TS b y IC P (A Q UA RE G IA A SH IN G ) ELEMENTS on WIPES E LE M EN TS by IC P (H O T B L O C K /H C l /H N O 3 D IG E S T IO N ) LEAD in DUST WIPES by C h emica l Spot Test L E AD S U LF ID E TERPENES V O L A TI LE O R G A N IC C P D S (Screen in g) A L D R IN a n d LI N DA N E E LE M E NT S b y IC P ELE M EN TS b y IC P (A Q UA RE G IA A SH IN G ) ALKA LINE DU STS E LE M E NT S b y IC P ELE M EN TS b y IC P (A Q UA RE G IA A SH IN G ) E LE M EN TS by IC P (H O T B L O C K /H C l /H N O 3 D IG E S T IO N ) ORG ANOPHO SPHORUS PESTICIDES M A L E IC A N H Y D R ID E MANEB MANEB E LE M E NT S b y IC P ELEMENTS on WIPES ELE M EN TS b y IC P (A Q UA RE G IA A SH IN G ) E LE M EN TS by IC P (H O T B L O C K /H C l /H N O 3 D IG E S T IO N ) KETONES I ISO C YA NA TES , M O NO M ER IC

Flow Ra te ( L /m i n ) 1-4

Vol. (L) min max 5 - 1000

E x tr a c ti o n

A n a ly t ic a l T e c h n iq u e ICP-AES

Sampler MC EF

H C l /H N O 3

La nthanum Lead Lead Lead Lead Lead Lead Lead Lead

9102 7082 7702 7105 7701 7300 7700 9100 7301

NA 1-4 1-4 1-4 1-4 1-4 2 NA 1-4

NA 200 - 1500 570 - 1900 1 - 1500 20 - 1500 1250 -2000 10 - 240 NA 50 - 2000

NA H N O 3/H 2O 2 NA H N O 3/H 2O 2 HNO3 H N O 3/HC lO 4

ICP-AES FAAS XR F (po rt) G FAAS Port ASV IC P !AES Sp ot A A S; IC P ICP-AES

Wipe MC EF MC EF MC EF MC EF MC EF MC EF Wipes MC EF

!
H N O 3/HC lO 4 H C l /H N O 3

Lead Lead

9102 7303

NA 1-4

NA Se e Ta ble

NA H C l /H N O 3

ICP-AES ICP-AES

Wipe MC EF

Lead

9105

NA

NA

NA

Sp ot

Wipe

Lead sulfide Limonene Limonene

7505 1552 2549

1.7 or 2 .2 0.01 - 0.2 0.01 - 0.05

600 - 1000 2 - 30 1-6

T HF C S2 t h erma l

XR D G C !FID TD /G C !M S

C Y C & P VC CCT TD

Lindane Lithium Lithium

5502 7300 7301

0.2 - 1.0 1-4 1-4

18 - 240 100 - 2000 100 - 2000

isooctane H N O 3/HC lO 4 H C l /H N O 3

G C !E C N IC P !AES ICP-AES

GFF & BuB MC EF MC EF

Lithium hydr o xide M agne sium M agne sium

7401 7300 7301

1-4 1-4 1-4

70 - 1000 5 - 67 5 - 67

HCl H N O 3/HC lO 4 H C l /H N O 3

T it ra t ion IC P !AES ICP-AES

PTFE MC EF MC EF

M agne sium

7303

1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

M alathio n M ale ic A nhydride M ane b M ane b Mang anese Mang anese Mang anese

5600 3512 3601 3600 7300 9102 7301

0.2 - 1 0.2 - 1.5 NA NA 1-4 NA 1-4

12 - 60 40 - 500 NA NA 5 - 200 NA 5 - 200

t ol/a cet H 2O NA Cy s/EDTA H N O 3/HC lO 4 NA H C l /H N O 3

G C !FPD HPLC !U V HP LC - U V HP LC - U V IC P !AES ICP-AES ICP-AES

O VS !2 BuB Hand wa sh Patch MC EF Wipe MC EF

Mang anese

7303

1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

MBK MDI (4,4'!methylene ! b isphe nyl iso c yanate ) MDI (4,4'!methylene ! b isphe nyl iso c yanate ) Me rcury

1300 5521

0.01 - 0.2 1.0

1 - 10 5 - 500

C S2 rea ge nts

G C !FID HPLC !EC HD

CCT IM P

5522

ISOCYANATES

1-2

15 - 360

tryptamine

HPLC !FL/EC HD

IM P

6009

MER CURY

0.15 - 0.25

2 - 100

H N O 3/H C l

AAS !cold va p

Ho pc alite

3/15/2003

MF!14

NIOSH Manual of Analytical Methods

Chemical Mercaptans M e sityl o xide M e sityl o xide M eta ls in air M e talwo r k ing F luids

M eth No. 2542 1301 2553 7300 5524

M e th od Na m e M E R C A P TA N S KE TO NE S II KE TO NE S II E LE M E NT S b y IC P META LWO RKING FLUIDS (MW F) ALL CATEGO RIES F O R M A L D E HY D E ORG ANOPHO SPHORUS PESTICIDES M E TH A NO L V O L A TI LE O R G A N IC C P D S (Screen in g) ORG ANIC and INORGANIC G ASES by EX TR ACTIV E FTIR SPE C T R O MET R Y ORG ANONITROGEN PESTICIDES ORG ANONITROGEN PESTICIDES CHLORINATED ORG ANONITROGEN H ER BIC ID ES (A IR SA M PL IN G ) CHLORINATED ORG ANONITROGEN HER BICIDES (HAND WAS H) CHLORINATED ORG ANONITROGEN HE RBIC IDES (DER M AL P ATC H)) ME THYL C ELLO SO LVE A CE TATE ALC O HO LS IV ME THYL A CE TATE ME THYL A CR YLATE ME THYL A CR YLATE M E TH A NO L METHYLAL p -TO LUE NE SU LFO NIC AC ID

Flow Ra te ( L /m i n ) 0.1 - 0.2 0.01 - 0.2 0.01 - 0.2 1-4 1.6 - 2.0

Vol. (L) min max 10 - 150 1 - 25 1 - 25 var - 2000 1000 - ND

E x tr a c ti o n

A n a ly t ic a l T e c h n iq u e G C !FPD G C !FID G C -FID IC P !AES Grav

Sampler GFF/HgAc CCT A -C M S MC EF PTFE/CYC

H C l/D C E M e O H /C S 2 IP A -C S 2 H N O 3/HC lO 4 D C M/MeO H/T ol MeOH ac eto nitr ile t ol/a cet H 2O/IPA t h erma l

M e thanal M e tham ido pho s M e thano l M e thano l

2016 5600 2000 2549

0.1 - 1.5 0.2 - 1 0.02 - 0.2 0.01 - 0.05

1 - 15 12 - 240 1-5 1-6

HP LC - U V G C !FPD G C -FID TD /G C !M S

SG/DNPH O VS !2 SG TD

M e thano l

3800

0.1 - 20

Inst r. d ep .

NA

FTIR

Di r. R e a d

Me thioca rb Methomyl M e to lac hlo r

5601 5601 5602

0.1 - 1 0.1 - 1 0.2 - 1

var - 480 var - 480 12 - 480

reagent reagent reagent

HP LC - U V HP LC - U V G C /E C D

OV S-2 OV S-2 OV S-2

M e to lac hlo r

9200

NA

NA

NA

G C - EC D

polyethylene bag PUF pad

M e to lac hlo r

9201

NA

NA

IPA/diazomethane

G C - EC D

2 !M etho xye thyl a ce tate 2 !M e tho xye thano l M ethy l ace tate M ethy l acry late M ethy l acry late M e thyl alco ho l M e thylal 4-M eth ylb en ze ne su lfon ic ac id N -Methyl-y-butyrolactone Methyl !(n !am yl) !ketone M eth yla rso nic ac id M e thyl br o m ide Methyl cellosolve M ethy l celloso lve a ce tate M e thyl c hlo r ide Me thyl chloro form Me thyl chloro form

1451 1403 1458 1459 2552 2000 1611 5043

0.01 - 0.2 0.01 - 0.05 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.02 - 0.2 0.01 - 0.2 1-3

0.2 - 20 6 - 50 0.2 - 10 1-5 1-5 1-5 1-3 10 - 1000

C S2 M e O H /C H 2C l2 C S2 C S2 C S2 H 2O/IPA hexane IPA/H 20

G C !FID G C !FID G C !FID G C !FID G C -FID G C !FID G C !FID HP LC - U V

CCT CCT CCT CCT A -C M S SG CCT GFF

1302 1301 5022 2520 1403 1451 1001 1003 2549

N - M E TH Y L -2 - PY R R O L ID I NO N E KE TO NE S II A R S E N IC , O R G A N O ! M E T H YL B RO M I D E ALC O HO LS IV ME THYL C ELLO SO LVE A CE TATE M E T H YL C H LO R I D E HYDROC ARBONS, HALOG ENATED V O L A TI LE O R G A N IC C P D S (Screen in g) AC ETON ITRILE HYDROC ARBONS, BP 36 !216 C M E TH YL CY C LO H EX AN O L M E T H YL C Y C LO H E X A N O N E ISOCYANATES, TOTAL (MAP)

0.05 - 0.2 0.01 - 0.2 1-3 0.01 - 0.1 0.01 - 0.05 0.01 - 0.2 0.01 - 0.1 0.01 - 0.2 0.01 - 0.05

0.5 - 125 1 - 25 50 - 1000 1-5 6 - 50 0.2 - 20 0.4 - 3 0.1 - 8 1-6

C H 2C l2/M e O H M e O H /C S 2 b u ffer C S2 M e O H /C H 2C l2 C S2 C H 2C l2 C S2 t h erma l

G C -NP D o r FID G C !FID IC !HYAAS G C !AED G C !FID G C !FID G C !FID G C !FID TD /G C !M S

CCT CCT PTFE P C T (2 ) +d ry t u b e CCT CCT 2 C C T (lg + sm ) CCT TD

M e thyl c yanide Methyl cyclohexane M e thylc yc lo he xano l Methylcyclohexanone 4,4 '-M eth yle ne -b is (c yc lo he xyl iso cy an ate ) (HM DI)

1606 1500 1404 2521 5525

0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.05 1-2

3 - 25 4-4 1 - 15 1-6 1 - 500

MEC l/MEO H C S2 C H 2C l2 a cet MAP

G C !FID G C !FID G C !FID G C !FID HP LC /UV

CCT CCT CCT Por Q G F F, IM P

3/15/2003

MF!15

NIOSH Manual of Analytical Methods

Chemical 4,4-Methylene-bis (phenyl isoc ya na te) (M DI) M e thyle ne c hlo r ide M e thyle ne c hlo r ide

M eth No. 5525

M e th od Na m e ISOCYANATES, TOTAL (MAP)

Flow Ra te ( L /m i n ) 1-2

Vol. (L) min max 1 - 500

E x tr a c ti o n

A n a ly t ic a l T e c h n iq u e HP LC /UV

Sampler G F F, IM P

MAP

1005 2549

M E T H YL E N E C H L O R ID E V O L A TI LE O R G A N IC C P D S (Screen in g) ORG ANIC and INORGANIC G ASES by EX TR ACTIV E FTIR SPE C T R O MET R Y 4,4'!M E T H YL E N ED I AN I LI N E ISOCYANATES

0.01 - 0.2 0.01 - 0.05

0.5 - 2.5 1-6

C S2 t h erma l

G C -FID TD /G C !M S

2 CCT TD

M e thyle ne c hlo r ide

3800

0.1 - 20

Inst r. d ep .

NA

FTIR

Di r. R e a d

4,4'!Methylenedianiline 4,4 !Methylene diphenyl diisoc ya nate Methyl ethyl ketone

5029 5522

1-2 1-2

10 - 1000 15 - 360

K O H/M e O H tryptamine

HPLC !U V HPLC !FL/EC HD

GF F/H 2SO 4 IM P

2549

V O L A TI LE O R G A N IC C P D S (Screen in g) M E T H YL E TH Y L K E TO N E KETONES I M E T H YL E TH Y L K E TO N E P E R O X ID E

0.01 - 0.05

1-6

t h erma l

TD /G C !M S

TD

Methyl ethyl ketone Methyl ethyl ketone Methyl ethyl ketone p er o xide 5 !Methyl !3 !heptanone 5-Methyl-3-heptanone M eth yl h ipp ur ic a cid

2500 2555 3508

0.01 - 0.2 0.01 - 0.2 0.5 - 0.2

0.25 - 12 1 - 10 52 - 520

C S2 C S2 reagent

G C !FID G C -FID VIS

Carbon be ads A -C M S IM P

1301 2553 8301

KE TO NE S II KE TO NE S II HIP PU RIC an d M ETH YL H IPP UR IC ACID in urine M E T H YL IO D I D E ESTERS I ALC O HO LS III ALCOHO LS COM BINED V O L A TI LE O R G A N IC C P D S (Screen in g) KETONES I KETONES I M E R C A P TA N S ME THYL a nd ETH YL M ETHA CR YLATE ORG ANOPHO SPHORUS PESTICIDES V O L A TI LE O R G A N IC C P D S (Screen in g) N - M E TH Y L -2 - PY R R O L ID I NO N E HY DR O C AR BO NS , AR O M ATIC HY DR O C AR BO NS , AR O M ATIC METH YL tert !BUTYL ETHER METHYLTIN CHLORIDES ORG ANOPHO SPHORUS PESTICIDES NAPHTHAS E LE M E NT S b y IC P EL EM EN TS b y IC P (A qu a R eg ia Ashin g) EL EM EN TS b y IC P (H ot B loc k/H C l/ H N O 3 Digestion) ELEMENTS on WIPES ORG ANOPHO SPHORUS PESTICIDES

0.01 - 0.2 0.01 - 0.2 NA

1 - 25 1 - 25 NA

M e O H /C S 2 IP A -C S 2 Et a c

G C !FID G C -FID HP LC - U V

CCT A -C M S NA

M e thyl io dide M ethy l isoam yl ac etate M e thyl iso butyl c ar binol M e thyl iso butyl c ar binol Methyl isobutyl ketone

1014 1450 1402 1405 2549

0.01 - 1.0 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.05

15 - 50 1 - 10 1 - 10 1 - 10 1-6

t ol C S2 IP A /C S 2 IP A -C S 2 t h erma l

G C !FID G C !FID G C !FID G C -FID TD /G C !M S

CCT CCT CCT CCT TD

Methyl isobutyl ketone Methyl isobutyl ketone M e thyl me r c aptan M ethy l me tha cryla te M e thyl par athio n M e thyl phe no l

1300 2555 2542 2537 5600 2549

0.01 - 0.2 0.01 - 0.2 0.1 - 0.2 0.01 - 0.05 0.2 - 1 0.01 - 0.05

1 - 10 1 - 10 10 - 150 1-8 12 - 240 1-6

C S2 C S2 H C l/D C E C S2 t ol/a cet t h erma l

G C !FID G C -FID G C !FPD G C !FID G C !FPD TD /G C !M S

CCT A -C M S GFF/HgAc XAD O VS !2 TD

N -methyl-2-pyrrolidinone

1302 1501 1501 1615 5526 5600 1550 7300 7301

0.05 - 0.2 0.01 - 0.2 0.01 - 0.2 0.1 - 0.2 0.25 - 1 0.2 - 1.0 0.01 - 0.2 1-4 1-4

0.5 - 125 1 - 30 1 - 30 2 - 96 15 - 75 12 - 240 1.3 - 20 5 - 67 5 - 67

C H 2C l2/M e O H C S2 C S2 C S2 AAA t ol/a cet C S2 H N O 3/HC lO 4 H C l /H N O 3

G C -NP D o r FID G C !FID G C -FID G C !FID GC-FPD G C !FPD G C !FID IC P !AES ICP-AES

CCT CCT CCT 2 CC T ( lg ) O VS O VS !2 CCT MC EF MC EF

"!Methyl styrene $ -Methylstyrene


M eth yl tert !butyl e ther M e thyltin c hlo r ide M e vinphos M inera l spirits M o lybde num M o lybde num

M o lybde num

7303

1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

M o lybde num M o no c r o to pho s

9102 5600

NA 0.2 - 1

NA 12 - 240

NA t ol/a cet

ICP-AES G C !FPD

Wipe O VS !2

3/15/2003

MF!16

NIOSH Manual of Analytical Methods

Chemical Monom ethylaniline Monom ethylhydrazine M yc o bac te rium Nap htha (coal tar) Naphthalene Naphthalene

M eth No. 3511 3510 0900 1550 1501 5506

M e th od Na m e M O N O M E T HY L AN I LI N E M O N O M E T HY L H YD R A Z IN E M YC O BA C TER IUM TUB ER C ULO SIS NAPHTHAS HY DR O C AR BO NS , AR O M ATIC PO LYN UC LEA R A RO M ATIC HYDR OC ARBO NS by H PLC PO LYN UC LEA R A RO M ATIC HYDROC ARBONS ISOCYANATES, TOTAL (MAP)

Flow Ra te ( L /m i n ) 0.2 - 1.0 0.5 - 1.5

Vol. (L) min max 11 - 100 3 - 20 va r ies 1.3 - 20 100 - 200 200 - 1000

E x tr a c ti o n

A n a ly t ic a l T e c h n iq u e G C !FID VIS reagent G C !FID G C !FID HPLC !FL/U V

Sampler BuB /H 2SO 4 B u B/H C l PTFE CCT CCT P T F E & X A D !2

N a OH P M A /H C l PCR C S2 C S2 ac eto nitr ile

$4
0.01 - 0.2 0.01 - 1.0 2.0

Naphthalene

5515

2.0

200 - 1000

va r ies

G C -FID

P T F E & X A D !2

1,5-Naphthalene diiso cy an ate (ND I) N a phthylamine s N eo dym ium

5525

1-2

1 - 500

MAP

HP LC - U V

G F F, IM P

5518 7303

NAPHTHYLAMINES EL EM EN TS b y IC P (H ot B loc k/H C l/ H N O 3 Digestion) E LE M E NT S b y IC P EL EM EN TS b y IC P (A qu a R eg ia Ashin g) EL EM EN TS b y IC P (H ot B loc k/H C l/ H N O 3 Digestion) ELEMENTS on WIPES NICKEL CARBONYL N I C O TI N E N I C O TI N E AC IDS , INO RG AN IC N I TR IC O X I D E & N IT R O G E N D IO X I D E

0.2 - 0.8 1-4

30 - 100 Se e Ta ble

acetic a /IPA H C l /H N O 3

G C !FID ICP-AES

GFF & SG MC EF

N i c ke l N i c ke l

7300 7301

1 !4 1-4

25 - 1000 5 - 1000

H N O 3/HC lO 4 H C l /H N O 3

IC P !AES ICP-AES

MC EF MC EF

N i c ke l

7303

1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

N i c ke l Nickel carbonyl Nicotine Nicotine Nit ric ac id N i tr ic o xide

9102 6007 2544 2551 7903 6014

NA 0.05 - 0.2 1.0 0.1 - 1.0 0.2 - 0.5 0.025

NA 7 - 80 60 - 400 0.5 - 600 3 - 100 1.5 - 6

NA HNO3 Et Ac ethy l ace tate H C O 3-/C O 3 reagent


2-

ICP-AES G FAAS G C !NPD GC-NPD IC VIS

Wipe C C T (lo w N i) X A D !2 XA D-4 S G ( w a s h ed ) M S w / T EA & o x id i ze r MC EF SG GFF + SG

p !Nitroaniline Nitrobenzene Nitrobenzene

5033 2005 2017

p !N I TR O A N IL IN E N I TR O A R O M A T IC C O M P O U N D S A N IL IN E , o - TO L U ID I NE , A N D N I TR O B E N Z EN E A N IL IN E , o - TO L U ID I NE , A N D N I TR O B E N Z EN E N I TR O A R O M A T IC C O M P O U N D S N I TR O E T H AN E N I TR IC O X I D E & N IT R O G E N D IO X I D E N I TR O G E N D IO X I D E N I TR O G E N D IO X I D E N ITR O G LY C ER IN & ETH YL EN E G LY C O L DINITRA TE N I TR O M E T H A N E 2 !N I TR O P R O P A N E 1-NITROPYRENE in DIESEL PARTICULATES NITROSAMINES N I TR O A R O M A T IC C O M P O U N D S ORG ANIC and INORGANIC G ASES by EX TR ACTIV E FTIR SPE C T R O MET R Y

1-3 0.01 - 1 0.2

20 10 - 150 5 - 50

IPA MeOH et h a nol

HPLC !U V G C !FID G C -FID

N i tr o be nzo l

2017

0.2

5 - 50

et h a nol

G C -FID

GFF + SG

p !Nitrochlorobenzene Nitroethane N i tr o ge n dio xide N i tr o ge n dio xide N i tr o ge n pe r o xide Nit ro gly ce rin

2005 2526 6014 6700 6700 2507

0.01 - 1 0.01 - 0.05 0.025 - 0.2 NA NA 0.2 - 1.0

1 - 150 1.5 - 3 1.5 - 6 NA NA 3 - 100

MeOH Et Ac reagent reagent reagent et h a nol

G C !FID G C !FID VIS VIS VIS G C !E C D

SG 2 X A D !2 MS w/TEA Diffusive Diffusive T e n a x!G C

Nitromethane 2 !Nitropropane 1-Nitropyrene

2527 2528 2560

0.01 - 0.05 0.01 - 0.05 1.0 - 2.0

1.2 - 3 0.1 - 2 480 - 960

Et Ac Et Ac T ol

G C !FPD G C !FID G C /N C D

Chrom 106 Chrom 106 GFF

N i tr o samine s o - ,m - , p -Nitrotoluene N i tr o us o xide

2522 2005 3800

0.2 - 2.0 0.01 - 0.2 0.1 - 20

15 - 1000 1 - 30 Inst r. d ep .

M e O H /C H 2C l2 MeOH NA

G C !TEA G C !FID FTIR

T D tu b e SG Di r. R e a d

3/15/2003

MF!17

NIOSH Manual of Analytical Methods

Chemical Nitr o us o xide n-Nonane NMP Nuisance dusts n !Octane

M eth No. 6600 1500 1302 0500 2549

M e th od Na m e N I TR O U S O X ID E HYDROC ARBONS, BP 36-216 oC N-Methyl-2-Pyrrolidinone PARTICU LATES N.O.R . V O L A TI LE O R G A N IC C P D S (Screen in g) HYDROC ARBONS, BP 36 !216 C V O L A TI LE O R G A N IC C P D S (Screen in g) 1 !O C TA N ETH IO L OIL MIST, MINER AL ORG ANONITROGEN PESTICIDES ORG ANOPHO SPHORUS PESTICIDES

Flow Ra te ( L /m i n ) NA 0.01 - 0.2 0.05 - 0.2 1-2 0.01 - 0.05

Vol. (L) min max 80% vol 4-4 0.5 - 125 7 - 133 1-6

E x tr a c ti o n

A n a ly t ic a l T e c h n iq u e IR G C -FID GC-FID/NPD G R AV TD /G C !M S

Sampler air bag CCT CCT P VC TD

NA C S2 C H 2C l2/M e O H NA t h erma l

n !Octane Oc tam ethylcy clotetra ! siloxane 1 !Oc tane thio l O il m ist (m ine ra l) O r gano nitro ge n pe sticides O r gano pho spho r us Pestic ide s Oxamyl O xyge n PA C

1500 2549

0.01 - 0.2 0.01 - 0.05

4-4 1-6

C S2 t h erma l

G C !FID TD /G C !M S

CCT TD

2510 5026 5601 5600

0.01 - 0.2 1-3 0.1 - 1 0.2 - 1

1 - 15 20 - 500 varies-480 12 - 240

a cet C C l4 reagent t ol/a cet

G C !FPD IR HP LC - U V G C !FPD

Te na x G C PVC or MCE OV S-2 O VS !2

5601 6601 5800

ORG ANONITROGEN PESTICIDES OXYG EN POLY AROM ATIC COMPO UNDS, TOTAL (PACs) EL EM EN TS b y IC P (H ot B loc k/H C l/ H N O 3 Digestion) PARAQUAT ORG ANOPHO SPHORUS PESTICIDES PARTICU LATES N.O.R ., TO T AL PARTICU LATES, N.O .R, RESPIRAB LE

0.1 - 1 NA 1-2

var - 480 1 - NA 5 - 1000

reagent NA hexane

HP LC , U V Sens or FI-FL

OV S-2 po rta ble PTFE + X AD -2

Palladium

7303

1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

Par aquat Par athio n Par tic ulate s N . O. R. Par tic ulate s N . O. R.

5003 5600 0500 0600

1-4 0.2 - 1.0 1-2 1.7, 2.2, 2.5 0.01 - 0.2 0.01 - 0.2 0.5 - 1.0 1-2 0.01 - 0.05

40 - 1000 12 - 240 7 - 133 20 - 400

H 2O t ol/a cet NA NA

HPLC !U V G C !FPD G R AV Grav.

PTFE O VS !2 P VC C Y C & P VC

Pentachlorobenzene Pentachloroethane Pe ntac hlo r o phe no l Pentamidine n !Pentane

5517 2517 5512 5032 2549

POLYCHLORO BENZENES P E N TA C H L O R O E TH A N E P EN TA C HL OR O PH EN O L PEN TAM IDINE ISETH ION ATE V O L A TI LE O R G A N IC C P D S (Screen in g) HYDROC ARBONS, BP 36 !216 C KETONES I KETONES I PE RC HL O RO ETH YL EN E (p or t G C ) in exha led bre ath a nd a ir V O L A TI LE O R G A N IC C P D S (Screen in g) ORG ANOPHO SPHORUS PESTICIDES ORG ANONITROGEN PESTICIDES NAPHTHAS PO LYN UC LEA R A RO M ATIC HYDR OC ARBO NS by H PLC PO LYN UC LEA R A RO M ATIC HYDROC ARBONS V O L A TI LE O R G A N IC C P D S (Screen in g)

3 - 12 1 - 10 48 - 480 50 - 1500 1-6

hexane hexane MeOH rea ge nts t h erma l

G C !E C D G C !E C D HPLC !U V HPLC/FL TD /G C !M S

P T F E & X A D !2 Por R MCEF & BuB P VC / o p a q u e TD

n !Pentane 2 !Pentanone 2-Pentanone Perchloroethylene

1500 1300 2555 3704

0.01 - 0.2 0.01 - 2.0 0.01 - 0.2 0.02 - 5

4-4 1 - 10 1 - 10 < 80% ca p

C S2 C S2 C S2 NA

G C !FID G C !FID G C -FID G C (po rt)-PID

CCT CCT A -C M S air bag

Perchloroethylene

2549

0.01 - 0.05

1-6

t h erma l

TD /G C !M S

TD

Pe stic ide s Pe stic ide s Pe tro leum e the r/naphtha Phenanthrene

5600 5601 1550 5506

0.2 - 1 0.1 - 1 0.01 - 0.2 2.0

12 - 240 var - 480 1.3 - 20 200 - 1000

t ol/a cet reagent C S2 ac eto nitr ile

G C !FPD HP LC - U V G C !FID HPLC !FL/U V

O VS !2 OV S-2 CCT P T F E & X A D !2

Phenanthrene

5515

2.0

200 - 1000

va r ies

G C -FID

P T F E & X A D !2

Phe no l

2549

0.01 - 0.05

1-6

t h erma l

TD /G C !M S

TD

3/15/2003

MF!18

NIOSH Manual of Analytical Methods

Chemical Phe no l Phe nyl e the r Phe nyl e the r!diphenyl mixture Phe nyl glyc idyl ethe r Phenylhydrazine Pho rate Phosdrin (mevinphos) Phosphine Ph os ph or ic a cid Pho spho rus Pho spho rus Pho spho rus

M eth No. 2546 1617 2013

M e th od Na m e C R ES O LS an d P HE NO L PHENYL ETHER PHENYL ETHER !DIPHENYL MIXT U R E

Flow Ra te ( L /m i n ) 0.01 - 0.1 0.01 - 0.2 0.01 - 0.2

Vol. (L) min max 1 - 24 1 - 50 1 - 40

E x tr a c ti o n

A n a ly t ic a l T e c h n iq u e G C !FID G C !FID G C !FID

Sampler X A D !7 CCT SG

MeOH C S2 bz

1619 3518 5600 5600 6002 7903 7300 7905 7301

PHENYL GLYCIDYL ETHER P H E N YL H Y DR A Z IN E ORG ANOPHO SPHORUS PESTICIDES ORG ANOPHO SPHORUS PESTICIDES P H O S P H IN E AC IDS , INO RG AN IC E LE M E NT S b y IC P PHOSPHOR U S EL EM EN TS b y IC P (A qu a R eg ia Ashin g) EL EM EN TS b y IC P (H ot B loc k/H C l/ H N O 3 Digestion) ELEMENTS on WIPES P H O S P H O R U S T R IC H L O R ID E TERPENES V O L A TI LE O R G A N IC C P D S (Screen in g) E LE M E NT S b y IC P PO LYN UC LEA R A RO M ATIC HYDROC ARBONS SUPER ABSORBENT POLYMER PO LYC YC LIC AR O M ATIC COM POU NDS, TOTAL EL EM EN TS b y IC P (H ot B loc k/H C l/ H N O 3 Digestion) POLY CH LORO BIPHENY LS

0.01 - 1 0.2 - 1.0 0.2 - 1 0.2 - 1 0.01 - 0.2 0.2 - 0.5 1-4 0.01 - 0.2 1-4

80 - 150 25 - 120 12 - 240 12 - 480 1 - 16 3 - 100 50 - 2000 5 - 100 25 - 2000

C S2 PMA t ol/a cet t ol/a cet reagent H C O 3 /C O 3


2-

G C !FID VIS G C !FPD G C !FPD VIS IC IC P !AES G C !FPD ICP-AES

CCT B u B/H C l O VS !2 O VS !2 S G / H g( C N )2 S G ( w a s h ed ) MC EF Te na x G C MC EF

H N O 3/HC lO 4 xylene H C l /H N O 3

Pho spho rus

7303

1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

Pho spho rus Pho spho rus tr ic hlor ide Pinene Pinene

9102 6402 1552 2549

NA 0.05 - 0.2 0.01 - 0.2 0.01 - 0.05

NA 11 - 100 2 - 30 1-6

NA rea ge nts C S2 t h erma l

ICP-AES VIS G C !FID TD /G C !M S

Wipe BuB /H 2O CCT TD

Pla tinum PA H

7300 5506

1-4 2.0

13 - 2000 200 - 1000

H N O 3/HC lO 4 va r ies

IC P !AES HPLC !FL/U V

MC EF P T F E & X A D !2

Poly ac rylate PACs

5035 5800

1-2 1-2

50 - 1500 5 - 1000

C u (Ac)2 hexane

IC P or AAS FI-FL

P VC

Platinum

7303

1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

Po lyc hlo ro bip he ny l (42 % & 5 4% C l) Po tassium

5503

0.05 - 0.2

1 - 50

hexane

G C !E C D

G FF & F lor isil

7301

EL EM EN TS b y IC P (A qu a R eg ia Ashin g) EL EM EN TS b y IC P (H ot B loc k/H C l/ H N O 3 Digestion) ALKA LINE DU STS E S TR O G E N I C C O M P O U N D S TR IAZ INE HE RB IC IDE S a nd the ir METABOLITES ORG ANONITROGEN PESTICIDES A L D EH Y D E S, SC R E E N IN G ALIPHATIC ALDEHYDES ORG ANONITROGEN PESTICIDES ESTERS I ALC O HO LS II ALCOHO LS COM BINED P R O P Y LE N E D IC H L O R ID E

1-4

5 - 1000

H C l /H N O 3

ICP-AES

MC EF

Po tassium

7303

1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

Po tassium hydr o xide Progesterone Propazine

7401 5044 8315

1-4 1 NA

70 - 1000 150 - 1000 NA

HCl M eth NA

t it ra t ion HP LC - U V GC-M SD

PTFE PTFE Urine

Pr o pham Pr o pio nalde hyde Pr o pio nalde hyde Pr o po xur n !Prop yl ac etate n !Pr o pyl alc o ho l n- Pro pyl alco ho l Pr o pyle ne dic hlor ide

5601 2539 2018 5601 1450 1401 1405 1013

0.1 - 1 0.01 - 0.05 0.1 - 1.5 0.1 - 1 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2

var - 480 5-5 1 - 15 var - 480 1 - 10 1 - 10 1 - 10 0.1 - 3.5

reagent t ol ACN reagent C S2 IP A /C S 2 IP A -C S 2 a cet /cy ch ex

HP LC , U V G C !F ID /M S HP LC - U V HP LC , U V G C !FID G C !FID G C -FID G C !E C N

OV S-2 X A D !2 /H M P SG-DNPH OV S-2 CCT CCT CCT PCT

3/15/2003

MF!19

NIOSH Manual of Analytical Methods

Chemical Pro pyle ne glyc o l Pr o pyle ne glyc o l m o no m e thyl e the r Pr o pyle ne glyc o l mo nom ethy l ethe r ac etate Pr o pyle ne o xide Pyrene

M eth No. 5523 2554 GLYC OLS

M e th od Na m e

Flow Ra te ( L /m i n ) 0.5 - 2 0.1 - 0.2

Vol. (L) min max 5 - 60 3 - 25

E x tr a c ti o n

A n a ly t ic a l T e c h n iq u e G C !FID G C -FID

Sampler O VS !7 A-747

MeOH M e C l2/Me th

GLYCOL ETHER S

2554

GLYCOL ETHERS

0.1 - 0.2

3 - 25

M e C l2/Me th

G C -FID

A-747

1612 5506

P R O P Y LE N E O X ID E PO LYN UC LEA R A RO M ATIC HYDR OC ARBO NS by H PLC PO LYN UC LEA R A RO M ATIC HYDROCARBONS PYRETHUM P Y R ID I NE R ES O RC IN O L RIB AV IRIN ORG ANOPHO SPHORUS PESTICIDES ROTENONE NAPHTHAS E LE M E NT S b y IC P EL EM EN TS b y IC P (A qu a R eg ia Ashin g) EL EM EN TS b y IC P (H ot B loc k/H C l/ H N O 3 Digestion) ELEMENTS on WIPES SILICA, AMOR PHOUS

0.01 - 0.2 2.0

0.5 - 5 200 - 1000

C S2 ac eto nitr ile

G C !FID HPLC !FL/U V

CCT P T F E & X A D !2

Pyrene

5515

2.0

200 - 1000

va r ies

G C !FID

P T F E & X A D !2

Pyr e thr um Pyridine R eso rc ino l Rib av irin R onne l Rotenone Rubber solvent S e le nium S e le nium

5008 1613 5701 5027 5600 5007 1550 7300 7301

1-4 0.01 - 1.0 0.2 - 1 1-4 0.2 - 1 1-4 0.01 - 0.2 1-4 1-4

20 - 400 18 - 150 5 - 160 5 - 1000 12 - 60 8 - 400 1.3 - 20 5 - 2000 13 - 2000

C H 3C N C H 2C l2 MeOH H 2SO 4 t ol/a cet C H 3C N C S2 H N O 3/HC lO 4 H C l /H N O 3

HPLC !U V G C !FID G C -FID HPLC !U V G C !FPD HPLC !U V G C !FID IC P !AES ICP-AES

GFF CCT OV S-7 GFF O VS !2 PTFE CCT MC EF MC EF

S e le nium

7303

1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

S e le nium S ilic a, amo rpho us

9102 7501

NA 1.7 or 2 .2

NA 50 - 400

NA ash

ICP-AES XR D

Wipe PVC (total) PVC&C YC C Y C & P VC

Silica, crystalline

7500

SILICA, CRYSTALLINE, by XR D

1.7, 2.2, 2.5 1.7, 2.2, 2.5 1.7, 2.2, 2.5 1.7, 2.2, 2.5 1.7, 2.2, 2.5 1-4 1-4

400 - 1000

a s h or T HF

XR D

Silica, crystalline

7601

S IL IC A , C R Y ST A LL IN E

400 - 800

H 3PO 4/HF

VIS

CYC & MC E or P VC CY C & M C E o r P VC C Y C & P VC

Silica, crystalline

7602

SILICA, CRYSTALLINE (IR )

400 - 800

ash

IR

S ilic o n dio xide

7500

S IL IC A , C R Y ST A LL IN E , b y X R D.

400 - 1000

a s h or T HF

XR D

Silica in coal mine dust

7603

QUA RTZ in coal mine dust

300 - 1000

ash

IR

C Y C & P VC

S ilve r S ilve r

7300 7301

E LE M E NT S b y IC P EL EM EN TS b y IC P (A qu a R eg ia Ashin g) ELEMENTS on WIPES CHLORINATED ORG ANONITROGEN H ER BIC ID ES (A IR SA M PL IN G ) CHLORINATED ORG ANONITROGEN HER BICIDES (HAND WAS H) CHLORINATED ORG ANONITROGEN HE RBIC IDES (DER M AL P ATC H)) EL EM EN TS b y IC P (H ot B loc k/H C l/ H N O 3 Digestion) FLUORIDES, aerosol & ga s

250 - 2000 250 - 2000

H N O 3+ H C l /H N O 3

IC P !AES ICP-AES

MC EF MC EF

S ilve r Simazine

9102 5602

NA 0.2 - 1

NA 12 - 480

NA reagent

ICP-AES G C /E C D

Wipe OV S-2

Simazine

9200

NA

NA

NA

G C - EC D

polyethylene bag PUF pad

Simazine

9201

NA

NA

IPA/diazomethane

G C - EC D

S o dium

7303

1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

S o dium hexa fluoro !alum inate

7902

1-2

12 - 800

N a OH

ISE

MCEF& pad w / N a2C O 3

3/15/2003

MF!20

NIOSH Manual of Analytical Methods

Chemical S odium hexa fluoro !alum inate S o dium hydr o xide Stibine Stoddard solvent S t ro ntium

M eth No. 7906

M e th od Na m e FLU O RID ES by IC

Flow Ra te ( L /m i n ) 1-2

Vol. (L) min max 120 - 800

E x tr a c ti o n

A n a ly t ic a l T e c h n iq u e IC

Sampler MCEF& pad w / N a2C O 3 PTFE S G w /H g C l2 CCT MC EF

N a OH

7401 6008 1550 7301

ALKA LINE DU STS S T IB IN E NAPHTHAS EL EM EN TS b y IC P (A qu a R eg ia Ashin g) EL EM EN TS b y IC P (H ot B loc k/H C l/ H N O 3 Digestion) ELEMENTS on WIPES S T RY C H N IN E HY DR O C AR BO NS , AR O M ATIC ORG ANIC and INORGANIC G ASES by EX TR ACTIV E FTIR SPE C T R O MET R Y S U LF U R D IO X I D E

1-4 0.01 - 0.2 0.01 - 0.2 1-4

70 - 1000 4 - 50 1.3 - 20 10 - 1000

HCl HCl C S2 H C l /H N O 3

T it ra t ion VIS G C !FID ICP-AES

S t ro ntium

7303

1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

S t ro ntium Strychnine Styrene Styrene

9102 5016 1501 3800

NA 1-3 0.01 - 1.0 0.1 - 20

NA 70 - 1000 1 - 14 Inst r. D ep .

NA rea ge nts C S2 NA

ICP-AES HPLC !U V G C !FID FTIR

Wipe GFF CCT Di r. R e a d

S ulfur dioxide

6004

0.5 - 1.5

4 - 200

H C O 3-/C O 32-

IC

MCEF& pad w / N a2C O 3 air bag SG(washed) CC T ( lg ) O VS !2 P VC Urine

S ulfur he xafluo ride Su lfur ic a cid S ulfuryl fluo r ide S ulpr o fo s S upe r abso rbe nt po lymer Simazine

6602 7903 6012 5600 5035 8315

S U LF U R H EX A F LU O R ID E AC IDS , INO RG AN IC S U LF U R Y L F L UO R I D E ORG ANOPHO SPHORUS PESTICIDES SUPER ABSORBENT POLYMER TR IAZ INE HE RB IC IDE S a nd the ir METABOLITES 2,4 !D an d 2,4,5 !T MYCO BACTERIUM TUBERCULOSIS, A IR B O R N E E LE M E NT S b y IC P EL EM EN TS b y IC P (A qu a R eg ia Ashin g) EL EM EN TS b y IC P (H ot B loc k/H C l/ H N O 3 Digestion) ELEMENTS on WIPES ORG ANOPHO SPHORUS PESTICIDES TERPENES o !TERPHENYL 1,1,2,2 !T E TR A B R O M O E T H AN E

0.01 - 0.05 0.2 - 0.5 0.05 - 0.1 0.2 - 1 1-3 NA

80% vol 3 - 100 1.3 - 10 12 - 240 50 - 1500 NA

NA H C O 3 /C O 3 N a OH t ol/a cet C u (Ac)2 NA


2-

G C !E C D IC IC G C !FPD IC P or AAS GC-M SD

2,4,5 !T TB

5001 0900

1-3

15 - 200 va r ies

MeOH reagent

HPLC !U V PCR

GFF PTFE

$4
1-4 1-4

T ellurium T ellurium

7300 7301

25 - 2000 25 - 2000

HNO3 H C l /H N O 3

IC P !AES ICP-AES

MC EF MC EF

T ellurium

7303

1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

T ellurium T erbufo s T erpe ne s o !Terphenyl 1,1,2,2 !Te tra bro m o ethane Te tra bu tylt in 1,2,4,5 !Tetrachlorobenzene 1,1,2,2 !Tetrach loro ! 2,2-difluoroethane

9102 5600 1552 5021 2003

NA 0.2 - 1 0.01 - 2 1-3 0.2 - 1.0

NA 12 - 240 2 - 30 2 - 30 50 - 100

NA t ol/a cet C S2 C S2 T HF

ICP-AES G C !FID G C !FID G C !FID G C !FID

Wipe O VS !2 CCT PTFE SG

5504 5517 1016

O R G A N O T IN C O M P O U N D S POLYCHLORO BENZENES 1,1,2,2 !TETRACHLORO !2,2 ! DIFLUOROETHANE & 1,1,2,2 !TETR ACHLOR O !1,2 ! D I FL U O R O E TH A N E 1,1,2,2 !TETRACHLORO !2,2 ! DIFLUOROETHANE & 1,1,2,2 !TETR ACHLOR O !1,2 ! D I FL U O R O E TH A N E 1,1,2,2 !T E TR A C H L O R O E TH A N E 1 , 1, 2 ,2 - TE T RA C H L O R O E TH A N E

1 - 1.5 0.01 - 0.2 0.01 -0.035

50 - 500 3 - 12 0.5 - 2

aaa hexane C S2

HP LC /G FAAS G C !E C D G C !FID

G F F & X A D !2 P T F E & X A D !2 CCT

1,1,1,2 !Tetrach loro !1,2 -d iflu oroethane

1016

0.01 -0.035

0.5 - 2

C S2

G C !FID

CCT

1,1,2,2 !Tetrachloroethane 1,1,2,2-Tetrachloroethane

1019 2562

0.01 - 0.2 0.01 - 0.2

3 - 30 3 - 30

C S2 C S2

G C !FID G C -FID

PCT A -C M S

3/15/2003

MF!21

NIOSH Manual of Analytical Methods

Chemical Tetrachloroethylene Tetrachloroethylene

M eth No. 1003 3704

M e th od Na m e HYDROC ARBONS, HALOG ENATED PE RC HL O RO ETH YL EN E (p or t G C ) in exha led bre ath a nd a ir GLYC OLS TETR AETHYL LEAD (as Pb ) TETRA ETHY L PYRO PHO SPH ATE ORG ANIC and INORGANIC G ASES by EX TR ACTIV E FTIR SPE C T R O MET R Y TETR AHYDR OFU R AN ORG ANIC and INORGANIC G ASES by EX TR ACTIV E FTIR SPE C T R O MET R Y TETRKIS(HYDR OX YM ETHYL) P H O S P H O N IU M C H L O R ID E TETRAMETHYL LEAD (as P b ) TETRAMETHYL THIOUREA T E TR A N IT R O M E TH A N E E LE M E NT S b y IC P EL EM EN TS b y IC P (A qu a R eg ia Ashin g) EL EM EN TS b y IC P (H ot B loc k/H C l/ H N O 3 Digestion) ORG ANONITROGEN PESTICIDES CAPTAN and THIOPHENATE-METHYL o n D E RM A L P A TC H CAPTAN and THIOPHENATE-METHYL in Hand Rinse THIO PH EN ATE -M ETH YL in AIR THIRAM EL EM EN TS b y IC P (A qu a R eg ia Ashin g) EL EM EN TS b y IC P (H ot B loc k/H C l/ H N O 3 Digestion) ORG ANOTIN CPDS. (as Sn) E LE M E NT S b y IC P EL EM EN TS b y IC P (A qu a R eg ia Ashin g) EL EM EN TS b y IC P (H ot B loc k/H C l/ H N O 3 Digestion) V O L A TI LE O R G A N IC C P D S (Screen in g) TOLU ENE (Diffusive sam pler) HYDROC ARBONS, BP 36 !216 C HY DR O C AR BO NS , AR O M ATIC ORG ANIC and INORGANIC G ASES by EX TR ACTIV E FTIR SPE C T R O MET R Y 2,4 ! & 2,6 !T O L UE N E D IA M I N E T O L UE N E !2,4 !DIISO CY ANA TE ISO C YA NA TES , M O NO M ER IC

Flow Ra te ( L /m i n ) 0.01 - 0.2 0.1 - 1

Vol. (L) min max 1 - 40 < 80% ca p

E x tr a c ti o n

A n a ly t ic a l T e c h n iq u e G C -FID Po rt G C -PID

Sampler CCT air bag

C S2 NA

T etr ae thyle ne glyc o l T etr ae thyl lead Tetra ethy l pyro ph osp ha te Tetrafluoroethylene

5523 2533 2504 3800

0.5 - 2 0.01 - 1.0 0.01 - 0.2 0.1 - 20

5 - 60 30 - 200 20 - 48 Inst r. d ep .

MeOH pentane toluene NA

G C !FID G C !PID G C !FPD FTIR

O VS !7 X A D !2 2 Chrom 102 Di r. R e a d

T etr ahydro furan T etr ahydro furan

1609 3800

0.01 - 0.2 0.1 - 20

1-9 Inst r. d ep .

C S2 NA

G C !FID FTIR

CCT Di r. R e a d

Te tra kis (hy dr ox ym eth yl) p ho spho nium c hlo ride T etr am e thyl lead T etr am e thyl thio ur e a Tetranitromethane T hallium T hallium

5046

1 - 1.7

1 - 400

ACN

HP LC - U V

GFF

2534 3505 3513 7300 7310

0.01 - 0.2 0.2 - 1.0 0.5 - 1.0 1-4 1-4

15 - 100 50 - 250 20 - 250 25 - 2000 25 - 2000

pentane rea ge nts

G C !PID VIS G C !FID IC P !AES ICP-AES

X A D !2 IMP /H 2O I M P /E t A c MC EF MC EF

!
H N O 3/HC lO 4 H C l /H N O 3

T hallium

7303

1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

Thiobe nca rb Thiophenate-methyl

5601 9205

0.1 - 1 NA

var - 480 NA

reagent IP A /A C N

HP LC , U V HP LC - U V

OV S-2 Patch

Thiophenate-methyl

9202

NA

NA

NA

HP LC - U V

Hand wa sh

Thiophenate-methyl T hir am Tin

5606 5005 7301

0.1 - 1.0 1-4 1-4

20 - 480 10 - 400 5 - 1000

IP A /A C N C H 3C N H C l /H N O 3

HP LC - U V HPLC !U V ICP-AES

QFF/SST PTFE MC EF

Tin

7303

1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

Tin, organic compds as Sn T itanium T itanium

5504 7300 7301

1 - 1.5 1-4 1-4

50 - 500 5 - 100 5 - 100

a c etic a /C H 3C N H N O 3/HC lO 4 H C l /H N O 3

HP LC /G FAAS IC P !AES ICP-AES

G F F & X A D !2 MC EF MC EF

T itanium

7303

1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

Toluene

2549

0.01 - 0.05

1-6

t h erma l

TD /G C !M S

TD

Toluene Toluene Toluene Toluene

4000 1500 1501 3800

NA 0.01 - 0.2 0.01 - 0.2 0.1 - 20

15 min-8h 2-8 1-8 Inst r. d ep .

C S2 C S2 C S2 NA

G C !FID G C !FID G C !FID FTIR

Diffusive CCT CCT Di r. R e a d

2,4 & 2,6 !Toluenediamine Toluene !2,4 !diisoc ya nate Toluene !2,4 !diisoc ya nate

5516 2535 5521

1.0 0.2 - 1.0 1.0

30 - 500 2 - 170 5 - 500

a ce ty la te /M e O H MeOH a ce ty la te /M e O H

HPLC !U V HPLC !U V HPLC !EC HD

IM P GW coated IM P

3/15/2003

MF!22

NIOSH Manual of Analytical Methods

Chemical Toluene !2,4 !diisoc ya nate Tolue ne 2 ,4-d issoc ya nate (2,4 -TD I) Toluene !2,6 !diisoc ya nate Toluene !2,6 !diisoc ya nate Tolue ne-2 ,6-d iisocy ana te (2,6 -TD I) p -To lue ne su lfon ic a cid o !Toluidine o !Toluidine

M eth No. 5522 5525

M e th od Na m e ISOCYANATES ISOCYANATES, TOTAL (MAP)

Flow Ra te ( L /m i n ) 1-2 1-2

Vol. (L) min max 15 - 360 1 - 500

E x tr a c ti o n

A n a ly t ic a l T e c h n iq u e HPLC !FL/EC HD HP LC - U V IM P

Sampler

tryptamine/DMSO MAP

G F F, IM P

5522 5521 5525

ISOCYANATES ISO C YA NA TES , M O NO M ER IC ISOCYANATES, TOTAL (MAP)

1-2 1.0 1-2

15 - 360 5 - 500 1 - 500

tryptamine/DMSO a ce ty la te /M e O H MAP

HPLC !FL/EC HD HPLC !EC HD HP LC - U V

IM P IM P G F F, IM P

5043 2002 2017

P-TO LUE NE SU LFO NIC AC ID AM INE S, A RO M ATIC A N IL IN E , o - TO L U ID I NE , A N D N I TR O B E N Z EN E DYES ANALINE an d o-TOLUIDINE in urine ANALINE an d o-TOLUIDINE in urine HYDROC ARBONS, HALOG ENATED TRIBUTY L PHO SPH ATE O R G A N O T IN C O M P O U N D S POLYCHLORO BENZENES HYDROC ARBONS, HALOG ENATED HYDROC ARBONS, HALOG ENATED V O L A TI LE O R G A N IC C P D S (Screen in g) HYDROC ARBONS, HALOG ENATED T R IC H L O R O E TH Y L EN E TR IC H LO R O ETH YL EN E b y p ort G C ORG ANIC and INORGANIC G ASES by EX TR ACTIV E FTIR SPE C T R O MET R Y F L UO R O T R IC H L O R O M E T H A NE HYDROC ARBONS, HALOG ENATED HYDROC ARBONS, HALOG ENATED O R G A N O T IN C O M P O U N D S 1,1,2 !TRICHLOR O !1,2,2 ! T R IF L UO R O E T H A N E V O L A TI LE O R G A N IC C P D S (Screen in g) AM INO ETH AN O L C O M PO UN DS II GLYC OLS ETHYLENEDIAMINE, DIETHY LENE TRIAM INE, & T R IE T HY L EN E TE T RA M I N E T R IF L UO R O B R O M O M E T HA N E T R IM E L LI TI C A N HY D R ID E 2,4,7 !TRINITR O !FLUOREN !9 !O N E TRIOR THO CR ESYL P HO SPH ATE TRIPHE NYL P HO SPH ATE T R IP H E N YL TI N C H L O R ID E

1-3 0.02 - 1.0 0.2

10 - 1000 10 - 150 5 - 50

IPA/H 2O Et h a nol et h a nol

HP LC - U V G C !FID G C -FID

GFF SG GFF + SG

o !Toluidine o !Toluidine o-Toluidine Tribromomethane Tributy l pho sph ate T ri butyltin c hlo r ide 1,2,4 !Trichlorobenzene 1,1,2 !Trichloroethane 1,1,1 !Trichloroethane 1,1,1 !Trichloroethane

5013 8317 8313 1003 5034 5504 5517 1003 1003 2549

1-3 NA NA 0.01 - 0.2 1-3 1 - 1.5 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.05

150 - 500 NA NA 4 - 70 2 - 100 50 - 500 3 - 12 2 - 60 0.1 - 8 1-6

H 2O ALK ALK C S2 d ieth y l et h er a c etic a /C H 3C N hexane C S2 C S2 t h erma l

HPLC !U V H P LC - EC D H P LC - EC D G C !FID G C !FPD HP LC /G FAAS G C !E C D G C -FID G C -FID TD /G C -M S

PTFE NA NA CCT MC EF G F F & X A D !2 P T F E & X A D !2 CCT CCT TD

Trichloroethylene Trichloroethylene Trichloroethylene Trichloroethylene

1003 1022 3701 3800

0.01 - 0.2 0.01 - 0.2 > 0.02 0.1 - 20

0.2 - 30 1 - 30 80% vol Inst r. d ep .

C S2 C S2 NA NA

G C -FID G C -FID GC -port FTIR

CCT CCT air bag Di r. R e a d

Trichlorofluoromethane Trichloromethane 1,2,3 !Trichloropropane T ri c hcylohe xyltin hydrox ide 1,1,2 !Tric hlo r o 1,2,2 !trifluoroethane 1,1,2 !Tric hlo r o 1,2,2 !trifluoroethane Triethanolamine T ri e thyle ne glyc o l Triethylenetetramine

1006 1003 1003 5504 1020

0.01 - 0.05 0.01 - 0.2 0.01 - 0.2 1 - 1.5 0.01 - 0.05

0.3 - 7 1 - 50 0.6 - 60 50 - 500 0.1 - 3

C S2 C S2 C S2 a c etic a /C H 3C N C S2

G C -FID G C -FID G C -FID HP LC - G FAAS G C -FID

CC T ( lg ) CCT CCT GF F & X AD -2 CCT

2549

0.01 - 0.05

1-6

t h erma l

TD /G C -M S

TD

3509 5523 2540

0.5 - 1.0 0.5 - 2 0.01 - 0.1

5 - 300 5 - 60 1 - 20

HSA MeOH DMF

IC G C -FID HP LC - U V

IM P OV S-7 XA D-2 W/1 0% NITC

Trifluorobromomethane T ri m e llitic anhydride 2,4,7 !Trin it ro flu o re n !9!o n e Triortho cre syl ph osp ha te Triphe nyl p ho sph ate T ri phenyltin c hlo r ide

1017 5036 5018 5037 5038 5527

0.01 - 0.05 1.5 - 2 1-3 1-3 1-3 1-4

0.1 - 1 400 - 1000 100 - 500 2 - 100 10 - 400 100 - 2000

C H 2C l2 MeOH toluene d ieth y l et h er d ieth y l et h er TW M

G C -FID G C -FID HP LC - U V GC-FPD GC-FPD H P LC - IC P

2 C C T(lg + sm ) P VC PTFE MC EF MC EF P VC

3/15/2003

MF!23

NIOSH Manual of Analytical Methods

Chemical Tu be rc le b ac illi T ungste n

M eth No. 0900 7301

M e th od Na m e M YC O BA C TER IUM TUB ER C ULO SIS EL EM EN TS b y IC P (A qu a R eg ia Ashin g) TU NGSTEN (sol ubl e/i nso lu b le) T U RP E N TI N E V O L A TI LE O R G A N IC C P D S (Screen in g) HYDROC ARBONS, BP 36-216 oC ALIPHATIC ALDEHYDES V A L ER A L D EH Y D E A L D EH Y D E S, SC R E E N IN G E LE M E NT S b y IC P EL EM EN TS b y IC P (A qu a R eg ia Ashin g) EL EM EN TS b y IC P (H ot B loc k/H C l/ H N O 3 Digestion) ELEMENTS on WIPES VANADIUM OX IDES VINYL A CE TATE HY DR O C AR BO NS , AR O M ATIC V IN Y L B R O M I D E V IN Y L C H L O R ID E V IN Y L ID E N E C H LO R I D E ORG ANIC and INORGANIC G ASES by EX TR ACTIV E FTIR SPE C T R O MET R Y HY DR O C AR BO NS , AR O M ATIC NAPHTHAS V O L A TI LE O R G A N IC C P D S (Screen in g) W AR FA RIN M E TH A NO L V O L A TI LE O R G A N IC C P D S (Screen in g) HY DR O C AR BO NS , AR O M ATIC ORG ANIC and INORGANIC G ASES by EX TR ACTIV E FTIR SPE C T R O MET R Y ORG ANIC and INORGANIC G ASES by EX TR ACTIV E FTIR SPE C T R O MET R Y ORG ANIC and INORGANIC G ASES by EX TR ACTIV E FTIR SPE C T R O MET R Y AM INE S, A RO M ATIC E LE M E NT S b y IC P EL EM EN TS b y IC P (A qu a R eg ia Ashin g) EL EM EN TS b y IC P (H ot B loc k/H C l/ H N O 3 Digestion) ELEMENTS on WIPES

Flow Ra te ( L /m i n )

Vol. (L) min max

E x tr a c ti o n

A n a ly t ic a l T e c h n iq u e PCR ICP-AES

Sampler PTFE MC EF

$4
1-4

va r ies 50 - 1000

reagent H C l /H N O 3

Tu ng ste n, s olu ble /ins olu ble Turpentine Turpentine

7074 1551 2549

1-4 0.01 - 0.2 0.01 - 0.05

200 - 1000 1 - 10 1-6

H F /H N O 3 C S2 t h erma l

FAAS G C -FID TD /G C -M S

MC EF CCT TD

n-Undecane V a ler alde hyde V a ler alde hyde V a ler alde hyde V a nadium V a nadium

1500 2018 2536 2539 7300 7301

0.01 - 0.05 0.1 - 1.5 0.01 - 0.04 0.01 - 0.05 1-4 1-4

2-2 1 - 15 0.5 - 10 5-5 5 - 2000 5 - 2000

C S2 ACN toluene toluene H N O 3/HC lO 4 H C l /H N O 3

G C -FID HP LC - U V G C -FID G C -F ID /M S ICP-AES ICP-AES

CCT SG-DNPH X AD -2 /H M P X AD -2 /H M P MC EF MC EF

V a nadium

7303

1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

V a nadium V a nadium o xide s Viny l ace tate Vinyl benzene V i nyl br o m ide V i nyl c hlor ide V i nylide ne c hlo r ide V i nylide ne F luo r ide

9102 7504 1453 1501 1009 1007 1015 3800

NA 1.7 or 2 .2 0.1 - 0.2 .01 - 1 0.01 - 0.2 0.05 0.01 - 0.2 0.1 - 20

NA 200 - 1000 0.75 - 24 1 - 14 2 - 10 0.7 - 5 2.5 - 7 Inst r. d ep .

NA T HF C H 2C l2/M e O H C S2 Et h a nol C S2 C S2 NA

ICP-AES XR D G C -FID G C -FID G C !FID G C !FID G C !FID FTIR

Wipe C Y C & P VC MS(carbon) CCT C CT ( lg ) 2 CCT CCT Di r. R e a d

Vinyl tolueneuene V M&P naphtha VOCs

1501 1550 2549

0.01 - 0.2 0.01 - 0.2 0.01 - 0.05

1 - 24 1.3 - 20 1-6

C S2 C S2 t h erma l

G C !FID G C !FID TD /G C !M S

CCT CCT TD

W ar far in W o o d alc o ho l Xylene

5002 2000 2549

1-4 0.02 - 0.2 0.01 - 0.05

200 - 1000 1-5 1-6

MeOH H 2O/IPA t h erma l

HPLC !U V G C !FID TD /G C !M S

PTFE SG TD

X yle ne (o,m ,p ) p -Xylene

1501 3800

0.01 - 0.2 0.1 - 20

2 - 23 Inst r. d ep .

C S2 NA

G C !FID FTIR

CCT Di r. R e a d

m -Xylene

3800

0.1 - 20

Inst r. d ep .

NA

FTIR

Di r. R e a d

o-Xylene

3800

0.1 - 20

Inst r. d ep .

NA

FTIR

Di r. R e a d

2,4 !Xylidine Y ttr ium Y ttr ium

2002 7300 7301

0.02 - 0.2 1-4 1-4

3 - 20 5 - 1000 5 - 1000

Et h a nol H N O 3/HC lO 4 H C l /H N O 3

G C !FID IC P !AES ICP-AES

SG MC EF MC EF

Y ttr ium

7303

1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

Y ttr ium

9102

NA

NA

NA

ICP-AES

Wipe

3/15/2003

MF!24

NIOSH Manual of Analytical Methods

Chemical Z in c and c o m po unds Zinc Zinc

M eth No. 7030 7300 7301

M e th od Na m e ZINC and compounds, as Zn E LE M E NT S b y IC P EL EM EN TS b y IC P (A qu a R eg ia Ashin g) EL EM EN TS b y IC P (H ot B loc k/H C l/ H N O 3 Digestion) ELEMENTS on WIPES Z IN C O X I D E E LE M E NT S b y IC P EL EM EN TS b y IC P (A qu a R eg ia Ashin g) ELEMENTS on WIPES

Flow Ra te ( L /m i n ) 1-3 1-4 1-4

Vol. (L) min max 2 - 400 5 - 200 5 - 200

E x tr a c ti o n

A n a ly t ic a l T e c h n iq u e FAAS IC P !AES ICP-AES

Sampler MC EF MC EF MC EF

HNO3 H N O 3/HC lO 4 H C l /H N O 3

Zinc

7303

1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

Y ttr ium Z inc o xide Z ir c o nium Z ir c o nium

9102 7502 7300 7301

NA 1-3 1-4 1-4

NA 10 - 400 5 - 200 5 - 200

NA -H N O 3/HC lO 4 H C l /H N O 3

ICP-AES XR D IC P !AES ICP-AES

Wipe P VC MC EF MC EF

Z ir c o nium METHODS BY NUM BER

9102

NA

NA

NA

ICP-AES

Wipe

0500 0600 0800 0801 0900 1000 1001 1002 1003 1004 1005 1006 1007 1008 1009 1010 1011 1012 1013 1014 1015 1016

PARTICU LATES N.O.R . PARTICULATES, N.O.R, RESP. B IO A E R O S O L SA M P L IN G A ER O BIC B AC TE RIA - G C -F AM E MYCO BACTERIUM TUBERCULOSIS A L LY L C H LO R I D E M E T H YL C H LO R I D E

1-2 1.7, 2.2 ,2.5 28.3 28.3 4 0.01 - 1.0 0.01 - 0.1 0.01 - 0.1 0.01 - 0.2 0.01 - 1.0 0.01 - 0.2 0.01 - 0.05 0.05 0.02 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 1.0 0.01 - 0.2 0.01 -0.035

7 - 133 20 - 400 va r ies 50 - 300 va r ies 16 - 100 0.4 - 3 1.5 - 8 3 - 70 2 - 15 0.5 - 2.5 0.3 - 7 0.7 - 5 0.1 - 25 2 - 10 2 - 30 0.5 - 4 2.5 - 10 0.1 - 3.5 15 - 50 2.5 - 7 0.5 - 2

NA NA NA hex/MTBE reagent bz C H 2C l2 C S2 C S2 C S2 C S2 C S2 C S2 b z/M e O H Et h a nol C S2 IPA IPA acet/cyclohexane t ol C S2 C S2

G R AV Grav. va r ies G C -FID PCR G C !FID G C !FID G C !FID G C !FID G C !FID G C !FID G C !FID G C !FID G C !E C D G C !FID G C !FID G C !FID G C !FID G C !E C N G C !FID G C !FID G C !FID

P VC CY C & P VC i m p a c to r I m p a c to r PTFE CCT 2 C C T (lg + sm ) CCT CCT CCT 2 CCT C CT ( lg ) 2 CCT CCT C CT ( lg ) CCT CCT 2 CCT PCT CCT CCT CCT

$!C H L O R O P R E N E
HYDROC ARBONS, HALOG ENATED DICHLOROETHYL ETHER M E T H YL E N E C H L O R ID E F L UO R O T R IC H L O R O M E T H A NE V IN Y L C H L O R ID E E T HY L EN E D IB R O M I D E V IN Y L B R O M I D E EP ICH LO RO HY DR IN E T HY L BR O M I D E D I FL U O R O D IB R O M O M E T H A N E P R O P Y LE N E D IC H L O R ID E M E T H YL IO D I D E V IN Y L ID E N E C H LO R I D E 1,1,2,2 !TETRACHLORO !2,2 ! DIFLUOROETHANE & 1,1,2,2 !TETR ACHLOR O !1,2 ! D I FL U O R O E TH A N E T R IF L UO R O B R O M O M E T HA N E DICHLORODIFLUORO METHANE, 1,2 !DICHLOROTETR AFLU O R O ! ETHANE& C H L O R O D IF L UO R O M E T H A N E 1,1,2,2 !T E TR A C H L O R O E TH A N E 1,1,2 !TRICHLOR O !1,2,2 ! T R IF L UO R O E T H A N E T R IC H L O R O E TH Y L EN E

1017 1018

0.01 - 0.05 0.01 - 0.05

0.1 - 1 1-4

C H 2C l2 C H 2C l2

G C -FID G C !FID

2 C C T(lg + sm ) 2 CCT (lg + sm )

1019 1020

0.01 - 0.2 0.01 - 0.05

3 - 30 0.1 - 3

C S2 C S2

G C !FID G C -FID

PCT CCT

1022 3/15/2003

0.01 - 0.2 MF!25

1 - 30

C S2

G C -FID

CCT

NIOSH Manual of Analytical Methods

Chemical

M eth No. 1024 1025 1026 1300 1301 1302 1400 1401 1402 1403 1404 1405 1450 1451 1452 1453 1454 1457 1458 1459 1460 1500 1501 1550 1551 1552 1600 1601 1602 1603 1604 1606 1608 1609 1610 1611 1612 1613 1614 1615 1616 1617

M e th od Na m e 1,3 !B U TA D IE N E 1 - a n d 2 -B R O M O P R O P A N E P- C H LO R O B E N Z O T RI FL U O R ID E KETONES I KE TO NE S II N - M E TH Y L -2 - PY R R O L ID I NO N E ALCOHO LS I ALC O HO LS II ALC O HO LS III ALC O HO LS IV M E TH YL CY C LO H EX AN O L ALCOHO LS COM BINED ESTERS I ME THYL C ELLO SO LVE A CE TATE ETHY L FO RM ATE VINYL A CE TATE ISOP RO PYL A CE TATE ETHY L AC ETATE ME THYL A CE TATE ME THYL A CR YLATE ISOP RO PYL A CE TATE HYDROC ARBONS, BP 36 !216 C HY DR O C AR BO NS , AR O M ATIC NAPHTHAS T U RP E N TI N E TERPENES C A R B O N D IS U LF ID E 1,1 !DICHLORO !1 !N I TR O E T H AN E D I O X AN E AC ETIC AC ID AC RYLO NITRILE AC ETON ITRILE G LY C ID O L TETR AHYDR OFU R AN ETHYL ETHER METHYLAL P R O P Y LE N E O X ID E P Y R ID I NE E T HY L EN E O X ID E METH YL tert !BUTYL ETHER BUTYL GLYCIDYL ETHER PHENYL ETHER

Flow Ra te ( L /m i n ) 0.01 - 0.5 0.01 - 0.2 0.01 - 0.2 0.01 - 2.0 0.01 - 0.2 0.05 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.05 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.1 - 0.2 0.02 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.02 - 0.2 0.01 - 0.2 0.01 - 1.0 0.01 - 0.2 0.01 - 0.2 0.01 - 2 0.01 - 0.2 0.01 - 1.0 0.01 - 0.2 0.01 - 0.1 0.01 - 0.2 0.01 - 0.2 0.01 - 1.0 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 0.2 0.01 - 1.0 0.05 - 0.15 0.1 - 0.2 0.01 - 0.2 0.01 - 0.2

Vol. (L) min max 5 - 25 0.1 - 12 0.1 - 10 1 - 10 1 - 25 0.5 - 125 1 - 10 2 - 10 1 - 10 6 - 50 1 - 15 2 - 10 1 - 10 0.2 - 20 0.3 - 10 0.75 - 24 0.1 - 9 0.1 - 10 0.2 - 10 1-5 0.1 - 9 2-7 1 - 30 1.3 - 20 1 - 10 2 - 30 2 - 25 1.5 - 15 0.5 - 15 20 - 300 3.5 - 20 1 - 25 5 - 100 1-9 0.25 - 3 1-3 0.5 - 5 18 - 150 1 - 24 2 - 96 15 - 30 1 - 50

E x tr a c ti o n

A n a ly t ic a l T e c h n iq u e G C !FID G C -FID G C -FID G C !FID G C !FID GC-FID/NPD G C !FID G C !FID C G !FID G C !FID G C !FID G C -FID G C !FID G C !FID G C !FID G C -FID G C !FID G C !FID G C !FID G C !FID G C -FID G C !FID G C !FID G C !FID G C -FID G C !FID G C !FPD G C !FID G C !FID G C !FID G C !FID G C !FID G C !FID G C !FID G C !FID G C !FID G C !FID G C !FID G C !E C D G C !FID G C !FID G C !FID

Sampler CCT CCT CCT CCT CCT CCT CCT CCT CCT CCT CCT CCT CCT CCT CCT MS(carbon) CCT CCT CCT CCT CCT CCT CCT CCT CCT CCT C CT & d ry tu b e PCT CCT CCT CCT CCT CCT CCT CCT CCT CCT CCT PC T w/HB r 2 CC T ( lg ) CCT CCT

C H 2C l2 C S2 C S 2/M e O H C S2 M e O H /C S 2 C H 2C L 2/M e O H C S2 IP A /C S 2 IP A /C S 2 M e O H /C H 2C l2 C H 2C l2 IP A -C S 2 C S2 C S2 C S2 C H 2C l2/M e O H C S2 C S2 C S2 C S2 C S 2/Me th C S2 C S2 C S2 C S2 C S2 t ol C S2 C S2 formic a a c et/C S 2 C H 2C l2/M e O H T HF C S2 C S2 hexane C S2 C H 2C l2 DMF C S2 C S2 C S2

3/15/2003

MF!26

NIOSH Manual of Analytical Methods

Chemical

M eth No. 1618 1619 1620 2000 2002 2003 2004

M e th od Na m e ISOPROPYL ETHER PHENYL GLYCIDYL ETHER ISOPROPYL GLYCIDYL ETHER M E TH A NO L AM INE S, A RO M ATIC 1,1,2,2 !T E TR A B R O M O E T H AN E DIMETHYLACETAMIDE and D I M E TH Y L FO R M A M I D E N I TR O A R O M A T IC C O M P O U N D S AMINOETHANO L COM POUNDS I C HLO RO AC ETIC AC ID AM INE S, A LIPH ATIC FO RM IC A C ID

Flow Ra te ( L /m i n ) 0.01 - 0.05 0.01 - 1 0.01 - 0.2 0.02 - 0.2 0.2 - 1.0 0.2 - 1.0 0.01 - 1.0

Vol. (L) min max 0.1 - 3 80 - 150 1 - 30 1-5 30 - 150 50 - 100 15 - 80

E x tr a c ti o n

A n a ly t ic a l T e c h n iq u e G C !FID G C !FID G C !FID G C !FID G C !FID G C !FID G C !FID

Sampler CCT CCT CCT SG SG SG SG

C S2 C S2 C S2 H 2O/IPA Et h a nol T HF MeOH

2005 2007 2008 2010 2011

0.01 - 1 0.01 - 0.2 0.05 - 0.2 0.01 - 1.0 0.05 - 0.2

1 - 150 4 - 24 1 - 100 3 - 30 1 - 24

MeOH M eO H/H 2O H 2O H 2SO 4/a q M e O H H 2O

G C !FID G C !FID IC G C !FID IC

SG SG SG SG P T FE & S G ( w a s h ed ) S G + H 2SO 4 SG SG SG SG/DNPH GFF + SG w/H 2SO 4 SG-DNPH Carbon be ads X A D !2 /H M P 2 Chrom 102 Por Q P or Q S T e n a x!G C

2012 2013 2014 2015 2016 2017

n !B U TY L AM I N E PHENYL ETHER !DIPHENYL MIXT U R E p !C H L O RO P H EN O L C H L O R O A C E T AL D E HY D E F O R M A L D E HY D E A N IL IN E , o - TO L U ID I NE , A N D N I TR O B E N Z EN E ALIPHATIC ALDEHYDES M E T H YL E TH Y L K E TO N E AC RO LEIN TETRA ETHY L PYRO PHO SPH ATE F UR FU RY L A LC O H O L AC ETO NE CY AN O HY DR IN N ITR O G LY C ER IN & ETH YL EN E G LY C O L DINITRA TE I SO P H O R O N E 1 !O C TA N ETH IO L ETH YLE NE CH LO RO HY DR IN A N IS ID I NE D I AZ O M E T H A N E D I C H LO R O F L U O R O M E T HA N E P E N TA C H L O R O E TH A N E HEXACHLOR O !1,3 !CYC LO P EN T AD I EN E E T HY L C H LO R I D E M E T H YL B RO M I D E

0.01 - 1.0 0.01 - 0.2 0.05 - 0.2 0.05 - 0.2 0.03 - 1.5 0.2

2 - 100 1 - 40 1.5 - 40 3 - 16 1 - 15 5 - 50

MeOH bz C H 3C N MeOH ac eto nitr ile et h a nol

G C !FID G C !FID HPLC !U V G C !E C D HP LC - U V G C -FID

2018 2500 2501 2504 2505 2506 2507

0.1 - 1.5 0.01 - 0.2 0.01 - 0.1 0.01 - 0.2 0.01 - 0.05 0.2 0.2 - 1.0

1 - 15 0.25 - 12 1.5 - 48 20 - 48 3 - 25 0.3 - 12 3 - 100

ACN C S2 t ol toluene a cet Et Ac Et h a nol

HP LC - U V G C !FID G C !NPD G C !FPD G C !FID G C !NPD G C !E C D

2508 2510 2513 2514 2515 2516 2517 2518

0.01 - 1.0 0.01 - 0.2 0.01 - 0.2 0.5 - 1.0 0.2 0.01 - 0.05 0.01 - 0.2 0.01 - 0.2

2 - 25 1 - 15 2 - 35 24 - 320 6 - 30 0.25 - 3 1 - 10 0.25 - 90

C S2 a cet IP A /C S 2 MeOH C S2 C S2 hexane hexane

G C !FID G C !FPD G C !FID HPLC !U V G C !FID G C !FID G C !E C D G C !E C D

PCT Te na x G C PCT X A D !2 X A D !2 ( c oa t e d ) 2 CC T ( lg ) Por R 2 Por T

2519 2520

0.02 - 0.05 0.01 - 0.1

0.3 - 3 1-5

C S2 C S2

G C !FID G C !AED

2 CC T ( lg ) PC T(2)+d ry tube Por Q The rma loso rb/N Chrom104/ ma leic anh .

2521 2522 2523

M E T H YL C Y C LO H E X A N O N E NITROSAMINES 1,3 !C Y C L O P E N TA D IE N E

0.01 - 0.05 0.2 - 2.0 0.01 - 0.05

1-6 15 - 1000 1-5

a cet M e O H /C H 2C l2 Et Ac

G C !FID G C !TEA G C !FID

3/15/2003

MF!27

NIOSH Manual of Analytical Methods

Chemical

M eth No. 2524 2525 2526 2527 2528 2529 2530 2532 2533 2534 2535 2536 2537 2538 2539 2540

M e th od Na m e DIM ETHY L SULFA TE n !BU TYL MER CAPTAN N I TR O E T H AN E N I TR O M E T H A N E 2 !N I TR O P R O P A N E FU R FU R AL DIPHENYL G L U TA R A LD E H Y D E TETR AETHYL LEAD (as Pb ) TETR AMETHYL LEAD (as P b ) T O L UE N E !2,4 !DIISO CY ANA TE V A L ER A L D EH Y D E ME THYL a nd ETH YL M ETHA CR YLATE A C E T AL D E HY D E A L D EH Y D E S, SC R E E N IN G ETHY LENE DIAM INE, DIETHY LENE TRIAM INE, & T R IE T HY L EN E TE T RA M I N E F O R M A L D E HY D E M E R C A P TA N S H E X A C H LO R O B U T A D IE N E N I C O TI N E ALLYL GLYCIDYL ETHER V O L A TI LE O R G A N IC C P D S (Screen in g) B EN ZO TH IA ZO LE IN AS PH A LT F UM E N I C O TI N E ME THYL A CR YLATE KE TO NE S II GLYCOL ETHER S KETONES I

Flow Ra te ( L /m i n ) 0.01 - 0.2 0.01 - 0.05 0.01 - 0.05 0.01 - 0.05 0.01 - 0.05 0.01 - 0.05 0.01 - 0.5 0.01 - 0.08 0.01 - 1.0 0.01 - 0.2 0.2 - 1.0 0.01 - 0.04 0.01 - 0.05 0.01 - 0.05 0.01 - 0.05 0.01 - 0.1

Vol. (L) min max 0.25 - 12 1-4 1.5 - 3 1.2 - 3 0.1 - 2 1 - 12 15 - 30 4 - 39 30 - 200 15 - 100 2 - 170 0.5 - 10 1-8 1 - 12 5-5 1 - 20

E x tr a c ti o n

A n a ly t ic a l T e c h n iq u e G C !E C N G C !FPD G C !FID G C !FPD G C !FID G C !FID G C !FID HPLC !U V G C !PID G C !PID HPLC !U V G C -FID G C !FID G C !F ID G C !F ID /M S HPLC !U V

Sampler Por P Chrom 104 2 X A D !2 Chrom 106 Chrom 106 X A D !2 /H M P Te na x G C SG/DNPH X A D !2 X A D !2 GW coated X AD -2 /H M P X A D !2 X A D !2 /H M P X A D !2 X A D !2 w/10 % N ITC

d iEt eth er a cet Et Ac Et Ac Et Ac t ol C C l4 C H 3C N pentane pentane MeOH toluene C S2 t ol t ol DMF

2541 2542 2543 2544 2545 2549

0.01 - 0.1 0.1 - 0.2 0.05 - 0.2 1.0 0.01 - 0.2 0.01 - 0.05

1 - 36 10 - 150 1 - 100 60 - 400 1.5 - 8 1-6

t ol H C l/D C E hexane Et Ac d ieth y l et h er t h erma l

G C !FID G C !FPD G C !E C D G C !NPD G C !FID TD /G C !M S

X A D !2 /H M P GFF/HgAc X A D !2 X A D !2 Tenax TD

2550 2551 2552 2553 2554 2555

1.0 - 2.0 0.1 - 1.0 0.01 - 0.2 0.01 - 0.2 0.1 - 0.2 0.01 - 0.2

480 - 960 0.5 - 600 1-5 1 - 25 3 - 25 0.5 - 3.0 1 - 10 2 - 25 1 - 10 1 - 10 48 - 960 480 - 960

hexane ethy l ace tate C S2 IP A -C S 2 M e C l2/Me th C S2

G C - SC D GC-NPD G C -FID G C -FID G C -FID G C -FID

PTFE + X D-2 XA D-4 A -C M S A -C M S A-747 A -C M S

2556 2557 2558 2559 2560

I SO P H O R O N E DIACETYL AC ETO IN D E C A B R O M O D I PH E N Y L O X I D E 1-NITROPYRENE in DIESEL PARTICULATES 2 -(D IM E TH YL AM IN O )E TH A NO L 1 -D IM E TH YL AM IN O -2 -P RO P AN O L 1 , 1, 2 ,2 - TE T RA C H L O R O E TH A N E F O R M A L D E HY D E H Y D R A ZI N E TETRAMETHYL THIOUREA A C E T IC A N H Y D R ID E

0.01 - 1 0.01 - 0.2 0.01 - 0.2 2.0 1.0 - 2.0

DEE Ac et-M eth Ac et-M eth DMSO T ol

G C -FID G C -FID G C -FID HP LC /UV G C - NC D

XAD A -C M S A -C M S QFF GFF

2561

0.02 - 1

10 - 24

MeOH

G C -FID

XAD

2562 3500 3503 3505 3506

0.01 - 0.2 0.2 - 1.0 0.2 - 1.0 0.2 - 1.0 0.2 - 1.0

3 - 30 1 - 100 7 - 100 50 - 250 25 - 100

C S2 NaHSO 3 rea ge nts rea ge nts reagent

G C -FID VIS VIS VIS VIS

A -C M S P TF E & 2 IM P BuB IMP /H 2O BuB

3/15/2003

MF!28

NIOSH Manual of Analytical Methods

Chemical

M eth No. 3507 3508 3509 3510 3511 3512 3513 3514 3515 3516 3518 3600 3601 3700 3701 3702 3704

M e th od Na m e A C E T AL D E HY D E M E T H YL E TH Y L K E TO N E P E R O X ID E AM INO ETH AN O L C O M PO UN DS II M O N O M E T HY L H YD R A Z IN E M O N O M E T HY L AN I LI N E M A L E IC A N H Y D R ID E T E TR A N IT R O M E TH A N E E T HY L EN I M IN E 1,1 !D I M E TH Y L HY D R A Z IN E C R O T O N A L D EH Y D E P H E N YL H Y DR A Z IN E MANEB MANEB B EN ZE NE by po rta ble G C TR IC H LO R O ETH YL EN E b y p ort G C E TH YL EN E O X ID E b y p orta ble G C P ER C H LO R O E TH Y LE N E (p o rta b le G C ) in e xh ale d b rea th a nd air ORG ANIC and INORGANIC G ASES by EX TR ACTIV E FTIR SPE C T R O MET R Y TOLU ENE (Diffusive sam pler) C A R BO N B LA C K 2,4 !D an d 2,4,5 !T W AR FA RIN PARAQUAT H Y D R O Q U IN O N E THIRAM CARBARYL ROTENONE PYRETHUM B E N Z O Y L P E R O X ID E BRO MO XYN IL and B 'OC TANO ATE ETHYLENE THIOUREA EPN DYES CH LORINA TED TERPH ENYL S T RY C H N IN E DIBUTY L PHO SPH ATE 2,4,7 !TRINITR O !FLUOREN !9 !O N E AZ ELA IC A C ID D I BU T YL P HT H A LA T E & DI(2 !ETHY LHEX YL) PHTH ALATE o !TERPHENYL ARSENIC, organo!

Flow Ra te ( L /m i n ) 0.1 - 0.5 0.5 - 0.2 0.5 - 1.0 0.5 - 1.5 0.2 - 1.0 0.2 - 1.5 0.5 - 1.0 0.2 0.2 - 1.0 0.1 - 0.2 0.2 - 1.0 NA NA > 0.02 > 0.02 > 0.02 0.1 - 1

Vol. (L) min max 6 - 60 52 - 520 5 - 300 3 - 20 11 - 100 40 - 500 20 - 250 1 - 48 2 - 100 1 - 49 25 - 120 NA NA 80% vol 80% vol 80% vol 8 0% V O L

E x tr a c ti o n

A n a ly t ic a l T e c h n iq u e HPLC !U V VIS IC VIS G C !FID HPLC !U V G C !FID HPLC !U V VIS DPP VIS HP LC - U V HP LC - U V GC GC -port G C !PID Po rt G C -PID BuB IM P IM P

Sampler

reagent reagent HSA P M A /H C l N a OH --

B u B/H C l BuB /H 2SO 4 BuB /H 2O I M P /E t A c BuB Bu B (. 1 M HC l) BuB B u B/H C l Patch Hand wa sh air bag air bag air bag air bag

!C H C l3 reagent b u ffer PMA Cy s/EDTA NA NA NA NA NA

3800

0.1 - 20

Inst r. d ep .

NA

FTIR

Di r. R e a d

4000 5000 5001 5002 5003 5004 5005 5006 5007 5008 5009 5010 5011 5012 5013 5014 5016 5017 5018 5019 5020

NA 1-2 1-3 1-4 1-4 1-4 1-4 1-3 1-4 1-4 1-3 1-3 1-3 1-2 1-3 1-3 1-3 1-3 1-3 1-3 1-3

15 min-8h 30 - 570 15 - 200 200 - 1000 40 - 1000 30 - 180 10 - 400 20 - 400 8 - 400 20 - 400 40 - 400 2 - 400 200 - 800 15 - 700 150 - 500 100 - 1500 70 - 1000 50 - 250 100 - 500 200 - 1000 6 - 200

C S2 NA MeOH MeOH H 2O ac etic ac id C H 3C N reagent C H 3C N C H 3C N d ieth y l et h er C H 3C N H 2O isooctane H 2O isooctane rea ge nts C H 3C N toluene Et h a nol C S2

G C !FID Grav HPLC !U V HPLC !U V HPLC !U V HPLC !U V HPLC !U V VIS HPLC !U V HPLC !U V HPLC !U V HPLC !U V VIS G C !FPD HPLC !U V G C !E C D HPLC !U V G C !FPD HP LC - U V G C !FID G C !FID

Diffusive P VC GFF PTFE PTFE MC EF PTFE GFF PTFE GFF MC EF PTFE PVC or MCEF GFF PTFE GFF GFF PTFE PTFE P VC MC EF

5021 5022 3/15/2003

1-3 1-3 MF!29

2 - 30 50 - 1000

C S2 b u ffer

G C !FID IC !HYAAS

PTFE PTFE

NIOSH Manual of Analytical Methods

Chemical

M eth No. 5025 5026 5027 5029 5030 5031 5032 5033 5034 5035 5036 5037 5038 5039 5040

M e th od Na m e C H L O R IN A T ED D IP H E N YL O X ID E OIL MIST, MINER AL RIB AV IRIN 4,4'!M E T H YL E N ED I AN I LI N E C YA NU RIC AC ID A SP AR TA M E PEN TAM IDINE ISETH ION ATE p !N I TR O A N IL IN E TRIBUTY L PHO SPH ATE SUPER ABSORBENT POLYMER T R IM E L LI TI C A N HY D R ID E TRIOR THO CR ESYL P HO SPH ATE TRIPHE NYL P HO SPH ATE C H L O R IN A T ED C A M P H E N E ELEMENTAL CARBON (DIESEL PARTICULATE) C AP SA ICIN an d D IHY DR O C AP SA ICIN B E N Z EN E S O LU B LE F R AC T IO N A N D TOTAL PARTICULATE (ASPHALT FUME) p -TO LUE NE SU LFO NIC AC ID E S TR O G E N I C C O M P O U N D S TETRAKIS (HYD RO XYM ETHYL) P H O S P H O N IU M C H L O R ID E A L D R IN & L IN D A N E POLY CH LORO BIPHENY LS O R G A N O T IN C O M P O U N D S PO LYN UC LEA R A RO M ATIC HYDROC ARBONS KEPONE BENZIDINE and 3,3'!DICHLORO !B E N Z ID I NE CHLORDANE

Flow Ra te ( L /m i n ) 0.5 - 1.5 1-3 1-4 1-2 1-3 1-3 1-2 1-3 1-3 1-3 1.5 - 2 1-3 1-3 0.2 - 1 2-4

Vol. (L) min max 8 - 200 20 - 500 5 - 1000 10 - 1000 10 - 1000 70 - 1200 50 - 1500 20 2 - 100 50 - 1500 400 - 1000 2 - 100 10 - 400 2 - 30 142 -19000

E x tr a c ti o n

A n a ly t ic a l T e c h n iq u e G C !E C N IR HPLC !U V HPLC !U V HPLC !U V HPLC !U V HPLC/FL HPLC !U V G C !FPD IC P or AAS G C -FID GC-FPD GC-FPD G C !E C D E G A/TO A

Sampler MC EF PVC or MCE GFF GF F/H 2SO 4 P VC PTFE P VC / o p a q u e MC EF MC EF P VC P VC MC EF MC EF MC EF QFF

isooctane C C l4 H 2SO 4 K O H/M e O H rea ge nts eluent rea ge nts IPA d ieth y l et h er C u (Ac)2 MeOH d ieth y l et h er d ieth y l et h er p et eth er t h erma l

5041 5042

1-3 1 -4

5 - 1000 28 - 400

C H 3C N benzene

HPLC !FL Grav

GFF tared PTFE

5043 5044 5046

1-3 1 1 - 1.7

10 - 1000 150 - 1000 1 - 400

1PA /H 20 M eth ACN

HP LC - U V HP LC - U V HP LC - U V

GFF PTFE GFF

5502 5503 5504 5506

0.2 - 1.0 0.05 - 0.2 1 - 1.5 2.0

18 - 240 1 - 50 50 - 500 200 - 1000

isooct hexane a c etic a /C H 3C N ac eto nitr ile

G C !E C N G C !E C D HP LC - G FAAS HPLC !FL/U V

GFF & BuB G FF & F lor isil GF F & X AD -2 P T F E & X A D !2

5508 5509

0.5 - 1.0 0.2

50 - 600 20 - 100

b z/M e O H triethyl amine /M e O H t ol

G C !E C D HPLC !U V

M C E F & IM P GFF

5510

0.5 - 1.0

10 - 200

G C !E C D

M C E F & Ch ro m 102 MCEF & BuB M C E F & X A D !2 P T F E & X A D !2

5512 5514 5515

P EN TA C HL OR O PH EN O L D EM E TO N PO LYN UC LEA R A RO M ATIC HYDROC ARBONS 2,4 ! & 2,6 !T O L UE N E D IA M I N E POLYCHLORO BENZENES NAPHTHYLAMINES EN DR IN

0.5 - 1.0 0.2 - 1.0 2.0

48 - 480 30 - 500 200 - 1000

MeOH t ol va r ies

HPLC !U V G C !FPD G C !FID

5516 5517 5518 5519

1.0 0.01 - 0.2 0.2 - 0.8 0.5 - 1.0

30 - 500 3 - 12 30 - 100 12 - 400

a ce ty la te /M e O H hexane acetic a /IPA t ol

HPLC !U V G C !E C D G C !FID G C !E C D

IM P P T F E & X A D !2 GFF & SG M C E F & Ch ro m 102 IM P IM P O VS !7

5521 5522 5523

ISO C YA NA TES , M O NO M ER IC ISOCYANATES GLYC OLS

1.0 1-2 0.5 - 2

5 - 500 15 - 360 5 - 60

rea ge nts tryptamine/DMSO MeOH

HPLC !EC HD HPLC !FL/EC HD G C !FID

3/15/2003

MF!30

NIOSH Manual of Analytical Methods

Chemical

M eth No. 5524

M e th od Na m e META LWO RKING FLUIDS (MW F) ALL CATEGO RIES ISOCYANATES, TOTAL (MAP) METHYLTIN CHLORIDES T R IP H E N YL TI N C H L O R ID E ORG ANOPHO SPHORUS PESTICIDES ORG ANONITROGEN PESTICIDES CHLORINATED ORG ANONITROGEN H ER BIC ID ES (A IR SA M PL IN G ) ALA C HLO R in AIR THIO PH EN ATE -M ETH YL in AIR FORM ALDEHYDE on dust R ES O RC IN O L P O L Y AR O M A T IC C O M P O U N D S (PACs) A R S IN E P H O S P H IN E S U LF U R D IO X I D E

Flow Ra te ( L /m i n ) 1.6 - 2.0

Vol. (L) min max 1000 - ND

E x tr a c ti o n

A n a ly t ic a l T e c h n iq u e Grav

Sampler PTFE/CYC

D C M/MeO H/T ol MeOH MAP AAA TW M t ol/a cet reagent reagent

5525 5526 5527 5600 5601 5602

1-2 0.25 - 1 1-4 0.2 - 1 0.1 - 1 0.2 - 1

1 - 500 15 - 75 100 - 2000 12 - 240 var - 480 12 - 480

HP LC - U V GC-FPD H P LC - IC P G C !FPD HP LC - U V G C /E C D

G F F, IM P O VS P VC O VS !2 OV S-2 OV S-2

5603 5606 5700 5701 5800

1 0.1 - 1.0 2 0.2 - 1 1-2

70 - 1750 20 - 480 240 - 1050 5 - 160 5 - 1000

MeOH IP A /A C N H 2O /D N PH /C H 3C N MeOH hexane

ELISA HP LC - U V HPLC !U V G C -FID FI-FL

SPE disk QFF/SST I O M / P VC OV S-7 PTFE + XA D-2 CCT S G / H g( C N )2 M CE F & p a d w / N a2C O 3 C C T w /alk ali P TF E & C C T w / o xi d iz e r C C T (lo w N i) S G w /H g C l2 Ho pc alite s od a lim e Ag F C CT ( lg ) P T FE & C CT ( lg ) M S w / T EA & o x id i ze r S G + H 2SO 4 S G + H 2SO 4 SL BuB /H 2O air bag po rta ble air bag air bag Port In str Diffusive MC EF MC EF MC EF

6001 6002 6004

0.01 - 0.2 0.01 - 0.2 0.5 - 1.5

0.1 - 10 1 - 16 4 - 200

HNO3 reagent H C O 3 /C O 3
2-

G FAAS VIS IC

6005 6006

I O D IN E D I BO R A N E

0.5 - 1.0 0.5 - 1.0

15 - 225 60 - 260

N a 2C O 3 H 2O 2

IC PES

6007 6008 6009 6010 6011 6012 6013

NICKEL CARBONYL S T IB IN E MER CURY H Y D R O G E N C Y A N ID E C H L O R IN E a n d B R O M I N E S U LF U R Y L F L UO R I D E H Y D R O G E N S UL F ID E (withdrawn) N I TR IC O X I D E & N IT R O G E N D IO X I D E

0.05 - 0.2 0.01 - 0.2 0.15 - 0.25 0.05 - 0.2 0.3 - 1.0 0.05 - 0.1 0.1 - 1.5

7 - 80 4 - 50 2 - 100 2 - 90 2 - 90 1.3 - 10 1.2 - 40

HNO3 HCl H N O 3/H C l H 2O N a 2S 2O 3 N a OH N H 4OH /H 2O 2

G FAAS VIS AAS !cold va p VIS IC IC IC

6014

0.025

1.5 - 6

reagent

VIS

6015 6016 6017 6402 6600 6601 6602 6603 6604 6700 7013 7020 7024

AM M O NIA by VIS AM M O NIA by IC H Y D R O G E N C Y A N ID E P H O S P H O R U S T R IC H L O R ID E N I TR O U S O X ID E OXYG EN S U LF U R H EX A F LU O R ID E C A R B O N D IO X I D E CARBON MONOXIDE NITR OGEN DIOX IDE (Di ffu sive) ALUMINUM & CPDS, as Al C A LC IU M a nd c pd s a s C a C H R O M IU M a nd c pd s, as C r

0.1 - 0.2 0.1 - 0.5 0.05 - 2 0.05 - 0.2 NA NA 0.01 - 0.05 0.02 - 0.1 NA NA 1-3 1-3 1-3

0.1 - 90 0.1 - 96 2 - 90 11 - 100 80% vol 1 - NA 80% vol 80% vol NA NA 10 - 400 20 - 400 10 - 1000

H 2O H 2O H 2O rea ge nts NA NA NA NA NA reagent HNO3 H N O 3/HC lO 4 H C l /H N O 3

VIS !Au to IC IC -D C Am p VIS IR Sens or G C !E C D G C !T C D Sens or VIS FAAS FAAS FAAS

3/15/2003

MF!31

NIOSH Manual of Analytical Methods

Chemical

M eth No. 7027 7029 7030 7048 7056 7074 7082 7102 7105 7300 7301

M e th od Na m e C O B A LT an d c p ds , a s C o CO PPER (dust & fumes) ZINC and compounds, as Zn C A D M IU M a nd c pd s, as C d B A R IU M , S O LU B LE C O M P O U N D S TU NGSTEN (sol ubl e/i nso lu b le) LEAD by FAAS BERYLLIUM and cpds, as Be LEAD by GFAAS E LE M E NT S b y IC P E LE M E NT S b y IC P (A Q UA RE G IA AS HIN G ) E LE M E NT S b y IC P (A Q UA RE G IA AS HIN G ) EL EM EN TS b y IC P (H ot B loc k/H C l/ H N O 3 Digestion) A S BE ST O S F IB ER S b y PC M ALKA LINE DU STS ASBESTOS FIBERS by TEM C E LL UL OS E IN SU LA TIO N S IL IC A , C R Y ST A LL IN E , b y X R D. SILICA, AMOR PHOUS

Flow Ra te ( L /m i n ) 1-3 1-3 1-3 1-3 1-4 1-4 1-4 1-4 1-4 1-4 1-4

Vol. (L) min max 30 - 1500 50 - 1500 2 - 400 25 - 1500 50 - 2000 200 - 1000 200 - 1500 25 - 2000 1 - 1500 V a r ies V a r ies

E x tr a c ti o n

A n a ly t ic a l T e c h n iq u e FAAS FAAS FAAS FAAS FAAS FAAS FAAS G FAAS G FAAS IC P !AES ICP-AES

Sampler MC EF MC EF MC EF MC EF MC EF MC EF MC EF MC EF MC EF MC EF MC EF PVCF MC EF

a q re g /H N O 3 H N O 3/H C l HNO3 H N O 3/H C l H 2O H F /H N O 3 H N O 3/H 2O 2 H N O 3/H 2SO 4 H N O 3/H 2O 2 H N O 3/HC lO 4 Aq R eg

7301

1-4

V a r ies

H C l /H N O 3

ICP-AES

7303

1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

7400 7401 7402 7404 7500 7501

0.5 - 16 1-4 0.5 - 16 1 1.7, 2.2 ,2.5 1.7, 2.2 ,2.5

400 - va r 70 - 1000 400 - va r NA 400 - 1000 50 - 400

NA HCl NA NA a s h or T HF ash

PCM T it ra t ion TEM SEM XR D XR D

MCEF open PTFE MCEF open ACF C Y C + P VC PVC (total) PVC&C YC P VC C Y C & P VC C Y C & P VC C Y C & P VC P VC CYC & MC E or P VC CYC & MC E or P VC C Y C & P VC P VC P VC

7502 7504 7505 7506 7600 7601

Z IN C O X I D E VANADIUM OX IDES L E AD S U LF ID E B O R O N C A R B ID E C H R O M I U M , HE X A V A LE N T S IL IC A , C R Y ST A LL IN E

1-3 1.7, 2.2 ,2.5 1.7, 2.2 ,2.5 1.7, 2.2 ,2.5 1-4 1.7, 2.2 ,2.5

10 - 400 200 - 1000 600 - 1000 100 - 1000 8 - 400 400 - 800

NA T HF T HF ash reagent H 3PO 4/HF

XR D XR D XR D XR D VIS VIS

7602

SILICA, CRYSTALLINE (IR )

1.7, 2.2 ,2.5

400 - 800

ash

IR

7603 7604 7605

SILICA in coal mine dust C H R O M I U M , HE X A V A LE N T CHROM IUM, HEXAV ALEN T b y IONCHROMATOG RAPHY LEAD in Air by Che mical Spot Test LEAD BY ULTRASOUND /ASV LEAD by Fi eld Portabl e XR F CHROM IUM, HEXAV ALEN T b y Field Portab le Spe ctroph otom etry AR SENIC & compoun ds , a s As AR SENIC TR IOX IDE, as A s FLUORIDES, aerosol & ga s

1.7, 2.2 ,2.5 1-4 0.1 - 4

300 - 1000 100 - 1000 1 - 400

ash N a O H / N a2 C O 3 N a O H - N a2C O 3

IR IC IC

7700 7701 7702 7703

2 1-4 1-4 1-4

10 - 240 20 - 1500 570 - 1900 10 - 1200

NA HNO3 NA ( N H4) 2SO 4/ N H 4O H H N O 3/H 2SO 4/HC lO 4 H N O 3/H 2O 2 N a OH H C O 3-/C O 32-

Sp ot Port ASV XR F (po rt) VIS

MC EF MC EF MC EF PVC, MCE, PTFE

7900 7901 7902

1-3 1-3 1-2

30 - 1000 30 - 1000 12 - 800

HYAAS G FAAS ISE

MC EF MC EF MCEF & pad w/ N a 2C O 3 SG(washed)

7903

AC IDS , INO RG AN IC

0.2 - 0.5

3.0 - 100

IC

3/15/2003

MF!32

NIOSH Manual of Analytical Methods

Chemical

M eth No. 7904 7905 7906

M e th od Na m e CYANIDES, aerosol an d g a s PHOSPHOR U S FLU O RID ES by IC

Flow Ra te ( L /m i n ) 0.5 - 1.0 0.01 - 0.2 1-2

Vol. (L) min max 10 - 180 5 - 100 s 1 - 800 i 120 - 800 NA

E x tr a c ti o n

A n a ly t ic a l T e c h n iq u e ISE G C !FPD IC

Sampler MCEF & BuB Te na x G C MCEF & pad w/ N a 2C O 3 NA

KOH xylene N a OH

8301

HIP PU RIC an d M ETH YL H IPP UR IC A C I D in U R IN E TR IAZ INE HE RB IC IDE S a nd the ir METABOLITES B U TO X Y A C E TI C A C ID in U R IN E ANALINE and o-TOLUIDINE in urine ASBESTOS, CHRYSOTILE b y XR D ASBES TOS (bulk) by PLM LEAD in Surface Wipe Sa mp les CHROM IUM, HEXAV ALENT in s ett led dust ELEMENTS on WIPES LEAD in DUST WIPES by C h emica l Spot Test CHLORINATED ORG ANONITROGEN HER BICIDES (HAND WAS H) CHLORINATED ORG ANONITROGEN HE RBIC IDES (DER M AL P ATC H)) C AP TA N a nd TH IO PH EN AT EM ETH YL in Handrinse CAPTAN and THIOPHENATEMETHYL on Dermal Patch

NA

Et a c

HP LC - U V

8315

NA

NA

NA

SC-MSD

Urine

8316 8317 9000 9002 9100 9101

NA NA NA NA NA NA

NA NA NA NA NA NA

NA ALK NA NA H N O 3/H 2O 2 NA

G C - EC D H P LC - EC D XR D PLM A A S; IC P Sp ot

NA NA bu lk bu lk Wipes Te st s trip

9102 9105

NA NA

NA NA

NA NA

ICP-AES Sp ot

Wipe Wipe

9200

NA

NA

NA

G C - EC D

polyethylene bag PUF pad

9201

NA

NA

IPA/diazomethane

G C - EC D

9202

NA

NA

NA

HP LC - U V

Hand wa sh

9205

NA

NA

IP A -A C N

HP LC - U V

Patch

3/15/2003

MF!33

NIOSH Manual of Analytical Methods

METHOD FINDER KEY TO ABBREVIATIONS


Sampling Media/Devices A-747 Anasorb 747 A-CMS Anasorb CMS Ag F Silver membrane filter BuB Bubbler CCT Coconut shell charcoal tube Chrom Chromosorb CYC Cyclone DNPH Dinitrophenylhydrazine Hcl Dry Drying tube GFF Glass fiber filter GW Glass wool HMP 2! (Hydroxymethyl)piperidine IMP Impinger IOM Inspirable dust sampler MCEF Mixed cellulose ester filter MS Molecular sieve NITC 1! naphthylisothiocyanate OVS! 2 OSHA versatile sampler (quartz filter/XAD! 2) OVS! 7 OSHA versatile sampler ( glass fiber filter/XAD! 7) Pad Cellulose backup pad PCT Petroleum charcoal tube Por Poropak PTFE Polytetrafluoroethylene (Teflon) filter PUF Polyurethane foam PVC Polyvinyl chloride filter QFF Quartz fiber filter SG Silica gel SL Soda lime TD Thermalalal desorption tube TEA Triethanolamine XAD Polymeric resin Extraction Media aaa acetic acid/acetonitrile a acid ac acetate ACN acetonitrile acet acetone al alcohol alk alkali aq aqueous / water aq reg aqua regia bz benzene cychex cyclohexane DCE dichloroethane DMF dimethylformamide DMSO dimethylsulfoxide DNPH dinitrophenyl hydrazine Et ethyl Etac ethyl acetate hex hexane HSA hexanesulfonic acid IPA isopropanol isooct isooctane MeCl2 /Meth methylene chloride/methanol Me methyl Meth methanol MTBE methyl-tert-butyl ether pet petroleum PMA phosphomolybdic acid pyr pyridine reag reagent THF tetrahydrofuran tol toluene TWM tropolone-water-methanol
3/15/2003 MF!34

Analytical Techniques AAS Atomic absorption spectrophotometry AMP Amperometric detector ASV Anodic stripping voltammetry CD Conductivity detector DPP Differential Pulse Polargraphy ECD Electron capture detector ECHD Electrochemical detector ECN Electrolytic conductivity detector EG Evolved gas analysis FAAS Flame AAS FI Flow injection FID Flame ionization detector FL Fluorescence detector FPD Flame photometric detector GC Gas chromatography Grav Gravimetric (filter weight) GFAAS Graphite furnace AAS HPLC High performance liquid chromatography HYAAS Hydride generation AAS IC Ion chromatography ICP! AES Inductively coupled plasma! atomic emission spectroscopy IR Infrared spoectrophotometry ISE Ion specific electrode MS Mass spectrometry NPD Nitrogen phosphorus detector PCM Phase contrast microscopy PES Plasma emission spectrometry PID Photoionization detector PLM Polarized light microscopy SCD Sulfur chemiluminescence detector SEM Scanning electron microscopy Spot Spot test TCD Thermalalal conductivity detector TEM Transmission electron microscopy TOA Thermal optical analyzer UV Ultraviolet VIS Visible absorption spectrophotometry XRD X! ray diffraction XRF X! ray fluorescence Other cap i NA port s var

capacity insoluble not applicable portable soluble varies / variable

NIOSH Manual of Analytical Methods

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