Standard Gas

method: C:\CHEM32\1\METHODS\STANDARD_ GAS.
M
Modified on: 10/10/2011 at 9:49:53 AM
Method Information
Method: C:\CHEM32\1\METHODS\STANDARD_ GAS.M
Modified: 10/10/2011 at 9:49:53 AM
Method Audit Trail

Operator
: DURGA
Date
: 3/8/2010 12:32:07 PM
Change Info: This method was created at 3/8/2010 12:32:07 PM and based on
method C:\CHEM32\1\METHODS\TOGA_PARAFFINOIL.M
Operator
: DURGA
Date
: 3/8/2010 12:32:08 PM
Change Info: Method saved. User comment: ""
Operator
: DURGA
Date
: 3/30/2010 7:18:13 PM
Operator
: Venu Gopal
Date
: 4/2/2010 1:41:50 PM
Operator
: Venu Gopal
Date
: 4/3/2010 7:50:47 PM
Operator
: Venu Gopal
Date
: 4/12/2010 7:30:30 PM
Operator
: Venu Gopal
Date
: 4/13/2010 4:27:34 PM
Operator
: Venu Gopal
Date
: 4/14/2010 8:25:29 PM
Operator
: Venu Gopal
Date
: 4/19/2010 1:04:32 PM
Operator
: Venu Gopal
Date
: 4/19/2010 1:08:47 PM
Operator
: Venu Gopal
Instrument 1 13/10/2011 3:32:26 PM Testing Engineer
Page
1 of 15
method: C:\CHEM32\1\METHODS\STANDARD_ GAS.M

Modified on: 10/10/2011 at 9:49:53 AM
Date
: 4/19/2010 1:09:19 PM
Operator
: Venu Gopal
Date
: 4/19/2010 1:32:53 PM
Operator
: Venu Gopal
Date
: 4/19/2010 1:36:07 PM
Operator
: Venu Gopal
Date
: 4/19/2010 1:37:38 PM
Operator
: Venu Gopal
Date
: 4/20/2010 11:01:15 AM
Operator
: Durga Sravan
Date
: 4/21/2010 10:13:29 AM
Operator
: Durga Sravan
Date
: 4/23/2010 3:31:58 PM
Operator
: Durga Sravan
Date
: 4/26/2010 10:54:16 AM
Operator
: Durga Sravan
Date
: 4/29/2010 5:31:06 PM
Operator
: Durga Sravan
Date
: 5/10/2010 3:37:32 PM
Operator
: HARI
Date
: 5/31/2010 9:58:49 AM
Operator
: Durga Sravan
Date
: 6/14/2010 5:58:00 PM
Operator
: Durga Sravan
Date
: 6/15/2010 11:17:30 AM
Operator
: Durga Sravan
Date
: 6/19/2010 2:44:31 PM
Page
2 of 15

Modified on: 10/10/2011 at 9:49:53 AM
Operator
: Durga Sravan
Date
: 6/23/2010 5:13:45 PM
Operator
: Durga Sravan
Date
: 6/24/2010 4:13:44 PM
Operator
: Durga Sravan
Date
: 6/26/2010 9:58:14 AM
Operator
: Durga Sravan
Date
: 6/29/2010 12:08:29 PM
Operator
: Durga Sravan
Date
: 7/6/2010 11:03:57 AM
Operator
: Durga Sravan
Date
: 7/6/2010 11:24:15 AM
Operator
: Durga Sravan
Date
: 7/6/2010 11:43:43 AM
Operator
: Durga Sravan
Date
: 7/26/2010 9:59:18 AM
Operator
: Durga Sravan
Date
: 9/8/2010 11:05:24 AM
Operator
: Testing Engineer
Date
: 9/17/2010 3:59:41 PM
Operator
: Testing Engineer
Date
: 9/23/2010 12:25:46 PM
Operator
: Testing Engineer
Date
: 10/20/2010 12:15:31 PM
Operator
: Testing Engineer
Date
: 10/22/2010 4:42:26 PM
Operator
Date
: Testing Engineer
: 11/26/2010 12:30:43 PM
Page
3 of 15

Modified on: 10/10/2011 at 9:49:53 AM
Operator
: Testing Engineer
Date
: 13\12\2010 5:14:05 PM
Operator
: Testing Engineer
Date
: 22\12\2010 3:52:56 PM
Operator
: Testing Engineer
Date
: 03\01\2011 12:33:46 PM
Operator
: Testing Engineer
Date
: 01\02\2011 11:19:36 AM
Operator
: Testing Engineer
Date
: 01\02\2011 11:19:45 AM
Operator
: Testing Engineer
Date
: 08\02\2011 10:56:07 AM
Operator
: Testing Engineer
Date
: 15\02\2011 3:53:33 PM
Operator
: Testing Engineer
Date
: 10\03\2011 6:31:20 PM
Operator
: Testing Engineer
Date
: 16\03\2011 11:57:55 AM
Operator
: Testing Engineer
Date
: 16\03\2011 11:58:02 AM
Operator
: Testing Engineer
Date
: 17\03\2011 12:22:18 PM
Operator
: Testing Engineer
Date
: 21\03\2011 12:31:29 PM
Operator
: Testing Engineer
Date
: 11\04\2011 3:57:58 PM
Page
4 of 15

Modified on: 10/10/2011 at 9:49:53 AM
Operator
: Testing Engineer
Date
: 11\05\2011 2:33:07 PM
Operator
: Testing Engineer
Date
: 14\05\2011 12:05:11 PM
Operator
: Testing Engineer
Date
: 16\06\2011 10:32:32 AM
Operator
: Testing Engineer
Date
: 16\06\2011 2:15:04 PM
Operator
: Testing Engineer
Date
: 16\06\2011 3:19:16 PM
Operator
: Testing Engineer
Date
: 17\06\2011 9:39:14 AM
Operator
: Testing Engineer
Date
: 17\06\2011 11:49:23 AM
Operator
: Testing Engineer
Date
: 17\06\2011 2:49:07 PM
Operator
: Testing Engineer
Date
: 17\06\2011 3:09:52 PM
Operator
: Testing Engineer
Date
: 17\06\2011 3:10:08 PM
Operator
: Testing Engineer
Date
: 17\06\2011 3:10:35 PM
Operator
: Testing Engineer
Date
: 17\06\2011 3:11:54 PM
Operator
: Testing Engineer
Date
: 17\06\2011 3:36:02 PM
Operator
Date
: Testing Engineer
: 29\06\2011 3:20:56 PM
Page
5 of 15

Modified on: 10/10/2011 at 9:49:53 AM
Operator
: Testing Engineer
Date
: 18\07\2011 6:02:46 PM
Operator
: Testing Engineer
Date
: 20\07\2011 3:09:37 PM
Operator
: Testing Engineer
Date
: 25\07\2011 10:20:52 AM
Operator
: Testing Engineer
Date
: 04\08\2011 10:23:37 AM
Operator
: Testing Engineer
Date
: 11\08\2011 9:03:52 AM
Operator
: Testing Engineer
Date
: 23\08\2011 11:49:19 AM
Operator
: Testing Engineer
Date
: 24\08\2011 10:18:53 AM
Operator
: Testing Engineer
Date
: 29\08\2011 11:36:23 AM
Operator
: Testing Engineer
Date
: 31\08\2011 10:19:53 AM
Operator
: Testing Engineer
Date
: 05\08\2011 11:15:03 AM
Operator
: Testing Engineer
Date
: 11\09\2011 12:17:24 PM
Operator
: Testing Engineer
Date
: 11\09\2011 12:17:53 PM
Operator
: Testing Engineer
Date
: 11\09\2011 1:09:24 PM
Page
6 of 15

Modified on: 10/10/2011 at 9:49:53 AM
Operator
: Testing Engineer
Date
: 11\09\2011 2:46:32 PM
Operator
: Testing Engineer
Date
: 14\09\2011 6:50:07 AM
Operator
: Testing Engineer
Date
: 15\09\2011 9:36:21 AM
Operator
: Testing Engineer
Date
: 16\09\2011 9:09:23 AM
Operator
: Testing Engineer
Date
: 17\09\2011 11:32:56 AM
Operator
: Testing Engineer
Date
: 17\09\2011 12:45:34 PM
Operator
: Testing Engineer
Date
: 19\09\2011 9:15:58 AM
Operator
: Testing Engineer
Date
: 20\09\2011 6:51:42 PM
Operator
: Testing Engineer
Date
: 21\09\2011 9:17:42 AM
Operator
: Testing Engineer
Date
: 22\09\2011 8:40:00 AM
Operator
: Testing Engineer
Date
: 26/09/2011 8:52:48 AM
Operator
: Testing Engineer
Date
: 27/09/2011 9:00:04 AM
Operator
: Testing Engineer
Date
: 30/09/2011 9:38:02 AM
Operator
Date
: Testing Engineer
: 06/10/2011 9:46:24 AM
Page
7 of 15

Modified on: 10/10/2011 at 9:49:53 AM
Operator
: Testing Engineer
Date
: 07/10/2011 9:12:21 AM
Operator
: Testing Engineer
Date
: 10/10/2011 9:49:53 AM
Run Time Checklist

Pre-Run Cmd/Macro:
off
Data Acquisition:
on
Standard Data Analysis:
on
Customized Data Analysis:
off
Save GLP Data:
off
Post-Run Cmd/Macro:
off
Save Method with Data:
on
Injection Source and Location

Injection Source:
Headspace Sampler
Injection Location: Front
Page
8 of 15

Modified on: 10/10/2011 at 9:49:53 AM
HEADSPACE PARAMETERS
Headspace Device:
Communications Mode:
Serial Number:
Firmware Revision:
Vial Size, mL:
Handshake Mode:
Oven Stabilization Time, min:
Pressure Units:
Carrier Connection:
Vial EPC:
Agilent G1888 Headspace Sampler

COM1
IT00943016
A.01.10
20
Headspace Proceed
1
psi
Front Inlet (EPC)
Aux1
Multi HS Extr:
Extractions Per Vial:
GC Cycle Time (Min):
Inject Time (Min):
Loop Equilibration Time (Min):
Loop Fill Time (Min):
Loop Temperature:
Oven Temperature:
Shake:
Transfer Line Temperature:
Vial Equilibration Time (Min):
Vial Pressurization Time (Min):
OFF
2
20.0
0.90
0.25
0.25
150
70
HIGH
150
1.0
0.25
=====================================================================
Agilent 7890A
=====================================================================
Oven
Equilibration Time
Oven Program
40 C for 6 min
then 24 C/min to 230 C for 0 min
Run Time
Thermal Aux 1 {Nickel Catalyst}

Heater
Temperature Program
375 C for 0 min
Run Time
0.5 min
On
13.917 min
On
On
13.917 min
Column #1
plot q + plot molesieve: Agilent toga
Page
9 of 15

Modified on: 10/10/2011 at 9:49:53 AM
plot q + plot molesieve
300 C: Packed
In: PCM C-1 ArMe
Out: Front Detector FID
Flow Program
6.8948E+05 mL/min for 0 min
Run Time
On
13.917 min
Front Detector FID

Heater
H2 Flow
Air Flow
Makeup Flow
Const Col + Makeup
Flame
Electrometer
On
On
On
On
Off
On
On
250 C
50 mL/min
400 mL/min
5 mL/min
Back Detector TCD

Heater
Reference Flow
Makeup Flow
Const Col + Makeup
Negative Polarity
Filament
On
On
On
Off
On
On
150 C
20 mL/min
5 mL/min
Valve 1
Other
Off
Aux EPC 4 ArMe

Aux EPC 5 N2
***Excluded from Affecting GC's Readiness State***
Aux EPC 6 N2
PCM C-1 ArMe: Supplies Column 1
Flow Program
15 mL/min for 0 min
Run Time
On
13.917 min
Page
10 of 15

Modified on: 10/10/2011 at 9:49:53 AM
PCM C-2 ArMe
Valve Box
Heater
On
Signals
Front Signal
Save On
20 Hz
Save On
20 Hz
Save Off
50 Hz
Save Off
50 Hz
Back Signal
Test Plot
Test Plot
Run Time Events

Time (min)
1.521
3.1
8.1
13.87
100 C
Event
Valve
Valve
Valve
Valve
Position
Valve 1
Valve 1
Valve 1
Valve 1
Setpoint
On
Off
On
Off
========================================================================
Integration Events
========================================================================
-----------------------------------------------------------------------Non signal specific Integration Events

-----------------------------------------------------------------------Event
Value
|--------------------------------------------------------|-------------|
Tangent Skim Mode
Standard
Tail Peak Skim Height Ratio
0.000
Front Peak Skim Height Ratio
0.000
Skim Valley Ratio
20.000
Baseline Correction
Classical
Peak to Valley Ratio
500.000
Page
11 of 15

Modified on: 10/10/2011 at 9:49:53 AM
-----------------------------------------------------------------------Default Integration Event Table "Event"
-----------------------------------------------------------------------Event
Value
Time
|------------------------------------------------|-------------|-------|
Initial Slope Sensitivity
1.000
Initial
Initial Peak Width
0.040
Initial
Initial Area Reject
1.000
Initial
Initial Height Reject
1.700
Initial
Initial Shoulders
OFF
Initial
-----------------------------------------------------------------------Detector Default Integration Event Table "Event_ADC"
-----------------------------------------------------------------------Event
Value
Time
|------------------------------------------------|-------------|-------|
20.000
Initial
Initial Peak Width
0.040
Initial
Initial Area Reject
1.000
Initial
1.000
Initial
Initial Shoulders
OFF
Initial
-----------------------------------------------------------------------Detector Default Integration Event Table "Event_ECD"
-----------------------------------------------------------------------Event
Value
Time
|------------------------------------------------|-------------|-------|
100.000
Initial
Initial Peak Width
0.080
Initial
Initial Area Reject
1.000
Initial
1.000
Initial
Initial Shoulders
OFF
Initial
-----------------------------------------------------------------------Detector Default Integration Event Table "Event_NPD"
-----------------------------------------------------------------------Event
Value
Time
|------------------------------------------------|-------------|-------|
500.000
Initial
Initial Peak Width
0.040
Initial
Initial Area Reject
1.000
Initial
1.000
Initial
Initial Shoulders
OFF
Initial
Page
12 of 15

Modified on: 10/10/2011 at 9:49:53 AM
-----------------------------------------------------------------------Detector Default Integration Event Table "Event_FPD"
-----------------------------------------------------------------------Event
Value
Time
|------------------------------------------------|-------------|-------|
50.000
Initial
Initial Peak Width
0.040
Initial
Initial Area Reject
1.000
Initial
1.000
Initial
Initial Shoulders
OFF
Initial
-----------------------------------------------------------------------Detector Default Integration Event Table "Event_uECD"
-----------------------------------------------------------------------Event
Value
Time
|------------------------------------------------|-------------|-------|
500.000
Initial
Initial Peak Width
0.080
Initial
Initial Area Reject
1.000
Initial
1.000
Initial
Initial Shoulders
OFF
Initial
-----------------------------------------------------------------------Detector Default Integration Event Table "Event_TCD"
-----------------------------------------------------------------------Event
Value
Time
|------------------------------------------------|-------------|-------|
100.000
Initial
Initial Peak Width
0.020
Initial
Initial Area Reject
0.500
Initial
1.000
Initial
Initial Shoulders
OFF
Initial
-----------------------------------------------------------------------Detector Default Integration Event Table "Event_FID"
-----------------------------------------------------------------------Event
Value
Time
|------------------------------------------------|-------------|-------|
50.000
Initial
Initial Peak Width
0.040
Initial
Initial Area Reject
10.000
Initial
1.000
Initial
Initial Shoulders
OFF
Initial
Page
13 of 15

Modified on: 10/10/2011 at 9:49:53 AM
-----------------------------------------------------------------------Signal Specific Integration Event Table "Event_TCD2B"
-----------------------------------------------------------------------Event
Value
Time
|------------------------------------------------|-------------|-------|
5.951
Initial
Initial Peak Width
0.041
Initial
Initial Area Reject
0.500
Initial
0.500
Initial
Initial Shoulders
OFF
Initial
Apply Manual Integration Events: No
=====================================================================
Calibration Table
=====================================================================
Calib. Data Modified
10/10/2011 9:49:47 AM
Rel. Reference Window :

Abs. Reference Window :
Rel. Non-ref. Window :
Abs. Non-ref. Window :
Uncalibrated Peaks
:
Partial Calibration
:
Correct All Ret. Times:
5.000 %
0.000 min
5.000 %
0.000 min
not reported
Yes, identified peaks are recalibrated
No, only for identified peaks
Curve Type
Origin
Weight
Linear
Included
Equal
:
:
:
Recalibration Settings:
Average Response
:
Average Retention Time:
Average all calibrations

Floating Average New 75%
Calibration Report Options :

Printout of recalibrations within a sequence:
Calibration Table after Recalibration
Normal Report after Recalibration
If the sequence is done with bracketing:
Results of first cycle (ending previous bracket)
Signal 1: FID1 A, Front Signal
Signal 2: TCD2 B, Back Signal
RetTime
Lvl
Amount
Area
Amt/Area Ref Grp Name
[min] Sig
[ppm]
-------|--|--|----------|----------|----------|---|--|--------------1.539 2 1
56.40000 2769.53516 2.03644e-2
Hydrogen
1.564 1 1
56.80000 551.36755 1.03017e-1
CO2
Page
14 of 15

Modified on: 10/10/2011 at 9:49:53 AM
RetTime
Lvl
Amount
Area
Amt/Area Ref Grp Name
[min] Sig
[ppm]
-------|--|--|----------|----------|----------|---|--|--------------1.772 1 1
53.90000 510.38730 1.05606e-1
Methane
2.273 1 1
54.20000 940.69464 5.76170e-2
Ethylene
2.507 1 1
55.80000 850.20538 6.56312e-2
Acetylene
2.762 1 1
53.10000 895.13556 5.93206e-2
Ethane
8.114 2 1 108.70000
68.79405
1.58008
Nitrogen
8.138 1 1
55.00000
90.95636 6.04686e-1
CO
=====================================================================
Peak Sum Table
=====================================================================
***No Entries in table***
=====================================================================
========================================================================
Sample related custom fields
========================================================================
Custom Field
Type
Mand. Default Value
-----------------------------------------------------------------------None defined
========================================================================
Compound related custom fields
========================================================================
Custom Field
Type
Mand. Default Value
-----------------------------------------------------------------------None defined
Page
15 of 15

Standard Gas

Uploaded by

Document Information

Copyright

Available Formats

Share this document

Share or Embed Document

Sharing Options

Did you find this document useful?

Is this content inappropriate?

Copyright:

Available Formats

Standard Gas

Uploaded by

Copyright:

Available Formats

method: C:\CHEM32\1\METHODS\STANDARD_ GAS.

Method Audit Trail

Instrument 1 13/10/2011 3:32:26 PM Testing Engineer

method: C:\CHEM32\1\METHODS\STANDARD_ GAS.M

method: C:\CHEM32\1\METHODS\STANDARD_ GAS.M

Instrument 1 13/10/2011 3:32:26 PM Testing Engineer

method: C:\CHEM32\1\METHODS\STANDARD_ GAS.M

Instrument 1 13/10/2011 3:32:26 PM Testing Engineer

method: C:\CHEM32\1\METHODS\STANDARD_ GAS.M

Instrument 1 13/10/2011 3:32:26 PM Testing Engineer

method: C:\CHEM32\1\METHODS\STANDARD_ GAS.M

Instrument 1 13/10/2011 3:32:26 PM Testing Engineer

method: C:\CHEM32\1\METHODS\STANDARD_ GAS.M

Instrument 1 13/10/2011 3:32:26 PM Testing Engineer

method: C:\CHEM32\1\METHODS\STANDARD_ GAS.M

Run Time Checklist

Standard Data Analysis:

Customized Data Analysis:

Save GLP Data:

Save Method with Data:

Injection Source and Location

Injection Location: Front

Instrument 1 13/10/2011 3:32:26 PM Testing Engineer

method: C:\CHEM32\1\METHODS\STANDARD_ GAS.M

Agilent G1888 Headspace Sampler

Thermal Aux 1 {Nickel Catalyst}

method: C:\CHEM32\1\METHODS\STANDARD_ GAS.M

Front Detector FID

Back Detector TCD

Aux EPC 4 ArMe

Instrument 1 13/10/2011 3:32:26 PM Testing Engineer

method: C:\CHEM32\1\METHODS\STANDARD_ GAS.M

Run Time Events

-----------------------------------------------------------------------Non signal specific Integration Events

Instrument 1 13/10/2011 3:32:26 PM Testing Engineer

method: C:\CHEM32\1\METHODS\STANDARD_ GAS.M

Instrument 1 13/10/2011 3:32:26 PM Testing Engineer

method: C:\CHEM32\1\METHODS\STANDARD_ GAS.M

Instrument 1 13/10/2011 3:32:26 PM Testing Engineer

method: C:\CHEM32\1\METHODS\STANDARD_ GAS.M

Calib. Data Modified

Rel. Reference Window :

Average all calibrations

Calibration Report Options :

method: C:\CHEM32\1\METHODS\STANDARD_ GAS.M

Instrument 1 13/10/2011 3:32:26 PM Testing Engineer

You might also like