Professional Documents
Culture Documents
2—1998
Australian Standard™
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Reference gases
Review of Australian Standards. To keep abreast of progress in industry, Australian Standards are subject
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important therefore that Standards users ensure that they are in possession of the latest edition, and any
amendments thereto.
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Australian Standard™
Reference gases
Originated as AS 2719—1984.
Revised and redesignated as AS 3536.2 — 1998.
PREFACE
This Standard was prepared by the Standards Australia Committee CH/27, Reference
Gases to supersede AS 2719 — 1984, Traceable reference gases — For analysis of emission
gases of internal combustion engines and motor vehicles — Preparation, analysis and
certification.
This Standard is part of a series as follows:
AS
3536 Reference gases
3536.1 Part 1: Preparation and certification of gravimetric standards
3536.2 Part 2: Preparation, analysis and certification of traceable reference gas mixtures
Within Australia, measurements made for any legal purpose including trade and
government regulation must be traceable to the Australian primary standards of
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measurement. When measurements are made for legal purposes, the appropriate
measurement units are prescribed as legal units of measurement and demonstration may be
required in courts of law of the traceability linkages between a measurement tendered as
evidence and Australia’s national measurement standards. There are specific legal
requirements for reference materials used to calibrate measuring instruments used to make
measurements for legal purposes. The National Measurement Act 1960 defines a certified
reference material as one that has been certified under the relevant provisions of the
National Measurement Regulations. As required by Section 10 of the Act such certified
reference materials have one or more of their property values traceable to Australia’s
primary standards of measurement.
The objectives of this Standard are as follows:
(a) Augments the range of available concentrations of reference materials by defining
and specifying additional gases traceable to International Standards. These are
defined as Reference Gas Mixture (RGM).
(b) Describes a protocol for the preparation, analysis and certification of RGM.
It is hoped that this Standard will improve the availability of such reference gases, reduce
their cost and reduce the preparatory work required to calibrate analytical instrumentation
in this field of application.
The term ‘informative’ has been used in this Standard to define the application of the
appendix to which it applies. An ‘informative’ appendix is only for information and
guidance.
CONTENTS
Page
1 SCOPE . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
2 REFERENCED DOCUMENTS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
3 DEFINITIONS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
4 PRINCIPLE . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5
5 APPARATUS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5
6 CALIBRATION GASES . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5
7 PROCEDURE . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
8 ANALYSIS OF REFERENCE GAS MIXTURE . . . . . . . . . . . . . . . . . . . . . . . 7
9 CALCULATIONS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
10 VERIFICATION OF THE STABILITY OF RGM . . . . . . . . . . . . . . . . . . . . . . 8
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APPENDICES
A EXAMPLE OF TYPICAL END USE OF RGM FOR VEHICLE EMISSIONS
AND FUEL CONSUMPTION ASSESSMENT . . . . . . . . . . . . . . . . . . . . . . 10
B ORDERING DATA FOR RGM AND/OR ANALYSIS REPORT . . . . . . . . . . 12
AS 3536.2 — 1998 4
STANDARDS AUSTRALIA
Australian Standard
Reference gases
1 SCOPE This Standard sets out requirements for the preparation, analysis and
certification procedures of traceable reference gas mixtures. This Standard applies to the
preparation, analysis and certification of a reference gas mixture (RGM) whose range of
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3 DEFINITIONS For the purpose of this Standard, the following definitions below
apply:
3.1 Analyte — the component gas of interest.
3.2 Balance gas — the matrix gas for the analytes of interest. A gas which is used to
make up the final gas mixture.
3.3 Certified reference gas mixture (CRGM) — a prepared gas mixture accompanied by
certificate where one or more values are certified by a procedure which establishes its
traceability to a national or international Standard.
COPYRIGHT
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