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Chapter 6
DESIGN OF EQUIPMENTS.
Design of Reactor :
Process Design:
The polymerization of styrene is an exothermic reaction. The amount of
energy released at any time is dependent on the volume of the reactor, and the rate of
removal of that heat is dependent on the surface area. Unless the heat is removed, the
temperature will rise and the reaction rate will increase. The result will be an
uncontrolled reaction that not only may ruin the batch but could also damage the
reactor and might cause fire or explosion to occur.
Therefore there is a maximum size reactor for each set of reaction condition.
This size will be calculated. The maximum rate of heat production will be first
calculated.
The heat of polymerization
-----------------------(2)
Where D = diameter of reactor
L = length of reactor.
It will be assumed that the reactor is generally 90% full and the height is twice
the diameter.
i.e.
L = 2D
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Production of Polystyrene
Production of Polystyrene
suspension.
Since 95% of the time, the air temperature is below 30C. It will be assumed that inlet
cooling water temperature never exceeds 30C.
The reaction temperature = 93C.
It is assumed the maximum cooling water temperature rise is
5C. Therefore outlet temperature of cooling water =35 C.
Therefore the average temperature of cooling water =(30+35)/2
= 32.5C.
Therefore,
T= 93-32.5 = 60.5C.
The area of heat transfer is the area covered by the suspension. This can be estimated
to be the bottom plus 90% of the sides. ( because the reactor is 90% filled).
A = 0.9DL + D2
4
= 6.44D2
Substituting values of A, T and U in equation (4), we get,
Q = 283.9*6.44D2 *60.5 ----------------------(5)
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Production of Polystyrene
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Production of Polystyrene
Mechanical design:
Data from literature:
Design pressure for the reactor = 220psi = 16.47 kg/cm2.
Design pressure for jacket
= 75psi = 6.27 kg/cm2.
Permissible stress of reactor
= 950kg/cm2.
Shell internal diameter
= 2.486m.
Agitator horse power for 5000gal = 50hp
Diameter of agitator
= 1035mm.
Speed
= 200rpm.
Agitator blades (flat)
=6
Width of blade
=75mm.
Thickness of blades
=8mm.
Shaft material commercial cold rolled steel.
Permissible shear stress in shaft = 550kg/cm2.
Elastic limit in tension
= 2460kg/cm2.
Modulus of elasticity
=19.5*105kg/cm2.
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Production of Polystyrene
Therefore,
t=
16.47*2486
+3
(2*950*0.85)-16.47
=28.0mm.
(b)
External pressure:
Let t =22mm.
L / Do=
3506.9
= 1.3758
(2486 + 44)
11200
14.22*(2486+44)/22
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Production of Polystyrene
Therefore,
t=
pi*di
2ft*J-pi
+C
= 6.27 * 2623
+2
2*950*.85 6.27
=11.7mm
Take 12mm as thickness of jacket.
3. Stiffening ring:
Required moment of inertia of stiffening ring is as per equation:
I = pcDo3L
24E
pc= 4pe = 4*6.27 = 25.08kg/cm2.
I = 25.08 * (2486)2 4.97 = 4.619*104 mm4.
24 * 1900*103
Value of I is reduced by 30% to take into account the resistance of the steel.
I = 4.916*104 0.3*4.916*104 = 3.441*104mm4.
Use equal angle IS 2020 (size 20*20mm thickness = 3mm).
Ixx=Iyy = 0.4cm4.
4.Head thickness:
(a) Internal pressure:
t b = pRcW
2fJ
W = 1 * ( 3 + (Rc/Rl)0.5)
4
= 1 * (3 + (2486/128)0.5)
4
= 1.85
Therefore,
t b = 16.47 * 2486 *1.85 = 46.90mm.
2*950*0.85
Use 48mm thickness including corrosion allowance.
(b)External pressure:
t b = 4.4*2486*(3(1-0.32)0.25*(6.27/(2*1900*103))0.5) = 43.179mm.
Therefore head thickness = 48mm.
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31
Production of Polystyrene
5. Shaft design:
From equation 14.8(M.V. Joshi)
Tc = 50 * 75 * 60
2**200
= 179.049kgm.
Tm = 1.5 * 179.049 = 269.57 kgm.
From equation 14.9 (M.V. Joshi)
Zp = 1.5Tc
fs
= 269.57*100 = 49.013 cm3.
550
d 3 = 49.013.
16
d = 6.296cm.
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Production of Polystyrene
6.Blade design:
From equation 14.6 and 14.7,
f = maximum bending moment
(bt*bw2/6)
= 346.09kg/cm2.
269.57
(0.8*7.52/6)
Which is well within the endurance limit for carbon steel.
=
= 1.5*shaft diameter.
= 1.5*10 = 15cm.
Take V = 2m/s.
A = D2
4
Therefore,
0.0134 = D2 *2
4
D = 0.0134*4/2
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Production of Polystyrene
= 0.0924m
= 92.4mm
From IS 803,
Nozzle for shell = 100mm
Thickness
= 10mm.
A = 2.085*10-3m2.
D = 51.5mm.
From IS 803,
Nozzle diameter = 75mm.
Thickness
= 7.5mm.
Distance from shell to flange = 175mm.
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Production of Polystyrene
Load on gland:
F = * 16.47*(13.162 102) = 946.69kg.
4
Size of stud:
946.69 = do2*n*ft
4
n= number of baffles = 4
ft = 587kg/cm2
2*Tmax
d + n/2
= 2*269.57*100
*0.25*10*4
= 1716.14kg.
Area of bolt = 1716.14
587
= 2.824cm2.
Diameter of bolt = (2.924*4/)0.5 = 1.929 cm = 19.29mm.
Use 20M size bolts.
Overall diameter of coupling = 2*10 = 20cm.
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Production of Polystyrene
C.
Ua = 20G0.16
D
----------(2)
Where,
Qt = Total energy transferred, kJ/hr.
Ua = Volumetric heat transfer coefficient, kJ/hr.m2. C.
Tm = Log mean temperature difference between hot gases and material,
G
D
V
Temperatures:
Polystyrene
Air
Outlet
80C.
85C.
Production of Polystyrene
The minimum air velocity is set by the particle size. A flow rate of 1000lb/hr.ft2 is
adequate for 420-micron particle. This will be used. The minimum velocity is used
since it gives the smaller dryer.
The amount of air required is determined by amount of energy the 150C. air
must supply to remove the moisture from the polystyrene.
m = Qt /( Cp.T).
Where,
Cp = heat capacity of air = 0.237 BTU/lb.C.
T = difference in air temperature entering and leaving dryer,C.
Qt = heat transferred in dryer =8.23765*105W.
m = mass flow rate of air.
m=
8.23765*105 = 12771.65kg/hr.
(0.9923*(150-85))
Maximum amount of water that can be in air = 12771.65(kg/hr)* 0.7(kg water/kg dry
air)
= 8940.155 kg water/hr.
Amount of water to be removed = 10416.67 * 0.0497
= 518 kg water/hr.
The amount of air is adequate. Add 10% to account for possible heat losses.
Therefore mass flow rate = 1.1* 12771.65
= 14048.87 kg/hr.
If the mass velocity = 1000lb/hr.ft2
= 4880 kg/hr.m2.
Then,
Area of dryer = 14048.82
4880
= 2.876m2.
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Production of Polystyrene
Therefore,
Diameter of dryer =(2.876*4/)
= 1.914m.
V=
7.80778*105
9.619*97.1348
= 835.699ft3
= 35.2198m3
Therefore,
L = V*4
D2
=
35.2198*4
*(1.9142)
= 12.24m.
Mechanical design:
1. Flight design:
Number of flights = 3*D.
= 3*6.28
=18.83 19 flights are required using lip angle of 45.
Radial height is taken as 1/8 of diameter,
Radial height = 1.914/8 = 0.2393m.
2. Thickness of dryer:
Let x be the thickness of drier.
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Production of Polystyrene
= 7.04 * 1049.2
= 7389.98kg.
The dryer is supported over two-trunsion roll assemblies, 20ft apart. It
is
uniformly distributed load.
Maximum bending moment = WL/8 = M.
M = (565.89x/8 + 7389.98/9)*12.24
= 865.81*103x + 11306.7
We know that,
M = f*Z.
-------------(1a).
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Production of Polystyrene
x(m)
0.5
0.25
0.125
0.1
0.01
0.04
0.02
RHS
14.712
5.84
2.208
1.542
1.02
0.027
-0.45
Production of Polystyrene
T1 = 150C
T2 = 85C
X = 6mm.
= 11.06m3/hr.
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Production of Polystyrene
= 0.00726
= 212.8kg/min.
= 212.8*22.4*368.62
29*298
= 203.09m3/min.
= 7172.06ft3/min.
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Production of Polystyrene
At outlet conditions,
Volume of air
= 170.5*(273+85)/303
= 201.45m3/min.
= 3.357m3/s.
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