REVISION:

617-249-902

KIT INSTRUCTIONS
REVISION DATE: ORIGINAL DATE: 01-14-08

1. INSTRUMENT(S) AFFECTED: C-200 Carbon Determination System C-230 Carbon Determination System C-600 Carbon Determination System CS-200 Carbon/Sulfur Determination System CS-230 Carbon/Sulfur Determination System CS-600 Carbon/Sulfur Determination System S-200 Sulfur Determination System S-230 Sulfur Determination System S-600 Sulfur Determination System ........................................................................................................................................................................ 2. KIT NUMBER AND PARTS LIST: 617-249-INT (Carbon and Sulfur) Fluorine and Chlorine Halogen Trap consists of: 4 163-021 Brass Inserts 1 501-081 Glass Wool 4 ft. 501-109 Neoprene Rubber Tubing 4 ft. 537-103 Poly-Flo Tubing 4 589-305 Sleeve 4 589-312 Flex Nut 1 617-249-902 Kit Instructions 2 760-193 Metal Screen 1 764-762 Glass Tube 2 766-061 Plastic Plug 1 769-605-INT Fluorine/Chlorine Trap Assembly 1 769-610 Fluorine/Chlorine Absorbent Reagent (225 grams) 2 771-299 Swage Tube 1 772-704 Fitting 1 773-136 Fitting NOTES: On the C-200, C-230, CS-200, CS-230, S-200 and S-230, the 769-605-INT Fluorine/Chlorine Trap Assembly will be installed between the manual cleaner and the anhydrone filter tube. On the C-600, CS-600 and S-600, the 769-605-INT Fluorine/Chlorine Trap Assembly will be installed between the autocleaner and the furnace gas scrubber (Figure 2). The 769-605-INT Fluorine/Chlorine Trap Assembly has an approximate capacity of 9 grams of fluorine and 6 grams of chlorine. The sample sizes of fluorspar and similar materials must not exceed 0.5 grams.

LECO Corporation, 3000 Lakeview Ave., St. Joseph, MI 49085-2396

PIB 202-961

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REVISION: REVISION DATE:

617-249-902
ORIGINAL DATE: 01-14-08

CS-200/CS230 WITH FLUORINE TRAP FIGURE 1

LECO Corporation, 3000 Lakeview Ave., St. Joseph, MI 49085-2396

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REVISION: REVISION DATE:

617-249-902
ORIGINAL DATE: 01-14-08

C-200, C-230, CS-200, CS-230, S-200, S-230 NOTE: Refer to Figure 5 and Figure 6 for packing of the 769-605-INT Fluorine/Chlorine Trap Assembly. Set the 769-605-INT Fluorine/Chlorine Trap Assembly next to the furnace (Figure 1 or Figure 2). Turn OFF the oxygen supply. Disconnect the tubing from the measure flow fitting on the cleaning head (Figure 1 or Figure 2). Remove the shipping plugs from the inlet and outlet of 769-605-INT Fluorine/Chlorine Trap Assembly (Figure 5 or Figure 6). 5. Connect a section of 537-103 Tubing between the OUTLET (top) port of the 769-605-INT Fluorine/Chlorine Trap Assembly and the measure flow fitting on the cleaning head (Figure 1 or Figure 2). 6. Connect a section of 537-103 Tubing between the INLET (bottom) port of the 769-605-INT Fluorine/Chlorine Trap Assembly and the tubing/fitting disconnected from the measure flow fitting in step 3 (Figure 1 or Figure 2). NOTE: Keep tubing length to a minimum. Excessive length necessitates increased combustion time. 1. 2. 3. 4.

CS-200/CS230 WITH CHLORINE TRAP FIGURE 2

LECO Corporation, 3000 Lakeview Ave., St. Joseph, MI 49085-2396

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REVISION: REVISION DATE:

617-249-902
ORIGINAL DATE: 01-14-08

CS-600 WITH FLUORINE TRAP FIGURE 3

LECO Corporation, 3000 Lakeview Ave., St. Joseph, MI 49085-2396

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REVISION: REVISION DATE:

C-600, CS-600, S-600

617-249-902
ORIGINAL DATE: 01-14-08

NOTE: Refer to Figure 5 and Figure 6 for packing of the 769-605-INT Fluorine/Chlorine Trap Assembly. 1. Position the 769-605-INT Fluorine/Chlorine Trap Assembly to the right of the unit (Figure 3 or Figure 4). 2. Turn OFF the oxygen supply. 3. Disconnect and remove the stainless steel delivery tube between from autocleaner and furnace gas scrubber. 4. Remove the shipping plugs from the 769-605-INT Fluorine/Chlorine Trap Assembly inlet and outlet (Figure 5 and Figure 6). 5. Connect a section of 537-103 Tubing between the OUTLET (top) port of the 769-605-INT Fluorine/Chlorine Trap Assembly and the fitting on the autocleaner (Figure 3 or Figure 4). 6. Connect another section of 537-103 Tubing between the INLET (bottom) port of the 769-605-INT Fluorine/Chlorine Trap Assembly and the top of the furnace gas scrubber tube (Figure 3 or Figure 4). NOTES: Keep tubing length to a minimum. Excessive length necessitates increased combustion time. Fluorides decrease the life of the autocleaner O-rings. It will be necessary to disassemble the cleaner daily and change or re-grease the internal O-rings of the cleaner.

CS-600 WITH CHLORINE TRAP FIGURE 4

LECO Corporation, 3000 Lakeview Ave., St. Joseph, MI 49085-2396

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REVISION: REVISION DATE:

589-480 SHIPPING PLUG FLOW TO ANALYZER OUTLET

617-249-902
ORIGINAL DATE: 01-14-08

760-899 ELBOW 521-295 DISCONNECT BLOCK

**

501-081 GLASS WOOL (1.5-INCHES) 769-608-HAZ METAL (1-INCH) 501-081 GLASS WOOL (1.5-INCHES)

760-193 METAL SCREEN

769-611 FILLED REAGENT TUBE OR 764-762 EMPTY GLASS TUBE

769-610 F, CL ABSORBENT (5.75-INCHES)

501-081 GLASS WOOL (1.5-INCHES) 760-193 METAL SCREEN 501-081 GLASS WOOL (1.5-INCHES) 769-608-HAZ METAL (1-INCH)

** 761-254 CONNECTOR FITTING

760-338 RING & PLUNGER ASSEMBLY *** **** INLET 764-687 PLUNGER BLOCK

FLOW FROM FURNACE

589-480 SHIPPING PLUG **** 760-316 RUBBER WASHER (2 REQUIRED) **** 760-841 O-RING (2 REQUIRED) **** 760-359 O-RING (2 REQUIRED) **** 760-346 SPRING

769-606 STAND

769-605-INT FLUORINE/CHLORINE TRAP PACKED FOR CHLORINE REMOVAL FIGURE 5

LECO Corporation, 3000 Lakeview Ave., St. Joseph, MI 49085-2396

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REVISION: REVISION DATE:

617-249-902
ORIGINAL DATE: 01-14-08

OPERATION 1. Turn ON the oxygen supply and set it for specified flows and pressures according to the appropriate instruction manual. 2. Set the combustion time on the C-200, C-230, CS-200, CS-230, S-200 and S-230 for 70 seconds. Set the combustion time on the C-600, CS-600 and S-600 for 50 seconds (nominal). This is to compensate for increases volume in the measure line. 3. After the system has purged for a minimum of 5 minutes, perform calibration according to the appropriate instruction manual.

MAINTENANCE CHLORINE TRAP NOTE: Replace the 769-605-INT Fluorine/Chlorine Trap Assembly reagent tube before it becomes completely depleted. The reagent changes color from white to yellow to orange to orange/brown. The reagent must be changed before it becomes to brown in color. Also, the reagent tube must be repacked if the 769-608-HAZ Metal at the outlet loses its luster and becomes dull in appearance. 1. Repack the tube as follows (Figure 4). a. Discard depleted reagent and all material in the trap tube except the screens and glass tube. b. Wash and dry the glass tube. c. Place a fresh 601-081 Glass Wool plug, approximately 1-inches (38 mm), at the bottom of the glass tube. d. Add a layer of 769-608-HAZ Absorbent Metal approximately 1-inch (25 mm or 32 grams 2 grams) deep. Tap the sides of the tube to allow settling. e. Cover the metal with -inch (13 mm) of glass wool. f. Add enough 769-610 Absorbing Reagent to fill all but the last 1-inches (38 mm) of the wider part of the tube (approximately 70 grams). g. Place -inch (13 mm) of glass wool over the reagent. h. Add enough 769-608-HAZ Absorbent Metal to make a layer 1-inch (25 mm) deep. i. Fill the remainder of the tube with glass wool and place 769-193 Screens at both ends. NOTE: Insert the filled tube immediately in the stand or plug both ends to avoid contamination by moisture from the atmosphere. Close all reagent bottles tightly.

LECO Corporation, 3000 Lakeview Ave., St. Joseph, MI 49085-2396

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REVISION: REVISION DATE:

617-249-902
ORIGINAL DATE: 01-14-08

769-605-INT FLUORINE/CHLORINE TRAP PACKED FOR FLUORINE REMOVAL FIGURE 6

LECO Corporation, 3000 Lakeview Ave., St. Joseph, MI 49085-2396

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REVISION: REVISION DATE:

617-249-902
ORIGINAL DATE: 01-14-08

FLUORINE TRAP NOTE: Replace the 769-605-INT Fluorine/Chlorine Trap Assembly reagent tube before it becomes completely depleted. The reagent changes color from orange to a darker orange/brown. The reagent must be changed before it becomes to brown in color. 1. Repack the tube as follows (Figure 4). a. Discard depleted reagent and all material in the trap tube except the screens and glass tube. b. Wash and dry the glass tube. c. Place a fresh 601-081 Glass Wool plug, approximately 1-inches (38 mm), at the bottom of the glass tube. d. Add a 502-351 Halogen Scrubber to fill all but the last 1-inches (38 mm) of the wider part of the tube. Tap the sides of the tube to allow settling. e. Fill the remainder of the tube with glass wool and place 769-193 Screens at both ends. NOTE: Insert the filled tube immediately in the stand or plug both ends to avoid contamination by moisture from the atmosphere. Close all reagent bottles tightly.

LECO Corporation, 3000 Lakeview Ave., St. Joseph, MI 49085-2396

ECN 52771

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