MIL-HDBK-17-2F Volume 2, Chapter 6 Glass Fiber Composites

CHAPTER 6 GLASS FIBER COMPOSITES 6.1 INTRODUCTION 6.2 GLASS\EPOXY COMPOSITES

6.2.1 S2-449 43k/SP381 unidirectional tape Material Description: Material: Form: S2-449 17k/PR381 Unidirectional tape, fiber areal weight of 111 g/m , typical cured resin content of 28-33%, typical cured ply thickness of 0.0033 - 0.0037 inches. Autoclave cure; 260 F, 50 psi for two hours
2

Processing:

General Supplier Information: Fiber: S2 glass has enhanced properties in strength, modulus, impact resistance and fatigue when compared to conventional E glass roving. The sizing for these fibers is an epoxy compatible 449 finish. Roving of 17,000 filaments. Typical tensile modulus is 12.5 to 13.0 Msi. Typical tensile strength is 665,000 psi. PR381 is a 250F curing epoxy resin providing properties similar to conventional 350F curing systems. Light tack for up to 30 days at 75F. 220F (dry), 160F (wet)

Matrix:

Maximum Short Term Service Temperature: Typical applications:

Primary and secondary structural applications where improved fatigue and excellent mechanical strength is important such as helicopters and general aviation.

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MIL-HDBK-17-2F Volume 2, Chapter 6 Glass Fiber Composites

6.2.1 S2-449 43k/SP381 unidirectional tape

SGI/Ep 284-UT S2-449/SP 381 Summary

MATERIAL: FORM: FIBER:

S2-449 43.5k/SP 381 unidirectional tape 3M Scotchply SP 381 Uni S29 284 BW 33RC Prepreg Owens Corning S2-449, no twist, no surface treatment, typical 449 glass sizing 280F Tg(wet): 234F MATRIX: 3M PR 381

Tg(dry): PROCESSING:

Tg METHOD:

SRM 18-94, RDA, G onset

Autoclave cure: 26010F, 12020 min., 50 psi

Date of fiber manufacture Date of resin manufacture Date of prepreg manufacture Date of composite manufacture

5/92 - 12/94 1/93 - 12/94 4/93 - 3/95 12/91 - 3/96

Date of testing Date of data submittal Date of analysis

5/93 - 4/95 6/96 2/97

LAMINA PROPERTY SUMMARY 75F/A Tension, 1-axis Tension, 2-axis Tension, 3-axis Compression, 1-axis Compression, 2-axis Compression, 3-axis Shear, 12-plane Shear, 23-plane Shear, 31-plane SBS, 31-plane S--S--S--S--SS-SS-SS-SS-SS-S SS-S SS-S SS-S BM-B SS-S -65F/A SS-S SS-S 180F/A SS-S SS-S 160F/W SS-S SS-S

Classes of data in Strength/Modulus/Poissons Ratio/Strain-to-Failure order: A = A75, a = A55, B = B30, b = B18, M = Mean, I = Interim, S = Screening, - = no data (See Table 1.4.2(c)) Data are also included for F
sbs

conditioned in eight fluids.

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MIL-HDBK-17-2F Volume 2, Chapter 6 Glass Fiber Composites

Nominal Fiber Density Resin Density Composite Density Fiber Areal Weight Fiber Volume Ply Thickness (g/cm ) (g/cm ) (g/cm ) (g/m ) (%) (in)
2 3 3 3

As Submitted

Test Method ASTM C 693 ASTM D 792

2.49 1.216 1.85 284 50 0.009 1.84 - 1.97 283 - 291 47.3 - 56.1 0.0070 - 0.0097

SRM 23B

LAMINATE PROPERTY SUMMARY 73F/A [45/0/ 45] Tension, x-axis Tension, y-axis SS-S SS-S

Classes of data in Strength/Modulus/Poissons Ratio/Strain-to-Failure order: A = A75, a = A55, B = B30, b = B18, M = Mean, I = Interim, S = Screening, - = no data (See Table 1.4.2(c))

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MIL-HDBK-17-2F Volume 2, Chapter 6 Glass Fiber Composites

MATERIAL: RESIN CONTENT: FIBER VOLUME: PLY THICKNESS: TEST METHOD: SRM 4-88 NORMALIZED BY: Temperature (F) Moisture Content (%) Equilibrium at T, RH Source Code Mean Minimum Maximum C.V.(%)
tu F1

S2-449 43.5k/SP 381 unidirectional tape 29-34 wt% 47.3-54.7 % 0.0080-0.0096 in. COMP: DENSITY: VOID CONTENT: 1.84-1.97 g/cm 0-0.07%
3

MODULUS CALCULATION: Chord between 1000 and 6000

Table 6.2.1(a) SGI/Ep 284-UT S2-449/SP 381 Tension, 1-axis [0]5 73/A, -65/A, 180/A B30, Mean, Screening

Specimen thickness and batch fiber areal weight to 50% (0.0090 in. CPT) 73 Ambient 69 Normalized 246 217 287 6.45 198 ANOVA 16.8 2.82 32 6 B30 6.91 6.32 7.54 4.34 32 6 Mean 6.83 6.47 7.22 2.68 Measured 243 228 267 3.89 219 ANOVA 9.78 2.45 -65 Ambient 69 Normalized Measured 236 246 204 218 257 261 7.44 5.19 (1) ANOVA 21.4 16.6 (1) Weibull 252 28.3 180 Ambient 69 Normalized 208 200 220 3.62 (1) ANOVA 8.15 9.69 11 2 Screening 6.62 6.42 6.78 1.62 11 2 Screening 6.70 6.55 7.09 2.48 Measured 211 200 228 4.79 (1) ANOVA 11.7 14.1

B-value Distribution C1 C2 No. Specimens No. Batches Data Class Mean Minimum Maximum C.V.(%) No. Specimens No. Batches Data Class Mean No. Specimens No. Batches Data Class Mean Minimum Maximum C.V.(%)

(ksi)

t E1

11 2 Screening 6.93 7.24 6.41 6.91 7.24 7.53 3.03 3.26 11 2 Screening

(Msi)

t 12

35600 33400 38300 3.83 32400 ANOVA 1400 2.28 32 6 B30

34100 29500 36700 6.23 (1) ANOVA 2440 13.9 11 2 Screening

31500 30000 33800 4.21 (1) ANOVA 1390 7.11 11 2 Screening

tu 1

B-value Distribution C1 C2 No. Specimens No. Batches Data Class

()

(1) Basis values are presented only for A and B data classes.

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MIL-HDBK-17-2F Volume 2, Chapter 6 Glass Fiber Composites

MATERIAL: RESIN CONTENT: FIBER VOLUME: PLY THICKNESS: TEST METHOD: SRM 4-88 NORMALIZED BY: Temperature (F) Moisture Content (%) Equilibrium at T, RH Source Code Mean Minimum Maximum C.V.(%)
tu F1

S2-449 43.5k/SP 381 unidirectional tape 32-33 wt% 49.3-51.1 % 0.0088-0.0092 in. COMP: DENSITY: VOID CONTENT: 1.89-1.97 g/cm 0-0.07%
3

MODULUS CALCULATION: Chord between 1000 and 6000

Table 6.2.1(b) SGI/Ep 284-UT S2-449/SP 381 Tension, 1-axis [0]5 160/W Screening

Specimen thickness and batch fiber areal weight to 50% (0.0090 in. CPT) 160 Wet (2) 69 Normalized Measured 113 115 105 106 119 120 3.90 3.22 (1) Weibull 115 32.6 13 2 Screening 6.86 6.52 7.25 3.19 13 2 Screening 6.95 6.71 7.16 2.06 (1) Weibull 116 40.5

Normalized

Measured

Normalized

Measured

B-value Distribution C1 C2 No. Specimens No. Batches Data Class Mean Minimum Maximum C.V.(%) No. Specimens No. Batches Data Class Mean No. Specimens No. Batches Data Class Mean Minimum Maximum C.V.(%)

(ksi)

t E1

(Msi)

t 12

16500 15600 17100 2.76 (1) Weibull 16700 45.9 13 2 Screening

tu 1

B-value Distribution C1 C2 No. Specimens No. Batches Data Class

()

(1) Basis values are presented only for A and B data classes. (2) Conditioned in 160F water for 14 days.

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MIL-HDBK-17-2F Volume 2, Chapter 6 Glass Fiber Composites

MATERIAL: RESIN CONTENT: FIBER VOLUME: PLY THICKNESS: TEST METHOD: SRM 4-88 NORMALIZED BY: Temperature (F) Moisture Content (%) Equilibrium at T, RH Source Code Mean Minimum Maximum C.V.(%)
tu F2

S2-449 43.5k/SP 381 unidirectional tape 31-32 wt% 51.0-53.2 % 0.0081-0.0092 in. COMP: DENSITY: VOID CONTENT: 1.84-1.86 g/cm 0-0.99%
3

MODULUS CALCULATION: Chord between 1000 and 3000 (2) Not normalized 73 Ambient 69 9.0 8.7 9.3 2.3 (1) Weibull 9.1 49 10 2 Screening 1.93 1.85 2.07 3.31 10 2 Screening -65 Ambient 69 9.1 8.3 9.8 4.7 (1) Weibull 9.3 24 11 2 Screening 2.10 1.88 2.31 5.57 11 2 Screening 180 Ambient 69 7.5 7.1 7.6 2.7 (1) Normal 7.5 0.20 6 1 Screening 1.53 1.47 1.59 2.58 6 1 Screening 160 Wet (3) 69 4.2 3.8 4.7 7.5 (1) Weibull 4.3 14 10 2 Screening 1.07 1.00 1.12 3.23 10 2 Screening

Table 6.2.1(c) SGl/Ep 284-UT S2-449/SP 381 Tension, 2-axis [90]10 73/A, -65A, 180/A, 160/W Screening

B-value Distribution C1 C2 No. Specimens No. Batches Data Class Mean Minimum Maximum C.V.(%) No. Specimens No. Batches Data Class Mean No. Specimens No. Batches Data Class Mean Minimum Maximum C.V.(%)

(ksi)

t E2

(Msi)

t 21

4700 4200 5100 4.6 (1) Nonpara. 6 2.1 10 2 Screening

4300 3800 4800 7.2 (1) Weibull 4500 16 11 2 Screening

4900 4600 5100 4.6 (1) Normal 4900 220 6 1 Screening

3900 3400 4300 6.7 (1) Weibull 4000 17 10 2 Screening

tu 2

B-value Distribution C1 C2 No. Specimens No. Batches Data Class

()

(1) Basis values are presented only for A and B data classes. (2) Exception to SRM 4-88. (3) Conditioned in 160F water for 14 days.

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MIL-HDBK-17-2F Volume 2, Chapter 6 Glass Fiber Composites

MATERIAL: RESIN CONTENT: FIBER VOLUME: PLY THICKNESS: TEST METHOD: SRM 1-88 NORMALIZED BY: Temperature (F) Moisture Content (%) Equilibrium at T, RH Source Code Mean Minimum Maximum C.V.(%)

S2-449 43.5k/SP 381 unidirectional tape 28-33 wt% 49.3-56.1 % 0.0080-0.0094 in. COMP: DENSITY: VOID CONTENT: 1.90-1.94 g/cm 0.12-0.50%
3

MODULUS CALCULATION: Chord between 1000 and 3000

Table 6.2.1(d) SGI/Ep 284-UT S2-449/SP 381 Compression, 1-axis [0]5 73/A, -65/A, 180/A Screening

Specimen thickness and batch fiber areal weight to 50% (0.0090 in. CPT) 73 Ambient 69 Normalized 168 141 199 10.4 (1) Weibull 176 10.6 20 2 Screening 6.96 6.71 7.20 2.43 10 2 Screening 7.06 6.67 7.34 2.68 Measured 182 149 215 10.8 (1) Weibull 191 10.5 -65 Ambient 69 Normalized Measured 170 177 153 162 184 196 5.20 5.59 (1) Weibull 174 22.0 (1) ANOVA 10.9 11.3 180 Ambient 69 Normalized 150 137 166 6.70 (1) ANOVA 12.3 16.6 Measured 166 154 179 4.93 (1) Weibull 170 22.2 12 2 Screening 6.95 6.75 7.16 2.22 10 2 Screening

F1cu
(ksi)

B-value Distribution C1 C2 No. Specimens No. Batches Data Class Mean Minimum Maximum C.V.(%) No. Specimens No. Batches Data Class Mean No. Specimens No. Batches Data Class Mean Minimum Maximum C.V.(%)

c E1

14 2 Screening 6.87 7.20 6.75 6.75 7.01 7.68 1.40 4.16 10 2 Screening

6.76 6.54 6.94 1.74

(Msi)

c 12

cu 1

B-value Distribution C1 C2 No. Specimens No. Batches Data Class

()

(1) Basis values are presented only for A and B data classes.

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MIL-HDBK-17-2F Volume 2, Chapter 6 Glass Fiber Composites

MATERIAL: RESIN CONTENT: FIBER VOLUME: PLY THICKNESS: TEST METHOD: SRM 1-88 NORMALIZED BY: Temperature (F) Moisture Content (%) Equilibrium at T, RH Source Code Mean Minimum Maximum C.V.(%)

S2-449 43.5k/SP 381 unidirectional tape 28-33 wt% 49.3-56.1 % 0.0082-0.0090 in. COMP: DENSITY: VOID CONTENT: 1.90-1.94 g/cm 0.12-0.50%
3

MODULUS CALCULATION: Chord between 1000 and 3000

Table 6.2.1(e) SGI/Ep 284-UT S2-449/SP 381 Compression, 1-axis [0]5 160/W Screening

Specimen thickness and batch fiber areal weight to 50% (0.0090 in. CPT) 160 Wet (2) 69 Normalized Measured 139 146 130 131 146 157 3.48 5.27 (1) Weibull 141 37.4 10 2 Screening 6.92 6.69 7.08 2.11 10 2 Screening 7.16 6.85 7.43 2.83 (1) Weibull 149 22.6

Normalized

Measured

Normalized

Measured

F1cu
(ksi)

B-value Distribution C1 C2 No. Specimens No. Batches Data Class Mean Minimum Maximum C.V.(%) No. Specimens No. Batches Data Class Mean No. Specimens No. Batches Data Class Mean Minimum Maximum C.V.(%)

c E1

(Msi)

c 12

cu 1

B-value Distribution C1 C2 No. Specimens No. Batches Data Class

()

(1) Basis values are presented only for A and B data classes. (2) Conditioned in 160F water for 14 days.

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MIL-HDBK-17-2F Volume 2, Chapter 6 Glass Fiber Composites

MATERIAL: RESIN CONTENT: FIBER VOLUME: PLY THICKNESS: TEST METHOD: SRM 7-88 NORMALIZED BY: Temperature (F) Moisture Content (%) Equilibrium at T, RH Source Code Mean Minimum Maximum C.V.(%)
su F12

S2-449 43.5k/SP 381 unidirectional tape 29-32 wt% 51.1-54.5 % 0.0081-0.0090 in. COMP: DENSITY: VOID CONTENT: 1.88-1.94 g/cm 0.21-0.60%
3

MODULUS CALCULATION:

Table 6.2.1(f) SGl/Ep 284-UT S2-449/SP 381 Shear, 12-plane [45]2S 73/A, -65A, 180/A, 160/W Screening

Chord between 500 and 3000 , axial Not normalized 73 Ambient 69 14.3 13.2 14.7 3.52 (1) Nonpara. 6 2.14 10 2 Screening 0.689 0.648 0.729 3.62 9 2 Screening -65 Ambient 69 13.6 12.9 14.5 3.77 (1) Normal 13.6 0.515 9 2 Screening 0.881 0.837 0.952 5.06 6 2 Screening 180 Ambient 69 11.8 10.8 12.3 3.66 (1) Weibull 12.0 38.4 10 2 Screening 0.555 0.541 0.578 2.26 10 2 Screening 160 Wet (2) 69 9.5 9.0 9.8 2.9 (1) Weibull 9.6 44 12 2 Screening 0.470 0.455 0.480 1.76 10 2 Screening

B-value Distribution C1 C2 No. Specimens No. Batches Data Class Mean Minimum Maximum C.V.(%) No. Specimens No. Batches Data Class

(ksi)

G12
(Msi)

(1) Basis values are presented only for A and B data classes. (2) Conditioned in 160F water for 14 days.

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MIL-HDBK-17-2F Volume 2, Chapter 6 Glass Fiber Composites

MATERIAL: RESIN CONTENT: FIBER VOLUME: PLY THICKNESS: TEST METHOD: SRM 8-88 NORMALIZED BY: Temperature (F) Moisture Content (%) Equilibrium at T, RH Source Code Mean Minimum Maximum C.V.(%) B-value Distribution C1 C2

S2-449 43.5k/SP 381 unidirectional tape 30-34 wt% 47.6-53.1 % 0.0070-0.0092 in. COMP: DENSITY: VOID CONTENT: 1.84-1.94 g/cm 0.0-0.64%
3

MODULUS CALCULATION:

Table 6.2.1(g) SGl/Ep 284-UT S2-449/SP 381 SBS, 31-plane [0]12 73/A, -65A, 180/A, 160/W Screening

Not normalized 73 Ambient 69 12.4 11.6 13.2 4.16 (1) ANOVA 0.573 3.85 25 4 Screening -65 Ambient 69 14.6 13.9 15.6 3.32 (1) Normal 14.6 0.485 14 2 Screening 180 Ambient 69 8.7 8.2 9.0 2.9 (1) ANOVA 0.31 18 14 2 Screening 160 Wet (2) 69 7.2 7.0 7.4 1.7 (1) Weibull 7.3 67 13 2 Screening

sbs F31

(ksi)

No. Specimens No. Batches Data Class

(1) Short beam strength test data are approved for Screening Data Class only. (2) Conditioned in 160F water for 14 days.

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MIL-HDBK-17-2F Volume 2, Chapter 6 Glass Fiber Composites

MATERIAL: RESIN CONTENT: FIBER VOLUME: PLY THICKNESS: TEST METHOD: SRM 8-88 NORMALIZED BY: Temperature (F) Moisture Content (%) Equilibrium at T, RH Source Code Mean Minimum Maximum C.V.(%)
sbs F31

S2-449 43.5k/SP 381 unidirectional tape 30 wt% 52.9-53.1 % 0.00792-0.00925 in. COMP: DENSITY: VOID CONTENT: 1.93-1.94 g/cm 0.0-0.64%
3

MODULUS CALCULATION:

Table 6.2.1(h) SGl/Ep 284-UT S2-449/SP 381 SBS, 31-plane [0]12 73/Fluids Screening

Not normalized 73 (2) 69 11.8 11.0 12.3 3.49 (1) Weibull 11.9 34.7 14 2 Screening 73 (3) 69 12.3 11.8 13.0 2.87 (1) Normal 12.4 0.355 14 2 Screening 73 (4) 69 11.6 9.40 12.8 8.23 (1) ANOVA 1.07 12.2 14 2 Screening 73 (5) 69 11.9 11.4 12.6 3.17 (1) Normal 11.9 0.376 14 2 Screening

B-value Distribution C1 C2 No. Specimens No. Batches Data Class

(ksi)

(1) Short beam strength test data are approved for Screening Data Class only. (2) Conditioned in MIL-A-8243 Anti-Icing Fluid at 32F for 30 days. (3) Conditioned in MIL-H-83282 hydraulic Fluid at 160F for 90 days. MIL-H-83282 was converted to MIL-PRF-83282 on September 30, 1997. (4) Conditioned in MIL-H-5606 hydraulic fluid at 160F for 90 days. (5) Conditioned in MIL-T-5624 fuel at 75F for 90 days. MIL-T-5624 was converted to MIL-PRF-5624 on November 22, 1996.

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MIL-HDBK-17-2F Volume 2, Chapter 6 Glass Fiber Composites

MATERIAL: RESIN CONTENT: FIBER VOLUME: PLY THICKNESS: TEST METHOD: SRM 8-88 NORMALIZED BY: Temperature (F) Moisture Content (%) Equilibrium at T, RH Source Code Mean Minimum Maximum C.V.(%)
sbs F31

S2-449 43.5k/SP 381 unidirectional tape 30 wt% 52.9-53.1 % 0.00758-0.00933 in. COMP: DENSITY: VOID CONTENT: 193-1.94 g/cm 0.0-0.64%
3

MODULUS CALCULATION:

Table 6.2.1(i) SGl/Ep 284-UT S2-449/SP 381 SBS, 31-plane [0]12 73/Fluids Screening

Not normalized 73 (2) 69 11.8 11.1 12.6 3.47 (1) Weibull 12.0 30.7 14 2 Screening 73 (3) 69 12.1 10.9 12.6 3.84 (1) Weibull 12.3 39.5 14 2 Screening 73 (4) 69 11.7 10.6 12.3 4.02 (1) Weibull 11.9 37.2 13 2 Screening 73 (5) 69 11.8 11.3 12.3 2.91 (1) ANOVA 0.386 12.6 14 2 Screening

B-value Distribution C1 C2 No. Specimens No. Batches Data Class

(ksi)

(1) Short beam strength test data are approved for Screening Data Class only. (2) Conditioned in MIL-L-23699 lubricating oil at 160F for 90 days. MIL-L-23699 was converted to MIL-PRF-23699 on May 21, 1997. (3) Conditioned in MIL-L-7808 lubricating oil at 160F for 90 days. MIL-L-7808 was converted to MIL-PRF-7808 on May 2, 1997. (4) Conditioned in MIL-C-87936 cleaning fluid at 75F for 7 days. MIL-C-87936 was canceled on March 1, 1995 and replaced with MIL-C-87937. MIL-C-87937 was converted to MIL-PRF-87937 on August 14, 1997. (5) Conditioned in ASTM D 740 methyl ethyl ketone (MEK) at 75F for 7 days.

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MIL-HDBK-17-2F Volume 2, Chapter 6 Glass Fiber Composites

MATERIAL: RESIN CONTENT: FIBER VOLUME: PLY THICKNESS: TEST METHOD: SRM 4-88 NORMALIZED BY: Temperature (F) Moisture Content (%) Equilibrium at T, RH Source Code Mean Minimum Maximum C.V.(%)
tu Fx

S2-449 43.5k/SP 381 unidirectional tape 30-31wt% 51.6-53.5 % 0.0086-0.0089 in. COMP: DENSITY: VOID CONTENT: 1.92-1.94 g/cm 0-0.50%
3

MODULUS CALCULATION: Chord between 1000 and 3000

Table 6.2.1(j) SGI/Ep 284-UT S2-449/SP 381 Tension, x-axis [45/0/45]S 73/A Screening

Specimen thickness and batch fiber areal weight to 50% (0.0090 in. CPT) 73 Ambient 69 Normalized 69.5 66.7 71.3 2.18 (1) ANOVA 1.74 13.7 10 2 Screening 2.87 2.78 2.96 2.21 10 2 Screening 3.01 2.94 3.11 1.58 Measured 72.9 71.4 75.6 1.67 (1) Normal 72.9 1.22 Normalized Measured Normalized Measured

B-value Distribution C1 C2 No. Specimens No. Batches Data Class Mean Minimum Maximum C.V.(%) No. Specimens No. Batches Data Class Mean No. Specimens No. Batches Data Class Mean Minimum Maximum C.V.(%)

(ksi)

t Ex

(Msi)

t xy

24200 23600 24900 1.69 (1) Weibull 24400 65.4 10 2 Screening

tu x
()

B-value Distribution C1 C2 No. Specimens No. Batches Data Class

(1) Basis values are presented only for A and B data classes.

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MIL-HDBK-17-2F Volume 2, Chapter 6 Glass Fiber Composites

MATERIAL: RESIN CONTENT: FIBER VOLUME: PLY THICKNESS: TEST METHOD: SRM 4-88 NORMALIZED BY: Temperature (F) Moisture Content (%) Equilibrium at T, RH Source Code Mean Minimum Maximum C.V.(%)
tu Fy

S2-449 43.5k/SP 381 unidirectional tape 30-31 wt% 51.6-53.5 % 0.0083-0.0090 in. COMP: DENSITY: VOID CONTENT: 1.92-1.94 g/cm 0-0.50%
3

MODULUS CALCULATION: Chord between 1000 and 3000

Table 6.2.1(k) SGI/Ep 284-UT S2-449/SP 381 Tension, y-axis [45/90/45]S 73/A Screening

Specimen thickness and batch fiber areal weight to 50% (0.0090 in. CPT) 73 Ambient 69 Normalized 24.9 23.9 25.9 2.29 (1) Weibull 25.1 47.1 10 2 Screening 2.15 2.10 2.20 1.33 10 2 Screening 2.26 2.18 2.39 3.50 Measured 26.2 24.7 27.3 2.94 (1) Weibull 26.5 42.2 Normalized Measured Normalized Measured

B-value Distribution C1 C2 No. Specimens No. Batches Data Class Mean Minimum Maximum C.V.(%) No. Specimens No. Batches Data Class Mean No. Specimens No. Batches Data Class Mean Minimum Maximum C.V.(%)

(ksi)

Et y
(Msi)

t yx

11600 10900 12000 2.65 (1) Weibull 11700 49.8 10 2 Screening

tu y
()

B-value Distribution C1 C2 No. Specimens No. Batches Data Class

(1) Basis values are presented only for A and B data classes.

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MIL-HDBK-17-2F Volume 2, Chapter 6 Glass Fiber Composites

6.2.2 S2-449 17k/SP 381 unidirectional tape Material Description: Material: Form: S2-449 43.5k/3M PR381 Unidirectional tape, fiber areal weight of 284 g/m , typical cured resin content of 28-33%, typical cured ply thickness of 0.0081 - 0.009 inches. Autoclave cure; 260 F, 50 psi for two hours
2

Processing:

General Supplier Information: Fiber: S2 glass has enhanced properties in strength, modulus impact resistance and fatigue when compared to conventional E glass roving. The sizing for these fibers is an epoxy compatible 449 finish material. Rovings of 43,500 filaments. Typical tensile modulus is 12.5 to 13.0 Msi. Typical tensile strength is 665,000 psi. PR381 is a 250F curing epoxy resin providing properties similar to conventional 350F curing systems. Light tack for up to 30 days at 75F. 220F (dry), 160F (wet)

Matrix:

Maximum Short Term Service Temperature: Typical applications:

Primary and secondary structural applications where improved fatigue and excellent mechanical strength is important such as helicopters and general aviation.

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MIL-HDBK-17-2F Volume 2, Chapter 6 Glass Fiber Composites 6.2.2 S2-449 17k/SP 381 unidirectional tape
SGI/Ep 111-UT S2-449/SP 381 Summary

MATERIAL: FORM: FIBER:

S2-449 17k/SP 381 unidirectional tape 3M Scotchply SP 381 Uni S29 111BW 33 RC Owens Corning S2-449, no twist, no surface treatment, typical 449 glass sizing 291F Tg(wet): 234F MATRIX: 3M SP 381

Tg(dry): PROCESSING:

Tg METHOD:

SRM 18, RDA, G peak

Autoclave cure: 26010F, 12020 min., 50 psi

Date of fiber manufacture Date of resin manufacture Date of prepreg manufacture Date of composite manufacture

8/91 - 12/94 11/91 - 5/95 11/91 - 2/96 12/91 - 3/96

Date of testing Date of data submittal Date of analysis

6/93 - 4/96 6/96 2/97

LAMINA PROPERTY SUMMARY 73F/A Tension, 1-axis Tension, 2-axis Tension, 3-axis Compression, 1-axis Compression, 2-axis Compression, 3-axis Shear, 12-plane Shear, 23-plane Shear, 31-plane SBS, 31-plane S--S--S--S--IS-IS-IS-SS-SS-S SS-S SS-S SS-S bM-b SS-S -65F/A SS-S SS-S 180F/A SS-S SS-S 160F/W SS-S SS-S

Classes of data in Strength/Modulus/Poissons Ratio/Strain-to-Failure order: A = A75, a = A55, B = B30, b = B18, M = Mean, I = Interim, S = Screening, - = no data (See Table 1.4.2(c)) Data are also included for Fsbs conditioned in eight fluids.

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MIL-HDBK-17-2F Volume 2, Chapter 6 Glass Fiber Composites

Nominal Fiber Density Resin Density Composite Density Fiber Areal Weight Fiber Volume Ply Thickness (g/cm ) (g/cm ) (g/cm ) (g/m ) (%) (in)
2 3 3 3

As Submitted

Test Method ASTM C 693 ASTM D 792

2.49 1.216 1.85 111 50 0.0035 1.82 - 1.94 111 - 113 47.6 - 55.2 0.00303 - 0.00375

SRM 23B

LAMINATE PROPERTY SUMMARY 73F/A [45/0/ 45] Tension, x-axis Tension, y-axis SS-S SS-S

Classes of data in Strength/Modulus/Poissons Ratio/Strain-to-Failure order: A = A75, a = A55, B = B30, b = B18, M = Mean, I = Interim, S = Screening, - = no data (See Table 1.4.2(c))

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MIL-HDBK-17-2F Volume 2, Chapter 6 Glass Fiber Composites

MATERIAL: RESIN CONTENT: FIBER VOLUME: PLY THICKNESS: TEST METHOD: SRM 4-88 NORMALIZED BY: Temperature (F) Moisture Content (%) Equilibrium at T, RH Source Code Mean Minimum Maximum C.V.(%)
tu F1

S2-449 17k/SP 381 unidirectional tape 29-36 wt% 47.6-54.0 % 0.0032-0.0038 in. COMP: DENSITY: VOID CONTENT: 1.85-1.93 g/cm 0.0-0.17%
3

MODULUS CALCULATION: Chord between 1000 and 6000

Table 6.2.2(a) SGI/Ep 111-UT S2-449/SP 381 Tension, 1-axis [0]12 73/A, -65/A, 180/A B18, Mean, Interim, Screening

Specimen thickness and batch fiber areal weight to 50% (0.0035 in. CPT) 73 Ambient 70 Normalized 255 243 277 3.40 238 Normal 255 8.65 21 4 B18 6.93 6.61 7.18 2.29 21 4 Mean 6.75 6.26 7.16 4.37 7.01 6.70 7.31 2.98 11 2 Screening Measured 248 228 274 5.07 (2) ANOVA 13.6 3.53 Normalized 267 233 287 6.52 (1) Weibull 274 21.3 11 2 Screening 7.19 6.98 7.49 2.19 6.73 6.50 7.09 2.80 11 2 Screening -65 Ambient 70 Measured 274 251 302 5.96 (1) Weibull 281 18.1 Normalized 225 218 237 3.13 (1) Weibull 228 32.9 11 2 Screening 6.73 6.50 7.09 2.95 180 Ambient 70 Measured 225 216 234 2.59 (1) Weibull 228 43.2

B-value Distribution C1 C2 No. Specimens No. Batches Data Class Mean Minimum Maximum C.V.(%) No. Specimens No. Batches Data Class Mean No. Specimens No. Batches Data Class Mean Minimum Maximum C.V.(%) B-value Distribution C1 C2 No. Specimens No. Batches Data Class

(ksi)

t E1

(Msi)

t 1 2

36800 34600 38600 3.09 34100 Weibull 37300 37.9 21 4 B18

38000 33500 40900 5.85 (1) Weibull 39000 22.5 11 2 Screening

33400 31000 35100 3.84 (1) Weibull 34000 34.9 11 2 Screening

tu 1

()

(1) Basis values are presented only for A and B data classes. (2) B-basis values calculated from less than five batches of data using the ANOVA method are not presented.

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MIL-HDBK-17-2F Volume 2, Chapter 6 Glass Fiber Composites

MATERIAL: RESIN CONTENT: FIBER VOLUME: PLY THICKNESS: TEST METHOD: SRM 4-88 NORMALIZED BY: Temperature (F) Moisture Content (%) Equilibrium at T, RH Source Code Mean Minimum Maximum C.V.(%)
tu F1

S2-449 17k/SP 381 unidirectional tape 29-31 wt% 49.0-50.1 % 0.0034-0.0038 in. COMP: DENSITY: VOID CONTENT: 1.90-1.93 g/cm 0.00%
3

MODULUS CALCULATION: Chord between 1000 and 6000

Table 6.2.2(b) SGI/Ep 111-UT S2-449/SP 381 Tension, 1-axis [0]12 160/W Screening

Specimen thickness and batch fiber areal weight to 50% (0.0035 in. CPT) 160 Wet (2) 70 Normalized Measured 116 113 107 108 123 123 4.34 3.54 (1) Weibull 118 26.8 13 2 Screening 6.84 6.50 7.12 2.57 13 2 Screening 6.71 6.49 6.97 1.99 (1) Normal 113 4.01

Normalized

Measured

Normalized

Measured

B-value Distribution C1 C2 No. Specimens No. Batches Data Class Mean Minimum Maximum C.V.(%) No. Specimens No. Batches Data Class Mean No. Specimens No. Batches Data Class Mean Minimum Maximum C.V.(%) B-value Distribution C1 C2 No. Specimens No. Batches Data Class

(ksi)

t E1

(Msi)

t 1 2

16900 15800 18100 3.90 (1) Weibull 17200 28.7 13 2 Screening

tu 1

()

(1) Basis values are presented only for A and B data classes. (2) Conditioned in 160F water for 14 days.

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MIL-HDBK-17-2F Volume 2, Chapter 6 Glass Fiber Composites

MATERIAL: RESIN CONTENT: FIBER VOLUME: PLY THICKNESS: TEST METHOD: SRM 4-88 NORMALIZED BY: Temperature (F) Moisture Content (%) Equilibrium at T, RH Source Code Mean Minimum Maximum C.V.(%)
tu F2

S2-449 17k/SP 381 unidirectional tape 29-31 wt% 48.8-50.1 % 0.0033-0.0036 in. COMP: DENSITY: VOID CONTENT: 1.88-1.92 g/cm 0.0%
3

MODULUS CALCULATION: Chord between 1000 and 3000 (2) Not normalized 73 Ambient 70 8.7 8.1 9.0 3.9 (1) Normal 8.7 0.34 5 1 Screening 1.84 1.82 1.91 2.05 5 1 Screening 3 1 Screening 2.11 2.06 2.15 2.14 3 1 Screening -65 Ambient 70 10.0 9.6 10.3 3.6 (4) 180 Ambient 70 6.4 5.9 6.7 4.0 (1) Normal 6.4 0.26 8 2 Screening 1.42 1.34 1.55 6.43 4 1 Screening 160 Wet (3) 70 3.6 3.1 3.9 9.0 (1) Normal 3.6 0.32 5 1 Screening 1.10 1.05 1.16 4.59 5 1 Screening

Table 6.2.2(c) SGI/Ep 111-UT S2-449/SP 381 Tension, 2-axis [90]20 73/A, -65/A, 180/A, 160/W Screening

B-value Distribution C1 C2 No. Specimens No. Batches Data Class Mean Minimum Maximum C.V.(%) No. Specimens No. Batches Data Class Mean No. Specimens No. Batches Data Class Mean Minimum Maximum C.V.(%) B-value Distribution C1 C2 No. Specimens No. Batches Data Class

(ksi)

t E2

(Msi)

t 21

4700 4400 4900 4.26 (1) Normal 4700 200.0 5 1 Screening

4730 4500 5000 5.32 (4)

4450 4200 4800 5.95 (1) Normal 4450 265

3280 3000 3600 8.18 (1) Normal 3280 268 5 1 Screening

tu 2

()

3 1 Screening

4 1 Screening

(1) (2) (3) (4)

Basis values are presented only for A and B data classes. Exception to SRM 4-88. Conditioned in 160F water for 14 days. The statistical analysis is not completed for less than four specimens.

6-20

MIL-HDBK-17-2F Volume 2, Chapter 6 Glass Fiber Composites

MATERIAL: RESIN CONTENT: FIBER VOLUME: PLY THICKNESS: TEST METHOD: SRM 1-88 NORMALIZED BY: Temperature (F) Moisture Content (%) Equilibrium at T, RH Source Code Mean Minimum Maximum C.V.(%)

S2-449 17k/SP 381 unidirectional tape 28-29 wt% 50.1-54.0 % 0.0032-0.0035 in. COMP: DENSITY: VOID CONTENT: 1.85-1.92 g/cm 0.22-1.53%
3

MODULUS CALCULATION: Chord between 1000 and 3000

Table 6.2.2(d) SGI/Ep 111-UT S2-449/SP 381 Compression, 1-axis [0]12 73/A, -65/A, 180/A Screening

Specimen thickness and batch fiber areal weight to 50% (0.0035 in. CPT) 73 Ambient 70 Normalized 172 145 193 8.09 (1) Weibull 178 15.2 13 2 Screening 6.86 6.43 7.24 3.79 10 2 Screening 7.14 6.81 7.52 3.39 6.91 6.63 7.10 2.35 10 2 Screening Measured 178 142 198 9.35 (1) Weibull 185 14.7 Normalized 166 147 184 6.62 (1) Weibull 171 17.7 13 2 Screening 7.19 6.96 7.49 2.22 6.97 6.63 7.24 3.18 10 2 Screening -65 Ambient 70 Measured 177 152 198 7.46 (1) Weibull 183 16.0 Normalized 165 146 185 6.81 (1) Weibull 170 16.6 12 2 Screening 7.47 7.19 7.59 1.85 180 Ambient 70 Measured 175 155 196 7.28 (1) Weibull 181 16.4

F1cu
(ksi)

B-value Distribution C1 C2 No. Specimens No. Batches Data Class Mean Minimum Maximum C.V.(%) No. Specimens No. Batches Data Class Mean No. Specimens No. Batches Data Class Mean Minimum Maximum C.V.(%) B-value Distribution C1 C2 No. Specimens No. Batches Data Class

c E1

(Msi)

c 1 2

cu 1

()

(1) Basis values are presented only for A and B data classes.

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MIL-HDBK-17-2F Volume 2, Chapter 6 Glass Fiber Composites

MATERIAL: RESIN CONTENT: FIBER VOLUME: PLY THICKNESS: TEST METHOD: SRM 1-88 NORMALIZED BY: Temperature (F) Moisture Content (%) Equilibrium at T, RH Source Code Mean Minimum Maximum C.V.(%)

S2-449 17k/SP 381 unidirectional tape 28-29 wt% 50.1-54.0 % 0.0033-0.0037 in. COMP: DENSITY: VOID CONTENT: 1.85-1.92 g/cm 0-1.15%
3

MODULUS CALCULATION: Chord between 1000 and 3000

Table 6.2.2(e) SGI/Ep 111-UT S2-449/SP 381 Compression, 1-axis [0]12 160/W Screening

Specimen thickness and batch fiber areal weight to 50% (0.0035 in. CPT) 160 Wet (2) 70 Normalized Measured 135 137 124 123 143 146 3.51 4.83 (1) Nonpara. 6 2.14 10 2 Screening 6.96 6.69 7.24 2.44 10 2 Screening 6.97 6.75 7.23 2.16 (1) ANOVA 8.02 16.7

Normalized

Measured

Normalized

Measured

F1cu
(ksi)

B-value Distribution C1 C2 No. Specimens No. Batches Data Class Mean Minimum Maximum C.V.(%) No. Specimens No. Batches Data Class Mean No. Specimens No. Batches Data Class Mean Minimum Maximum C.V.(%) B-value Distribution C1 C2 No. Specimens No. Batches Data Class

c E1

(Msi)

c 1 2

cu 1

()

(1) Basis values are presented only for A and B data classes. (2) Conditioned in 160F water for 14 days.

6-22

MIL-HDBK-17-2F Volume 2, Chapter 6 Glass Fiber Composites

MATERIAL: RESIN CONTENT: FIBER VOLUME: PLY THICKNESS:

S2-449 17k/SP 381 unidirectional tape 29-32 wt% 48.8-51.6 % 0.0032-0.0037 in. COMP: DENSITY: VOID CONTENT: 1.85-1.89 g/cm 0-0.74%
3

TEST METHOD: SRM 7-88 NORMALIZED BY: Temperature (F) Moisture Content (%) Equilibrium at T, RH Source Code Mean Minimum Maximum C.V.(%)
su F12

MODULUS CALCULATION: Chord between 1000 and 3000 , axial Not normalized 73 Ambient 70 19.7 18.9 20.3 2.18 (1) Weibull 20.0 61.1 16 3 Interim 0.681 0.627 0.745 5.29 9 2 Screening -65 Ambient 70 25.7 24.7 26.2 1.85 (1) Weibull 25.9 73.2 16 3 Interim 0.808 0.772 0.850 3.32 9 2 Screening 180 Ambient 70 15.0 14.0 15.5 2.67 (1) ANOVA 0.452 4.88 16 3 Interim 0.539 0.513 0.583 4.06 10 2 Screening 160 Wet (2) 70 11.1 10.7 11.9 3.43 (1) ANOVA 0.442 5.83 14 3 Screening 0.467 0.440 0.490 2.96 10 2 Screening

Table 6.2.2(f) SGI/Ep 111-UT S2-449/SP 381 Shear, 12-plane [45]5S 73/A, -65/A,180/A, 160/W Interim, Screening

B-value Distribution C1 C2 No. Specimens No. Batches Data Class Mean Minimum Maximum C.V.(%) No. Specimens No. Batches Data Class

(ksi)

G12
(Msi)

(1) Basis values are presented only for A and B data classes. (2) Conditioned in 160F water for 14 days.

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MIL-HDBK-17-2F Volume 2, Chapter 6 Glass Fiber Composites

MATERIAL: RESIN CONTENT: FIBER VOLUME: PLY THICKNESS:

S2-449 17k/SP 381 unidirectional tape 27-35 wt% 48.3-55.2 % 0.0029-0.0035 in. COMP: DENSITY: VOID CONTENT: 1.85-1.94 g/cm 0.0-0.12%
3

TEST METHOD: SRM 8-88 NORMALIZED BY: Temperature (F) Moisture Content (%) Equilibrium at T, RH Source Code Mean Minimum Maximum C.V.(%)
sbs F31

MODULUS CALCULATION:

Table 6.2.2(g) SGI/Ep 111-UT S2-449/SP 381 SBS, 31-plane [0]30 73/A, -65/A, 180/A, 160/W Screening

Not normalized 73 Ambient 70 12.6 11.6 13.7 4.64 (1) ANOVA 0.613 2.77 32 5 Screening -65 Ambient 70 14.9 13.1 16.8 6.89 (1) Weibull 15.4 17.1 14 2 Screening 180 Ambient 70 9.5 9.1 9.8 2.2 (1) Normal 9.5 0.21 17 3 Screening 160 Wet (2) 70 7.6 7.0 8.7 7.1 (1) ANOVA 0.63 5.2 18 3 Screening

B-value Distribution C1 C2 No. Specimens No. Batches Data Class

(ksi)

(1) Short beam strength test data are approved for Screening Data Class only. (2) Conditioned in 160F water for 14 days.

6-24

MIL-HDBK-17-2F Volume 2, Chapter 6 Glass Fiber Composites

MATERIAL: RESIN CONTENT: FIBER VOLUME: PLY THICKNESS: TEST METHOD: SRM 8-88 NORMALIZED BY: Temperature (F) Moisture Content (%) Equilibrium at T, RH Source Code Mean Minimum Maximum C.V.(%) B-value Distribution C1 C2

S2-449 17k/SP 381 unidirectional tape 27-30 wt% 50.1-51.6 % 0.0033-0.0037 in. COMP: DENSITY: VOID CONTENT: 1.92-1.94 g/cm 0.0-0.12%
3

MODULUS CALCULATION:

Table 6.2.2(h) SGI/Ep 111-UT S2-449/SP 381 SBS, 31-plane [0]30 73/Fluids Screening

Not normalized 73 (2) 70 12.0 10.7 13.0 5.20 (1) Weibull 12.3 24.0 12 2 Screening 73 (3) 70 12.4 10.9 13.4 5.81 (1) Weibull 12.7 21.9 14 2 Screening 73 (4) 70 12.6 11.3 13.5 4.44 (1) Weibull 12.9 27.8 14 2 Screening 73 (5) 70 12.1 10.5 12.8 5.22 (1) ANOVA 0.683 9.78 14 2 Screening

sbs F31

(ksi)

No. Specimens No. Batches Data Class

(1) Short beam strength test data are approved for Screening Data Class only. (2) Conditioned in MIL-A-8243 Anti-Icing Fluid at 32F for 30 days. (3) Conditioned in MIL-H-83282 hydraulic fluid at 160F for 90 days. MIL-H-83282 was converted to MIL-PRF-83282 on September 30, 1997. (4) Conditioned in MIL-H-5606 hydraulic fluid at 160F for 90 days. (5) Conditioned in MIL-T-5624 fuel at 75F for 90 days. MIL-T-5624 was converted to MIL-PRF-5624 on November 22, 1996.

6-25

MIL-HDBK-17-2F Volume 2, Chapter 6 Glass Fiber Composites

MATERIAL: RESIN CONTENT: FIBER VOLUME: PLY THICKNESS: TEST METHOD: SRM 8-88 NORMALIZED BY: Temperature (F) Moisture Content (%) Equilibrium at T, RH Source Code Mean Minimum Maximum C.V.(%)
sbs F31

S2-449 17k/SP 381 unidirectional tape 27-30 wt% 50.1-51.6 % 0.0033-0.0037 in. COMP: DENSITY: VOID CONTENT: 1.92-1.94 g/cm 0.0-0.12%
3

MODULUS CALCULATION:

Table 6.2.2(i) SGI/Ep 111-UT S2-449/SP 381 SBS, 31-plane [0]30 73/Fluids Screening

Not normalized 73 (2) 70 12.6 10.3 13.5 6.49 (1) Weibull 12.9 23.1 14 2 Screening 73 (3) 70 12.6 11.6 13.6 3.86 (1) Weibull 12.8 26.6 14 2 Screening 73 (4) 70 11.8 11.1 12.4 3.79 (1) Weibull 12.0 32.8 13 2 Screening 73 (5) 70 11.9 10.2 12.9 6.19 (1) Weibull 12.2 21.5 13 2 Screening

B-value Distribution C1 C2 No. Specimens No. Batches Data Class

(ksi)

(1) Short beam strength test data are approved for Screening Data Class only. (2) Conditioned in MIL-L-23699 lubricating oil at 160F for 90 days. MIL-L-23699 was converted to MIL-PRF-23699 on May 21, 1997. (3) Conditioned in MIL-L-7808 lubricating oil at 160F for 90 days. MIL-L-7808 was converted to MIL-PRF-7808 on May 2, 1997. (4) Conditioned in MIL-C-87936 cleaning fluid at 75F for 7 days. MIL-C-87936 was canceled on March 1, 1995 and replaced with MIL-C-87937. MIL-C-87937 was converted to MIL-PRF-87937 on August 14, 1997. (5) Conditioned in ASTM D 740 methyl ethyl ketone (MEK) at 75F for 7 days.

6-26

MIL-HDBK-17-2F Volume 2, Chapter 6 Glass Fiber Composites

MATERIAL: RESIN CONTENT: FIBER VOLUME: PLY THICKNESS: TEST METHOD: SRM 4-88 NORMALIZED BY: Temperature (F) Moisture Content (%) Equilibrium at T, RH Source Code Mean Minimum Maximum C.V.(%)
tu Fx

S2-449 17k/SP 381 unidirectional tape 29-32 wt% 50.1-51.6 % 0.0034-0.0036 in. COMP: DENSITY: VOID CONTENT: 1.88-1.89 g/cm 0.0-0.74%
3

MODULUS CALCULATION: Chord between 1000 and 3000

Table 6.2.2(j) SGI/Ep 111-UT S2-449/SP 381 Tension, x-axis [45/0/45]2S 73/A Screening

Specimen thickness and batch fiber areal weight to 50% (0.0035 in. CPT) 73 Ambient 70 Normalized 69.7 68.1 72.5 1.78 (1) Normal 69.7 1.24 10 2 Screening 2.90 2.80 2.96 1.86 10 2 Screening 2.97 2.85 3.08 2.30 Measured 71.4 69.8 73.9 1.92 (1) Weibull 72.1 55.0 Normalized Measured Normalized Measured

B-value Distribution C1 C2 No. Specimens No. Batches Data Class Mean Minimum Maximum C.V.(%) No. Specimens No. Batches Data Class Mean No. Specimens No. Batches Data Class Mean Minimum Maximum C.V.(%)

(ksi)

t Ex

(Msi)

t xy

24100 23300 25200 2.49 (1) Weibull 24400 40.9 10 2 Screening

tu x
()

B-value Distribution C1 C2 No. Specimens No. Batches Data Class

(1) Basis values are presented only for A and B data classes.

6-27

MIL-HDBK-17-2F Volume 2, Chapter 6 Glass Fiber Composites

MATERIAL: RESIN CONTENT: FIBER VOLUME: PLY THICKNESS: TEST METHOD: SRM 4-88 NORMALIZED BY: Temperature (F) Moisture Content (%) Equilibrium at T, RH Source Code Mean Minimum Maximum C.V.(%)
tu Fy

S2-449 17k/SP 381 unidirectional tape 30-32 wt% 50.1 % 0.0035-0.0036 in. COMP: DENSITY: VOID CONTENT: 1.87-1.88 g/cm 0.0-0.60%
3

MODULUS CALCULATION: Chord between 1000 and 3000

Table 6.2.2(k) SGI/Ep 111-UT S2-449/SP 381 Tension, y-axis [45/90/45]2S 73/A Screening

Specimen thickness and batch fiber areal weight to 50% (0.0035 in. CPT) 73 Ambient 70 Normalized 36.2 35.3 37.1 1.77 (1) ANOVA 0.813 18.6 Measured 36.6 35.8 37.6 1.77 (1) ANOVA 0.755 14.8 Normalized Measured Normalized Measured

B-value Distribution C1 C2 No. Specimens No. Batches Data Class Mean Minimum Maximum C.V.(%) No. Specimens No. Batches Data Class Mean No. Specimens No. Batches Data Class Mean Minimum Maximum C.V.(%)

(ksi)

10 2 Screening 2.21 2.14 2.28 1.88 10 2 Screening 2.24 2.17 2.31 2.01

Et y
(Msi)

t xy

16400 15600 16800 2.40 (1) Weibull 16500 58.7 10 2 Screening

tu y
()

B-value Distribution C1 C2 No. Specimens No. Batches Data Class

(1) Basis values are presented only for A and B data classes.

6-28

MIL-HDBK-17-2F Volume 2, Chapter 6 Glass Fiber Composites

6.2.3 7781G 816/PR381 plain weave fabric Material Description: Material: Form: 7781 E-glass/3M PR381 Fiber areal weight of 300 g/m , typical cured resin content of 32-38%, typical cured ply thickness of 0.009 - 0.0105 inches. Autoclave cure; 260 F, 50 psi for two hours
2

Processing:

General Supplier Information: Fiber: Continuous, E-glass fiber. strength is 500,000 psi. Typical tensile modulus is 10 x 10 psi.
6

Typical tensile

Matrix:

PR381 is a 250F curing epoxy resin providing properties similar to conventional 350F curing systems. Light tack for up to 30 days at 75F. 220F (dry), 160F (wet)

Maximum Short Term Service Temperature: Typical applications:

Aircraft secondary structure, fuselage skins and general industrial applications where improved fatigue and excellent mechanical strengths are required.

6-29

MIL-HDBK-17-2F Volume 2, Chapter 6 Glass Fiber Composites

6.2.3 7781 G-816/PR381 plain weave fabric

MATERIAL: 7781G 816/PR 381 plain weave fabric EGl/Ep 300-PW 7781G/PR 381 FORM: FIBER: 3M SP 381/7781 E-Glass Fabric Prepreg, 57 Yarn Count/in. (Warp), 54 Yarn Count/in. (Fill) Clark-Schwebel 7781 E-glass Fabric, per MATRIX: 3M PR 381 MIL-C-9084C Type VIII B, Yarn DE-75 1/0.0 twist, no surface treatment, 558 Finish 282/F Tg(wet): 225 /F Summary

Tg(ambient): PROCESSING:

Tg METHOD: SRM-18, DMA E knee

Autoclave cure: 260/F, 100 min., 50 psi

Date of fiber manufacture Date of resin manufacture Date of prepreg manufacture Date of composite manufacture

11/92 - 7/95 Date of testing 12/92 - 3/96 Date of data submittal 12/92 - 3/96 Date of analysis 3/93 - 4/96 LAMINA PROPERTY SUMMARY 73/F/A 220/F/A

3/93 - 4/96 6/96 8/97

Tension, 1-axis Tension, 2-axis Tension, 3-axis Compression, 1-axis Compression, 2-axis Compression, 3-axis Shear, 12-plane Shear, 23-plane Shear, 31-plane SBS, 31-plane Flexure

II-I

SS-S

S--I--S---

Classes of data in Strength/Modulus/Poissons Ratio/Strain-to-Failure order: M = Mean, I = Interim, S = Screening, - = no data (See Table 1.4.2(c))

A = A75, a = A55, B = B30, b = B18,

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MIL-HDBK-17-2F Volume 2, Chapter 6 Glass Fiber Composites

Nominal Fiber Density Resin Density Composite Density Fiber Areal Weight Fiber Volume Ply Thickness (g/cm ) (g/cm ) (g/cm ) (g/m ) (%) (in)
2 3 3 3

As Submitted

Test Method ASTM C 693 ASTM D 792

2.6 1.85 300 48 0.0099 1.75 - 2.04 288 - 297 43.0 - 50.9 0.0087 - 0.0104

ASTM D 792 SRM 23B SRM 10

LAMINATE PROPERTY SUMMARY

Classes of data in Strength/Modulus/Poissons Ratio/Strain-to-Failure order: A = A75, a = A55, B = B30, b = B18, M = Mean, I = Interim, S = Screening, - = no data (See Table 1.4.2(c))

6-31

MIL-HDBK-17-2F Volume 2, Chapter 6 Glass Fiber Composites

MATERIAL: RESIN CONTENT: FIBER VOLUME: PLY THICKNESS: TEST METHOD: SRM 4-88 (1) NORMALIZED BY: Temperature(F) Moisture Content(%) Equilibrium at T, RH Source Code Mean Minimum Maximum C.V. (%)
tu F1

7781G 816/PR 381 plain weave fabric 34-36 wt% 43.0-48.4% 0.0091-0.0104 in. COMP. DENSITY: VOID CONTENT: 1.75-1.97 g/cm 3

MODULUS CALCULATION: Chord between 1000 and 6000

Table 6.2.3(a) EGl/Ep 300-PW 7781G/PR 381 Tension, 1-axis [0]5 73/A, 220/A Interim, Screening

Specimen thickness and batch fiber areal weight to 50% (0.0091 in. CPT) 73 Ambient 72 Normalized 74.9 70.4 79.6 3.66 (2) ANOVA 2.90 3.10 16 5 Interim 3.83 3.70 3.97 2.63 15 5 Interim 3.64 3.37 3.96 4.51 Measured 70.9 62.9 77.8 7.07 (2) ANOVA 5.37 3.26 Normalized 71.3 67.0 77.4 4.02 (2) Weibull 72.7 24.9 220 Ambient 72 Measured 67.5 60.5 74.4 5.89 (2) ANOVA 4.22 3.45

B-value Distribution C1 C2 No. Specimens No. Batches Data Class Mean Minimum Maximum C.V. (%) No. Specimens No. Batches Data Class Mean No. Specimens No. Batches Data Class Mean Minimum Maximum C.V. (%)

(ksi)

t E1

13 4 Screening 3.64 3.44 3.45 3.24 3.75 3.77 2.78 5.40 13 4 Screening

(Msi)

t 12

17800 15200 19600 6.23 (2) ANOVA 1310 3.32 15 5 Interim

19600 18400 21100 4.01 (2) Weibull 20000 25.7 13 4 Screening

tu 1

B-value Distribution C1 C2 No. Specimens No. Batches Data Class

()

(1) Three batches were tested according to SRM 4R-94 with modulus calculated as noted above. (2) Basis values are presented only for A and B data classes.

6-32

MIL-HDBK-17-2F Volume 2, Chapter 6 Glass Fiber Composites

MATERIAL: RESIN CONTENT: FIBER VOLUME: PLY THICKNESS: TEST METHOD: SRM 8-88 (1) NORMALIZED BY: Temperature(F) Moisture Content(%) Equilibrium at T, RH Source Code Mean Minimum Maximum C.V. (%)
sbs F13

7781G 816/PR 381 plain weave fabric 34-36 wt% 43.0-50.9% 0.0088-0.0103 in. COMP. DENSITY: 1.76-2.04 g/cm VOID CONTENT: %
3

MODULUS CALCULATION: NA Not normalized 73 Ambient 72 10.4 9.6 11.5 4.8 (2) ANOVA 0.53 3.2 22 5 Screening

Table 6.2.3(b) EGl/Ep 300-PW 7781G/PR 381 SBS, 13-axis [0]5s 73/A Screening

B-value Distribution C1 C2 No. Specimens No. Batches Data Class

(ksi)

(1) Three batches were tested according to SRM 8R-94. (2) Short beam strength test data are approved for Screening Data Class only.

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MIL-HDBK-17-2F Volume 2, Chapter 6 Glass Fiber Composites

MATERIAL: RESIN CONTENT: FIBER VOLUME: PLY THICKNESS: TEST METHOD:

7781G 816/PR 381 plain weave fabric 34-36 wt% 43.4-48.7% 0.0091-0.0103 in. COMP. DENSITY: 1.76-1.97 g/cm VOID CONTENT: %
3

MODULUS CALCULATION: NA

Table 6.2.3(c) EGl/Ep 300-PW 7781G/PR 381 Flexure [0]5s 73/A, 220/A Interim, Screening

ASTM D 790 Method 1 NORMALIZED BY: Temperature(F) Moisture Content(%) Equilibrium at T, RH Source Code Mean Minimum Maximum C.V. (%) B-value Distribution C1 C2 No. Specimens No. Batches Data Class Not normalized 73 Ambient 72 109 94.2 121 7.52 (1) ANOVA 8.92 3.33 21 5 Interim

220 Ambient 72 93.2 83.4 104 8.15 (1) ANOVA 8.45 4.13 14 4 Screening

flex

(ksi)

(1) Basis values are presented only for A and B data classes.

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MIL-HDBK-17-2F Volume 2, Chapter 6 Glass Fiber Composites

6.2.4 E-Glass 7781/EA9396 8-harness satin weave fabric Material Description: Material: Form: E7781/EA9396 Eight harness satin fabric of style 7781, fiber areal weight of 295 g/m , dry fabric impregnated in a wet lay-up process, typical cured resin content of 25.9 to 30.4%, typical cured ply thickness of 0.008 inches. Vacuum Bag cure; 200F, 25 inches Hg, 45 minutes
2

Processing:

General Supplier Information: Fiber: Continuous E-glass fiber woven by Hexcel using F-16 (Volan-A) sizing. Typical tensile 6 modulus is 10 x 10 psi. Typical tensile strength is 500,000 psi. EA9396 is a 200F curing toughened epoxy resin with improved hot/wet properties. 75 minute pot life for 1 lb batch. This resin is a two part, unfilled version of EA 9394. Not determined from available data, but at least 150F.

Matrix:

Maximum Short Term Service Temperature: Typical applications: Aircraft repair

Data Analysis Summary: 1. This material was tested at fiber volumes that may be higher than what are typically used for repair. Data should be substantiated if used at lower fiber volumes. 2. Glass transition temperature (Tg) values were not reported because they were determined on neat resin using a non-standard method. 3. Wet properties are very low because of the glass and sizing combination. 4. Contrary to expectations, the fill tensile strengths and stiffnesses were greater than the warp properties. 5. Most tension failures were under the tabs, but were included since the strengths were consistent with correct failure modes. 6. Variability between batches is high. Documentation does not reveal a reason. 7. High end outliers for the following properties were discarded: a. Transverse tension strain at 72F ambient b. Transverse tension modulus at -65F ambient and 72F wet c. Transverse compression modulus at 72F wet 8. Data are from publicly available report, Reference 4.2.27. 9. Test method dates were assumed from the testing dates rather than obtained from the data source.

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MIL-HDBK-17-2F Volume 2, Chapter 6 Glass Fiber Composites

6.2.4 E-Glass 7781/EA 9396 8-harness satin weave fabric * MATERIAL: FORM: E-Glass 7781/EA 9396 8-harness satin weave fabric Dry E-Glass fabric impregnated with epoxy resin in a wet lay-up impregnation process. Hexcel/Burlington 7781, F-16 Volan A-Type/538 Silane sizing (1) Tg(wet): (1) MATRIX: Dexter-Hysol EA 9396 EGl/Ep 295-8HS E-7781/EA 9396 Summary

FIBER:

Tg(dry):

Tg METHOD:

PROCESSING: Vacuum Bag Cure: 200F, 45 min., 25 in. Hg. (1) See Data Analysis Note #2 in data set description * ALL DOCUMENTATION PRESENTLY REQUIRED WERE NOT SUPPLIED FOR THIS MATERIAL. Date of testing 8/88-10/88 NA 11/88-5/91 Date of data submittal Date of analysis 11/88-5/91 3/98 8/98

Date of fiber manufacture Date of resin manufacture Date of prepreg manufacture Date of composite manufacture

LAMINA PROPERTY SUMMARY 72F/A Tension, 1-axis Tension, 2-axis Tension, 3-axis Compression, 1-axis Compression, 2-axis Compression, 3-axis Shear, 12-plane Shear, 23-plane Shear, 31-plane II-II-II-II-II-II-II-I II-I II-I SS-S II-I II-I SS-S II-I IISI IISS IISS IISI IISI -65F/A 200F/A -65F/W 72F/W IISI ISSI IISI 200F/W

Classes of data in Strength/Modulus/Poissons Ratio/Strain-to-Failure order: A = A75, a = A55, B = B30, b = B18, M = Mean, I = Interim, S = Screening, - = no data (See Table 1.4.2(c))

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MIL-HDBK-17-2F Volume 2, Chapter 6 Glass Fiber Composites

ALL DOCUMENTATION PRESENTLY REQUIRED WERE NOT SUPPLIED FOR THIS MATERIAL. Nominal As Submitted Test Method D 792 1.88-1.96 51.2-56.9 0.0083-0.0087 D 792 D 2584

Fiber Density Resin Density Composite Density Fiber Areal Weight Fiber Volume Ply Thickness

(g/cm ) (g/cm ) (g/cm ) (g/m ) (%) (in)

2 3 3

2.54 1.14 1.91 295 54 0.0085

Nominal composite densities assume void content of 0%. LAMINATE PROPERTY SUMMARY

Classes of data in Strength/Modulus/Poissons Ratio/Strain-to-Failure order: A = A75, a = A55, B = B30, b = B18, M = Mean, I = Interim, S = Screening, - = no data (See Table 1.4.2(c))

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MIL-HDBK-17-2F Volume 2, Chapter 6 Glass Fiber Composites

* ALL DOCUMENTATION PRESENTLY REQUIRED WERE NOT SUPPLIED FOR THIS MATERIAL. Table 6.2.4(a) MATERIAL: E-Glass 7781/EA 9396 8-harness satin weave fabric EGl/Ep 295-8HS 3 E-7781/EA 9396 RESIN CONTENT: 25.9-27.7 wt% COMP: DENSITY: 1.89-1.93 g/cm Tension, 1-axis FIBER VOLUME: 54.1-55.8 % VOID CONTENT: 3.7-5.4% [0f]8 PLY THICKNESS: 0.0085-0.0086 in. 72/A,72/W Interim, Screening TEST METHOD: MODULUS CALCULATION: ASTM D 3039-76 NORMALIZED BY: Temperature (F) Moisture Content (%) Equilibrium at T, RH Source Code Mean Minimum Maximum C.V.(%) B-value Distribution C1 C2 No. Specimens No. Batches Data Class Mean Minimum Maximum C.V.(%)
t E1

Chord between 1000 and 3000 Specimen thickness and batch fiber areal weight to 50% fiber volume (0.0085 in. CPT) 72 Ambient 30 Normalized 48.3 45.5 54.1 4.77 (2) Nonpara. 8 1.54 15 3 Interim 3.39 3.25 3.48 2.18 3.62 3.45 3.77 2.51 3.16 2.97 3.30 2.64 15 3 Interim 0.084 7 3 Screening 5100 4260 5850 8.83 (2) Weibull 5290 13.8 Measured 51.8 48.0 57.9 5.17 (2) Normal 51.8 2.68 72 (1) 140, 95-100 30 Normalized Measured 15.7 16.4 13.4 13.6 17.0 18.3 6.44 7.74 (2) Weibull 16.1 17.8 15 3 Interim 3.30 3.07 3.52 3.93 (2) Weibull 16.9 15.8

Normalized

Measured

tu F1 (ksi)

(Msi)

t 12

No. Specimens No. Batches Data Class Mean No. Specimens No. Batches Data Class Mean Minimum Maximum C.V.(%) B-value Distribution C1 C2

15 3 Interim 0.115 6 3 Screening 17700 16400 21800 7.72 (2) Nonpara. 8 1.54

tu 1

()

No. Specimens 15 15 No. Batches 3 3 Data Class Interim Interim (1) Unknown weight gain (2) Basis values are presented only for A and B data classes. (3) Most failures were under the tabs, but were included since the strengths were consistent with correct failure modes.

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MIL-HDBK-17-2F Volume 2, Chapter 6 Glass Fiber Composites

* ALL DOCUMENTATION PRESENTLY REQUIRED WERE NOT SUPPLIED FOR THIS MATERIAL. Table 6.2.4(b) MATERIAL: E-Glass 7781/EA 9396 8-harness satin weave fabric EGl/Ep 295-8HS 3 E-7781/EA 9396 RESIN CONTENT: 25.9-27.7 wt% COMP: DENSITY: 1.89-1.94 g/cm Tension, 2-axis FIBER VOLUME: 54.0-56.5 % VOID CONTENT: 3.7-5.4 % [0f]8 PLY THICKNESS: 0.0085-0.0086 in. 72/A, -65/A, 200/A Interim, Screening TEST METHOD: MODULUS CALCULATION: ASTM D 3039-76 NORMALIZED BY: Temperature (F) Moisture Content (%) Equilibrium at T, RH Source Code Mean Minimum Maximum C.V.(%) B-value Distribution C1 C2 No. Specimens No. Batches Data Class Mean Minimum Maximum C.V.(%) No. Specimens No. Batches Data Class Mean No. Specimens No. Batches Data Class Mean Minimum Maximum C.V.(%) B-value Distribution C1 C2 No. Specimens No. Batches Data Class (1) Chord between 1000 and 3000 Specimen thickness and batch fiber areal weight to 50% fiber volume (0.0085 in. CPT) 72 Ambient 30 Normalized 50.5 45.1 54.1 5.96 (1) Weibull 51.8 19.5 15 3 Interim 3.41 3.25 3.82 5.39 15 3 Interim 0.127 6 3 Screening 18200 15400 20300 8.37 (1) Weibull 18900 15.7 14 3 Screening 7 3 Screening 3.67 3.38 4.15 6.11 3.89 3.74 3.96 1.63 14 3 Screening 0.157 7 3 Screening 24000 20500 26200 7.76 (1) Normal 24000 1870 15 3 Interim Measured 54.3 48.5 59.0 6.14 (1) Weibull 55.7 20.5 -65 Ambient 30 Normalized Measured 67.2 71.9 56.7 59.2 78.7 83.2 8.62 9.03 (1) Weibull 69.7 11.2 15 3 Interim 4.15 3.97 4.30 2.68 3.31 3.19 3.48 2.50 15 3 Interim 0.101 6 3 Screening 14400 9750 16500 11.6 (1) Weibull 15000 13.0 (1) ANOVA 74.7 36.8 200 Ambient 30 Normalized Measured 42.4 45.2 35.4 37.0 47.9 50.5 6.42 6.80 (1) Weibull 43.6 15.4 15 3 Interim 3.53 3.36 3.68 2.79 (1) Weibull 46.5 18.3

tu F2 (ksi)

t E2

(Msi)

t 21

tu 2

()

Basis values are presented only for A and B data classes.

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MIL-HDBK-17-2F Volume 2, Chapter 6 Glass Fiber Composites

* ALL DOCUMENTATION PRESENTLY REQUIRED WERE NOT SUPPLIED FOR THIS MATERIAL. Table 6.2.4(c) MATERIAL: E-Glass 7781/EA 9396 8-harness satin weave fabric EGl/Ep 295-8HS 3 E-7781/EA 9396 RESIN CONTENT: 25.9-27.7 wt% COMP. DENSITY: 1.89-1.94 g/cm Tension, 2-axis FIBER VOLUME: 54.0-56.5 % VOID CONTENT: 3.7-5.4 % [0f]8 PLY THICKNESS: 0.0085-0.0086 in. -65/W, 72/W, 200/W Interim, Screening TEST METHOD: MODULUS CALCULATION: ASTM D 3039-76 NORMALIZED BY: Temperature (F) Moisture Content (%) Equilibrium at T, RH Source Code Mean Minimum Maximum C.V.(%) B-value Distribution C1 C2 No. Specimens No. Batches Data Class Mean Minimum Maximum C.V.(%) No. Specimens No. Batches Data Class Mean No. Specimens No. Batches Data Class Mean Minimum Maximum C.V.(%) B-value Distribution C1 C2 No. Specimens No. Batches Data Class 15 3 Interim Chord between 1000 and 3000 Specimen thickness and batch fiber areal weight to 50% fiber volume (0.0085 in. CPT) -65 (1) 140, 95-100 30 Normalized Measured 19.7 21.2 14.4 15.5 23.0 25.2 10.9 12.3 (2) Weibull 20.5 10.5 15 3 Interim 3.54 3.32 3.74 2.97 3.81 3.47 4.03 3.65 3.01 2.89 3.11 1.96 13 3 Screening 0.066 6 3 Screening 5420 3040 6510 19.2 (2) ANOVA 1120 4.58 15 3 Interim 15 3 Interim (2) Weibull 22.3 10.1 72 (1) 140, 95-100 30 Normalized Measured 16.3 17.5 14.6 15.7 18.8 20.4 8.11 8.42 (2) ANOVA 1.44 4.06 15 3 Interim 3.22 3.09 3.36 2.47 2.81 2.44 3.52 11.7 (2) ANOVA 1.59 4.37 200 (1) 140, 95-100 30 Normalized Measured 12.6 13.5 11.2 11.9 14.3 15.9 6.17 7.04 (2) Weibull 13.0 14.3 15 3 Interim 3.01 2.58 3.67 11.5 (2) Normal 13.5 0.953

tu F2 (ksi)

t E2

(Msi)

t 21

15 3 Interim 0.135 6 3 Screening 6240 4000 7300 14.2 (2) ANOVA 936 3.88

15 3 Interim 0.079 6 3 Screening 4470 3360 4900 10.6 (2) Nonpara. 8 1.54

tu 2

()

(1) Unknown weight gain (2) Basis values are presented only for A and B data classes.

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MIL-HDBK-17-2F Volume 2, Chapter 6 Glass Fiber Composites

* ALL DOCUMENTATION PRESENTLY REQUIRED WERE NOT SUPPLIED FOR THIS MATERIAL. Table 6.2.4(d) MATERIAL: E-Glass 7781/EA 9396 8-harness satin weave fabric EGl/Ep 295-8HS 3 E-7781/EA 9396 RESIN CONTENT: 27.6-30.4 wt% COMP: DENSITY: 1.89-1.93 g/cm Compression, 1-axis FIBER VOLUME: 54.1-55.8% VOID CONTENT: 3.7-5.4% [0f]16 PLY THICKNESS: 0.0085-0.0086 in. 72/A,72/W Interim TEST METHOD: MODULUS CALCULATION: ASTM D 3410B-87 NORMALIZED BY: Temperature (F) Moisture Content (%) Equilibrium at T, RH Source Code Mean Minimum Maximum C.V.(%) B-value Distribution C1 C2 No. Specimens No. Batches Data Class Mean Minimum Maximum C.V.(%) No. Specimens No. Batches Data Class Mean No. Specimens No. Batches Data Class Mean Minimum Maximum C.V.(%) B-value Distribution C1 C2 No. Specimens No. Batches Data Class 15 3 Interim Chord between 1000 and 3000 Specimen thickness and batch fiber areal weight to 50% fiber volume (0.0085 in. CPT) 72 Ambient 30 Normalized 46.4 41.1 51.2 5.96 (2) Weibull 47.6 17.5 15 3 Interim 3.45 2.96 3.86 6.24 15 3 Interim 3.68 3.17 4.11 5.98 3.06 2.56 3.77 10.1 15 3 Interim Measured 49.6 43.9 55.5 5.84 (2) Weibull 51.0 18.5 72 1.68-2.33 (1) 30 Normalized Measured 20.3 21.0 11.2 11.0 26.3 27.0 27.6 27.8 (2) ANOVA 6.40 4.91 15 3 Interim 3.18 2.56 3.85 10.1 (2) ANOVA 6.71 5.67

Normalized

Measured

cu F1 (ksi)

c E1

(Msi)

c 12

14700 11700 19600 12.8 (2) ANOVA 3.25 1940 15 3 Interim

7160 4160 10600 27.3 (2) ANOVA 4.72 2130

cu 1

()

(1) Specimens conditioned at 140F, 95-100% R.H for 68-180 days. (2) Basis values are presented only for A and B data classes.

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MIL-HDBK-17-2F Volume 2, Chapter 6 Glass Fiber Composites

* ALL DOCUMENTATION PRESENTLY REQUIRED WERE NOT SUPPLIED FOR THIS MATERIAL. Table 6.2.4(e) MATERIAL: E-Glass 7781/EA 9396 8-harness satin weave fabric EGl/Ep 295-8HS 3 E-7781/EA 9396 RESIN CONTENT: 27.6-30.4 wt% COMP: DENSITY: 1.89-1.93 g/cm Compression, 2-axis FIBER VOLUME: 51.2-53.8 % VOID CONTENT: 4.0-5.0 % [0f]16 PLY THICKNESS: 0.0083-0.0085 in. -65/A, 72/A, 200/A Interim, Screening TEST METHOD: MODULUS CALCULATION: ASTM D 3410B-87 NORMALIZED BY: Temperature (F) Moisture Content (%) Equilibrium at T, RH Source Code Mean Minimum Maximum C.V.(%) B-value Distribution C1 C2 No. Specimens No. Batches Data Class Mean Minimum Maximum C.V.(%) No. Specimens No. Batches Data Class Mean No. Specimens No. Batches Data Class Mean Minimum Maximum C.V.(%) B-value Distribution C1 C2 No. Specimens No. Batches Data Class 15 3 Interim Chord between 1000 and 3000 Specimen thickness and batch fiber areal weight to 50% fiber volume (0.0085 in. CPT) 72 Ambient 30 Normalized 37.7 32.4 42.9 8.72 (1) Weibull 39.2 11.6 15 3 Interim 3.37 2.94 3.61 6.04 15 3 Interim 3.66 3.13 3.93 6.70 3.89 3.38 4.17 5.79 15 3 Interim Measured 40.8 35.3 46.0 7.60 (1) Weibull 42.3 15.1 -65 Ambient 30 Normalized Measured 59.2 63.8 50.8 55.8 68.9 73.5 9.72 9.58 (1) ANOVA 6.54 4.81 15 3 Interim 4.18 3.63 4.55 5.84 (1) ANOVA 5.33 6.87 200 Ambient 30 Normalized Measured 26.9 29.0 20.4 23.4 34.4 37.2 16.1 15.1 (1) ANOVA 5.07 5.00 (1) ANOVA 5.75 5.16

cu F2 (ksi)

Ec 2 (Msi)

12 3 Screening 3.23 3.49 2.82 2.98 3.54 3.83 7.64 7.23 12 3 Screening

c 21

11900 9020 17800 20.1 (1) Weibull 12900 5.04 15 3 Interim

16800 13400 20800 11.8 (1) ANOVA 5.06 2200

8650 6550 12400 19.5 (1) Weibull 9340 5.42 12 3 Screening

cu 2
()

(1) Basis values are presented only for A and B data classes.

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MIL-HDBK-17-2F Volume 2, Chapter 6 Glass Fiber Composites

* ALL DOCUMENTATION PRESENTLY REQUIRED WERE NOT SUPPLIED FOR THIS MATERIAL. Table 6.2.4(f) MATERIAL: E-Glass 7781/EA 9396 8-harness satin weave fabric EGl/Ep 295-8HS 3 E-7781/EA 9396 RESIN CONTENT: 27.6-30.4 wt% COMP: DENSITY: 1.89-1.93 g/cm Compression, 2-axis FIBER VOLUME: 51.2-53.8 % VOID CONTENT: 4.0-5.0 % [0f]16 PLY THICKNESS: 0.0083-0.0085 in. -65/W, 72/W, 200/W Interim, Screening TEST METHOD: MODULUS CALCULATION: ASTM D 3410B-87 NORMALIZED BY: Temperature (F) Moisture Content (%) Equilibrium at T, RH Source Code Mean Minimum Maximum C.V.(%) B-value Distribution C1 C2 No. Specimens No. Batches Data Class Mean Minimum Maximum C.V.(%) No. Specimens No. Batches Data Class Mean No. Specimens No. Batches Data Class Mean Minimum Maximum C.V.(%) B-value Distribution C1 C2 No. Specimens No. Batches Data Class 15 3 Interim Chord between 1000 and 3000 Specimen thickness and batch fiber areal weight to 50% fiber volume (0.0085 in. CPT) -65 1.48-2.33 (1) 30 Normalized Measured 43.5 46.5 36.4 38.6 52.5 56.1 9.58 10.0 (2) Weibull 45.4 9.65 15 3 Interim 3.81 3.32 4.16 6.22 15 3 Interim 4.07 3.41 4.46 6.76 (2) Weibull 48.6 10.9 72 1.48-2.33 (1) 30 Normalized Measured 22.0 23.6 16.8 18.9 26.4 27.7 13.3 12.8 (2) ANOVA 3.50 1.39 10 2 Screening 3.11 2.96 3.25 3.40 9 2 Screening (2) ANOVA 15.3 3.56 200 1.48-2.33 (1) 30 Normalized Measured 13.4 14.2 11.3 11.8 17.2 18.3 14.8 14.8 1.88 ANOVA 2.36 4.31 18 3 Interim 3.34 3.23 3.49 2.40 2.91 2.25 3.73 13.6 18 3 Interim 3.08 2.32 3.92 13.8 1.84 ANOVA 4.95 2.49

cu F2

(ksi)

Ec 2 (Msi)

c 21

12400 9890 15700 13.3 (2) Weibull 13100 8.42 10 2 Screening

7800 4570 9310 18.8 (2) Weibull 8330 7.91 18 3 Interim

4540 2880 6890 22.9 (2) Weibull 4950 4.68

cu 2
()

(1) Specimens conditioned at 140F, 95-100% RH for 68-180 days. (2) Basis values are presented only for A and B data classes.

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MIL-HDBK-17-2F Volume 2, Chapter 6 Glass Fiber Composites

* ALL DOCUMENTATION PRESENTLY REQUIRED WERE NOT SUPPLIED FOR THIS MATERIAL. Table 6.2.4(g) MATERIAL: E-Glass 7781/EA 9396 8-harness satin weave fabric EGl/Ep 295-8HS 3 E-7781/EA 9396 RESIN CONTENT: 25.0-27.7 wt% COMP: DENSITY: 1.92 g/cm Shear, 12-plane FIBER VOLUME: 54.2-56.9 % VOID CONTENT: 3.6-5.7 % [+/-45f]s PLY THICKNESS: 0.0083-0.0085 in. 72/A, -65/A, 200/A, -65/W, 72/W, 200/W Interim TEST METHOD: MODULUS CALCULATION: ASTM D 3518-76 NORMALIZED BY: Temperature (F) Moisture Content (%) Equilibrium at T, RH Source Code Mean Minimum Maximum C.V.(%)
su F12

Not normalized 72 Ambient 30 11.5 9.45 13.5 9.20 (2) Weibull 12.0 11.8 23 3 Interim 0.758 0.625 0.928 11.3 22 3 Interim -65 Ambient 30 16.9 13.1 20.3 14.1 (2) Weibull 17.9 8.15 18 3 Interim 1.03 0.901 1.29 10.5 18 3 Interim 200 Ambient 30 7.11 4.59 9.56 15.8 (2) Weibull 7.59 6.77 19 3 Interim 0.458 0.289 0.549 12.9 19 3 Interim -65 1.52-2.32 (1) 30 8.52 6.74 10.7 13.3 (2) Weibull 9.01 8.08 18 3 Interim 0.860 0.624 0.976 11.6 16 3 Interim 72 1.52-2.32 (1) 30 5.49 4.16 6.44 11.9 (2) Weibull 5.76 11.0 18 3 Interim 0.490 0.336 0.666 16.7 18 3 Interim 200 1.52-2.32 (1) 30 2.73 2.17 3.42 12.9 (2) Weibull 2.890 8.60 17 3 Interim 0.242 0.146 0.436 33.0 17 3 Interim

B-value Distribution C1 C2 No. Specimens No. Batches Data Class Mean Minimum Maximum C.V.(%) No. Specimens No. Batches Data Class Mean No. Specimens No. Batches Data Class

(ksi)

s G12

(Msi)

s 12

()

(1) Specimens conditioned at 140F, 95-100% RH for 111-117 days. (2) Basis values are presented only for A and B data classes.

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MIL-HDBK-17-2F Volume 2, Chapter 6 Glass Fiber Composites

This section is reserved for future use.

6.3 GLASS - POLYESTER COMPOSITES 6.4 GLASS - BISMALEIMIDE COMPOSITES 6.5 GLASS - POLYIMIDE COMPOSITES 6.6 GLASS - PHENOLIC COMPOSITES 6.7 GLASS - SILICONE COMPOSITES 6.8 GLASS - POLYBENZIMIDAZOLE COMPOSITES 6.9 GLASS - PEEK COMPOSITES

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