PETRONAS TECHNICAL STANDARDS

DESIGN AND ENGINEERING PRACTICE

MANUAL

ON-LINE PROCESS STREAM ANALYSIS SAMPLE CONDITIONING

PTS 32.31.50.11 DECEMBER 2007

2010 PETROLIAM NASIONAL BERHAD (PETRONAS) All rights reserved. No part of this document may be reproduced, stored in a retrieval system or transmitted in any form or by any means (electronic, mechanical, photocopying, recording or otherwise) without the permission of the copyright owner

PETRONAS TECHNICAL STANDARDS

DESIGN AND ENGINEERING PRACTICE (CORE)

MANUAL

ON-LINE PROCESS STREAM ANALYSIS SAMPLE CONDITIONING

PTS 32.31.50.11 SEPTEMBER 2002

PREFACE

PETRONAS Technical Standards (PTS) publications reflect the views, at the time of publication, of PETRONAS OPUs/Divisions. They are based on the experience acquired during the involvement with the design, construction, operation and maintenance of processing units and facilities. Where appropriate they are based on, or reference is made to, national and international standards and codes of practice. The objective is to set the recommended standard for good technical practice to be applied by PETRONAS' OPUs in oil and gas production facilities, refineries, gas processing plants, chemical plants, marketing facilities or any other such facility, and thereby to achieve maximum technical and economic benefit from standardisation. The information set forth in these publications is provided to users for their consideration and decision to implement. This is of particular importance where PTS may not cover every requirement or diversity of condition at each locality. The system of PTS is expected to be sufficiently flexible to allow individual operating units to adapt the information set forth in PTS to their own environment and requirements. When Contractors or Manufacturers/Suppliers use PTS they shall be solely responsible for the quality of work and the attainment of the required design and engineering standards. In particular, for those requirements not specifically covered, the Principal will expect them to follow those design and engineering practices which will achieve the same level of integrity as reflected in the PTS. If in doubt, the Contractor or Manufacturer/Supplier shall, without detracting from his own responsibility, consult the Principal or its technical advisor. The right to use PTS rests with three categories of users : 1) 2) 3) PETRONAS and its affiliates. Other parties who are authorised to use PTS subject to appropriate contractual arrangements. Contractors/subcontractors and Manufacturers/Suppliers under a contract with users referred to under 1) and 2) which requires that tenders for projects, materials supplied or - generally - work performed on behalf of the said users comply with the relevant standards.

Subject to any particular terms and conditions as may be set forth in specific agreements with users, PETRONAS disclaims any liability of whatsoever nature for any damage (including injury or death) suffered by any company or person whomsoever as a result of or in connection with the use, application or implementation of any PTS, combination of PTS or any part thereof. The benefit of this disclaimer shall inure in all respects to PETRONAS and/or any company affiliated to PETRONAS that may issue PTS or require the use of PTS. Without prejudice to any specific terms in respect of confidentiality under relevant contractual arrangements, PTS shall not, without the prior written consent of PETRONAS, be disclosed by users to any company or person whomsoever and the PTS shall be used exclusively for the purpose they have been provided to the user. They shall be returned after use, including any copies which shall only be made by users with the express prior written consent of PETRONAS. The copyright of PTS vests in PETRONAS. Users shall arrange for PTS to be held in safe custody and PETRONAS may at any time require information satisfactory to PETRONAS in order to ascertain how users implement this requirement.

PTS 32.31.50.11 September 2002 Page 3

TABLE OF CONTENTS 1. 1.1 1.2 1.3 1.4 1.5 1.6 2. 3. 3.1 3.2 3.3 3.4 3.5 3.6 3.7 4. 4.1 4.2 4.3 4.4 4.5 4.6 4.7 5. 5.1 5.2 5.3 5.4 5.5 6. 6.1 6.2 6.3 6.4 7. 8. 9. 10. 11. INTRODUCTION .......................................................................................................5 SCOPE .......................................................................................................................5 DISTRIBUTION, INTENDED USE AND REGULATORY CONSIDERATIONS ........5 DEFINITIONS ............................................................................................................5 ABBREVIATIONS ......................................................................................................6 CROSS-REFERENCES ............................................................................................6 SUMMARY OF REVISIONS FROM PREVIOUS EDITION .......................................7 GENERAL ..................................................................................................................8 SPECIFICATIONS FOR SAMPLE CONDITIONING SYSTEMS ..............................9 GENERAL ..................................................................................................................9 SPECIFICATION OF COMPONENTS ......................................................................9 FLOW RATE TO ANALYSERS ...............................................................................11 COOLING AND HEATING OF SAMPLES ...............................................................11 TEST AND CALIBRATION VESSELS .....................................................................11 MOUNTING ARRANGEMENTS ..............................................................................12 ANALYSER SYSTEM INTEGRATOR .....................................................................13 SPECIAL APPLICATIONS ......................................................................................14 GENERAL ................................................................................................................14 OXYGEN SERVICES ..............................................................................................14 CORROSIVE SERVICES ........................................................................................14 TOXIC AND NOXIOUS SERVICES ........................................................................14 SOUR SERVICES ...................................................................................................14 SHELL ANALYSER IMPLEMENTATION LOGIC (SAIL) .........................................15 CONTINUOUS EMISSION MONITORING SYSTEM (CEMS) ................................15 SAMPLE DISPOSAL SYSTEMS ............................................................................17 GENERAL ................................................................................................................17 GAS DISPOSAL TO FLARE ....................................................................................17 LIQUID DISPOSAL TO RECOVERY SYSTEM .......................................................17 LIQUID DISPOSAL TO EFFLUENT SYSTEM ........................................................17 VENT AND DRAIN SYSTEMS ................................................................................18 HEATING, WINTERIZING AND INSULATION .......................................................19 GENERAL ................................................................................................................19 HEATING AND WINTERIZING ................................................................................19 ELECTRIC HEATING ..............................................................................................19 INSULATION AND ENCLOSURE ...........................................................................19 REQUIREMENTS FOR ELECTRIC AND ELECTRONIC EQUIPMENT ................21 DRAWINGS .............................................................................................................22 TESTING AND INSPECTION ..................................................................................23 REFERENCES ........................................................................................................25 APPENDICES ..........................................................................................................27

PTS 32.31.50.11 September 2002 Page 4

APPENDICES APPENDIX 1 APPENDIX 2 APPENDIX 3 APPENDIX 4 APPENDIX 5 APPENDIX 6 APPENDIX 7 INDEX OF SAMPLE CONDITIONING SYSTEM DRAWINGS .......................28 TYPICAL SAMPLE CONDITIONING SYSTEM FOR OIL ANALYSERS .......29 COMPONENTS LIST OF THE SAMPLE CONDITIONING SYSTEM ............41 TYPICAL VENT AND DRAIN SYSTEM FOR ANALYSER HOUSES ............42 REFERENCE VESSEL FOR VALIDATION AND CALIBRATION SERVICES ...................................................................................................44 FUNNEL AND SYPHON .................................................................................46 TYPICAL LAYOUT DRAWING OF SAIL ........................................................48

PTS 32.31.50.11 September 2002 Page 5 1. 1.1 INTRODUCTION SCOPE This PTS specifies requirements and gives recommendations for the design and construction of sample conditioning systems for on-line process stream analysers and for the disposal of sample fluids. This PTS is a revision of the PTS of the same number dated September 1986. This PTS is one of a series of on-line process stream analysis PTS. The other publications are: PTS 32.31.50.10, Sample take-off/transport; PTS 32.31.50.12, Analysers; PTS 32.31.50.13, Analyser Houses. 1.2 DISTRIBUTION, INTENDED USE AND REGULATORY CONSIDERATIONS Unless otherwise authorised by PETRONAS, the distribution of this PTS is confined to companies forming part of PETRONAS or managed by a Group company, and to Contractors nominated by them. This PTS is intended for use in oil refineries, chemical exploration/production and supply/marketing installations. plants, gas plants

If national and/or local regulations exist in which some of the requirements may be more stringent than in this PTS, the contractor shall determine by careful scrutiny which of the requirements are more stringent and which combination of requirements will be acceptable as regards safety, environmental, economic and legal aspects. In all cases, the Contractor shall inform the Principal of any deviation from the requirements of this PTS which is considered to be necessary in order to comply with national and/or local regulations. The Principal may then negotiate with the Authorities concerned with the objective of obtaining agreement to follow this PTS as closely as possible. 1.3 1.3.1 DEFINITIONS General definitions The Contractor is the party that carries out all or part of the design, engineering, procurement, construction, commissioning or management of a project or operation of a facility. The Principal may undertake all or part of the duties of the Contractor. The Manufacturer/Supplier is the party that manufactures or supplies equipment and services to perform the duties specified by the Contractor. The Principal is the party that initiates, and ultimately pays for, the project. The Principal will generally specify the technical requirements. The Principal may also include an agent or consultant, authorised to act for the Principal. The word shall indicates a requirement. The word should indicates a recommendation.

PTS 32.31.50.11 September 2002 Page 6

1.3.2

Specific definitions Pipe Sizes: Data/Information Stainless Steel Analyser system house integrator Heated Box The international nomenclature Diameter Nominal written as DN 15, 25, 40, 50, etc. Where indicated as 'specified by the Principal' shall form a part of the requisition. AISI type stainless steel Contractor who specialises in providing one-stop integrated services for all design, engineering, procurement, testing and commissioning of an analyser package. A prefabricated thermal insulated enclosure with heating facility designed to house the analyser sampling components

1.4

ABBREVIATIONS NACE SAIL National Association of Corrosion Engineers Shell Analyser Implementation Logic - A set of QMI hardware and software designed to provide automated validations of QMIs in Oil Movements area in accordance with ASTM D 3764 philosophy. Analyser Maintenance And Data Acquisition System Continuous Emission Monitoring System - An analyser package specially designed to provide continuous monitoring and record of stack emissions. Quality Measuring Instruments Near Infrared

AMADAS CEMS

QMI NIR

1.5

CROSS-REFERENCES Where cross-references to other parts of the PTS are made, the referenced section number is shown in brackets. Other documents referenced by this PTS are listed in (10).

PTS 32.31.50.11 September 2002 Page 7

1.6

SUMMARY OF REVISIONS FROM PREVIOUS EDITION The previous edition of this PTS was dated September 1986. Other than editorial revisions, the following are the main changes to that edition: Old section New Section 4.6 4.7 Appendix 1 Appendix 1 Appendix 2 Appendix 3 Appendix 3 Appendix 7 Appendix 7 Change Added SAIL Added CEMS Deleted Index of typical sample conditioning system drawings Simplified and made more selective. Deleted Was Appendix 7 in the last PTS Relocated to Appendix 3 Added Typical layout drawing of SAIL

PTS 32.31.50.11 September 2002 Page 8 2. GENERAL Sample conditioning systems should be designed and constructed as described in (3). Typical drawings of sample conditioning systems for some commonly used analysers are attached in (Appendix 2). Depending on the application, users may adapt or modify the drawings to suit the local environment and the properties of the process samples to be analysed. The materials of construction should be stainless steel. However, for oxygen, corrosive or toxic/noxious services, other materials and/or additional provisions should be considered, see (4). Sections (4.6) and (4.7) describe SAIL & CEMS complex analyser systems requirements. These should be customised for the specific needs of the site or project specifications. A typical layout drawing of SAIL is given in (Appendix 7). Sample disposal systems are described in (5) and typical details of a vent and drain system are given in (Appendix 4). Heating, winterizing and/or insulation requirements are given in (6). The requirements for electric and electronic equipment are specified in (7). Detailed drawings shall be prepared, as set out in (8). The requirements for testing and inspection are given in (9).

PTS 32.31.50.11 September 2002 Page 9 3. 3.1 SPECIFICATIONS FOR SAMPLE CONDITIONING SYSTEMS GENERAL The sample conditioning system shall be designed to supply the sample at the analyser inlet whilst meeting the conditions as specified in the analyser technical specifications. It shall be designed so that none of the samples analytical properties are altered between the sample take off and analyser inlet. Utility connections or supplies such as air, cooling water, coolant, carrier gas and flushing oil, etc., shall be taken into consideration in the design of the sample conditioning system after the suitable type of analyser has been chosen for the intended application. Depending on the application, a sample conditioning system will consist of the following components: filter(s); pressure gauge(s) & reducer(s); flow meter(s); isolation ball valve(s), needle valve(s), relief valve(s), selection valves and automated valves; temperature gauge/dial or temperature controller; multi-stream switching valve; excess flow check valve; cooler(s) and refrigerated chillers; heater(s) for heating or preventing freezing; vessel(s) for test/calibration services; sample pump(s); sample recovery system; utility connections/supplies such as air, steam, cooling water, carrier gas, flushing oil, etc.; tubing and compression fittings etc.

A sample conditioning rack/panel from the analyser manufacturer may be used. Sample conditioning systems may be located in the field or at the analyser house, depending on the location of its associated analyser, see PTS 32.31.50.12 The sample conditioning system for a moisture analyser shall be field-mounted with its sample transport line as short as practicable. The sample conditioning system for an H2S/SO2 analyser shall be close coupled, housed in a heated box directly mounted on top of the process line with a steam jacketed isolation valve. The sample transport system shall normally be a fast loop system with bypass and isolation valves at the sample conditioning system. Single line sample transport systems may also be used for certain applications, see PTS 32.31.50.10 Stainless steel sample transport lines shall not be run next to galvanised pipes or come into contact with any galvanised structure support to avoid corrosion. For typical examples, see (Appendix 2). The selected make(s) and type(s) of component shall be as specified in the requisition. 3.2 SPECIFICATION OF COMPONENTS All components selected shall be rated for the relevant process conditions. For general applications, all wetted parts shall be of stainless steel. The make(s) and type(s) of components, tubing and compression fittings shall be as specified by the Principal.

PTS 32.31.50.11 September 2002 Page 10 Preference shall be given to components with compression fitting-ends, if specified in the requistion, manufactured by the same compression fitting Manufacturer. The design pressure of components and tubing shall be in accordance with ANSI/ASME B31.3. The design pressure for sample conditioning systems provided with a relief valve, referred to the pressure level at which the relief is installed, shall be not less than: - for MOP between atmospheric and 17 bar (ga) = MOP + 1.7 bar; - for MOP between 17 bar (ga) and 40 bar (ga) = 110 % of MOP; - for MOP between 40 bar (ga) and 80 bar (ga) = MOP + 4 bar; - for MOP above 80 bar (ga) = 105 % of MOP; where MOP is defined as Maximum Operating Pressure. Special attention shall be paid to the pressure ratings and the tolerances for outside diameter and wall thickness of the tubing. The tubing shall meet the requirements of ISO 4200 for metric sizes and, when applicable, ASTM A 269 for imperial sizes. The application of either metric or imperial sized tubing and compression fittings shall be specified in the requisition. The reliable application of compression fittings requires that: the fittings and tubing are installed strictly in accordance with the Manufacturer's instructions; - the systems are pressure-tested after construction; - it shall be ensured that imperial sized tubing and metric compression fittings or metric sized tubing and imperial compression fittings are not used in conjunction with one another because this will result in unreliable joints. Sample conditioning systems shall have facilities for flushing, venting and/or draining, with vent and/or drain valve(s). The vent/drain outlets shall be connected to a vent or a drain system (5.5). Instrument air supply lines and pneumatic signal lines should normally be made up from polyvinylchloride (PVC) covered copper tubing and brass compression fittings and components. However, if specified by the Principal, the air supply and signal lines shall be made up from stainless steel tubing and stainless steel compression fittings.
NOTE: Mixing of different materials, e.g. brass and stainless steel, is not permitted.

Steam heating circuits for heat tracing of a sample line or heated box should normally be 0.25 in. or 0.375 in. copper tubing, with brass compression fittings and components, and also equipped with a steam trap to drain off condensate. If specified by the Principal, supply lines for nitrogen, carrier gas and cooling water shall also be colour coded. Pressure gauges for sampled fluids should have a 50-mm dial and be provided with a 0.25 in. threaded connection. The type of thread shall be as specified in the requisition. Pressure gauges which can be depressurized in the conditioning system shall be installed on a gauge adapter or connected to a 0.5 in. female threaded compression fitting, supported from the mounting plate. Pressure gauges that cannot be depressurized in the conditioning system shall be provided with isolate-and-vent valve facilities. The vent/drain outlet shall be connected to a vent or drain system (5.5). Instrument air supply and nitrogen supply lines shall be provided with a filter reducer complete with a pressure gauge and back flow protection. The nitrogen reducer shall be of the non-bleeding type.
NOTE: Pressure gauges for reducers and filter reducers should have a 50 mm dial and shall be provided with a 0.25 in. NPT threaded connection.

PTS 32.31.50.11 September 2002 Page 11 Special attention shall be paid to the following: Solenoid valves shall be used only for switching instrument air and nitrogen. For all other fluids a pneumatically operated valve in combination with a solenoid valve shall be selected. The pneumatic actuator shall be provided with a direct-coupled mechanical position indicator. Glass components or parts should not be used for flammable and toxic/noxious fluids. If all stainless steel components for a particular range and/or duty are not commercially available, the Contractor/Manufacturer shall obtain written agreement from the Principal to use glass-containing components. If utilized, glass or glass-containing components shall be suitable for 1.5 times the maximum operating pressure of the related system and shall be provided with 5-mm thick polycarbonate screens for personnel protection. Deviation requires the written approval of the Principal.
NOTE: Variable-area flow meters shall have a metal metering tube.

Relief valve(s) shall be installed to protect those components installed in a system which have a limited pressure rating, e.g., sample conditioning vessels and glass-containing components. The relief valves shall be connected to a vent or a drainage or flare system as required.

3.3

FLOW RATE TO ANALYSERS An excess flow valve shall limit the total amount of flammable fluids flowing to the analyser. The following requirements shall be met: the maximum flow rate of flammable gases shall not exceed 20 Nl/h; the liquid flow rate shall not exceed the maximum required flow rate, as specified by the Manufacturer of the analyser concerned.
1. Flow rates exceeding the above limits require the approval of the Principal in writing. 2. The excess flow valve shall be a self-closing type to prevent the above limits from being exceeded.

NOTES:

3.4

COOLING AND HEATING OF SAMPLES Cooling or heating as appropriate shall be provided in the sample conditioning system for analysers requiring a sample inlet temperature within specified limits. Where cooling is required, fresh water from the main cooling system or industrial water should be used. Seawater shall not be used as a cooling medium.
NOTE: The maximum temperature of the cooling water supply during hot seasons and in tropical locations shall be the design temperature.

If the cooling water temperature is too high, cooling by means of cold air from a vortex tube or by refrigeration or other mechanical cooling shall be considered. However, the use of refrigerated or mechanical coolers requires the written approval of the Principal. For refrigerated coolers, an electric motor with single-phase power supply according to the site standard should be used. The use of three-phase power supply requires the approval of the Principal. If heating is required to lower the viscosity or to prevent condensation of gaseous samples or absorption in materials, the application shall be in accordance with (6). 3.5 TEST AND CALIBRATION VESSELS A vessel shall be provided for analysers that require liquid samples for testing and calibration. Depending on applications and requirements, calibration vessels may be of different sizes and may be custom built or supplied by Manufacturer/Suppliers as a standard item. The capacity of the calibration vessel should be sized so that frequent

PTS 32.31.50.11 September 2002 Page 12 topping up of reference standard/sample is not necessary. Depending on the check frequency and usage/wastage of the reference standard, the capacity of the calibration vessel should be sufficient to hold a batch of reference standard for 3 months before replenishment is necessary. If heat is required to lower the viscosity or to prevent freezing of the liquid, a stainless steel steam heating coil shall be installed around the vessel. If steam is not available, electrical heating tape of the self-regulating type should be applied. The thermal insulation around vessel and heating facilities shall have a guaranteed maximum chloride content of 10 mg/kg and be sealed against water ingress in order to prevent chloride stress corrosion. Piston type sample calibration vessels could be considered as an alternative to the vessel described in (Appendix 5). Where nitrogen is used as a pressurising medium, the pressure should not exceed 0.5 bar (ga) and a miniature pump should be used to pressure up sample delivery to the analyser. 3.6 MOUNTING ARRANGEMENTS All components shall be installed on a stainless steel mounting plate, secured to the sample conditioning rack with flat, countersunk headed stainless steel bolts. The sample conditioning rack shall be selected from one of the following types: freestanding; floor mounting (which will require additional support); wall mounting,

and constructed in accordance with one of the following methods: welded, all material of stainless steel; welded, all material of carbon steel, hot-dip galvanized in accordance with the requirements of ASTM A 123 or BS 729, after drilling and welding. The nuts shall be retapped after galvanizing; bolted, all materials of prefabricated stainless steel, U or H profile, with mounting strips/plates, bolts and nuts.
The Manufacturer/Supplier shall design the conditioning rack(s), mounting plate(s) and support(s) for the total weight of all the components including the weights of fluid(s).

NOTE:

Components should be attached to the mounting plate with bolts and nuts, the nuts being permanently fixed to the mounting plate. Special attention shall be paid to the position of the components in relation to the connections to be made.
NOTE: Components such as ball valves and non-return valves may be supported by their connecting tubing by means of stainless steel attachments adjacent to the tubing connections. Non-metallic spacer material, e.g., teflon hose, shall be used to isolate the tubing from the supports.

Components such as filters, coalescers and flow cells/electrodes that require frequent maintenance should be mounted at a suitable height and be easily accessible. Bulkhead unions shall be supported from the mounting plate. The lock nut shall be located on the conditioning side of the system. Prefabricated sample conditioning systems shall be supplied with engraved nameplates in accordance with PTS 32.31.00.32 The nameplates should be fixed directly to the mounting plate but if their descriptions may be obstructed by components and/or tubing, a separate nameplate support shall be provided attached to the mounting plate. Nameplates shall be fixed to the supports with stainless steel screws.

PTS 32.31.50.11 September 2002 Page 13 All incoming and outgoing connections shall be identified with engraved nameplates. Components such as relief valves, excess flow valves and variable-area flow meters shall also be provided with nameplates showing their settings. In addition to the above, incoming and outgoing connections at thermal insulation enclosures for sample conditioning systems, shall be provided with nameplates on the outside of the enclosure. Analysers mounted outdoors and susceptible to direct sunshine shall be installed with an appropriate sunshade. Compression fittings shall be provided with parallel threaded connections.
NOTE: The thread surfaces require lubrication with a suitable compound.

The compression fitting shall be locked to the body of the relevant component with a locking pin.
NOTES: 1. NPT threaded compression type elbows shall not be used, because the length of engagement of the threads is considered insufficient when correct alignment is obtained. 2. NPT threaded connections require special provisions to prevent seizing and leakage. For temperatures between -100 C and +200 C, PTFE tape (MESC 85.15.78.038.1) shall be applied as follows: Place tape on the male thread, leaving two threads at the small end free from tape, hold in place and wrap clockwise once only with a half tape width overlap. Draw tightly around the threads so that it conforms to the threaded surface.

The tubing shall be arranged so that the removal of one component will not require the dismantling of other parts. The components shall also be installed in different planes to avoid the need for bends when crossings have to be made. The tubing shall be cut dead square with a tube cutter and the tube edges shall be deburred. The tube end shall be undamaged, round and without scratches over the length which fits into the compression fitting. Any coating or painting shall be removed. The tubing shall be bent with a high-quality tube bender to at least the minimum bending radius as specified by the tubing Manufacturer.
NOTE: Special attention shall be paid to tubing made of other materials such as Monel, Hastelloy or Incoloy (4.3). The recommended minimum bending radii for tubing in these materials may be larger than those specified for stainless steel.

3.7

ANALYSER SYSTEM INTEGRATOR Analyser system integrators are specialist contractors providing one-stop integrated services for all design, engineering, procurement, testing and commissioning activities of an analyser system, including optional fabrication of analyser houses to clients requirements. Qualified analyser system integrators shall be contracted as far as possible to design sampling systems as part of the total analyser system package.

PTS 32.31.50.11 September 2002 Page 14 4. 4.1 SPECIAL APPLICATIONS GENERAL To ensure an efficient operation of the sample conditioning system under all operational and climatic conditions, certain applications require provisions in addition to, or in deviation from those specified in (3), e.g., the use of special materials and/or components and heating (6), or a combination thereof. 4.2 OXYGEN SERVICES All materials for gaseous-oxygen applications shall be carefully degreased and inspected in accordance with the requirements of PTS 31.10.11.31 4.3 CORROSIVE SERVICES For applications where stainless steel is not suitable, preference shall be given to materials such as Monel, Hastelloy or Incoloy. When components made of the above materials cannot be commercially obtained, then Teflon may be considered. The application of any of the above materials requires the written approval of the Principal. 4.4 TOXIC AND NOXIOUS SERVICES All vents for toxic and/or noxious services shall be connected to a vent for toxic products or alternatively to a flare system. If the quantity of toxic and/or noxious process sample being released from the vents is below the acceptable limit as advised by the Principal and/or indicated in the Project Specifications, it may be released to the atmosphere at a safe height and in a safe direction. In this case, written approval of the Principal shall be required. All drains shall be directed to a drainage vessel or a covered pit allocated to receive toxic products. The sample conditioning system shall have flushing facilities terminating in a valve with a compression fitting. An armoured hose or coiled tubing, provided with compression fitting ends, should be used to flush the components and tubing. When the flushing connection is not in use it shall be closed with a compression fitting type plug, secured by means of a bead-type chain to the compression fitting or to the isolating valve body. The sample conditioning system shall be provided with a red nameplate bearing the inscription in white: CAUTION: TOXIC/NOXIOUS SERVICE The nameplate shall be in accordance with the requirements of PTS 32.31.00.32, but shall be screwed and not glued. The letter height shall be 20 mm. 4.5 SOUR SERVICES

Amended per Circular 38/04

All components installed in sour services shall comply with the requirements of PTS 31.38.01.11 Sour services or sour environments are defined as fluids containing water as a liquid and hydrogen sulphide exceeding the limits prescribed in ISO 15156 or NACE MR0103, as applicable. These environments may cause sulphide stress cracking of susceptible materials.

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NOTES: 1. ISO 15156 shall apply to oil and gas production facilities and natural gas sweetening plants. NACE MR0175 is equivalent to ISO 15156. 2. NACE MR0103 shall apply to other applications (e.g. oil refineries, LNG plants and chemical plants).

If components cannot be obtained in accordance with the the above standards, Hastelloy-C or type 17-4 PH stainless steel should be used. Typical examples are: Amended per Circular 38/04

valve head spindles; compression fittings.

The wetted parts of the components shall meet the hardness requirements of ISO 15156 or NACE MR0103, as applicable (see above). The application of complete components made of Hastelloy-C requires the written approval of the Principal. The threads of screwed components shall be coated with a lubricant/sealing material before installation to prevent corrosion. 4.6 SHELL ANALYSER IMPLEMENTATION LOGIC (SAIL) The Shell Analyser Implementation Logic (SAIL) is based mainly on ASTM D 3764, the standard method for analyser validation using the reference sample method. SAIL is normally used for QMIs in the blenders as part of a Quality Release system. SAIL consists of a set of QMI system hardware and SAIL software. For each QMI application, the SAIL software module must be specified according to the local operational philosophy and ASTM D 3764. When an on-line NIR analyser is used, validation shall be based on ASTM D 6122. SAIL software is implemented by DCS Manufacturers/Suppliers and specialist SAIL Implementation Suppliers. Sample system component selection and design for SAIL shall be specified as part of a SAIL implementation project. A functional specification will form the basis for detailed engineering for SAIL. Reports MF 94-0515, OP 97-30425 and OP 00-30408 provide guidelines for the formulation of such a functional specification. This PTS shall be used to meet the requirements for sample conditioning. A qualified analyser system integrator shall be contracted to design and supply the sampling system and components. Pre-qualified DCS or SAIL Implementation Suppliers will supply the SAIL logic. Any communication link between the SAIL and DCS systems will be in the scope of supply of the DCS Supplier. The integrated operation of the SAIL logic and sampling system shall be specified to be tested by and be in the scope of the Main Automation Contractor for major projects, or the SAIL logic Supplier for a stand-alone SAIL implementation project. A SAIL application shall be supplied with a full as-built program listing of the logic. The listing shall include commentary text to clarify the logic. Additionally, a flow sheet indicating the full logic sequence shall be provided. 4.7 CONTINUOUS EMISSION MONITORING SYSTEM (CEMS) For CEMS, there are two types of sampling techniques used, i.e. extractive and in-situ. Extractive method: A gas sample shall be continuously extracted from the stack, filtered to remove the particulate content and all the water vapour to provide a dry measurement, or heated with the water vapour retained to provide a wet measurement.

PTS 32.31.50.11 September 2002 Page 16 If specified, the sample may also be diluted by plant air in or outside the stack, before it enters the sample conditioning system. A sonic air dilution probe complete with monitoring system could be considered. The extractive method shall use valves, pump, chiller or heater, dilution device, sample tubings, heat traced sample lines, filters and other components necessary for gas transport and conditioning to condition the sample to near standard temperature and pressure. The sample conditioning system shall maintain the sample in hot/wet condition to provide a wet measurement, or in cool/dry condition (the gas temperature is reduced to ambient temperature and moisture is removed) to provide a dry measurement as specified in the requisition. In-situ method: An analyser using a probe or sensor that is directly inserted into the stack to provide measurement does not require a sample conditioning system. The CEMS shall be selected and designed to meet the performance specifications laid down by the local authority, and the sample conditioning shall be specified to the CEMS Supplier as an integral package.

PTS 32.31.50.11 September 2002 Page 17 5. 5.1 SAMPLE DISPOSAL SYSTEMS GENERAL Samples should be returned to the process stream. For those applications where other arrangements are required for technical reasons, the samples should be directed to one of the following: a flare system; a recovery system; an effluent system.

Waste samples and/or by products of the analysis process shall not be discharged to atmosphere unless approved by the Principal. Exemptions are air and moderate amounts of hydrogen, e.g., column vent of a gas chromatogram, nitrogen and other non-toxic and/or non-odorous compounds that are considered as safe and non-hazardous for the environment. If waste gases or vapours cannot be returned to one of the above systems they should be vented to the atmosphere in such a way that: they are discharged at a safe height and in a safe direction; flammable conditions are not created; the number of venting points is limited to a minimum.

For typical vent details, see (Appendix 4). Venting to atmosphere requires the Principal's written approval. 5.2 GAS DISPOSAL TO FLARE Hydrocarbon gases or vapours which cannot be returned to the process should be discharged to a flare system, via a non-return check valve. Flare systems normally operate at varying pressures; the Principal shall specify the maximum operating pressure. The effluent gas pressure shall be kept constant by means of a back-pressure regulator. 5.3 LIQUID DISPOSAL TO RECOVERY SYSTEM Hydrocarbon liquids that cannot be returned to the process shall be discharged into one of the following systems: plant hydrocarbon recovery system; drain pit for hydrocarbon products.

The total quantity of liquids disposed of shall be limited to the minimum necessary for adequate sampling. Liquid hydrocarbons with low boiling point which can easily vaporise at ambient temperature should not be discharged to an open drain. 5.4 LIQUID DISPOSAL TO EFFLUENT SYSTEM Aqueous effluents shall be disposed of via one of the following dedicated effluent systems: 'clean effluent' for aqueous fluids which are always clean; 'normally clean effluent' for aqueous fluids which are normally clean but may become contaminated in emergencies; 'contaminated effluent'.
Aqueous fluids from analysers using reagents shall be discharged into contaminated effluent systems.

NOTE:

PTS 32.31.50.11 September 2002 Page 18 At locations where there is no dedicated effluent system, non-toxic and/or non-noxious aqueous effluents, such as boiler feed water or de-mineralised water, may be discharged to the ground or the nearest drain. 5.5 VENT AND DRAIN SYSTEMS Vent and drain systems should be installed in the conditioning area against the outside wall(s) of the analyser house and should be adequately supported at maximum intervals of 1 m. The vent and drain systems will be selected by the Principal from the following options to suit the application: carbon steel, all-welded construction; stainless steel, AISI type 316, all-welded construction or with compression fittings; rigid PVC plastic, cemented construction in accordance with the requirements of PTS 31.38.01.12

The minimum size of the piping for vent header(s) shall be DN 50 and for liquid headers DN 80. The interconnecting piping shall be minimum DN 15. Connections to drain headers without an isolating valve shall be provided with a goose neck liquid seal. Where required, a funnel syphon for liquid seal shall be installed, see (Appendix 6). Special attention shall be given to ensure the segregation of water and oil drain headers, (5.3) and (5.4).
NOTE: Cooling water shall not be discharged into condensate return systems.

For a typical example of a vent and drain system, see (Appendix 4).

PTS 32.31.50.11 September 2002 Page 19 6. 6.1 HEATING, WINTERIZING AND INSULATION GENERAL Heating of sample conditioning systems, if required, should preferably be by steam. If steam is not available, or if specifically requested by the Principal, electric heating shall be applied. A prefabricated thermal insulating enclosure with heating facilities (heated box) shall be provided to house the sampling components. Where sample lines enter or leave the heated box, insulating grommets or similar shall be installed to avoid metal to metal contact with the enclosure. Proper installation/insulation procedures shall be applied for the heat traced sample lines to avoid ingress of rainwater. Open drains, such as funnels, shall be installed outside the enclosure. Electric and electronic components, such as solenoid valves, switches and timer devices, should not be installed inside the enclosure. All electrical and electronic components shall meet the requirements specified in (9). 6.2 HEATING AND WINTERIZING Low-pressure steam at 3.5 bar (ga) should be used for heating purposes. If higher temperatures are required, medium-pressure steam up to 18 bar (ga) may be considered. The steam heating shall be arranged so that the heating equipment does not obstruct other components. Sample conditioning systems that operate at constant temperature shall be provided with a self-acting temperature controller installed in or on top of the enclosure. A temperature gauge of dial size 50 mm shall be installed in the door with the indicator outside the enclosure. Each sample conditioning system shall have its own steam supply, complete with isolating valves labelled with the tag number of the system. The valves shall be installed outside the enclosure. Each steam header shall terminate in a condensate return line. Steam supply and condensate return lines form part of Mechanical Engineering. 6.3 ELECTRIC HEATING Electric heaters shall be provided with a thermostat that controls the temperature within 3 C of the required setting. Alternatively, self-regulating heating tape may be used. All electric equipment shall meet the requirements specified in (9). The electric heating shall be arranged so that the heating equipment does not obstruct other components. 6.4 INSULATION AND ENCLOSURE The type of enclosure shall be as specified by the Principal. Sample conditioning systems provided with heating facilities shall have enclosures that are constructed from glass-fibre-reinforced polyester or from stainless steel plates insulated with mineral wool. The enclosure shall meet the requirements of IP 65 to prevent rainwater ingress. The chloride content in the mineral wool insulation should not exceed 10 mg/kg. The enclosures shall be provided with a door in the front. Enclosures in which the temperature needs to be kept above 50 C shall be provided on the front of the door with a red nameplate bearing the inscription in white: CAUTION: HIGH-TEMPERATURE SERVICE

PTS 32.31.50.11 September 2002 Page 20 The nameplate shall be in accordance with the requirements of PTS 32.31.00.32, but shall be screwed and not glued. The letter height shall be 20 mm. Hinges and locks shall be made of stainless steel.
NOTE: Special attention shall be paid to the installation of the mounting plate inside the enclosure and to the accessibility of components.

Vent, drain and condensate return lines may also require insulation and/or heat tracing to prevent freezing.

PTS 32.31.50.11 September 2002 Page 21 7. REQUIREMENTS FOR ELECTRIC AND ELECTRONIC EQUIPMENT Unless otherwise specified, all electric and/or electronic equipment shall have a type of protection adequate for the zone in which they are installed. For open ventilated areas, components shall have a minimum Zone 2 classification. Electric equipment installed inside the sample conditioning enclosure shall meet the requirements of IEC 60079-14 and shall: have a type of protection adequate for Zone 2, if the sources of release do not contain flammable substance; have a type of protection adequate for Zone 1, if only secondary grade sources of release of flammable substance are present; have a type of protection adequate for Zone 0, if primary grade sources of release of flammable substance are present.
1. The use of non-ventilated sample systems with primary grade sources of release requires written approval of the Principal. 2. Continuous grade sources of release of flammable substance are not permitted. 3. Components without a type of protection adequate for Zone 2 shall be installed in the analyser house, see PTS 32.31.50.12 and be located close to the relevant analyser. 4. For details of area classification, refer to IEC 60079-10.

NOTES:

The sample conditioning rack, the mounting plate, and if applied, the stainless steel enclosure shall each be provided with a brass M8 earthing bolt. All electrical equipment shall be connected to the plant earth by an insulated wire for personnel protection. The colour coding of the insulation shall be yellow/green.

PTS 32.31.50.11 September 2002 Page 22 8. DRAWINGS A set of drawings shall be prepared by the Manufacturer/Supplier for all sample conditioning systems, showing in detail: the correct position of components on the mounting plate; the arrangement of the interconnections; the method of support; a list of materials required.

For each analyser, an overview drawing showing the complete schematic from sample take-off to transport, conditioning, analyser and vent/drain and return line shall be provided. 'Engineering notes', e.g., operation of double block and bleed system, multiple stream switching valves, process conditions, line/tubing sizes, connections etc., shall be included on the drawings to assist in the proper use. The drawings shall be assembled in one set for each sample conditioning system, complete with cover sheet, index sheet, list of materials, list of settings, technical information and, if applicable, test certificates. If specified by the Principal, the Manufacturer/Supplier shall include operating instructions for start-up and maintenance of the sample conditioning system. The Manufacturer/Supplier shall send the drawings to the Principal for comments at least 30 working days before construction work commences. Three copies of the as-built drawings shall be shipped together with the sample conditioning system.
NOTE: The Manufacturer/Supplier may wish to apply a computerized system for the handling of components and installation materials that should provide the following information: itemized material requirements per conditioning system; total requirements per item; information of material ordering.

There are some examples of drawings attached to this PTS for sample conditioning systems for the various types of analysers. The drawings are to be read in conjunction with this PTS which provides comprehensive coverage of the design requirements of a sample conditioning system. The drawings are typical drawings and intended to serve as a guide; users may modify and/or adapt the drawings when necessary to suit the intended applications depending on the actual process conditions and the properties of the process samples to be analysed. The drawings are not intended to be exhaustive or to cover all types of analysers for all possible applications.

PTS 32.31.50.11 September 2002 Page 23 9. TESTING AND INSPECTION The Manufacturer/Supplier shall pressure test and inspect the sample conditioning system before offering the system for inspection by the Principal or the Principals representative. The Manufacturer/Supplier shall make available for the test and/or inspection: sufficient qualified labour to perform the test; air or nitrogen at a minimum pressure of 10 bar (ga) for the full duration of the test/inspection; air bubbler, maximum working pressure 10 bar (ga); a leak detector, measuring equipment for supplies and outputs; special measuring tools/equipment for components installed; power supply units as applicable, e.g. 24 V DC and 220 V AC; three copies of the as-built drawings.
The Manufacturer/Supplier shall ensure that all documentation, including material and/or construction certificate(s) for vessel(s) and/or components as applicable, is available before inspection starts.

NOTE:

The system shall be checked against the as-built drawings and the requirements of this PTS. When applicable, the related certificates shall be checked or verified. Site inspection and testing shall be carried out in accordance with PTS 62.10.08.11 and the Manufacturers own procedures. Attention shall also be paid on the ease of removal of sampling components and all the associated taggings and markings. The following tests and inspection procedures shall be performed: 1. Leak test The complete system shall be leak-tested by pressurizing via a bubbler with air or nitrogen at 1.1 times the design pressure of the system. If relief valve(s) form part of the system, the relief setting shall be the maximum applied pressure to test the system. Inlets and outlets shall be capped off with the exception of those which are provided with a valve. The isolating valve shall be closed for these connections. All other valves and reducers shall be fully opened. The maximum pressure applied shall not exceed 10 bar (ga). The system shall be pressurized for at least 5 minutes, while the bubbler is carefully observed. If there are signs of leakage, the Manufacturer/Supplier shall correct the leaking connection(s)/component(s). Manufacturer/Supplier shall be liable to repair any leakage problem on site when the sample conditioning system has been commissioned with actual sample flowing at process conditions. 2. Hydrostatic test Systems or parts of systems with a design pressure up to 9 bar (ga) shall be isolated from other parts of the system having a higher design pressure, and shall be opened to atmosphere during the hydrostatic test. Systems or parts of systems with a design pressure higher than 9 bar (ga) shall be pressurized at 1.5 times the design pressure via a tight shut-off valve and a high-quality pressure gauge (error to be within 0.5 % of the maximum scale value in the range of 10 % to 100 % of the scale).
NOTE: Fluids used for testing shall be compatible with the fluids to be analysed.

The pressure in the system shall remain constant for at least 10 minutes after the tight shut-off valve has been closed.

PTS 32.31.50.11 September 2002 Page 24 The system shall be thoroughly dried with clean dry air or nitrogen after draining. 3. Function test All electrical and electronic components shall be connected to the applicable power supplies and shall be function-tested. All pneumatic or electrically operated switching valves shall be tested to confirm the correct switching action and/or sequence as designed. All components of a SAIL system shall be tested in accordance with the functional specifications.

PTS 32.31.50.11 September 2002 Page 25 10. REFERENCES In this PTS, reference is made to the following publications.
NOTE: Unless specifically designated by date, the latest edition of each publication shall be used, together with any amendments/supplements/revisions thereto.

PETRONAS STANDARDS Index to PTS publications and standard specifications Gaseous-oxygen systems Piping - general requirements Piping classes - refining and chemicals Instruments for measurement and control On-line process stream analysis: - Sample take-off and transport - Analysers - Analyser houses Electrical engineering guidelines Inspection and functional testing of equipment Analyser Maintenance And Data Acquisition Systems (AMADAS) Guidelines for Implementation of ASTM D 6122 Product Release Using QMIs Materials and Equipment standards code (MESC) Buying Description AMERICAN STANDARDS Chemical Plant and Petroleum Refinery Piping
Issued by: The American Society of Mechanical Engineers, 345 East 47th Street, New York 10017, USA

PTS 00.00.05.05

PTS 31.10.11.31 PTS 31.38.01.11 PTS 31.38.01.12 PTS 32.31.00.32 PTS 32.31.50.10 PTS 32.31.50.12 PTS 32.31.50.13 PTS 33.64.10.10 PTS 62.10.08.11 OP 97-30425 OP 00-30408 MF 94- 0515 85.15.78.038.1

ASME B31.3

Specification for zinc (hot galvanized) coatings on products fabricated from rolled, pressed and forged steel shapes, plates bars and strip Specification for seamless and welded austenitic stainless steel piping for general refinery service
Issued by American Society for Testing and Materials, 1916 Race St., Philadelphia, Pa. 19103, USA

ASTM A 123

ASTM A 269

Standard specification for stainless steel bars and shapes Standard practice for validation of process stream analyzers Standard practice for the validation of multivariate process infrared spectrophotometers

ASTM A 276 ASTM D 3764 ASTM D 6122

PTS 32.31.50.11 September 2002 Page 26

Amended per Circular 38/04 Issued by: American Society for Testing and Materials 100 Barr Harbor Drive, West Conshohocken, PA 19428-2959 USA

Materials resistant to sulfide stress cracking in corrosive petroleum refining environments Petroleum and natural gas industries Materials for use in H2S-containing environments in oil and gas production
Issued by: NACE International 1440 South Creek Dr. Houston, TX 77084-4906, USA

NACE MR0103 NACE MR0175

BRITISH STANDARDS Hot dip galvanized coatings on iron and steel articles
Issued by: British Standards Institution 2 Park Street, London W1A 2BS, United Kingdom

BS 729

INTERNATIONAL STANDARDS
Amended per Circular 38/04

Petroleum and natural gas industries Materials for use in H2S-containing environments in oil and gas production Plain end steel tubes, welded and seamless General tables of dimensions and masses per unit length
Issued by International Organization for Standardization, 1, rue de Varemb, Post Box 56, CH-1211 Geneve 20, Switzerland

ISO 15156 ISO 4200

Electrical apparatus for explosive gas atmospheres: Part 10: Classification of hazardous areas Part 14: Electrical installations in hazardous areas (other than mines)

IEC 60079-10 IEC 60079-14

Issued by: Central Office of IEC (sales dept.) 3, rue de Varemb, 1211 Geneve 20, Switzerland Copies can also be obtained from most national standards organisations

PTS 32.31.50.11 September 2002 Page 27 11. APPENDICES Appendix 1 2 3 4 5 6 7

Index of typical sample conditioning system drawings Typical drawings of sample conditioning systems Components list of the sample conditioning system Typical vent and drain system for analyser houses Reference vessel for validation and calibration services Funnel and Syphon Typical layout drawing of SAIL

PTS 32.31.50.11 September 2002 Page 28 APPENDIX 1 INDEX OF SAMPLE CONDITIONING SYSTEM DRAWINGS

Typical liquid sample conditioning system for: Oil analysers (e.g. Colour, Flash point, Distillation, RVP) Fast Loop Oil analysers (e.g. Flash point, Distillation, RVP) - Fast Loop with Cooling Facility Oil analysers (e.g. Flash Point, Distillation) - Fast Loop and Reference Vessel Oil analysers (e.g. Cloud Point, CFPP, Freeze Point, Viscosity) - Fast Loop, Cooling Facility and Reference Vessel Water analysers (e.g. pH, Conductivity) - Single Line Water analysers (e.g. Dissolved Oxygen, Oil in Water) Single Line and Cooling Facility Chromatograph - Fast Loop

Typical gas sample conditioning system for: Water content analyser Density analyser Oxygen (Zicronic type) Chromatograph O2, H2S, SO2, NOx, CO, CO2, analyser etc.

PTS 32.31.50.11 September 2002 Page 29 APPENDIX 2 TYPICAL SAMPLE CONDITIONING SYSTEM FOR OIL ANALYSERS (Fast loop)

PTS 32.31.50.11 September 2002 Page 30 TYPICAL SAMPLE CONDITIONING SYSTEM FOR OIL ANALYSERS (Fast loop with cooling facility)

PTS 32.31.50.11 September 2002 Page 31 TYPICAL SAMPLE CONDITIONING SYSTEM FOR OIL ANALYSER (Fast loop with reference vessel)

PTS 32.31.50.11 September 2002 Page 32 TYPICAL SAMPLE CONDITIONING SYSTEM FOR OIL ANALYSERS (Fast loop with cooling facility and reference vessel)

PTS 32.31.50.11 September 2002 Page 33 TYPICAL SAMPLE CONDITIONING SYSTEM FOR WATER ANALYSERS (Single Line)

PTS 32.31.50.11 September 2002 Page 34 TYPICAL SAMPLE CONDITIONING SYSTEM FOR WATER ANALYSERS (Single line with cooling facility)

PTS 32.31.50.11 September 2002 Page 35 TYPICAL SAMPLE CONDITIONING SYSTEM FOR LIQUID ANALYSERS (Chromatograph)

PTS 32.31.50.11 September 2002 Page 36 TYPICAL SAMPLE CONDITIONING SYSTEM FOR WATER CONTENT ANALYSER

PTS 32.31.50.11 September 2002 Page 37 TYPICAL SAMPLE CONDITIONING SYSTEM FOR GAS DENSITY ANALYSER

PTS 32.31.50.11 September 2002 Page 38 TYPICAL SAMPLE CONDITIONING SYSTEM FOR OXYGEN ANALYSER (Zirconia type)

PTS 32.31.50.11 September 2002 Page 39 TYPICAL SAMPLE CONDITIONING SYSTEM FOR CHROMATOGRAPH ANALYSER

PTS 32.31.50.11 September 2002 Page 40 TYPICAL SAMPLE CONDITIONING SYSTEM FOR GAS ANALYSERS (e.g. O2, H2S, SO2, Nox, CO, CO2, etc).

PTS 32.31.50.11 September 2002 Page 41 APPENDIX 3 COMPONENTS LIST OF THE SAMPLE CONDITIONING SYSTEM

The Items refer to the drawings of Appendix 2. Item BVH Description Ball valve Size 0 12 0 1/2 0 1/2 0 1/2 0 12 0 1/2 0 6 0 1/4 0 6 0 1/4 0 6 0 1/4 0 6 0 1/4 mm OD in OD in in BSP NPT Item PRQ Description Pressure regulator Pressure gauge Flow meter Size 0 1/4 0 1/4 0 1/2 0 1/2 0 1/2 0 1/2 0 1/4 0 1/4 0 1/4 0 1/4
0 0 0 0 1/4 1/4 1/4 1/4

in in In in in in in in in in
in in in in

BSP NPT BSP NPT BSP NPT BSP NPT BSP NPT
BSP NPT BSP NPT

BLV

Block/bleed valve Globe valve

PGH

GVH

mm OD in OD mm OD in OD mm OD in OD mm OD in OD mm OD in OD

FIH

BVQ

Ball valve

FIV

NVQ

Needle valve

FIQ

Flow meter (with needle valve) Flow meter

CVQ

Check valve

FCQ

Flow controller
Excess flow valve

BVS

Ball valve 3-way

EFV

RVQ

Relief valve

0 0 0 0

6 1/4 1/4 1/4

mm in in in in in in in mm in in in in in mm in in in in in

OD OD BSP NPT BSP NPT BSP NPT OD OD BSP NPT BSP NPT OD OD BSP NPT BSP NPT

TGQ

Temperature gauge

0 0

1/4 1/4

in in

BSP NPT

FLF BPF

Fast loop filter By-pass filter Sintered filter

0 1/2 0 1/2 0 1/4 0 1/4 0 0 0 0 6 1/4 1/4 1/4

FNL SPH

Funnel

0 0 0

1/2 1/2 1/2

in in in

BSP NPT NPT

Syphon

STF

SGL

Sight glass

0 0

1/2 1/2

in in

BSP NPT

FCL

Filter/ coalescer In-line filter

0 1/4 0 1/4 0 0 0 0 6 1/4 1/4 1/4

RFV

Reference vessel Water cooler 0 1/4 0 1/4 in in BSP NPT

ILF

WCL

CLS
NOTE:

Coalescer

0 1/4 0 1/4

FPR

Filter/ regulator

0 1/4 0 1/4

n in

BSP NPT

Select the component required by placing a X in the 0

PTS 32.31.50.11 September 2002 Page 42 APPENDIX 4 TYPICAL VENT AND DRAIN SYSTEM FOR ANALYSER HOUSES

PTS 32.31.50.11 September 2002 Page 43 TYPICAL VENT AND DRAIN SYSTEM FOR ANALYSER HOUSE (Cont'd)

PTS 32.31.50.11 September 2002 Page 44 APPENDIX 5 REFERENCE VESSEL FOR VALIDATION AND CALIBRATION SERVICES

PTS 32.31.50.11 September 2002 Page 45 REFERENCE VESSEL FOR VALIDATION AND CALIBRATION SERVICES (cont'd)

PTS 32.31.50.11 September 2002 Page 46 APPENDIX 6 FUNNEL AND SYPHON

PTS 32.31.50.11 September 2002 Page 47 FUNNEL AND SYPHON (cont'd)

PTS 32.31.50.11 September 2002 Page 48 APPENDIX 7 TYPICAL LAYOUT DRAWING OF SAIL

Last page of this PTS