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, K. Prasad Rao
Department of Metallurgical and Materials Engineering, Indian Institute of Technology Madras, Chennai 600036, India
a r t i c l e i n f o
Article history:
Received 21 March 2013
Accepted 29 July 2013
Available online 6 August 2013
a b s t r a c t
The effect of post-weld heat treatments on the microstructure and mechanical properties of friction
welded joints of alloy 718 was studied in the present work. Alloy 718 rods were friction welded with
two prior heat treatments solution treatment and solution treatment and aging. Solution treatment
was done at 995 C for 1 h. Aging was done at 720 C for 8 h followed by furnace cooling to 620 C and
holding at 620 C for 8 h followed by air cooling. After friction welding, the joint samples were subjected
to two types of post-weld heat treatments direct aging (aging after welding, the same aging treatment
mentioned above) and solution treatment and aging. Electron back scattered diffraction technique and
transmission electron microscopy were used to study the development of microstructure. Hardness
and tensile properties of the weld joints were evaluated. In the as-welded condition, samples welded
with prior solution treatment and aging condition exhibited lower hardness at the weld zone and inferior
tensile properties compared to the base material due to the dissolution of strengthening precipitates in
the weld zone. On the other hand, formation of ne grains due to dynamic recrystallization led to higher
hardness at the weld zone compared to the base material welded with prior solution treatment condition.
Solution treatment and aging post-weld heat treatment resulted in an abnormal grain growth in the weld
zone and thermomechanically affected zone. Owing to the formation of strengthening precipitates, solu-
tion treatment and aging post-weld heat treatment resulted in a signicant increase in tensile strength of
joint samples compared to that of as-welded friction weld joints. However, solution treatment and aging
post-weld heat treatment done on friction weld joint samples with prior solution treatment or solution
treatment and aging heat treatment condition resulted in inferior tensile properties compared to those of
samples subjected to direct aging post-weld heat treatment. This may be attributed to grain coarsening
that occurred during the post-weld solution treatment. Therefore, direct aging after welding is the recom-
mended post-weld heat treatment for friction welded alloy 718 joints as compared to solution treatment
and aging after welding.
2013 Elsevier Ltd. All rights reserved.
1. Introduction
Alloy 718 is a c
00
(Ni
3
Nb) strengthened NiFe based superalloy
that exhibits excellent corrosion resistance and outstanding
strength at elevated temperatures. Alloy 718 is commonly welded
using fusion welding techniques such as tungsten inert gas weld-
ing, electron beam welding, and laser welding [1]. However, there
are problems associated with fusion welding of alloy 718 such as
the formation of Laves phase, Niobium segregation, microssuring,
which could occur in the fusion zone or heat affected zone (HAZ),
and affect the mechanical properties and service life [26]. Appli-
cation of a solid state welding process like friction welding could
be an alternative joining method to overcome these problems.
Friction welding has been commercially used in joining of aero
engine components, such as turbine blade disk (blisk) assemblies,
compressor wheel, compressor rotor, and rotor drum [7,8]. During
friction welding process, the material at the weld zone, thermome-
chanically affected zone (TMAZ) and HAZ undergoes changes in
temperature, gradient of strain, strain rate and microstructure.
Friction weld zone, in general, consists of very ne grains due to
the occurrence of dynamic recrystallization during the process
[9]. Wang et al. [10] reported an average grain size of 25 lm in
friction weld zone of alloy 718.
As the temperatures experienced during friction welding are
above the solvus temperatures of the strengthening precipitates,
dissolution of the precipitates can occur in the weld zone and
TMAZ/HAZ. Post-weld heat treatment is hence recommended to
regain the mechanical properties of alloy in the weld zone. Wang
et al. [11] observed no change in the ne grain microstructure of
weld zone after post-weld solution treatment at 1050 C followed
by aging treatment. Daus et al. [12] observed a reduction in hard-
ness value in the weld zone compared to base material due to dis-
solution of c
00
precipitates and loss in hardness could be recovered
0261-3069/$ - see front matter 2013 Elsevier Ltd. All rights reserved.
http://dx.doi.org/10.1016/j.matdes.2013.07.091