Professional Documents
Culture Documents
|
.
|
(
B
( ) ( ) log log , log log log ,
log
10 10 10 10 10 2
10
2
0 8 0 8 V V
B
T
T
x
x
+ = +
+
|
\
|
.
|
(
(
7
CALCULATION PROCEDURES
7.1 VISCOSITY
The viscosities given in Annex D are taken directly
from assay data. Where it is considered necessary to
calculate a viscosity at a particular temperature, other
than those quoted, a Refutas type equation can be used:
(7.1)
where:
V
x
is the unknown viscosity at temperature T
x
V
2
is the known viscosity at temperature T
2
B is the temperature/viscosity slope and is a constant
for each crude type
Note: The unit of kinematic viscosity is mm
2
/s,
formerly called the centistokes (cSt). The unit of
temperature is the Kelvin (K).
where: K = C + 273 (7.2)
Although the equation (7.1) is using Log
10
Log
10
(logs to
the base 10) throughout, natural logs (lnln) could also
be used. It is essential to use a constant log base.
The B factor for a particular crude oil may be
determined by substituting the two viscosity/
temperature pairs into equation (7.1). This factor can
then be used with one of the two known viscosity/
temperature pairs to determine the viscosity at a third
temperature, T
x
. Where available the tabulated data
include viscosities at two temperatures.
If only one viscosity/temperature pair is known
from assay data an average B factor of 3,50 can be used.
7.1.1 Example 1 - Calculation of a viscosity B
factor
Using the data for Maya crude oil given in Annex D,
the following viscosity/temperature pairs are obtained:
T
1
= 40,0C; V
1
= 84,30 mm
2
/s
T
2
= 60,0C; V
2
= 40,35 mm
2
/s
The two temperatures must first be converted from
Celsius to Kelvin:
T
1
= 40 + 273 = 313 K
T
2
= 60 + 273 = 333 K
Using equation (7.1) let T
x
= T
1
= 313 K, let V
x
=V
1
= 84,30 mm
2
/s, let T
2
= 333 K, and let V
2
= 40,35 mm2/s.
0,2855 = 0,2080 + (B x 0,0269)
B = (0,2855 0,2080)/0,0269
B = 2,88
HM 40 GUIDELINES FOR THE CRUDE OIL WASHING OF SHIPS TANKS AND THE HEATING OF CRUDE OIL BEING TRANSPORTED BY SEA
20
log log ( , ) log log ( , , )
, log
10 10 10 10
10
0 8 84 3 0 8
2 88
313
308
V
x
+ = +
+
|
\
|
.
|
(
log log ( , ) , ,
10 10
0 8 0 2855 0 0201 V
x
+ = +
( )
V
x
= +
(log log ( , , ) ,
10
1
10
1
0 2855 0 0201 0 8
7.1.2 Example 2 - Calculation of viscosity of a
typical crude oil at an arrival temperature
of 35C
In this example the B factor is 2,88 as calculated in
example 1.
T
x
= 35 + 273 = 308 K
From the two viscosity/temperature pairs given in
Annex D choose the pair whose temperature is closest
to T
x
. That is 84,3 mm
2
/s at 40C.
Using equation (7.1) the viscosity V
x
is calculated as
follows:
V
x
= 104,19 mm
2
/s
Viscosity at 35C is 104,19 mm
2
/s.
7.2 CLOUD POINT (CALC)
Two methods were used to calculate the cloud points in
Annex D. These methods assume different wax
concentration curves and neither method has been
proven to be more reliable than the other. The cloud
points for both methods are given as a temperature
range.
7.2.1 Method 1
This method is based on an early equation developed by
Dr T.J. Gunner:
Cloud Point (C) = 104,26(loglogF - 1,55) (7.3)
where: F
T
=
+ = a |
2
and = 4(W
550
x M
550
x C
550
)
= 2(W
509
x M
509
x C
509
)
= (W
369
x M
369
x C
369
)
T = C
149
,C
232
,C
342
,C
509
,C
550
and W
x
is the wax content (% weight) of the
relevant C
x
'cut'.
M
x
is the melting point (C) of the wax
content W
x
.
C is the % weight of the given distillation
'cut'.
Note: The subscript numbers have been used to indicate
the distillation fraction (boiling range) on a crude oil
assay such that:
149 means the cut between C
5
and 149C
232 means the cut between 149C and 232C
342 means the cut between 232C and 342C
369 means the cut between 342C and 369C
509 means the cut between 369C and 509C
550 means the cut between 509C and 550C
Generally the assay cut points are company dependent
and will not conform to those given above. However,
there are software distillation packages available that
will transform any series of 'cut' points to conform to
those shown above.
Many crude oil assays do not report the melting
points of the wax contents of the various fractions. A
survey of the data available from 150 crude oils
revealed the mean values and standard deviation from
the mean of the three relevant fractions to be:
Crude 'Cut'
(C)
Mean Melting
Point
(C)
Standard
deviation
(C)
550 65 4
509 53 3
369 39 1
It is recommended that if wax melting points are not
available then the above values are used.
7.2.2 Method 2
This utilises the blending indices of the various
distillation 'cuts'. The blending index is calculated using
the following equation:
Log
10
I = 0,02916(Cloud Point(C) + 73,33)
(7.4)
where I is the blending index of the fraction under
consideration. However, it is usual to add a subscript to
indicate the particular fraction.
For fractions distilling below 149C the index is
assumed to be zero. For the fraction boiling between
CALCULATION PROCEDURES
21
CPI
W W I W I W I
B
=
+ + + |
\
|
.
|
( , ) ( ) ( ) ( )
149 232 232 342 342 369 369
4 8
100
149C and 232C, denoted by I
149
, the index is 4,8. For
the middle distillate fractions in the higher boiling
ranges the blending index has to be calculated from
cloud points given in the crude oil assay. To do this, the
cloud point for each fraction is substituted into equation
(7.4). For residues where only the pour point is
reported, the cloud point is assumed to be 2C above
the pour point and the index calculated.
The blending indices for each cut are now
combined on a weight basis, according to the
percentage weight of each fraction in the crude oil, to
derive what may be termed the cloud point index of the
blend, CPI
B
. That is, the cloud point index for the crude
oil in question:
(7.5)
where:
W
149
is the percent weight of the fraction boiling
between 149C and 232C.
W
232
is the percent weight of the fraction boiling
between 232C and 342C.
W
342
is the percent weight of the fraction boiling
between 342C and 369C.
W
369
is the percent weight of the fraction boiling
greater than 369C
I
232
,I
342
and I
369
are the cloud point indices
calculated for the above fractions.
Once the CPI
B
has been derived it can be entered into
equation (7.6) to calculate the required cloud point of
the crude oil:
Log
10
CPI
B
= 0,02916(Cloud Point(C) + 73,33)
(7.6)
Where the assay data do not include boiling data at the
temperatures prescribed above, other boiling points can
be used along with their corresponding cloud points.
7.2.3 Simplified procedure
Another equation is available to readers having no
assay data. This is especially true for marine staff who
may only have a load port Certificate of Quality. It is
based upon the crude oil pour point and may be subject
to very high uncertainty.
Cloud Point(C) = (20,2 x 10
(0,00708y - 0,1157714)
)+8
(7.7)
where: y is the crude oil pour point (C).
7.2.4 Example 3 - Calculation of Cloud Point
using equation (7.7)
Consider a cargo of Brent Blend crude oil where the
Certificate of Quality advises that the pour point is
3C.
First calculate the exponential term in equation (7.7):
Exponential term = (0,00708 x pour point) 0,1157714
Exponential term = (0,00708 x 3) 0,1157714
Exponential term = -0,1370114
Cloud Point = (20,2 x 10
0,1370114
) + 8
Cloud Point = 23C
The cloud points calculated from methods 1 and 2, and
given in Annex D, give the range 20C to 26C. For
this crude oil the simplified method appears reasonable.
Further information can be found in the IMO Crude Oil
Washing Systems, Section 9 of the Standard Formats
(page 26- page 29).
HM 40 GUIDELINES FOR THE CRUDE OIL WASHING OF SHIPS TANKS AND THE HEATING OF CRUDE OIL BEING TRANSPORTED BY SEA
22
23
ANNEX A
IP CRUDE OIL
DATA SUBMISSION FORM
Users having data or experience in handling a crude oil
not fully described in these guidelines, or more recent
data than that shown, please complete a copy of the
following form and return to:
Technical Department
Hydrocarbon Management Section
Energy Institute
61 New Cavendish Street
London W1G 7AR
United Kingdom
Test methods
The data for API Gravity, RVP, Pour Point and
Kinematic Viscosity should be based upon the results
obtained from current standard test methods. The
procedures to be employed can be found in the IPs
Standard methods for analysis and testing of petroleum
and related products and British Standard 2000 Parts
(latest available edition - published annually) or the
annual book of ASTM Standards, Section 5, Petroleum
Products, Lubricants, and Fossil Fuels, volumes 1 to 6
(latest available edition published annually).
Alternatively there may be equivalent ISO or National
Standards.
Gas to C
4
will only be available from assay data.
Total wax and cloud point may only be available after
calculation based upon assay data.
Suggested temperatures
The carriage and discharge temperatures should be
based on a balance between operational requirements,
as well as financial and environmental concerns.
Comments on experiences of handling crude
Even if quality data are not available, should users be
involved in the handling of a crude oil where an
unusual characteristic was observed please spend a few
moments in completing the comments section on the
form. Other useful information to be included would be
COW programme, voyage route and dates, air and sea
temperatures (averages on route and those experienced
during discharge).
The above information will be used in future
editions of this publication.
HM 40 GUIDELINES FOR THE CRUDE OIL WASHING OF SHIPS TANKS AND THE HEATING OF CRUDE OIL BEING TRANSPORTED BY SEA
24
IP CRUDE OIL DATA SUBMISSION FORM
Name: Indicate Test Standards Used ()
Organisation: Standard Edition
Address: IP
ASTM
Other (Specify)
Date:
Crude Oil:
Test Data Test Method Used
API Gravity
RVP (psi)
Gas to C
4
(% m/m)
Total Wax (% m/m)
Pour Point (C)
H
2
S (ppm)
Liquid Phase
H
2
S (ppm) *
Vapour Phase
Benzene (% m/m)
Liquid Phase
Kinematic
Viscosity mm
2
/s
T
1
(C) V
1
(cSt)
T
2
(C) V
2
(cSt)
Loaded Temp.
(C)
Carriage Temp.
(C)
Discharge Temp.
(C)
Recommended COW codes: AW/AS BW/BS
Comments on Experiences of Handling this Crude Oil
* - If H
2
S reading in vapour space, please list previous cargo.
25
ANNEX B
CLIMATIC CHARTS OF THE WORLD
Permission to reproduce the following four figures was
kindly given by the Controller of Her Majestys
Stationery Office. The attached charts have been
included to show mean air and sea temperatures for
February and August.
It is hoped they will enable the user to gain better
insight into the expected ambient conditions which may
be experienced during a proposed voyage. Other factors
not included in this publication, but which may have a
large effect on the vapour emission from the cargo, are
wind speed, wind direction and sea state.
26
F
i
g
u
r
e
B
.
1
M
e
a
n
s
e
a
s
u
r
f
a
c
e
t
e
m
p
e
r
a
t
u
r
e
(
C
)
,
F
e
b
r
u
a
r
y
27
F
i
g
u
r
e
B
.
2
M
e
a
n
s
e
a
s
u
r
f
a
c
e
t
e
m
p
e
r
a
t
u
r
e
(
C
)
,
A
u
g
u
s
t
28
F
i
g
u
r
e
B
.
3
M
e
a
n
a
i
r
t
e
m
p
e
r
a
t
u
r
e
o
v
e
r
t
h
e
o
c
e
a
n
s
(
C
)
,
F
e
b
r
u
a
r
y
29
F
i
g
u
r
e
B
.
4
M
e
a
n
a
i
r
t
e
m
p
e
r
a
t
u
r
e
o
v
e
r
t
h
e
o
c
e
a
n
s
(
C
)
,
A
u
g
u
s
t
HM 40 GUIDELINES FOR THE CRUDE OIL WASHING OF SHIPS TANKS AND THE HEATING OF CRUDE OIL BEING TRANSPORTED BY SEA
30
31
ANNEX C
COMMENTS ON THE HANDLING OF
SOME CRUDE OILS
Each comment is preceded by the date of the
observations in the format (month/year).
Brent Blend
(11/01)
A number of cargoes have been reported as having been
found to have vapour space H
2
S readings in excess of
60 ppm at the receiving port. Further reports were
received at the 05/02 meeting. A general warning was
posted on the website.
Ezzaouia crude oil
(4/94)
This is a crude oil that must be heated to at least 57C.
It is often carried as a small single grade and can be
treated as a heavy fuel oil. If the vessel is fitted with
COW machines a wash with the hot crude has been
found to be beneficial.
Flotta
(9/94)
Experiences of some parts of the industry indicate that
there may be problems with varying cloud point from
cargo to cargo. Sedimentation may be a problem but
when heating is applied losses of light ends are evident.
Some companies do not COW with this grade
especially on short haul voyages where the cargo
retains its heat.
Iranian Light
(4/95)
It was reported that a cargo of Iranian Light loaded at
20C, but unheated, lost 0,2 % of vapour during loaded
passage. Cargo cooling during the voyage led to
significant sludge deposition which took 14,5 hours to
COW and seven hours to educt.
Maya
(4/95)
This crude has been reported as being carried unheated
with a parcel of Isthmus. The Isthmus was used to wash
all tanks.
Miskar Condensate
(10/02)
This warning was posted onto the website. Miskar has
been found to contain 4,7% vol benzene in the liquid
phase. Vapour levels are usually below permissible
exposure levels. However, personnel involved in
transportation and inspection should wear appropriate
protective equipment. Benzene content of vapour
spaces should be checked prior to inspection and
appropriate precautions taken.
HM 40 GUIDELINES FOR THE CRUDE OIL WASHING OF SHIPS TANKS AND THE HEATING OF CRUDE OIL BEING TRANSPORTED BY SEA
32
Nile Blend
(10/00)
Members were referred to an article in Lloyds List
dated 20/10/00 where it was reported that difficulties
had been found when discharging this grade. High
ROBs were being experienced.
(11/01)
It was reported that large quantities of wax were being
deposited from Nile Blend cargoes. 100 m
3
was not
unknown on a number of cargoes. These deposits were
being carried over onto subsequent voyages.
Palanca crude oil
(9/94)
This crude oil has a relatively high total wax content
which makes the outturn very uncertain. This crude oil
will COW but the wash fluid may become saturated
during the washing and lose its solvency. Once this
occurs stripping becomes very difficult. For this crude
oil re-cycled oil must not be used for COW. However,
good discharge results have been obtained by using gas
oil for washing.
(4/95)
It has been reported as having been carried without
heating, loading at 28C and discharging at 18C.
Another crude oil grade was backloaded and used for
COW. The backloaded crude oils successfully tried
were Saharan Blend and Qua Iboe. There was less loss
using Qua Iboe which may have been due to the lower
gas content of this crude oil when compared to Saharan
Blend.
Urals (previously Russian export blend)
(05/02)
High vapour space H
2
S levels have been reported above
this grade.
Syrian Light crude oil
(4/94)
This crude oil can be very difficult to handle as the wax
content is relatively high. Ambient weather conditions
are very important and will affect the discharge. If
transported within the Mediterranean Sea heating will
not be required in summer, however it is likely that
heating will be required in winter. If the vessel
discharges in Northern Europe then it is probable that
heating will be required even in the summer.
Although the cargo may need to be heated good
outturn results can be obtained by heating the contents
of the slop tanks by a further 10C, just prior to
discharge, and using for COW.
(5/97)
There was a recommendation to L-4B that Syrian Light
crude oil should be heated to 35C from the time of
sailing, and maintained at that temperature, to
completion of discharge. A warning was given that if
no heating is applied then the final ROB in the winter
may constitute 0,5% of the loss (3 000 US Barrels on a
standard parcel size), whereas in the summer this may
reduce to 0,25%, 1 500 Barrels. However, washing with
Syrian Light has been known to cause accumulation of
paraffins and wax on cold tanker bulkheads.
Carriage at temperatures greater than 40C will
result in light end loss thereby contributing to the
overall outturn loss.
(05/02)
High vapour space H
2
S levels have been reported above
this grade.
Further up-to-date reports can be found on the HM L-4
website at www.oil-transport.info or via the EI website
www.energyinst.co.uk.
33
ANNEX D
CRUDE OIL DATA
Explanations for the assay categories can be found in
Section 5. The following codes should be referred to in
conjunction with the data sheets that follow. For ease of
viewing it was decided to display the tabulated data in
landscape mode, thus qualities and remarks concerning
each crude are spread over two pages.
The committee has made every attempt to ensure
that the data are correct. However, differences may be
experienced from that described in this section since the
quality of crude oil can change rapidly in a short time,
especially if it is blended from a number of small fields.
Should the user of this publication become aware
of any information that may be relevant under the scope
of this document, please forward the information to the
Institute on the form provided in Annex A.
D.1 COW CODES
D.1.1 Clean Ballast Tankers (CBT)
A1 Minimum MARPOL. Maximum possible safe trim
for stripping tanks and lines. Strip all cargo tanks
at least twice, three times if time permits.
Note: Minimum MARPOL: is that defined in Section
6.1 of the Revised specifications for the design,
operation and control of crude oil washing systems
found in IMO publication Crude oil washing systems,
fourth edition 2000.
A2 Minimum MARPOL: plus a bottom wash of
remaining cargo tanks.
A3 Full cycle wash of all cargo tanks.
A4 Minimum MARPOL: plus a full wash of remaining
wing tanks and a bottom wash of remaining centre
tanks.
A5 No COW, except with a suitable crude oil or cutter
stock such as heated gas oil. Otherwise treat as
heavy fuel oil with maximum possible safe trim
for stripping.
A6 Cargoes are small, normally carried in heavy fuel
oil tankers, and treated in the same way as heavy
fuel oil.
A7 Minimum MARPOL: plus a bottom wash of
remaining cargo tanks, using the contents of the
slop tanks. Oil in the slop tanks should be heated to
at least 10C above the average cargo temperature.
A8 Full cycle wash of all cargo tanks, using the
contents of the slop tanks for COW. The COW
medium should be heated to at least 10C above
the average cargo temperature.
D.1.2 Segregated ballast tankers (SBT) (Heavy
Weather ballast tanks are subject to
MARPOL COW requirements, see D.1.1)
B1 No COW. Maximum possible safe trim for
stripping tanks and lines. Strip all tanks at least
twice, three times if time permits.
HM 40 GUIDELINES FOR THE CRUDE OIL WASHING OF SHIPS TANKS AND THE HEATING OF CRUDE OIL BEING TRANSPORTED BY SEA
34
B2 Bottom wash only required.
B3 Full cycle wash of all cargo tanks.
B4 Full cycle wash for cargo wing tanks and a bottom
wash for cargo centre tanks.
B5 No COW, except with a suitable crude oil or cutter
stock such as heated gas oil. Otherwise treat as
heavy fuel oil with maximum possible safe trim for
stripping.
B6 Cargoes are small, normally carried in heavy fuel
oil tankers, and treated in the same way as heavy
fuel oil.
B7 Bottom wash all cargo tanks, using the contents of
the slop tanks. Oil in the slop tanks should be
heated to at least 10C above the average cargo
temperature.
B8 Full cycle wash of all cargo tanks, using the
contents of the slop tanks for COW. The COW
medium should be heated to at least 10C above
the average cargo temperature.
35
ANNEX D.2
CRUDE OIL DATA SHEETS
A
N
N
E
X
D
-
C
R
U
D
E
O
I
L
D
A
T
A
S
H
E
E
T
S
3
6
C
R
U
D
E
T
Y
P
E
U
P
D
A
T
E
D
A
P
I
V
A
P
O
U
R
G
A
S
<
C
4
T
O
T
A
L
P
O
U
R
C
L
O
U
D
V
I
S
C
O
S
I
T
Y
H
2
S
H
2
S
B
e
n
z
e
n
e
G
R
A
V
I
T
Y
P
R
E
S
S
U
R
E
W
A
X
P
O
I
N
T
P
O
I
N
T
(
C
a
l
c
)
m
m
2
/
s
O
i
l
P
h
a
s
e
V
a
p
o
u
r
P
h
a
s
e
(
p
s
i
g
)
(
%
m
/
m
)
(
%
m
/
m
)
(
C
)
(
C
)
(
p
p
m
)
C
o
n
f
i
r
m
e
d
(
%
m
/
m
)
(
T
y
p
i
c
a
l
)
(
R
a
n
g
e
)
(
R
a
n
g
e
)
(
R
a
n
g
e
)
T
1
V
1
T
2
V
2
(
T
y
p
i
c
a
l
)
A
b
u
A
l
B
u
K
h
o
o
s
h
F
e
b
-
0
2
3
3
,
6
4
,
7
0
-
1
,
1
5
5
,
5
0
-
3
7
-
1
2
1
4
3
2
2
0
9
,
9
5
4
0
5
,
7
2
-
-
A
b
u
S
a
f
a
h
A
p
r
-
9
8
2
8
,
9
0
3
,
1
0
-
6
,
5
0
-
-
2
9
-
1
8
-
-
2
0
2
4
,
3
1
4
0
1
1
,
8
8
1
3
,
0
-
A
C
G
B
l
e
n
d
J
u
l
-
9
8
3
4
,
6
0
-
-
0
,
8
5
6
,
5
1
-
3
-
2
4
2
9
2
0
1
5
,
6
2
4
0
6
,
7
4
-
-
A
i
r
l
i
e
B
l
e
n
d
M
a
y
-
9
6
4
3
,
7
0
1
,
8
0
-
0
,
9
5
4
,
1
7
-
1
8
-
1
5
2
7
2
0
2
,
4
8
3
0
2
,
0
5
-
-
A
k
s
a
i
C
o
n
d
e
n
s
a
t
e
N
o
v
-
0
0
4
4
,
3
-
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