Experiment Report of Inorganic Chemistry 2

Experiment Report of Inorganic Chemistry 2

VIII. Table Result Of Experiment
No

Procedure

1.

Result
Before :

Manganese powder (point of spoon)

- Added same grain of NaCl into test tube

- Added a little H2SO4
- Heated

Hypothesis
2H2SO4(aq) +2NaCl(s)

MnO2 (s) : black powder

HCl(aq) + NaHSO4(aq)

NaCl (s) : white granule

MnO2(s) + 2H2SO4(aq)

Conclusion
Test tube formed gas
chlorin

H2SO4 0.1M :colorless

+2NaCl(s) Na2SO4(aq)

The faster of filter

KI : colorless

+ MnSO4(aq) + 2H2O(l) +

paper show the color

Amylum : colorless

Cl2(g)

is 1b (mixed with

2 I-(aq) + Cl2(g) I2(g) +

gas
After :
- Hold filter paper wet KI and amylum
-

solution above gas

MnO2 (s) +NaCl (s) +

H2SO4 = black color and

result

theres back precipitate

-

After test with wet filter

paper of KI and amylum
the filter paper become
purple

After heated theres gas of

chlor

2Cl-(aq)

KBr) and 1a is slower

(mixed with NaCl)

Experiment Report of Inorganic Chemistry 2

1b

Manganese powder (point of spoon)

Before :

MnO2 + 2H2SO4

Bromin gas can make

MnO2 (s) : black powder

+2KBr K2SO4 +

by reaction between

- Added same grain of KBr into test tube

KBr (s) : white granule

MnSO4 + 2H2O + Br2

MnO2(s) + 2H2SO4(aq)

- Added a little H2SO4

H2SO4 0.1M :colorless

- Heated

KI : colorless
Amylum : colorless

gas
- Hold filter paper wet KI and amylum
solution above gas

After :
- MnO2 (s) +KBr(s) + H2SO4
= black color and theres

result

black pecipitate
-

After heated theres gas of

bromin

After that test with wet

filter paper of KI and
amylum the filter paper
become purplish blue

+ KBr(s)
2 I- + Br2 I2 + 2Br-

Experiment Report of Inorganic Chemistry 2

2a

1mL NaCl + little

drops AgNO3 0.1M

1mL NaCl + little

drops Pb(CH3COO)2

Before
NaCl(aq) : colorless
AgNO3(aq) : colorless

mixed

mixed

precipitate

precipitate

1mL NaCl + little

drops HgNO3 0.1M

HgNO3(aq) : colorless
Pb(CH3COO)2(aq) :
colorless

precipitate

Tube 1
NaCl(aq) + AgNO3(aq)
become white precipitate
Tube 2

comparison

AgCl(s) + NaNO3(aq)

NaCl(aq) + HgNO3(aq)
become little turbid
Tube 3
NaCl(aq) + Pb(CH3COO)2(aq)
: white turbid

When chlorine reacts

with Ag, Hg, Pb. It

NaCl(aq) + HgNO3(aq) form salt that can not

HgCl(s) + NaNO3(aq)
2NaCl(aq) +
Pb(CH3COO)2(aq)
PbCl2(s) + 2CH3COONa

After
mixed

NaCl(aq) + AgNO3(aq)

soluble and white

precipitate

Experiment Report of Inorganic Chemistry 2

2b

Before
1mL KBr + little
drops AgNO3 0.1M

1mL KBr + little

drops Pb(CH3COO)2

KBr(aq) : colorless
AgNO3(aq) 0.1 M :

mixed

mixed

precipitate

precipitate

HgNO3(aq) 0.1 M :
Pb(CH3COO)2(aq) 0.1M :
colorless

mixed
precipitate

After
Tube 1
KBr(aq) + AgNO3(aq) :
white precipitate +

comparison

colorless

colorless
1mL KBr + little
drops HgNO3 0.1M

Tube 2
KBr(aq) + HgNO3(aq) :
prceipitate dissolved
Tube 3

KBr(aq) +
Pb(CH3COO)2(aq) : white
precipitate

KBr(aq)+AgNO3(aq)

When bromine reacts

KNO3(aq)+ AgBr(s)

with Ag, Hg and Pb, it

2KBr(aq)+2HgNO3(aq)

forms salt that can not

2KNO3(aq)+ Hg2Br2 (s)

soluble, pale yellow

KBr (aq) + CH3COOPb

and white precipitate

(aq)

CH3COOK (aq) +

PbBr (s)

Experiment Report of Inorganic Chemistry 2

3

Caporyte (CaOCl)2(s)
filter

2CaOCl2(s) + H2O(l) +

The tube without HCl

Caporite : white powder

CO2 CaCO3 +HOCl

is more lower to make

HCl : colorless

+ CaCl2

a sheet of colored

Before

Aquadess : colorless

filtrate

HOCl + H+ + Cl- Cl

paper become white

+ H2O
Test tube
Let it
Result

Test tube 2
Entered some drops of HCL
0.1M

After

Test tube 2 with HCl

After filtrate the solution

is faster to make
asheet of colored

become colorless

paper become

After entered a sheet of

Entered a sheet of colored paper

white(pale)

colored paper on the two,

the colored paper

Result

become white
4a

NaCl +H2SO4 concentrated

NaCl = colorless

- Heated

H2SO4 = colorless

- Flowed to water dilluted

KI : colorless

Amylum : colorless

- Connected to pipe

solution

Before

NaCl(s)+H2SO4(aq)NaH a. Theres gas of

SO4(aq) + HCl (g)

chlorin
b. Theres gas of
bromin
c. Theres gas of iodin

Test tube 2

After
After flowet to water
dilluted theres gas of

KI formed much
purplish black color
in filter paper

Experiment Report of Inorganic Chemistry 2

chlorin the gas is very
solution

Test tube 2

bad smell and colorless

- Tested

with

litmus

paper
- Entered a sheet of

- Tested

filter

paper that wet by KI +

amylum

color paper

Result

with

Result

The filter paper become

KBr formed yellow

color in top of filter
paper

and

the

purple but just a little in

bottom is purplish

top of filter paper

blue

After solution test with

NaCl formed purple

litmus paper, red litmus

color but just a little

still red and blue litmus

in top of filter paper

paper become red

The most
concentrated color
are :
KI > KBr > NaCl

Experiment Report of Inorganic Chemistry 2

4.2

KBr

Before

KBr +H2SO4 concentrated

- Heated

After
After flowed to water

solution

dilluted theres gas of

Test tube 2

bromin it have bad smell

- Tested

with

litmus

paper
- Entered a sheet of

- Tested

filter

paper that wet by KI +

amylum

and colorless
The precipitate become
orange but not all, just a

color paper

Result

with

Result

part
The filter paper theres
yellow color in top of and
the bottom purplish blue
litmus paper , red and
blue
changed

litmus

+ H2SO4

(aq)

HBr (g) + KHSO4 (aq)

KBr : colorless
- Connected to pipe

- Flowed to water dilluted

(s)

doesnt

Experiment Report of Inorganic Chemistry 2

4.3

After

KI +H2SO4 concentrated

After flowed to water

- Connected to pipe
- Heated

dilluted theres gas of iod

- Flowed to water dilluted

it have bad smell and

KI (s) + H2SO4 (aq)

HI(g) + KHSO4 (aq)

colorless
solution
- Tested

The precipitate become

Test tube 2
with

- Tested

litmus

with

filter

paper that wet by KI +

paper

amylum

- Entered a sheet of

yellow little, its to much

purplish black color
The precipitate become
purplish black

color paper

Result

Result

Red and blue litmus paper

doesnt changed

5.

Test tube 1

Test tube 2

Test tube 1

1mL NaCl
solution

1mL KBr
solution

1mL KI
solution

Before
NaCl : colorless
KI : colorless
KBr : colorless

- In each test tube flowed chlorine gas

- Added CS2
- Comparared

CS2 : colorless

NaCl(aq) + Cl2(g)

The much gel is when

mixed with KI, the

NaCl(aq) +Cl2(g)
2KBr (aq) + Cl2 (g)
(g)

Br2

NaCl and the little gel

+ 2KCl (aq)

2KI (aq) + Cl2 (g)

+ 2KCl (aq)

second is mix with

I2 (g)

is when mixed with

KBr

Experiment Report of Inorganic Chemistry 2

Result

After :
Test tube 1 : After flowed
chlorine gas formed chlorin
colorless 2 layer
After added CS2 theres gel
(+) in bottom

Test tube 2 : after flowed

chlorine gas formed Bromin
After added CS2 theres gel
in bottom

Test tube 3 : after flowed

chlorine gas formed Iod
After added CS2 theres gel
(++)

Experiment Report of Inorganic Chemistry 2

6

Before
Test tube 1

Test tube 2

Test tube 1

iodine

Iodine

Iodine

Added
water

Added KI

Added HCl

- Compared the solubility and the color of

Iodine granule : black

granule
Aquadess : colorless
KI : colorless
HCl : colorless

solution
After
Result

Test tube 1 : I2(s) +

aquadest: solute but not all,
the color brown (+)
Test tube 2 : I2(s) + KI more
solute the color dark brown
Test tube 3 :
I2(s) + KI: solute but not all, the
color light brown (++)

I2 (s) + H2O (l)

2HI +

HCl > H2O

O2

I2 (s) + KI (aq)

I2 (s) + HCl (aq) HI

+ Cl2

I2 most soluble in KI >

KI3 (aq)

Experiment Report of Inorganic Chemistry 2

Experiment Report of Inorganic Chemistry 2