You are on page 1of 16

Tapas Kumar Pal et. al.

/ International Journal of Engineering Science and Technology


Vol. 2(9), 2010, 4775-4790

DESIGN, FABRICATION AND RF


CHARACTERIZATION OF KA-BAND
SILICON IMPATT DIODE
TAPAS KUMAR PAL
Research Centre Imarat
Vignyana Kancha
Hyderabad 500 069, INDIA.

J. P. BANERJEE
Centre for Millimeterwave Semiconductor Devices and Systems
Institute of Radiophysics and Electronics
University of Calcutta, Kolkata 700009, INDIA.

Abstract:
A silicon (p+nn+) SDR IMPATT diode for Ka-band operation has been designed by using a double iterative DC
and Small signal simulation which involves simultaneous solution of Poissons equation and Carrier continuity
equation, satisfying appropriate boundary conditions in the depletion layer edges. Using the design parameters,
silicon epitaxial n/n+ wafers of appropriate thickness and resistivity of the epitaxial layer have been selected for
fabrication of (p+nn+) SDR IMPATT diode for Ka-band operation. The (p+nn+) SDR IMPATT diode has been
fabricated through diffusion technique. The optimized process steps of fabrication, starting from wafer cleaning
to packaging have been described in details. The DC V-I and RF characteristics of fabricated IMPATT diode
have been measured by using an integrated heat sink cum resonant cap waveguide cavity.
Keywords: Design, Fabrication, RF characterization, Small signal simulation, Silicon SDR IMPATT diode.
1.

Introduction

IMPact Avalanche Transit Time (IMPATT) devices have emerged as most powerful solid-state devices for
generation of high CW and pulsed power at millimeter wave frequencies [1], [2]. These devices provide high
oscillator output power with high DC to RF conversion efficiency in Silicon Monolithic Millimeter Wave
Integrated Circuits (SIMMWIC) [3]. The authors have designed a silicon (p+nn+) SDR IMPATT diode for Kaband operation by using double iterative DC and Small signal simulation methods which involve simultaneous
solution of Poissons and Carrier continuity equation with appropriate boundary conditions at the depletion
layer edges [4]. Based on the DC and Small Signal simulation the authors have appropriately selected silicon
epitaxial wafers with phosphorus and antimony as n and n+ dopants respectively. The substrate resistivity is
selected in the range of 0.0174 - 0.0185 ohm-cm and epitaxial resistivity in the range of 0.45-0.55 ohm-cm [5]
for fabrication of (p+nn+) SDR Ka- band IMPATT Diode.
The metallurgical junction of a silicon (p+nn+) SDR IMPATT diode can be grown by different techniques i.e. (i).
Diffusion (ii). Ion implantation (iii). Chemical vapor deposition and ( iv). Molecular Beam Epitaxy (MBE) . The
authors have chosen the diffusion route since it is the simplest method of fabrication of single drift diode, which
involves diffusion of p-type impurities in n/n+ epitaxial wafer [6]. The authors have used Boron as p-type dopant
since it can be diffused into silicon by solid source like Boron Nitride (BN), liquid source like Boron Tri
Bromide (BBr3) and gaseous source like Diborane (B2H6). The source BBr3 is highly volatile in nature and B2H6
is highly toxic, therefore solid source BN is chosen for easy handling of the doping source.
The major process steps adopted by the authors for fabrication of SDR IMPATT diodes are (i) wafer cleaning
(ii) Activation of Boron Nitride (BN) (iii) Stabilization of BN (iv) Pre-deposition of Boron (v) Drive in
Diffusion (vi) Low Temperature Oxidation (LTO) (vii) Cr-Au Metallization of p+ side (viii) Electroplating of
metalized p+ side (ix) Thinning of n+ side (x) CrAu Metallization of n+ side (xi) Photolithography (xii) Mesa
etching (xiii) Chip separation (xiv) Die/wire Bonding and packaging.

ISSN: 0975-5462

4775

Tapas Kumar Pal et. al. / International Journal of Engineering Science and Technology
Vol. 2(9), 2010, 4775-4790
For DC and RF characterization the diode is to be placed in a suitable microwave/mm wave cavity and mm
wave power is delivered by the device biased to break down [7]. The authors have used a resonant cap wave
guide mount [8] consisting of a resonant cap structure under which the diode is embedded and the two together
are mounted in a rectangular wave guide. The cap and the bottom surface of the wave guide form a localized
radial cavity around the diode. The mm wave signal generated by the diode is coupled to the main rectangular
wave guide cavity through the vertical open edges of the radial cavity.
2.

DC and Small Signal Simulation

One-dimensional model of a reverse biased


junction diode considered by the authors for DC and Small
signal simulation has been schematically shown in Fig.1, with symbols having their usual meaning [9]. The total
current is composed of conduction current and displacement current only because the diffusion current is
negligibly small. The total current density is thus given by
(1)
The spatial variation of electric field in the space charge layer is obtained from Poissons equation as
(2)
= ionized donor density,
Where E = electric field, q = electronic charge,
hole density, n = electron density, = permittivity of the semiconductor.
The equations of continuity for electrons and holes are given by

= ionized acceptor density, p =

(3.a)
(3.b)
where g is the generation rate,
is the ionization rate and
is the velocity of charge carriers.
The above mentioned parameters are expressed in the following equations
(3.c)
(3.d)

(3.e)
where

indicates the saturated drift velocity and

n, p is the mobility of charge carriers.

From the above equations the fundamental time and space dependent differential equation involving the electric
field and the total current density under dynamic condition is given by

(4)
Where,

ISSN: 0975-5462

4776

Tapas Kumar Pal et. al. / International Journal of Engineering Science and Technology
Vol. 2(9), 2010, 4775-4790

n+

P+

= Position of field maximum (E0),

= Position of Avalanche centre

= Drift layer widths for electrons and holes,

= Total active layer widths =

= Avalanche layer width =

= Total current density =

Fig. 1 The active layer of a reverse biased p n junction

To linearize the non-linear Eq. (4), we introduce a parameter H [10] mentioned above. Hence
(5)
where

= ac impedance.

regions be at the co-ordinates


Let the boundaries of
(
.
Eq. (1), the boundary condition at

and

respectively. Thus from

(6a)
(6b)
from these two equations
(6c)

ISSN: 0975-5462

4777

Tapas Kumar Pal et. al. / International Journal of Engineering Science and Technology
Vol. 2(9), 2010, 4775-4790
at the left edge at

(n region)
(6d)

Considering
and separating the real and imaginary parts, the following second order
differential equations are obtained.
(7)

(8)

The boundary conditions are, at


(9a)

(9b)
Similarly at
(9c)
(9d)
The device negative resistance and reactance are obtained from the following
and
Conductance G =

(10.a)

Susceptance B

(10.b)

Quality factor

(11)

3.

Design of Ka-band SDR IMPATT Diode

The authors have carried out DC and Small signal simulation to design a Ka-band (p+nn+) SDR IMPATT diode.
The current density and junction temperature have been taken to be 9107 A/m2 and 2250C respectively. The
realistic field and temperature dependence of carrier ionization rates and the drift velocities [11], [12] at 2250 C
and the effect of mobile space charge have been considered in the simulation. The admittance plot has been
optimized to get the peak negative conductance at around 36.5 GHz of Ka-band. Fig.3 to Fig.5 shows the electric
field E(x) profile, normalized current density

profiles and doping profile respectively. Fig.6 shows

the admittance (G-B) plot of Ka-band (p+nn+) SDR IMPATT diode with peak frequency at 36.5 GHz.

ISSN: 0975-5462

4778

Tapas Kumar Pal et. al. / International Journal of Engineering Science and Technology
Vol. 2(9), 2010, 4775-4790

6x107
Epilayer resistivity = 0.50 ohm-cm

1.0

Epilayer resistivity = 0.50 ohm-cm


Current density = 9x107 Amp/m2
Temp = 2250 C

Temp = 2250 C

0.5

0.0

0.0

-0.5

-0.5

-1.0

-1.0

p n
0

2x107

0.5

P(x)=(J -J )/J

3x107

Electric Field E(x) [Volt/m]

4x107

1.0

Current density = 9x107 Amp/m2

5x107

1x107

-1.6x10-6

-1.4x10-6 -1.2x10-6

-1.0x10-6

-8.0x10-7 -6.0x10-7

-4.0x10-7

-2.0x10-7

0
0.0

-1.6x10-6

-1.4x10-6

-1.2x10-6

-1.0x10-6

-8.0x10-7

-6.0x10-7

-4.0x10-7

0.0

-2.0x10-7

x [meter]

x [meter]

Fig. 3. P(x) profiles of silicon SDR (p+nn+) IMPATT Diode

Fig. 2. Electric field E(x) profiles of silicon


SDR (p+nn+) IMPATT Diode

3.0x1022

20
Epilayer resistivity = 0.50 ohm-cm
Current density = 9x107 Amp/m2
Temp = 2250 C

42 GHz

Susceptance(B)x106 in mho/m2

Doping density [m3]

2.5x1022

2.0x1022

1.5x1022

40 GHz

15
38 GHz
37 GHz
36.5 GHz
36 GHz
35 GHz

10

34 GHz

32 GHz

5
30 GHz

Epilayer resistivity = 0.50 ohm-cm


Current density = 9x107 Amp/m2

28 GHz

Temp = 2250 C

26.5 GHz

1.0x1022
-1.6x10-6 -1.4x10-6 -1.2x10-6 -1.0x10-6 -8.0x10-7 -6.0x10-7 -4.0x10-7 -2.0x10-7

0
0.0

2.0x10-7

x [meter]

Fig. 4. Doping profiles of silicon SDR (p+nn+) IMPATT Diode

-4.5

-4.0

-3.5

-3.0
-2.5
-2.0
Conductance(G)x106 in mho/m2

-1.5

-1.0

Fig. 5. Conductance Susceptance Plot of silicon


SDR (p+nn+) IMPATT Diode

4. Fabrication of SDR IMPATT Diode


Based on the DC and Small signal simulation described in the previous section, the authors have selected the
silicon epitaxial n/n+ wafers having the following specification [5] for fabrication of a (p+nn+) SDR Ka- band
IMPATT Diode through diffusion route . Fig.6 shows schematic diagram of a silicon epitaxial n/n+ wafer. The
optimized process steps followed by the authors are described in details in the following section.

Wafer Characteristics:
Type /dopant
Wafer Diameter
Substrate Thickness
Substrate Resistivity
Crystal orientation
Epitaxial Thickness
Epitaxial Resistivity
Type/dopant

ISSN: 0975-5462

: N/Phosphorus
: 7.57 - 7.67 cm
: 381 25 (micron)
: 0.0174 - 0.0185 (ohm-cm)
: <111>
: 3.6-4.4 micron
: 0.45-0.55 ohm-cm
: N/Antimony

Fig. 6. n/n+ Silicon Epitaxial Wafer

4779

Tapas Kumar Pal et. al. / International Journal of Engineering Science and Technology
Vol. 2(9), 2010, 4775-4790
4.1 Wafer cleaning
Wafer cleaning is a very important step in mm wave device fabrication process because of the variety of organic
and inorganic contaminants of unknown origin, which are present on the semiconductor surface, which
deteriorate the performance of the device [13].
a) Wafer is kept in a clean beaker containing DI water having 18 M resistivity which is then placed inside an
ultrasonic cleaner for 2- 4 minutes. This cleaning removes contaminating additives from the wafer surface
through acoustic streaming [14-15].
b) The wafer is then transferred to a beaker containing hot (80-850C) trichloro-ethelyene (TCE) for 10 to 15
minutes to remove the organic particles like air born bacteria, grease and wax from the surface of the wafer.
c) Trichloro - ethelyene (TCE) is removed by acetone.
d) The wafer is then rinsed thoroughly by running in DI water to remove acetone.
e) The wafer is then transferred to a beaker containing solution of NH4OH : H2O2 : H2O in ratio of 10:20:70
and heated to 80-850C for 10 to 15 minutes to remove heavy metallic impurities [16].
f) The wafer is rinsed with running DI water.
g) The wafer is immersed in a beaker containing solution of HCL: H2O2 : H2O in the ratio of 10:20:70 and
heated to 80-850C for 10-15 minutes to remove light metallic impurities.
h) It is then rinsed thoroughly in running DI water.
i) To make the mirror like hydrophobic surface, the wafer is dipped into a solution containing H2O : HF ::
90:10 for 1-2 minutes.
j) The wafer is finally rinsed by running DI water. Then N2 gas blower is used to dry up the wafer.
4.2 Activation of Boron Nitride (BN)
a) The starting wafer was n/n+ type and p+n junction was formed by boron diffusion. For this purpose, solid
source of boron, viz, Boron Nitride (BN) cakes having same diameter as that of silicon wafer was used.
b) The BN wafer is placed on a quartz boat and is very slowly pushed to the uniform temperature zone of the
furnace, shown in Fig.7. The BN wafer is activated in Oxygen ambient at 9750 C in the furnace for 20 25
minutes with 2-3 lit/minute flow rate of oxygen. During activation, a skin of B2O3 is formed on the surface
of BN wafer according to the following reaction: 4BN+3O2=2B2O3+2N2.

20 min
O2

Fig.7. Boron Activation

4.3 Stabilization
After activation, oxygen is shut off and nitrogen is passed into the furnace with a flow rate of 2-3 lit/minute for
20 minutes at temperature of 9750C , shown in Fig. 8.

ISSN: 0975-5462

4780

Tapas Kumar Pal et. al. / International Journal of Engineering Science and Technology
Vol. 2(9), 2010, 4775-4790

20 min

Fig.8. Stabilization

4.4 Pre-deposition of Boron


The cleaned silicon wafer and the activated BN are then placed in the quartz boat side by side with a spacing of
2 mm in between them. The quartz boat with BN and silicon wafers is then pushed slowly into the middle zone
of the furnace, maintained at a temperature of 9750C in N2 ambient. Pre-deposition of Boron was carried out for
1 hour. Boron was transported to the silicon surface by the inert carrier gas (N2) at the diffusion temperature,
shown in Fig. 9. Diffusion of Boron takes place according to the following reaction: 2B2O3 + 3Si = 3SiO2 + 4B.

Fig.9. Pre deposition of Boron

4.5 Drive in Diffusion


In drive-in cycle, the impurities (boron) penetrate slowly up to the desired depth into the silicon and results in
1.5 2.0 microns epitaxial layer width. During this process only the pre-deposited wafer is placed on quartz
boat inside the quartz tube of the furnace in nitrogen ambient. The drive in temperature has been kept at 11000C.
Pre-deposited boron layer gradually penetrates deeper inside the wafer with gradual decrease of surface
concentration with increase of drive-in diffusion time, shown in Fig.10.
After drive in diffusion the wafer is subjected to annealing at a temperature of 9750 C for 30 minutes so that the
deposited impurity atoms can be located at the substitutional sites.

ISSN: 0975-5462

4781

Tapas Kumar Pal et. al. / International Journal of Engineering Science and Technology
Vol. 2(9), 2010, 4775-4790

11000C

Fig.10. Drive in (Boron diffusion)

4.6 Low Temperature Oxidation (LTO)


During drive-in process at temperature of 11000C, the Boron-Silicate-Glass (BSG) formed during pre deposition
process becomes very hard and also acts as an insulating layer. Presence of this layer prevents proper metallic
contact with silicon. The wafer (after drive-in) is placed on a quartz boat inside a quartz tube at temperature of
8000C and wet oxygen is passed through the tube for 20 minutes, shown in Fig.11. After Low Temperature
Oxidation (LTO), BSG layer is softened which can be easily removed from the surface by treating with low
concentrate HF solution (Fig.12).

Fig.11. Low temperature oxidation

Fig.12. BSG removal

4.7 Cr-Au Metallization of p+ side


Metallization is one of the important steps of IMPATT device fabrication. Better adhesion gives always better
performance of the fabricated device. The wafer is placed on the substrate-holder, which is attached with
substrate heater inside the vacuum chamber where vacuum level is achieved up to 10-6 mm of Hg with the help
of Rotary Pump (RP) and Diffusion Pump (DP). After pouring liquid Nitrogen into Liquid-Nitrogen-Trap (LNT)
chamber, vacuum level increases up to 10-7 mm of Hg. The substrate temperature is kept at 2200 C and 2800 C
respectively during chromium (Cr) and gold (Au) deposition to form a total metallization thickness of 1.0
micron on the p+ side by electron beam evaporation technique as shown in Figs.13. (a) and (b). The process
parameters for chromium and gold deposition by electron beam technique have been tabulated in Table : 1 and
the Cr Au metalized wafer is shown in Fig.14.

ISSN: 0975-5462

4782

Tapas Kumar Pal et. al. / International Journal of Engineering Science and Technology
Vol. 2(9), 2010, 4775-4790

Table : 1
The Process Parameters for Chromium and Gold deposition by Electron Beam evaporation technique

Metal
Chromium (Cr)
Gold (Au)

Vacuum
(mm of Hg)
3.410-5
2.010-5

E-Beam Voltage
(KV)
5.4 - 5.5
5.4 - 5.5

Fig.13.(a). Chromium metallization of p+ side by e-beam

E-Beam Current
(mA)
100
100

Substrate
Temperature(0C)
2200C
2800C

Fig.13. (b). Gold metallization by e- beam

Fig.14. Metallization of p+ side with Chromium and Gold

4.8 Electroplating of p+ side


Due to low efficiency of SDR IMPATT diode maximum part of input d.c power is converted into heat at p+n
junction region of SDR device. For better heat sinking, integral heat-sink is necessary. The integral heat-sink is
formed by electroplating gold to a thickness of 20-30 micron on p+ side after e-beam evaporation of Cr and Au,
shown in Fig.15.

ISSN: 0975-5462

4783

Tapas Kumar Pal et. al. / International Journal of Engineering Science and Technology
Vol. 2(9), 2010, 4775-4790

Fig.15. Electroplating process

4.9 Thinning of n+ side


Thinning of the substrate is the most important process step to reduce the series resistance caused by undepleted
epitaxial layer. The negative resistance of the device can be improved by reducing the parasitic series resistance
arising mostly from unswept epitaxy. This is achieved by thinning the substrate first mechanically and then
chemically. The initial substrate thickness was 385 micron and thinning was carried out by mechanical lapping
upto 100 micron. The wafer is placed on a stainless steel holder and then lapping of n+ side is carried out by
carborandum power. Next the substrate is thinned upto 50 micron by using Alumina as polishing material. Then
the substrate is thinned by chemical etching [17] process by using an appropriate mixture of Hydrofluoric acid,
Nitric acid and Acetic acid in volume ratio of 8:1:1.The substrate thickness is thus reduced up to 20-25 micron
(Fig.16). During etching, the p+ side was covered with epizone wax.

Fig.16. Thinning of n+ side

4.10 Cr Au Metallization of n+ side


To get good ohmic contact on n+ side Cr-Au metallization is carried out (Fig.17) by electron beam evaporation
technique at a vacuum level of 10-7 mm of Hg and substrate temperatures of 220o and 2800 C for Cromium and
gold metallization respectively, as described in section 4.7.

ISSN: 0975-5462

4784

Tapas Kumar Pal et. al. / International Journal of Engineering Science and Technology
Vol. 2(9), 2010, 4775-4790

Fig.17. Metallization of n+ side with Chromium and Gold

4.11 Photolithography
An array of circular dots are reproduced on silicon wafer by using ultraviolet source and photo resist. The dotlike image is formed with a dark field mask. The wafer is coated with negative photo-resist by keeping the
wafer on spinner by using vacuum. The spinning speed is set at 2000 rpm and timer is set at 2 minutes so that
the thickness of the photo-resist is neither too thin nor too thick. Pre-baking is done in a baking furnace at a
temperature of 700C for duration of 30 minutes. This is followed by exposing the photo-resist coated wafer with
UV source for 2 minutes in a Mask aligner. Post baking is done at a temperature of 800C for duration of 30
minutes. Then the wafer is dipped in a developer.
4.12 Mesa etching
After photolithography process, first gold (Au) and then (Cr) chromium is removed from n+ side of the silicon
wafer by using selective chemicals. After removing metalized layers, the wafer was dipped into mesa etching
solution of HF, HNO3 and CH3COOH for 20 minutes and an array of mesa chips with appropriate diameter of
50 micron is obtained, shown in Fig.18 and photographs of array of mesa chips in Fig.19. All the chips are now
ready for bonding and packaging.

Fig.18. Array of mesa chips

Fig.19. Photograph of mesa chip

4.13 Chip separation


Chip separation is a very difficult task because the substrate is thinned up to 20 microns. During chip separation
at least 50 % of mesa chips are damaged due to irregular shape and breaking of mesa structure. The square chips
of 0.5 mm size are successfully separated by using a surgical blade. Fig.20 shows the complete IMPATT chip
with dimensions and Fig.21 shows the photograph of IMPATT chip developed.

ISSN: 0975-5462

4785

Tapas Kumar Pal et. al. / International Journal of Engineering Science and Technology
Vol. 2(9), 2010, 4775-4790

Fig.20. IMPATT Chip

Fig.21. Photograph of IMPATT Chip

4.14 Die and wire Bonding


After chip separation, the separated chips are die-bonded inside the S4 package using Gold Eutectic. Wire
bonding of the devices was carried out using the wire edge bonder. One end of a 25 micron diameter of gold
wire is bonded on the top of chip by thermo sonic compressor and other end is connected with gold coated ring
of S4 package by using silver epoxy baked at 1500C for 30 minutes as shown in Fig.22. Fig. 23 shows the
photograph of packaged IMPATT chip. Then the S4 packages are bonded to gold coated copper cylinders of
diameter 3 mm and length 5 mm for integral heat sink purpose. Now the IMPATT diodes are ready for DC and
RF characterization.

Fig.22. Wire bonding of IMPATT chip S4 package

5.

Fig.23. Photograph of wire bonded IMPATT Chip

DC and RF characterization of IMPATT diode

For DC and RF characterization of IMPATT diode, the diode is placed in a proper microwave / mm wave cavity
to get oscillation and RF power. The diode having device admittance (GD + jBD) is mounted in a microwave /
mm wave cavity .The device is biased to breakdown and connected to load having admittance (GL + j BL). The
condition for stable oscillation is fulfilled when the magnitude of the negative conductance of the device equals
the magnitude of the positive conductance of the load, i.e.
GD = GL

ISSN: 0975-5462

4786

Tapas Kumar Pal et. al. / International Journal of Engineering Science and Technology
Vol. 2(9), 2010, 4775-4790
and the magnitude of the capacitive susceptance of the device equals the magnitude of the inductive susceptance
of the load.
BD = BL
The authors have used a resonant cap cavity [8], in which the device is placed between the broad lower face of
a mm wave guide and the bottom face of a circular metal disc called resonant cap, schematically shown Fig.24.
The bias is given by a constant current power supply through a low pass mm wave filter connected with the top
surface of the resonant cap. The low pass type filter prevents high frequency oscillations from coupling with
the power supply when dc or low frequency bias current can pass through the filter and the diode. Considerable
heat is generated in the diode junction where large current is flowing at breakdown. Therefore an integral heat
sink cum wave guide cavity is used whose photograph is shown in Fig.25. The cap and the bottom surface of the
wave guide form a localized radial cavity around the diode. The mm wave signal generated by the diode is
coupled to the main rectangular wave guide cavity through the vertical open edges of the radial cavity.

Fig.24. Schematic diagram of a Ka-band resonant cap


waveguide cavity

DC Bias

Sliding short tuner

Fig.25. Photograph of resonant cap oscillator

Ampere meter

IMPATT Oscillator

Isolator

Attenuator

Voltmeter

Power meter

Directional coupler

10 dB
Spectrum Analyzer

Directional coupler

10 dB
Frequency counter

Fig. 26. Block Diagram of Ka-band Measurement Test Set up

Fig.26 shows a block diagram of a Ka-band measurement test set up used for DC and RF characterization of
IMPATT diode. Fig. 27 shows the DC V-I characteristic of the fabricated IMPATT diode. It is seen from the
graph that the diode has a soft break down in the range of 25 -31 volt. A maximum current up to 85 mA is
pushed through the device. Fig. 28 and Fig. 29 shows the plot of DC bias current vs output power and frequency
respectively. Fig. 30 shows a typical Ka-band spectrum (34.891 GHz) of the fabricated diode. A power output of

ISSN: 0975-5462

4787

Tapas Kumar Pal et. al. / International Journal of Engineering Science and Technology
Vol. 2(9), 2010, 4775-4790
14. 65 mW has been achieved at a frequency of 35.70 GHz with a bias current of 85 mA and break down
voltage of 31 volt.

Fig. 27. V- I Characteristic of Ka-band IMPATT diode

Fig. 29. Bias current Vs Frequency

Fig. 28. Bias current Vs output power

Fig. 30. Typical Ka-band spectrum

6. Conclusion
In this paper the design of a SDR Ka-band IMPATT diode and then fabrication process steps following the
diffusion technique are described in details followed by measurement of DC and RF characterization of
developed IMPATT diode. A silicon (p+nn+) SDR IMPATT diode for Ka-band operation has been designed by
using double iterative DC and Small signal simulation methods which involve simultaneous solution of
Poissons equation and Carrier continuity equation under appropriate boundary conditions. The computation
starts from the field maximum point in the depletion layers and proceeds towards the depletion layer edges. The
current density and junction temperature have been taken to be 9107 A/m2 and 2250C respectively. The realistic
field and temperature dependence of carrier ionization rates and the drift velocities at 2250 C and the effect of
mobile space charge have been considered in the simulation. The design has been optimized to get the peak
negative conductance at 36.5 GHz. Based on the DC and Small signal simulation, the authors have selected the
thickness and resistivity of silicon epitaxial n/n+ wafers for fabrication of a (p+nn+) SDR Ka-band IMPATT
Diode through diffusion route . The optimized process flow chart for realization of Ka-band SDR IMPATT is
shown below.
A resonant cap cavity has been used for DC and RF characterization of the fabricated diode. A power output of
14. 65 mW at a frequency of 35.70 GHz has been achieved at a bias current of 85 mA with break down voltage
of 31 volt. It is observed that the frequency of operation of the fabricated diode closely matches with the design
frequency. The power and frequency can be optimized by thinning the substrate in the range of 5 -10 micron so
as to minimize the effects of series resistance. To get the maximum output power at the desired frequency the
operating dc bias current is in the range of 150 - 200 mA without the problem of thermal burnout of the device.

ISSN: 0975-5462

4788

Tapas Kumar Pal et. al. / International Journal of Engineering Science and Technology
Vol. 2(9), 2010, 4775-4790

IMPATT Diode Fabrication Process Flow

Wafer cleaning

Activation of Boron
Nitride (BN)

Stabilization

Low Temperature
Oxidation

Drive in Diffusion

Pre-deposition of
Boron

Cr-Au Metallization
of p+ side

Electroplating of
metalized p+ side

Thinning of n+ side

Mesa etching

Photolithography

CrAu Metallization
of n+ side

Chip separation

Die/wire Bonding
and packaging

RF characterization

Acknowledgement
The first author is thankful to Shri. S.K. Ray, DS & Director, Research Centre Imarat, Hyderabad, Shri. R. Das,
Director, RF Systems, Dr. V.G. Borkar, Head, Antenna & Components Group and Shri. J.V. Prasad, Head,
MMW Seekers & Sensors Division for their consistent support and encouragement for carrying out the research
work.
References
[1]
[2]
[3]
[4]
[5]
[6]
[7]
[8]
[9]
[10]
[11]
[12]
[13]
[14]
[15]
[16]
[17]

Roy, S.K., Transit Time Device, Encyclopaedia of Electron Devices vol. 24, Edited by John G. Webster, Wiley & Sons, New
York 1999.
Banerjee, J.P., Luy, J.F. and Schaffler, F., Comparison of theoretical and experimental 60GHz silicon Impatt diode performance,
Electronic Lett. (UK) vol 27, No.. 12, pp. 1049-1051 (1991).
Russer, Peter., Si and SiGe Millimeter-wave Integrated Circuits, IEEE Trans. on MTT, Vol. 46, No. 5, pp. 590-603,1998.
Sharfetter, D.L. and Gummel, H.K., Large signal analysis of a silicon Read diode oscillator, IEEE Trans. Electron Devices, Vol ED16, No.1, pp.64-77, Jan.1969.
Wolf, Helmut F., Silicon Semiconductor Data, Signetics Corporation, Pergamon Press, First Edition 1969.
Howes, M. J. and Morgan, D.V., Microwave Devices; Device Circuit Interactions, A Wiley Interscience Publication, Jhon Wiley &
Sons, 1976.
Gibbons, G., Avalanche diode microwave oscillators, Oxford University Press, Oxford 1973, Ch.4, pp. 45-65.
Pal, Tapas Kumar., A Tunable Millimeter wave (Ka-Band) IMPATT Source Using an Integrated Heat Sink cum Waveguide mount,
Patent no. 221758, INDIA, 15.02.2001.
Roy, S.K., Banerjee, J.P. and Pati, S.P., A computer analysis of the distribution of high frequency negative resistance in the depletion
layer of IMPATT diodes, Proceedings of the conference on Numerical Analysis of Semiconductor Devices (NASECODE IV)
(Dublin, Republic of Ireland: Bolle Press), p. 494, 1985.
Gummel, H. K. and Blue, J. L., A small signal theory of avalanche noise in IMPATT diodes, IEEE Trans. Electron Devices, vol.
ED-14, pp.569-580.1967.
Grant, W. N., Electron and hole ionization rates in epitaxial silicon at high electric field, Solid State Electron.,Vol. 16, p.1189,1973.
Canali, C., Ottaviani, G. and Quaranta, A.A., Drift velocity of electron and holes and associated anisotropic effects in silicon, J.
Phys. Chem. Solids, Vol. 32, p.1707. 1971.
Kern, Werner., The Evolution of Silicon Wafer Cleaning Technology , J. Electrochem. Soc., vol.137, No. 6, June 1990, pp. 18871892.
Nadtochiy, A., Podolian, A., Kuryluik,V. Kuryliuk, A., Korotchenkov,O., Schmid, Julian., and Schlosser , Viktor., Electrical and
Micromechanical Performance of Ultrasonically Cleaned Silicon Wafers Published, 27th International Conference on Microelectronics
(Miel 2010), NIS, Serbia, 16-19 May, 2010.pp. 261-264.
Gale, G. W. and Busnaina, A. A., Removal of particulate contaminants using ultrasonic and megasonics: A Review, Particulate Sci.
Technol., 1995, vol.13, pp.197 -211.
Itano, Mitsushi., Kern, Frederick W., Mayashita, Jr. and Ohmi ,Tadahiro., Particle Removal from Silicon Wafer Surface in Wet
Cleaning Process , IEEE Transactions on Semiconductor Manufacturing, Vol.6. No.3, Aug, 1993. Pp. 258 -269.
William, Kirt R. and Muller Richard S., Etch Rates for Micromachining Processing, Journal of Microelectromechanical Systems,
Vol.5. No.4, December 1996. pp. 256-269.

ISSN: 0975-5462

4789

Tapas Kumar Pal et. al. / International Journal of Engineering Science and Technology
Vol. 2(9), 2010, 4775-4790
Authors
Shri Tapas Kumar Pal, born in October, 1976 at Kolkata, obtained his M.Sc degree in Physics with
specialization in Microwaves from University of Calcutta in 1999. He has worked as a Senior
Research Fellow and Senior Scientist at Centre of Advanced Study in Radiophysics & Electronics,
University of Calcutta for a period of 2.5 years from Feb 2000 onwards. Later he worked as an
Examiner of Patents & Designs at Patent Office, Kolkata till July 2005. Presently he is working as a Scientist
D at Research Centre Imarat, DRDO, Hyderabad. He is currently engaged in development of MMW Seekers
and Sensors. His special interests are Design and Development of MMW IMPATT Diodes, Oscillators and
Amplifiers and their computer simulations. He has also been pursuing Ph.D (Tech) Degree at Institute of
Radiophysics & Electronics, University of Calcutta, on Millimeter wave IMPATT Diodes and Oscillators. He
is a Life Member of IETE and Member of IEEE.

Dr J. P. Banerjee obtained B.Sc. (Hons.) and M.Sc. in Physics and Ph.D. in Radio Physics and
Electronics from the University of Calcutta. He is presently a full Professor in the Institute of
Radio Physics and Electronics, C.U. He is the recipient of Indian National Science Academy
Award and Griffith Memorial Prize in Science of the Calcutta University in 1986. He is the
principal co-author of more than 125 research papers in international journals in the fields of Semiconductor
Science and Technology, Microwave and Millimeter wave avalanche transit time devices and Avalanche Photodetectors. He has authored a text book on solid state electronic devices published by Vikas Publishing Ltd, New
Delhi, India. He is a fellow of IETE, Senior Member of IEEE, a life member of the Society of EMI and EMC
and Semiconductor Society, India. He served as a referee for various National and International technical
journals. Presently he is also serving as the Director of a collaborative research centre entitled Centre of
Millimeter wave Semiconductor Devices and systems in the University of Calcutta.

ISSN: 0975-5462

4790

You might also like