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Indian Standard
METHODS OF TEST FOR
AGGREGATES FOR CQNCRETE
PART Ill SPECIFIC GRAVITY, DENSITY, VOIDS,
ABSORPTldN AND BULKING
0 Copyright 1963
BUREAU
OF INDIAN
MANAKBHAVAN, 9 BAHADUR
STANPARDS
SHAH ZAFAR MARG
Gr 5
October 1963
1
,
I!s:2386(Paq-III)-1963
Indian Standard
METHODS OF TEST FOR
AGGREGATES FOR CONCRETE
PART III SPECIFIC GRAVITY, DENSITY, VOIDS,
ABSORPTION AND BULKING
Cerhent and Concrete
Committee,
BIIC 2
&pWS#?lling
The Concrete Association of India, Bombay
Chairman
K. K. NAM~IAR
SHRI
Sectional
Members
SHR~1.:. v. TIXADAN~Y( Aiternate to
Sbri K. K. Nambiar )
M. N. Dastur & Co Private Ltd, Calcutta
SHRI K. F. ANTIA
Bhakra Dam Designs Directorate, New Delhi
SHRI P. S. BHATNACAR
,R I. C. DOS M. PArS CUDDC;J
Central Water 82 Power Commission
( Ministry
Irrigation & Power )
SHRI Y. k. MVRTHY ( Altemote)
Khira Steel Works Private Ltd. Bombav
SHRI N. D. DAFTARY
Central Public Works Departmknt
S~r.1 N. G. DEWAN
SUPERINTENDING
ENGINE~~R,
ZNDCIRCLE ( Al&male )
The Associated Cement Companies Ltd, Bnmbay
DR R. R. HATTIANoADI
SIiRI
v.
N.
PA1 ( &crn&
SHR~P. C. HAZRA
DIHI~CTOR
JOINT
Geological
STANDARDS Rexarc!,
( Bz~~
DIRECTOR STAND
ARDS ( B&S ) ( A&emote)
S. B. JOSHI
M. M..LAL
SHRI B. N. MAJUUDAR
SHRI
StIRI
&RI
P. L. DAS ( Alkrnalr )
Pao~ S. R. MEHRA
of
. Designs
6
Standards
( Mnustry of Kailways )
Organization
Central
Road
Research
Institute
( CSIR );
New Delhi
The Concrete Association of India, Bombay
SARI N. v. MOHILE
Government Test House, Calcutta
SHRI S. N. MuaERJt
SRRI N. C. SEN GUPTA ( Alfematc )
Institution of Engineers ( India )! Calcutta
SHIU ERACH A. NADIR.SHAII
sxku C. B. PATEL
National
Buildings
Organisatlon
(Ministry
of
Works, Housing & Rehabilitation )
Y&RI RABINDERSINGH ( AU17note)
PROPG. S. RAMA~WAMY
Central
Building
Research
Institute
( CSXR j,
Roorkee
SHRI K. SIVA PRMAD ( Alturnafe )
( Conhued
on #age 2 )
BUREAU
OF
INDMN
STANDARDS
MANAK BHAVAN, 9 BAHADUR SHAH ZAFAR MARG
NEW DELHL 110002
IS:Z386(PartIII)-1963
( -fiamPw
1)
Aidhnbers
Rdnanring
Gammon India Ltd, Bombay
SHU T. N. S. RAO
Sum S. R. PINHEIR ( Altmrok )
Martin Burn Ltd, Calcutta
RxPuEusNTATtvz
Dalmia Cement ( Bhatat ) Ltd, Calcutta
Sstsu Nmm Clurmlu
ROY
Central Board of Irrigation & Power (Ministry of
f&CRETARY
Irrigation & Power )
Engineer-in-Chiefs
Branch, Army Headquarters
Bmo G. S. Strmr~
SHRI R. S. MEHANDRU
( Alhrnal )
Indian Roads Congress, New Delhi
I)r &. SVBBARAJU
Roads Wing, Ministry of Transport
& CommuSanr J. M. Tarsum
nications
Sum N. H. Kzsw~~l ( Afkra&)
Director, IS1 ( Ex_odiicioMrmbcr )
DaH.C.
bWIWARAYA,
Deputy Director ( Bldg )
Secre#q
Stint A. Parrtitvt RAJ
Extra Assistant Director ( Bldg ), IS1
Concrete
Subcommittee,
cont*nff
Sm
S. B. Josut
lutmbcrs
Asstttv~~
DIRECTOR
BDC 2 : 2
STANDARDS
Sn%H
BHAGWANANX
DR I. d. l&s M. Pm Cunnou
Sum Y. K. MURRIY ( Alkmatc )
S~nr P. L. DUI
Research,
Designs
&
Standards
Organization
( Ministry of Railways )
Engineer-in-Cl&fs
Branch, Army Headquarters
Central Water & Power Commission
( Ministry of
Irrigation & Power )
Directorate
General
of Supplies
&
Disposals
( Ministry of Economic & Defence Co-ordination )
SHRI 0. P. GGEL (
SHRI J. M. TREHAN
Altemnte )
Roads Wing,
cations
Braith$h;Uw
2
Ministry
of Transport
B Jessop
& Communi-
cGnstructi0n
CG La
Indian Standard
METHODS OF TEST FOR
AGGREGATES FOR CONCRETE
PART III SPECIFIC GRAVITY, DENSITY, VOIDS,
ABSORPTION AND BULKING
0.
FOREWORD
Part
II
of
Deleterious
Materials
and
Organic
Part
III
Part
IV
Mechanical Properties
Part
Part
VI
Soundness
Measuring Mortar Making Properties of Fine Aggregate
Part VII
Part VIII
Petrographic Examination
ISt2386(PartIII)L1963
different countries of the world has also been recognized.
These considerations led the Sectional Committee to derive assistance from the
published standards and publications of the following organizations:
British Standards Institution
American Society for Testing and Materials
0.4. Wherever a reference to any Indian Standard appears
methods, it shall be taken as a reference to its latest version.
in these
1.. SCOPE
1.1 This standard
concrete:
of surface
OF
moisture
SPECIFIC
in fine aggregate
GRAVPPY
AND
fine
(field
WATER
2.1 Object-i This test covers the procedures for determining the specific
gravity, apparent specific gravity and water absorption of aggregates.
Nor~ 1 -Threl
main methods are specified for use according
to whc&r
he &e of the aggregate is large
than 10 mm ( Method I ) between 40 mm
and 10 mm (Method I or II may be used ); or smaller than 10 mm ( Method III).
An alternate method ( Method IV ) is al.30 permitted.
Nora 2 -The C&r absorptiontest willnot alwaysbe reproduciblewithaggregatu
OfiLigh
paccmity.
4
Is:2386(PartIll)-1963
2.2 Method I - Aggregate Larger than 10 mm
2.2.1 Apparatus 4
Balance -A
balance
readable and accurate
to permit the basket
the beam and weighed
b! Oven -
controlled,
to
Two dry soft absorbent cloths each not less than 75 x 45 cm.
4
f > A shallow tray of area not less than 650 ems.
g> An airtight container of capacity similar to that of the basket.
23.2 Sample - A sample of not less than 2 000 g of the aggregate
shall be tested. Aggregates which have been artificially heated shall not
normally be used. If such ,mat@xl is used the fact shall be stated in the
report.
Two tests shall be made, and it is recommended that the two
samples should not be tested concurrently.
2.2.3
finerparticles
lst23as(P#la)-1963
233.4 The aggregate placed on the dry cloth shall be gently
surface dried with the cloth, transferring it to the second dry cloth when
the first will remove no further moisture. It shall then be spread out not
more than one stone deep on the second cloth, and lest exposed to the
atmosphere away from direct sunlight or any other source of heat for not
less than 10 minutes, or until it appears to be completely surface dry
( which with some aggregates may take an hour or more ). The aggregate
shall be turned over at least once during this period and a gentle current
of unheated air may be used after the first ten minutes to accelerate the
drying of difficult aggregates. The aggregate shall then be weighed
( weight B).
NO%%-If
the spparcnt spcci6c gravity onIy ia rcquimd the opaztiom described
in 2.2.3.4 may be omit&d.
speciiicgravity=
Bc_A
lO(B-C)
C
where
aggregate in
air, and
C = the weight in g of ovendried
aggregate in air.
A#rmtus -The
&tupecn4O~WdlO~
apparatus shall consist of the following:
lst2386(Partlu)-1963
W Okn-
IS:23S6(PartIU)-1963
shall be turned over at least once during this period and a gentle current
of unheated air may be used after the first ten minutes to accelerate the
fTi;htoi
)difficult aggregates. The aggregate shall then be weighed
NOTE-If
the apparentspecificgravityonly is
in 233.4
may be omitted.
2.3.3.5 The aggregate shall be placed in the oven in the shallow tray,
at a temperature of 100 to 110C for 24 f l/2 hours. It shall then be
cooled in airtight container and weighed ( weight D ).
2.3.4 Calculations - Spe.ctic gravity, apparent specific gravity and water
absorption shall be calculated as follows:
D
Specific gravity
= c- (A-B)
D
Apparent specific gravity
=
D-(A-B)
Water absorption ( percent
_lOO(C-D)
of dry weight )
D
where
A = weight in g of vessel containing sample and filled
with distilled water,
B = weight in g of vessel filled with distilled water only,
C = weight in g of saturated surface-dry sample, and
D = weight in g of oven-dry sample..
23.5 Re#ortiQ of Results - The individual and mein results shall be
reported. The grading of aggregate tested shall be stated, and whether
it has been artificially heated.
2.4 Method
III -
Is:2386(r~m)-1%3
one litre capacity having a metal conical screw top with
a 6-mm diameter hole at its apex.
The screw top shall
be watertight when it is screwed on to the jar, and, if
necessary, a rubber or fibre washer shall be inserted in
the joint.
If such a washer is used, a mark shall be made
on the jar to correspond with a mark on the screw top so
that the screw is tightened
to the same position every
time and the volume contained
by the jar is constant
throughout
the test.
A suitable vessel can be made from
a l-kg fruit preserving jar in which the glass lid normally
used is replaced
by a sheet metal cone as shown in
Fig. 1; or
2) A wide-mouthed
glass vessel, such as a gas jar, of about
1.25 litres capacity, with a flat ground lip and a plane
ground disc of plate glass to cover it, giving a virtually
watertight fit.
d) A means of supplying a current
container
Test Procedure
2.4.2.1
Using the pycnometer - A sample of about 1 kg for 10 mm
to 4-75 mm or 500 g if finer than 4.75 mm, shall be placed in the tray
and covered with distilled water at a temperature
of 22 to 32C.
Soon
air entrapped
in or bubbles on the surface of the
after immersion,
aggregate shall be removed by gentle agitation with a rod.
The sample
shall remain immersed for 24 f l/2 hours.
The water shall then be carefully drained from the sample, by
decantation
through a filter paper, any material retained being return&
to the sample.
The aggregate
including any solid matter retained on
the filter paper shall be exposed to a gentle current of warm air to
evaporate surface moisture and shall be stirred at frequent intervals to
ensure uniform drying until no free surface moisture can be seen and the
material just attains a free-running condition.
Care shall be taken to
The saturated and surface-dry sample
ensure that this stage is not passed.
shall be weighed ( weight A ).
specific gravity
only is required,
the operations
If the apparent
NoTed&bed
in this paragraph may he omitted, although for materml finer
&
475 mm some surface drying may be desirable to facilitate handling.
The aggregate
shall then be placed in the pycnometer which shall
&?filled with distilled water.
Any trapped air shall be eliminated
hy rota&g
the
pycnometer
on its side, the hole in the apex of
lsr2386(Partlll)-1963
Fro. 1
SECTION OF PYCNO~TER
FROM FRUIT JAR
MADE
10
lsr2386(PartllI)-1963
The water shall then be carefully drained from the sample by
deeantation through a filter paper and any material retained returned to
the sample. The sample shall be placed in the oven in the tray at a
temperature of 100 to 110C for 24 f l/2 hours, during which period
It shall be cooled in
it shall be stirred occasionally to facilitate drying.
the air-tight container and weighed ( weight D ).
Two tests shall be made.
2.4.2.2 Using the second ( gas jar ) apparatus described in 2.4.1 (c),
the procedure shall be the same except that in filling the jar with
water it shall be tilled just to overflowing and the glass plate slid over
it to exclude any air bubbles.
2.4.3 CaIculations- Specific gravity,
apparent
water &sorption shall be calculated as follows:
Specific gravity
Apparent
specific
gravity
gravity
and
A-(L)
=
D-
wate&aw~;$n
specific
(DB-C)
( percent Of = 100 ( A _ D )
D
where
M&hod
Iv -
Attemate
Method
1963
as given in 2.4.
After transferring
the sample to the bucket, water shall
be added to cover the aggregate
by at least 25 mm and the sample
stirred to remove air.
The bucket shall then be filled with water and the
level of water in the tank raised slowly to avoid, as far as possible, the loss
of fine particles from the sample in the bucket to the tank.
3. DETERMINATION
OF BULK
DENSITY
AND VOIDS
3.1 Object -
for determining
NOTE 1 - The bulk density is the weight of material in a given volume, and for the
purpose of this standard it is measured in kilograms per litre. The bulk density of an
aggregate is affected by several factors, including the amount of moisture present and the
amount of effort introduced in filling the measures.
NOTE 2 -It
is emphasized that this is a laboratory test intended fbr comparing
properties of different aggregates.
It is not generally suitable for use as a basis for
quoting mix design conversion factors.
NOTE 3- Considerably more compactive effort is used in the determination of
angularity number [ see IS : 2336 ( Part I )-1963 ] than in this test, and hence the valuer
for bulk density and voids are different.
of the
sample to be weighed.
b)
Measure-The
measure
shall preferably
be
machined to accurate internal dimensions and shall be provided
with handles.
It shall also be watertight, and of sufficient rigidity
to retain its form under rough usage, and should be protected
against corrosion.
Cylindrical Metal
Tamping Rodsection
TABLB
SIZE
OF CONTAINER
OF LARal?sT
PARTroLes
NOMINAL
r-B
CAPACITY
DUXRTRR
INQDE
HRmiT
TmasNlsal
OF MRTAL
Min
litre
cm
15
17
$15
over475mmto4Omm
15
25
30
400
over4omm
30
35
31
500
12
cm
mm
m23&(Partm)a63
3.3 Calibration - The measure shall be calibrated
by determining
the
weight of water at 27C required to fill it such that no meniscus is present
above the rim of the container.
The capacity in litres shall be obtained
by dividing the weight of water in kilograms required to fill the container
at 27C by the weight of water in one litre at 27C, which may be taken
as one kilogram.
3.4
Procedure
3.3 Calculation
as follows:
Percentage
The percentage
of voids = 7
Ge-Y
I
of voids shall
be calculated
X 100
where
G, = specific gravity
Y
3.6 Reporting
of Resulh kg/litre to the nearest O-Ok kg.
The
number.
of the aggregate,
and
voids
shall
The
be reported
bulk
density
as a percentage
shall
be
reported
to the nearest
in
whole
Ir2386(PartHI)-1963
4. DETERMINATION
OF NECESSARY ADJUSTMENT
FOR
BULKING OF FINE AGGREGATE ( FIELD METHOD )
4.1 Object-
the necessary
for determining
Srocednre
4.3.1 The procedure to be adopted may be varied, but two methods are
suggested in 4.3.2 and 4.3.3.
Both depend on the fact that the volume of
inundated sand is the same as if the sand were dry.
4.3.2 Put sufficient quantity of
Level
it is about two-thirds full.
steel rule vertically down through
measure the height.
Suppose this
4.3.2.1
Empty the sand out of the container into another container
where none of it will be lost.
Half fill the first container with water.
Put back about half the sand and rod it with a steel rod, about 6 mm in
diameter,
so that its volume is reduced to a minimum.
Then add the
remainder of the sand and rod it in the same way,. Smooth and level the
top surface of the inundated
sand and measure its depth at the middle
with the steel rule.
Suppose this is h cm.
4.3.2.2
The percentage of bulking
be calculated from the formula:
Percentage
bulking
= ($,-I)
X 100
shall
4.4 Reporting
of Resdts
FINE AGGREGATE
shall be calculated
Report
the percentage
bulking
OF SURFACE MOISTURE
(FIELD METHOD)
of the sand
lN
5.1 Object
-This
method of test covers the procedure
for determining,
in the field, the amount of surface moisture in fine aggregates by displacement in water.
The accuracy
of the method
depends upon accurate
information on the specific gravity of the material in a saturated surfacedry condition.
The same procedure,
with appropriate
changes in the
size of sample and dimensions of the container.
may be applied to coarse
aggregates.
55
Apparatus
The apparatus
a capacity
of
kg
or more
and
Procedure
container
shall be filled up to
5.4.2 Determination by Weight -The
The container
the mark with water and the weight in grams determined.
Enough water shall be placed in the container
to
shall be emptied.
cover the sample, after which the sample of fine aggregate
shall be
The
introduced
into the container
and the entrained
air removed.
container shall then be filled to the original mark and the weight in grams
15
IS:2386(PartIII)-1963
The amount
determined.
calculated as follows:
of water
displaced
by
the
sample
shall
be
VS =M,+M,-M
where
5.4.3 Determination
by Volume- A volume
of water sufficient
to
cover the sample shall be measured
in millilitres
and placed in the
The weighed sample of fine aggregate shall then be admitted
container.
The combined volume
into the container and the entrained air removed.
of the sample and the water shall be determined by direct reading when
a graduated
flask is used. Where a pycnometer
or volumetric flask of
known volume is used, the combined volume of the sample and the water
shall be determined
by filling up to the mark with a measured volume
of water and subtracting
this volume from the volume of the container.
The
amount
of water displaced
by the sample shall be calculated
as follows:
v, =
vs -
v,
where
V, -
volume
in ml of water displaced
by the sample,
cialculation
100
where
P, = percentage
surface
dry fine aggregate;
moisture
in terms of saturated
surface-
I6t2366(PartIlI)-1963
Vd = the weight of the sample ( it4, in 5.4.2 ) divided by the
specific gravity
on saturated
and surface-dry
basis,
determined as prescribed;
NOTE-
These formulae
are
Jr in terms
the weight
convenience,
express
surface moisture
to
that:
I==
readily
derived
from
basic
relationships.
For
of the ratio r, that is, the ratio of the weight
of
of the saturated
surface-dry
sample.
It follows
M*-__3_
I+7
MS
1+r
of the saturated
Vs=+++
. . . . . . . . . . . ...*... ( 1 )
surface-dry
fine aggregate,
. . . . . . . . . . . . . . . . . . (2)
MC+&)
where
the first term gives the water displaced
by the saturated
aggregate,
and the second that displaced by the surface moisture.
From
equation
then
surface-dry
fine
2,
Vs- M.
1
----1
G
PI M*
1+r
. . . . . . . . . . . . . . . . . . (3)
By definition,
M,=V&x
M*
. . . . . . . . . . . . . . . . . . (4)
1, and simplifying
vs-
vd
....... . . . . . . . . . . . (5)
Mb*
The formula
for Ps, since
for
Ps may be derived
by
V8 Pi E
reasoning,
or
directly
from
that
vd
Mb-_Vav
I+*;
similar
x 100
. . . . . . . . . . . . . . . . . . (6)
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