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Although heat treatment operations have strong bearing on the final product quality, H
trial and error methods. The present work describes an engineering approach to the de
Industry accepted heat treatment processing cycles might sometimes lead to longer pr
efficiency, and higher energy consumption. This article elaborates on important engine
austenitising temperature and soaking time, selection of appropriate salt, rectification o
was successfully applied to an industrial scale heat treating operation for the productio
The heat treatment operation is an important step in the manufacturing of these precis
product with stringent dimensional control as well as high wear-resistance. The commo
equipment are:
salt bath hardening operation, where the components are heated in a salt bath fu
Accurate Engineering recently procured a large amount of steel from Germany at a ver
used by one of the leading German slip gauge manufacturers. Although, the compositio
At the Accurate heat treatment shop, attempts were made to develop the heat treatme
from 30 to 45 HRC were observed during these trials, well below the required hardness
During the past two decades, the process engineering group of Tata Research Developm
projects on model based optimization of various metallurgical operations. The Frank Gr
this steel to obtain uniform hardness of HRC 60 after quenching and tempering operati
The important metallurgical issues in designing a hardening cycle for tool steels are:
However, several other practical aspects, such as selection of salt and its neutrality ma
These issues are elaborated in the following section.
Steel Grade
Identification of the steel grade is the most important parameter for
Frank grade steel are tabulated in Table I. The composition falls in th
is a shallow hardening tool steel and in rods above 0.5 inch in diame
soft and tough core. These characteristics make it desirable for man
and is readily formable by forging. W2 grade responds uniformly to
The ease with which the salt is washed from the workpiece after heat treatment
At present, Accurate uses a proprietary MNC-661 heat treatment salt, supplied by Mata
that its melting point is 1220 F (660 C) and recommended working range is 1508 to 15
as high as 1832 F (1000 C). Using a salt above its recommended working temperature
oxidation and decarburization in the workpiece. Therefore, a suitable alternative had to
Barium chloride-based salts are widely used for salt bath heat treatment of tool steels.
salts are given in Table II. For the Frank Grade steel, Salt #2 with 70% BaCl2 and 20%
enable the
recommended
time of
Salt
Neutral salts used
oxides and
the case of salt
based salts (Salt#
graphite rod for
Rectification
for austenitizing steel become contaminated with
dissolved metals renders the bath oxidizing and d
bath furnaces with immersed electrodes, daily re
1,2,3 in Table II) rectification should be done by
one hour for every 4 hours of operation.
Fig. 3 Suggested
locations for
uniformity survey.
Tempering
Tempering modifies the properties of quenched h
and toughness. In general, two or more shorter t
retained austenite and for tempering the freshly
suggested double tempering process for the Fran
hardened tool steels like this steel should be tem
temperature, to prevent or minimize cracking.
EXPERIMENTATION AND RESULTS
Quenching in Water
The mean hardness and standard deviation of the center point and the corners are plot
the as-heat treated sample had an average hardness value of 44.8 HRC with a standar
variation is not acceptable in the final product. In the 0.1 mm depth sample, the avera
deviation to 9.8. The hardness value further improved to an average of 60.6 with a sta
hardness value is highly desirable for the slip gauges. It must be noted that the hardne
company.
The low hardness and wide variability of the as-heat treated samples was primarily due
mm to 0.3 mm suggests decarburization in the product. It is believed that the decarbu
used at Accurate Engineering.
It is interesting to note that in all the three cases, the center points showed a lower ha
be the result of a higher tendency of vapor blanket formation in the sample center as c
vapor blanket during the first state of quenching and could improve hardness uniformit
RECOMMENDATIONS
The summary of recommendations as determined by the process analysis and the expe
Salt mixture of 70% BaCl2 + 30% NaCl should be used at an austenitizing tempe
Rectification of the above salt must be done every four hours of operation with 1
in the bath for 1 hour.
The workpiece should be cleaned from scale before heating in the salt bath furna
The workpiece should be quickly transferred from the salt bath to the quench wa
When the part can be held by hand, it should be quickly transferred to the tempe
The parts should be cleaned in a solution of 10% NaOH by weight in water follow
SUMMARY
By using the suggested heat treatment cycle determined for the Frank Grade steel, the
was observed and attributed to the use of salt bath at higher than recommended temp