Professional Documents
Culture Documents
594
2003 by Bla Liptk
(1995)
S. EDVI, J. E. JAMISON
(2003)
Types of Designs:
A. Calibrators that use simulators (devices that simulate the output signal of thermometers). B. Calibrators that use calibration baths, which provide accurate temperature
environments for calibration purposes (systems use hot air, oil, sand, or aluminum
blocks for heat storage; some are fluidized beds).
Costs:
595
Temperature calibrators range from simple hand-held instruments to large permanently installed baths, chambers, and
water-proof test cases. Calibrators reproduce temperatures
with an accuracy and stability adequate for the range of
devices to be checked. The thermometers are normally calibrated at one specific temperature at a time, although a series
of baths can be assembled for sequential immersion to enable
a range of temperature points to be checked. Correspondingly, the temperature can be reset in stages or as a ramp
function for multipoint checking.
Simulators duplicate the outputs of temperature sensors,
enabling measuring instruments to see a simulated but precise
temperature value. This output may be a millivoltage to
simulate thermocouples (TCs), a resistance to simulate
resistance temperature detectors (RTDs), or a light or radiant energy level to calibrate instruments based on optical
or infrared (IR) energy. Simulators can usually be connected
locally (at the sensor) and then at the readout instrument
so as to check the operation of transmitters, multiplexers,
and cabling.
A fixed resistor connected to a multipoint monitor is an
example of a simulator that continuously checks the calibration of indicators, recorders, and alarms. Some calibrators
incorporate both temperature environment and sensor output
functions.
in particular are defined in terms of their R0 value, or resistance value at the ice point (e.g., 100 Pt.). Immersion in
an ice point bath is a useful way of compensating for calibrating drift even though the thermometer is normally used
at higher temperatures.
Adjustable temperature baths contain a fluid (liquid or
fluidized solid) circulated through a chamber in which the
thermometers can be immersed. Controllers maintain a temperature at the desired set point. A block establishes temperature uniformity among sensors at temperatures below
1472F (800C), or where conduction is the primary means
of heat transfer.
TABLE 4.3a
Defining Fixed Points of the International Practical Temperature Scale (ITS-90)
Temperature
Point
Number
T90 / K
3 to 5
13.8
t90 / C
Substance
State
270.15 to
268.15
He
VP
259.35
eq. H2
TP
17
256.15
VP (or GT)
20.3
252.85
VP (or GT)
24.6
248.6
Ne
TP
54.36
218.8
O2
TP
83.8
189.34
Ar
TP
234.32
38.83
Hg
TP
273.16
0.01
H2O
TP
10
302.92
29.77
Ga
MP
11
429.75
156.60
In
FP
12
505.08
231.93
Sn
FP
13
692.68
419.53
Zn
FP
14
933.47
660.32
Al
FP
15
1234.93
961.78
Ag
FP
16
1337.33
1064.18
Au
FP
17
1357.77
1084.62
Cu
FP
FP = freezing point
MP = melting point
GT = gas thermometer point
TP = triple point
VP = vapor pressure point
eq. H2 = hydrogen at the equilibrium concentration of the ortho- and
para-molecular forms
596
Temperature Measurement
Platinum RTD
Handle
Thermocouple
Calibrator
Water Vapor
Type
K
Borosilicate Glass
Cell
Degrees
F
Liquid Water
Out
Hi
Set
Lo
Store
In
Off
Max
Read
Min
Reset
Thermowell
Ice
FIG. 4.3b
Sealed container used to obtain the triple-point temperature of
water used in the calibration of RTDs.
SIMULATORS
Simulators for TCs and RTDs consist of voltage sources
and/or resistors having values that correspond to the required
temperature readings. TC simulators require provision for
reference junction compensation and alloy terminals.
Simulators for optical or total radiation pyrometer calibration may be as simple as a 25-watt lamp or as sophisticated
as a controlled output arc furnace. It is usual to use these
simulators with comparison standards. By comparing one
optical pyrometer with a standard or with a laboratory-calibrated optical pyrometer, one can avoid errors that may arise
due to their large ambient temperature coefficients. Such
calibrations can, for example, be performed in an outdoor
shed or pyrometer shop adjacent to a steel mill.
A typical handheld calibrator is illustrated in Figure 4.3c.
A laboratory-type thermocouple calibrator/simulator is shown
in Figure 4.3d. This unit combines both the simulation and
calibration functions in one unit.
A simulator for optical pyrometry is shown in
Figure 4.3e. The unit incorporates a copper fixed point to
provide a reference temperature 1985F (1085C) independent of a standards laboratory. A very high temperature
3002F (1650C) TC and optical/radiation pyrometer calibration system incorporating a palladium freezing point,
molybdenum block, and standard lamp was built for a steel
mill in Brazil where traceability to a national laboratory
was unavailable.
FIG. 4.3c
Handheld thermocouple calibrator. (Courtesy of Altek Industries
Corp.)
CONCLUSIONS
Table 4.3f provides some recommendations for the type of
calibration equipment that is best suited for particular temperature sensors and industrial or laboratory environments.
Bibliography
Adler, C.B., Reliability Aspects of Temperature Measurement, Instrumentation, Systems, and Automation Society Conference, 2002.
American Society for Testing and Materials, Annual Book of ASTM Standards,
Section 14, General Methods and Instrumentation, West Conshohocken,
PA, 2003.
Calibration Technology Goes Digital, InTech, September 1989, pp. 8687.
Daneman, H.L., The Dos and Donts of Temperature Calibration, NCSL
Annual Conference Proceedings, June 1991.
Daneman, H.L., The Precise Calibration of Industrial Pyrometers to 1,650C,
Measurement Science Conference, Anaheim, CA, January 1986.
Gray, W.T., Calibration of Optical Pyrometers, ISA Transactions, Vol. 6,
1967.
Hussselbaugh, B., Temperature Calibration Chamber, M & C News, September 1992.
Kaufman, A., Liquid Cooling of Electronics, Measurements and Control,
September 1979, pp. 120121.
Kaufman, A., Temperature Transducer Calibration Baths, Measurements
and Control, February 1986, pp. 188189.
597
Precision Thermometer/Calibrator
CuKo FeKo E R
S B N T K J Pt100
Probe
mV
int
man
Cl
Mode
TC
Type
Rate
Diff
Min
Max
Reset
STO
Pt100
RCL
+/-
ENT
On
Clear Display
CL
Tc&mV TC
Norm
Store Displayed
Value in Memory
Recall
Stored Value
TC
Off
/mv
Measurement/Calibration Switch to
Select Operating Mode
FIG. 4.3d
Thermocouple calibrator/simulator used in the laboratory.
High Temperature
Detector Calibration
Accessory
Copper Point Blackbody
Accessory
Optical Bench
Lamp with WaterCooled Base
Pyrometer Control
Filter System
Pyrometer
Pyrometer Mount
Optical Bench
Writing Shelf
Control
Panels
FIG. 4.3e
Two pyrometer calibration system with copper point, blackbody furnace, and standard lamp.
598
Temperature Measurement
TABLE 4.3f
Calibration Equipment Recommended as a Function of the Type
of Thermometer and of the Operating Environment
Temperature Sensor
Being Calibrated
Thermocouples
RTDs
Laboratory
Environment
Industrial Installation
Triple point
Portable calibrator
Fluidized bath
Portable simulator
Triple point
Portable calibrator
Freezing points
Portable bath
Laboratory simulator
Portable simulator
Optical pyrometers
Comparison system
Lamp comparator
Radiation detectors
Comparison system
Optical pyrometer
Kaufman, A. and Drees, W., How Accurate Are Your Transducer Calibrations?, Instruments & Control Systems, November 1959, pp.
16821685.
Kaufman, A. and Mitchell, P., How Accurate Are Your Temperature Reference Baths?, Instruments & Automation, March 1955, pp. 450451.
Kerlin, T.W., Practical Thermocouple Thermometry, ISA Press, 1999.
Mangum, B.W. and Furukawa, G.T., Guidelines for Realizing the International Temperature Scale of 1990 (ITS-90), NIST Tech. Note 1265,
August 1990.
Michalski, L., Eckersdorf, K., and McGhee, J., Temperature Measurement,
New York: John Wiley & Sons, 1991.
National Bureau of Standards, Thermometer Calibration: A Model for State
Calibration Laboratories, NBS Monograph 174.
Standards, Simulators, Calibrators, Measurements and Control, September
1991.
Temperature Calibration Baths, Measurements and Control, September
1991.
Withers, P., Thermocouple Calibration, Measurements and Control, September 1990, pp. 144147.