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MAGNETIC PARTICLE EXAMINATION

PROCEDURE FOR WELDS IN


API 1104 CARBON STEEL PIPELINES

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IMSN/MT/11
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June 1, 2010
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1. SCOPE
1.1

This procedure covers the performance of Magnetic Particle Examination and evaluation
against applicable acceptance standards for ferromagnetic welds (including their heataffected zone) using combination of Yoke magnetization technique with non-fluorescent wet
particles.

1.2

This procedure is not intended to replace visual examination but will act as supplementary
NDE method for finding open to the surface discontinuities.

1.3

This procedure is applicable in the performance of magnetic particle examination by PT. Inti
Mutu Sejahtera Nusantara (IMSN).

1.4

Weld configurations to be examined, including thickness dimensions and base material


product form shall follow Customers Drawing Requirements or NDE Map.

1.5

This procedure only applicable for pipelines with outside diameter above 4 inch.

2. CODES AND REFERENCES


2.1
2.2
2.3
2.4
2.5

API 1104 Welding of Pipelines and Related Facilities - 20th Edition, November 2005.
ASME Pressure Piping Code B31.8 Gas Transmission and Distribution Piping Systems, 2007
Edition.
ASME Pressure Piping Code B31.4 Pipeline Transportation Systems for Liquid Hydrocarbons
and Other Liquids, 2006 Edition.
ASTM E-709 Standard Guide for Magnetic Particle Testing, 2008 Edition.
IMSNs NDE Personnel Qualification and Certification Procedure Doc. No.: IMSN/WP/01
Revision 0.

3. PERSONNEL QUALIFICATION
Magnetic particle examination shall be performed by qualified and certified personnel in
accordance with IMSNs NDE Personnel Qualification and Certification Procedure Doc. No.:
IMSN/WP/01 Revision 0 which is in compliance with SNT-TC-1A 2006 Edition.
4. EQUIPMENT AND MATERIALS
4.1

Magnetizing Equipment
Equipment used under this procedure shall be Alternating Current (AC) Yokes or Direct
Current (DC) Yokes or Permanent Yokes type. The equipment shall satisfactorily meet the
requirement defined in Par. 6.2 of this procedure.
Table 1 Magnetic Particle Examination Medium

4.1

Manufacturer

White Contrasting Paint

Prepared
Black Ink Bath

Temp. Range

MAGNAFLUX

WCP-2

7HF

5C 52C

CHEMETALL-ELY

WCP-722

SUPRAMOR 4

5C 52C

CIRCLE SYSTEM

MI-GLOW WCP

CIRCLESAFE
820AX

5C 52C

Examination Medium
Table 1 shall be used in the performance of Magnetic Particle Examination under this
procedure. At all times, valid materials certificates shall be available to any concerning
parties for verification between the batch number stated in the certificate against the one
printed on the aerosol cans.

MAGNETIC PARTICLE EXAMINATION


PROCEDURE FOR WELDS IN
API 1104 CARBON STEEL PIPELINES

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5. SURFACE PREPARATION
5.1

Examination shall be conducted on uncoated (free from non-magnetic coatings) surfaces.

5.2

Surface preparation by grinding or machining may be necessary where surface irregularities


could mask discontinuities indications by non-relevant indications.

5.3

Cleaning shall be accomplished using either detergents, organic solvents, de-scaling


solutions, paint removers (for painted surface) or sand blasting.

5.4

Prior to magnetic particle examination, the surface to be examined and all adjacent areas
within at least 1 inch (25 mm) shall be dry and free from dirt, grease, lint, scale, welding
flux and spatter, oil, or any non-magnetic coating.

5.5

Temperature on surface of the part to be examined shall be controlled within those specified
in Table 1.

6. CALIBRATION
6.1

Calibration of Lifting Weight Standard


Each lifting weight standard shall be weighed with a scale from a reputable manufacturer or
independent laboratory and stenciled with the applicable nominal weight. A certificate of
the lifting standard stating its nominal weight shall be maintained on file. A weight
standard need only be calibrated again if damaged in a manner that could have caused
potential loss of material.

6.2

Calibration of Electromagnetic Yokes

6.3

6.2.1

Each AC yoke shall be able to lift a standard weight of at least 10 lb (4.5 kg) at
minimum 6 inch pole spacing that will be used for minimum of 3 seconds. This
calibration shall be verified every year or whenever the electromagnetic yoke is
suspected to have been damaged or after being repaired. At the minimum, the last
calibration report (see Exhibit B) from that one that is presently applicable shall be
maintained on file.

6.2.2

Each DC yoke shall be able to lift a standard weight of at least 40 lb (18 kg) at
minimum 6 inch pole spacing that will be used for minimum of 3 seconds. This
calibration shall be verified every year or whenever the electromagnetic yoke is
suspected to have been damaged or after being repaired. At the minimum, the last
calibration report (see Exhibit B) from that one that is presently applicable shall be
maintained on file.

6.2.3

Each permanent yoke shall be able to lift a standard weight of at least 40 lb (18 kg)
at the maximum pole spacing that will be used. This calibration shall be verified
daily prior to use. This check doesnt have to be maintained on file.

Calibration of Visible Light Meter


Visible light meter shall be calibrated at least once a year or whenever the meter has gone
through major repair. If meters have not been in used for one year or more, calibration shall
be done before being used. At the minimum, the last calibration report from the one that is
presently applicable shall be maintained on file.

7. EXAMINATION PROCEDURE
7.1

Viewing Conditions
A minimum light intensity of 100 fc (1000 lx) is required on the surface to be examined to
ensure adequate sensitivity during the examination and evaluation of indications.

7.2

Surface Contrast Enhancement


Surface contrast enhancer shall be applied temporarily to uncoated surfaces only in the
amounts sufficient to enhance viewing contrast. The material used as contrast enhancer
shall be of the white paint type and shall follow those specified in Table 1 for each particle
manufacturer. After surface preparation in accordance with Par. 5, shake the contrasting

MAGNETIC PARTICLE EXAMINATION


PROCEDURE FOR WELDS IN
API 1104 CARBON STEEL PIPELINES

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paint to ensure uniform distribution of particles. Apply a uniform thin film of the contrasting
paint to the test surface. Wait at least 30 seconds to allow the contrasting paint film
to dry. Apply magnetic particles to the examination surface.
7.3

Method of Examination
Examination shall be done by the continuous method; that is, wet magnetic particles
applied from the aerosol spray cans may be applied before and/or after magnetizing current
is applied. Accumulation of excess particles during examination shall be removed by blowing
or other source of low pressure dry air. The examination current or power shall be
maintained for at least 3 seconds while removing the excess particles. Observe any
indications formed.

Figure 1 Yoke Placement and Orientation for Detection of Flaws [in mm]
7.4

Direction of Magnetization
At least two separate examinations shall be performed on each area. During the second
examination, the line of magnetic flux shall be approximately perpendicular to those used
during the first examination. Figure 1 shows example of typical yoke placement, poles
configuration and orientation for detection of flaws.

7.5

Magnetizing Field Adequacy and Direction


All examinations shall be conducted with sufficient overlap to assure 100% coverage at the
required sensitivity. Yokes overlap shall not exceed that detailed in Figure 1. Verification of
magnetic field adequacy due to reduction of contact surface between the yoke leg and the
part, a magnetic flux strip indicator (Burmah Castrol Type 1 containing three
artificial defects) shall be used. Attach one flux indicator on the part surface under
examination so that its length is at right angles to the direction of the applied flux.
Magnetize the work piece by the use of the same pole spacing and contact area as the ones

MAGNETIC PARTICLE EXAMINATION


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to be used for the examination. The magnetization time shall not be less than 3
seconds. While the work piece is being magnetized apply the magnetic particles. It is
essential that the application of magnetic particles stops before the end of magnetization.
The direction and field adequacy of the induced magnetic field is seen readily from the
response of the flux indicators. The exact direction can be checked by re-orientating the
indicators with respect to the direction of the field. The direction and field adequacy are
considered sufficient when 3 (three) lines on the strip are clearly defined.
7.6

Evaluation of Indication(s)
Discontinuities are indicated by retention of the examination medium. However, localized
surface irregularities due to machining marks, magnetic permeability variations such as at
the edge of heat affected zones or other surface condition may produce non-relevant
indications. Broad areas of particle accumulation, which might mask indications from
discontinuities, are prohibited, and such areas shall be cleaned and reexamined.

8. ACCEPTANCE STANDARDS
An indication of an imperfection may be larger than the imperfection that causes it; however the
size of the indication is the basis for acceptance evaluation.
Acceptance Standards for weld parts and their base metal fabricated according to API 1104 shall
be as described below. Any indication with a maximum dimension of 1.5 mm or less shall be
classified as non-relevant. Any larger indication believed to be non-relevant shall be regarded as
relevant until re-examined by magnetic particle other nondestructive examination method to
determine whether or not an actual imperfection exist. The surface may be re-conditioned before
examination. After an indication is determined to be non-relevant, other non-relevant indications
of the same type need not be re-examined.
Relevant indications are those caused by imperfections. Linear indications are those in which the
length is more than three times the width. Rounded indications are those in which the length is
three times the width or less.
Relevant indications shall be considered as defects should any of the following conditions exist:
a.
b.
c.
d.

Linear indications which are evaluated as crater cracks or star cracks and exceed 4 mm in
length.
Linear indications which are evaluated as cracks other than crater cracks or star cracks.
Linear indications which are evaluated as IF and exceed 25 mm in total length in a continuous
300 mm length of weld or 8% of the weld length.
Rounded indications shall be evaluated according to the criteria of Paragraph 9.3.9.2 and
9.3.9.3 of API 1104 (see Exhibit C) as applicable. For evaluation purposes, the maximum
dimension of a rounded indication shall be considered its size.

9. EXAMINATION OF AREAS FROM WHICH IMPERFECTION HAVE BEEN REMOVED


Upon request, the area in which the defect has been removed (prior to making weld repairs) shall
be re-examined in accordance with this procedure to ensure that the defect has been removed or
reduced to acceptable size of imperfection.
10. RE-EXAMINATION OF REPAIRED AREA
After the weld is completed and the surface has been smoothly finished, the re-examination of
repaired area shall be performed in accordance with this procedure.
11. DEMAGNETIZATION
Unless specified in the contracting documents, demagnetization is not necessary to be done. If
the part is to be heat treated after examination, it is also not necessary to conduct
demagnetization of the part previously examined.

MAGNETIC PARTICLE EXAMINATION


PROCEDURE FOR WELDS IN
API 1104 CARBON STEEL PIPELINES

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12. POST EXAMINATION CLEANING


Unless directed otherwise by contracting documents, all parts and objects that have been
examined by magnetic particle method are not necessary to be cleaned. When required by
contracting document, post examination cleaning should be conducted as soon as practical using
a process that doesnt adversely affect the part. Typical post examination cleaning employed are:
-

Drying of wet particles and subsequent removal by brushing or with compressed air.
Removal of wet particles by flushing it with acetone.

13. EXAMINATION REPORT


All relevant and rejectable indications shall be recorded. As a minimum, the type of indications as
defined in this procedure, location and extent (length or diameter or aligned) shall be recorded on
Magnetic Particle Examination Report form as shown in Exhibit A of this procedure. The record
shall be stored for a period as specified in the contracting documents.
14. SAFETY PRECAUTIONS

14.1 Care shall be exercised during examination for magnetic particle materials which are
relatively toxic and highly flammable.

14.2 Manufacturers directions shall be followed at all times.


14.3 Smoking is prohibited while performing magnetic particle examination.
14.4 Electrical hazards like opened electrical wire from lighting source or magnetizing equipment
and the presence of short circuiting medium shall be treated with care.

14.5 Material Safety Data Sheet (MSDS) for each magnetic particle materials shall be
consulted in determining the proper method for the disposal of used pressurized spray cans
and liquid residue waste.

MAGNETIC PARTICLE EXAMINATION


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API 1104 CARBON STEEL PIPELINES

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Exhibit A MAGNETIC PARTICLE EXAMINATION REPORT FORM

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MAGNETIC PARTICLE EXAMINATION


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Exhibit B ELECTROMAGNETIC YOKE CALIBRATION REPORT FORM

PERIODIC CALIBRATION OF ELECTROMAGNETIC YOKES

Yoke's make and model

Yoke's serial no.

Referenced weight standard ID

YOKE'S LIFTING POWER TEST RESULT


POWER SOURCE

REFERENCED
WEIGHT

POLE SPACING

LIFTING
TIME

RESULT

This is to confirm that the instrument above meets the requirement of PT. Inti Mutu Sejahtera
Nusantara Document No.: IMSN/MT/11 Rev. 0

Calibrated by

Date of Calibration

Next recommended calibration

MAGNETIC PARTICLE EXAMINATION


PROCEDURE FOR WELDS IN
API 1104 CARBON STEEL PIPELINES

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Exhibit C Excerpt from API 1104 Par. 9.3.9.2 and Par. 9.3.9.3

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MAGNETIC PARTICLE EXAMINATION


PROCEDURE FOR WELDS IN
API 1104 CARBON STEEL PIPELINES

PROC. NO.
REV. NO.
DATE
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IMSN/MT/11
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June 1, 2010
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MAGNETIC PARTICLE EXAMINATION


PROCEDURE FOR WELDS IN
API 1104 CARBON STEEL PIPELINES

PROC. NO.
REV. NO.
DATE
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June 1, 2010
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