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10. The experiment was repeated by increasing the power to 0.75 kW, 1.00 kW, 1.25 kW and
1.50 kW.
11. Graph of pressure drop versus boil up rate was plotted based on the result.
Experiment B: Determining the mixture compositions
1. The equipment was set up to determine the refractive index of pure methylcyclohexane,
MCH and pure toluene.
2. The small quantities of methylcyclohexane, MCH approximately 25 mol%, 50 mol% and
75 mol% were used up and the refractive index for each quantity was measured.
3. The volume of constituents (MCH and toluene) used could be calculated by using the
following formula:
Vol
( MCH )
( Toluene)
+(Vol Toluene )
MW MCH
MW Toluene
( MCH )(100)
( MCH)
MW MCH
25=
( MCH)
Results
Experiment
A: Determining column pressure drop
Given:
Power (kW)
Boil up rate
(L/hr)
0.50
0.75
3.60
10.80
Pressure drop
(mm
H2O
70
82
Degree of
Refractive index
foaming on trays
Gentle localized
Violent localized
1.43875
1.44357
1.00
14.72
130
Foaming gently
1.44442
1.25
22.34
145
1.45484
violently over
1.50
33.51
whole tray
Liquid flooding
145
1.46090
in column
Refractive Index
1.47536
1.46132
1.47996
Pressure drop mm HO
130
100
145
82
70
50
145
0
0
10
15
20
25
30
35
40
Calculations
Here are the calculations to determine the volume of constituents needed to fulfill the following
requirements:
Vol
( MCH )
( Toluene)
+(Vol Toluene )
MW MCH
MW Toluene
( MCH )(100)
( MCH)
MW MCH
25=
( MCH )
25=
100
Vol
MW MCH Toluene
1+ Toluene +
+
Vol MCH MW Toluene MCH
Vol Toluene
MW Toluene MCH
=3
Vol MCH
MW MCH Toluene
Vol Toluene
92.15 0.774
=3
Vol MCH
98.19 0.867
Vol Toluene
=2.513 4
Vol MCH
1Vol Toluene :2.5134 Vol MCH
Thus, for 100 mL of mixture, quantities required would be as follow since the total volume is
3.5134 mL,
Volume of toluene
Volume of MCH
3.5134 mL :100 m L
3.5134 mL :100 mL
mLmixture
100 mL
Volmol%
Toluene@MCH
100 = and 50 mol% toluene,
Forx50
3.5134 mL
mLmixture
mLmixture
( 100 mL ) ( 2.51 34 )
3.5134 mL
Vol
Vol
( MCH )
( Toluene)
+(Vol Toluene )
MW MCH
MW Toluene
( MCH )(100)
( MCH)
MW MCH
50=
( MCH )
50=
100
Vol Toluene MW MCH Toluene
1+
+
+
Vol MCH MW Toluene MCH
Vol Toluene
MW Toluene MCH
=1
Vol MCH
MW MCH Toluene
Vol Toluene
92.15 0.774
=1
Vol MCH
98.19 0.867
Vol Toluene
=0.8378
Vol MCH
1Vol Toluene :0.8378 Vol MCH
Thus, for 100 mL of mixture, quantities required would be as follow since the total volume is
1.8378 mL,
Volume of toluene
Volume of MCH
1.8378 mL:100 m L
1.8378 mL :100 mL
mLmixture
100 mL
1.8378 mL
mLmixture
( 100 mL ) ( 0.8378 )
1.8378 mL
Vol
( MCH )
( Toluene)
+(Vol Toluene )
MW MCH
MW Toluene
( MCH )(100)
( MCH)
MW MCH
75=
( MCH )
75=
100
Vol
MW MCH Toluene
1+ Toluene +
+
Vol MCH MW Toluene MCH
Vol Toluene
MW Toluene MCH
=0.333
Vol MCH
MW MCH Toluene
Vol Toluene
92.15 0.774
=0.333
Vol MCH
98.19 0.867
Vol Toluene
=0.2790
Vol MCH
1Vol Toluene :0.2790 Vol MCH
Thus, for 100 mL of mixture, quantities required would be as follow since the total volume is
1.2790 mL,
Volume of toluene
Volume of MCH
1.2790 mL:100 m L
1.2790 mL :100 mL
mLmixture
100 mL
1.2790 mL
mLmixture
( 100 mL ) ( 0.2790 )
1.2790 mL