Professional Documents
Culture Documents
A PROJECT REPORT ON
MASTER OF TECHNOLOGY
IN
DESIGN ENGINEERING
By:
SHIVARAJA.H.B
USN: 1DB12MDE12
Under the guidance of
Mr. B.S. PRAVEEN KUMAR
Associate professor Department of Mechanical Engineering
Don Bosco Institute of Technology
TABLE OF CONTENTS
CHAPTER 1
INTRODUTION
Page No
1.1 Preamble
1.4 Methodology
CHAPTER 2
LITERATURE REVIEW
4-10
CHAPTER 3
INTRODUCTION TO COMPOSITE
3.1 Background
11
3.2 Composites
12
13
14
14
16
16
16
17
18
18
18
19
19
3.3.3.3Laminated Composites
19
19
20
20
21
21
21
22
22
23
23
23
24
3.7 Examples
27
27
28
CHAPTER 4
SELECTION OF MATERIALS
4.1 Matrix Material: Al 356
29
29
30
31
32
32
33
33
35
37
39
40
41
41
43
46
48
6.7 Microstructure
48
6.8 Etching
49
50
51
53
54
55
57
59
7.6 Microstructure
60
CHAPTER 8
CONCLUSION
CHAPTER 9
6
6
5
63
LIST OF TABLES
Table No
Description
Page No
4.1
30
4.2
30
4.3
33
5.1
39
6.1
41
7.1
53
7.2
54
7.3
55
7.4
57
7.5
59
LIST OF FIGURES
Fig No
Description
Page No
1.1
Project Methodology
3.1
16
3.2
16
Materials
18
4.1
29
4.2
31
4.3
32
5.1
34
5.2
36
5.3
36
5.4
Electric furnace
37
5.5
38
5.6
Formation of Vortex
38
5.7
38
5.8
38
5.9
38
6.1
SENB specimen
41
6.2
42
6.3
43
6.4
45
6.5
45
6.6
47
6.7
47
6.8
48
6.9
Polishing machine
49
6.10
50
6.11
51
6.12
FE mesh model
51
6.13
52
7.1
54
7.2 Variation of tensile strength and yield strength with different wt%
Reinforcement
56
7.3
58
7.4
59
7.5
Microstructure of Al356+0%SiC+8%ZrSiO4
60
7.6
Microstructure of Al356+6%SiC+2%ZrSiO4
60
7.7
Microstructure of Al356+2%SiC+6%ZrSiO4
61
7.8
Microstructure of Al356+4%SiC+4%ZrSiO4
61
7.9
Microstructure of Al356+8%SiC+0%ZrSiO4
62
CHAPTER 1
INTRODUTION
1.1 Preamble
New and high performance particle reinforced metal matrix composites (PRMMC) are
expected to satisfy many requirements for a wide range of performance-driven, and
price sensitive, applications in aerospace, automobiles, bicycles, golf clubs, and in
other structural applications. In general, these materials exhibit higher strength and
stiffness, in addition to isotropic behavior at a lower density, when compared to the unreinforced matrix material. PRMMC benefits from the ceramics ability to withstand high
velocity impacts, and the high toughness of the metal matrix, which helps in preventing
total shattering. This contribution leads to an excellent balance between cost and
mechanical properties, which are appealing for many applications.
The recognition of the potential weight savings that can be achieved by using the advanced
composites, which in turn means reduced cost and greater efficiency, was responsible for this
growth in the technology of reinforcements, matrices and fabrication of composites. If the first
two decades saw the improvements in the fabrication method, systematic study of properties
and fracture mechanics was at the focal point in the 60s. Since then there has been an everincreasing demand for new, strong, stiff and yet light-weight materials in fields such as
aerospace, transportation, automobile and construction sectors. These materials have low
specific gravity that makes their properties particularly superior in strength and modulus to many
traditional engineering materials such as metals. As a result of intensive studies into the
fundamental nature of materials and better understanding of their structure property relationship,
it has become possible to develop new composite materials with improved physical and
mechanical properties.
Page 1
Page 2
1.4 Methodology
The methodology of the project in presented in figure 1.1
Literature review
Identification of the
problem
Development of Metal
matrix composites
Tensile
Fracture Toughness
Testing
Compression
Hardness
Microstructure
FE analysis
Conclusion
Page 3
CHAPTER 2
LITERATURE REVIEW
J.Jenix Rino, Dr.D.Sivalingappa, Halesh Koti, V.Daniel Jebin[1] The present study deals
with the investigation of the mechanical behaviour of Aluminium6063 alloy composites
reinforced by Zircon sand(ZrSiO4) and Alumina(Al2O3) particles were taken in to
account for investigating the properties such as density tensile strength and hardness
of the composites synthesized by Stir casting technique. The mechanical properties
evaluation reveals variations in hardness and the tensile strength values with the
composite combinations. From the experimental studies, the optimum volume fraction
of hybrid reinforcement in Al 6063 alloy on the basis of microstructure and mechanical
properties it is found that the (4+4) wt% combination.
The unique tailor ability of the composite materials for the specific
requirements makes these materials more popular in a variety of applications such
as aerospace, automotive (pistons, cylinder liners, bearings), and structural
components, resulting in savings of material and energy. Discontinuous reinforced
aluminum metal matrix composites (DRAMMCs) are a class of composite materials
having desirable properties like low density, high specific stiffness, high specific
strength, controlled co-efficient of thermal expansion, increased fatigue resistance
and superior dimensional stability at elevated temperatures etc. The properties and
behavior of various Al alloys and their composites are much explored in terms of
microstructure, mechanical properties, loading conditions and applications.
K.K. Alaneme, A.O. Aluko [2] The tensile and fracture behavior of as-cast and age-hardened
aluminium (6063), silicon carbide particulate composites produced, using borax additive and a
two step stir casting method, was investigated. Al (6063), SiCp composites having 3, 6, 9, and
12 volume percent of SiC were produced, and sample representatives of each composition were
subjected to age-hardening treatment at 1800 C for 3 hours. Tensile and Circumferential
Notched Tensile (CNT) specimens were utilized for tension testing to evaluate, respectively, the
tensile properties and fracture toughness of the composites. Experimental results show that the
ageing treatment resulted in little improvement in the tensile strength of the composites. The
tensile strength and yield strength increased to almost the same magnitude with an increase in
SiC volume percent
Page 4
Mohan Vanarotti, SA Kori, BR Sridhar, Shrishail B.Padasalgi [3] Aluminum alloy and silicon
carbide metal matrix composites are finding applications in aerospace, automobile and general
engineering industries owing to their favourable microstructure and improved mechanical
behavior. Aluminium alloy A356 and silicon carbide composites were obtained by stir casting
technique. Silicon carbide content in the alloy was fixed at 5 Weight % and 10 weight % during
the casting. Microstructure revealed a uniform distribution of the silicon carbide throughout the
matrix. Hardness and tensile properties of the composite showed an improvement as compared
to the alloy without silicon carbide additions.The present paper highlights the salient features of
casting technique and characterization of aluminum alloy A356 and silicon carbide metal matrix
composite.
J.E. Perez Ipina, A.A. Yawny, R. Stukeb, C. Gonzalez Oliver[4] Metal matrix composites (MMC)
are materials made from the dispersion of a ceramic phase, typically SiC or Al203 fibers or
particles, in order to improve the mechanical and physical properties of the matrix. In the
particular situation of Aluminum MMCs, both pure Al and alloys are employed. Continuous fibers
(Continuous metal matrix composites CMMC) as well as short fibers and particles
(Discontinuous Aluminum reinforced DAR) are employed. The production and use of composite
materials is under intensive development because of the interesting physical and mechanical
properties that these materials present and also due to the possibility to manipulate them by
means of the variation of the type and proportion of
Page 5
Khalid Mahmood Ghauri1, Liaqat Ali [6] The present work was mainly carried out to characterize
the SiC/Al composite which was produced by reinforcing the various proportions of SiC (5, 10,
15, 25 and 30%) in aluminum matrix using stir casting technique. Mechanical properties of test
specimens made from stir-casted Aluminum-Silicon Carbide composites have been studied using
metallographic and mechanical testing techniques. However, beyond a level of 25-30 percent
SiC, the results are not very consistent, and depend largely on the uniformity of distribution of
SiC in the aluminum matrix It was observed that as the volume fraction of SiC in the composite is
gradually
Page 6
Page 7
This study shows that the failure is initiated by micro void nucleation at the different
initiation sites. Void initiation is more pronounced in the matrix near the interface.
The micro cracks can grow from these micro voids to absorb available strain
energy. Crack propagation occurs by linking these micro cracks locating the crack
path preferentially in the matrix adjacent to the interface. This study shows that this
material must have adequate wettability with both Al and SiC to achieve good
bonding. Moreover, the proposed material must have high value of tensile ductility
and a low yield stress in order to accommodate the plastic strain developed during
processing and relax stress concentrations introduced by particle geometry.
Shuyi Qin, Guoding Zhang [9] A structure-toughened SiC particle reinforced 6061
aluminum alloy matrix composite (SiCp-6061Al/6061Al) was designed and fabricated
by vacuum infiltration processing. Its fracture toughness KQ was tested by three-point
bending method and compared with a conventionally stirring-cast SiCp/6061Al
composite's in case of same particle size and volume fraction. The fractography of the
SiCp-6061Al/6061Al composite was observed on a Cambridge Instrument S360
Scanning Electron Microscopy (SEM). The results showed that SiCp-6061Al/6061Al
Page 8
Page 9
Page 10
CHAPTER 3
INTRODUCTION TO COMPOSITE
3.1 Background
New and high performance particle reinforced metal matrix composites (PRMMC) are expected
to satisfy many requirements for a wide range of performance-driven, and price sensitive,
applications in aerospace, automobiles, bicycles, golf clubs, and in other structural applications.
A PRMMC consists of a uniform distribution of strengthening ceramic particles embedded within
a metal matrix. In general, these materials exhibit higher strength and stiffness, in addition to
isotropic behavior at a lower density, when compared to the un-reinforced matrix material.
PRMMC benefits from the ceramics ability to withstand high velocity impacts, and the high
toughness of the metal matrix, which helps in preventing total shattering. This contribution leads
to an excellent balance between cost and mechanical properties, which are appealing for many
applications.
The recognition of the potential weight savings that can be achieved by using the advanced
composites, which in turn means reduced cost and greater efficiency, was responsible for this
growth in the technology of reinforcements, matrices and fabrication of composites. If the first
two decades saw the improvements in the fabrication method, systematic study of properties
and fracture mechanics was at the focal point in the 60s. Since then there has been an everincreasing demand for new, strong, stiff and yet light-weight materials in fields such as
aerospace, transportation, automobile and construction sectors. Composite materials are
emerging chiefly in response to unprecedented demands from technology due to rapidly
advancing activities in aircrafts, aerospace and automotive industries. These materials have low
specific gravity that makes their properties particularly superior in strength and modulus to many
traditional engineering materials such as metals. As a result of intensive studies into the
fundamental nature of materials and better understanding of their structure property relationship,
it has become possible to develop new composite materials with improved physical and
mechanical properties. Based on information now in the public domain, the following military
applications for MMCs appear attractive: high-temperature fighter aircraft engines and
structures; high-temperature missile structures; and spacecraft structures. Testing of a National
Aerospace Plane (NASP) prototype is scheduled for the early to mid 1990s, which might be too
early to include MMCs. However, it may be possible to incorporate MMCs in the structure or
engines of the production vehicle.
Page 11
3.2 Composites
Three decades of intensive research have provided wealth of new scientific knowledge
on the intrinsic and extrinsic effects of ceramic reinforcement to metals and their alloys.
The successes of these various researches have stimulated application of composite in
the design of many engineering and non engineering component.
Further, the need of composite for lighter construction materials and more seismic
resistant structures has placed high emphasis on the use of new and advanced
materials that not only decreases dead weight but also absorbs the shock & vibration
through tailored microstructures. Composites are now extensively being used for
rehabilitation/ strengthening of pre-existing structures that have to be retrofitted to make
them seismic resistant, or to repair damage caused by seismic activity.
While composites have already proven their worth as weight-saving materials, the
current challenge is to make them cost effective. The efforts to produce economically
attractive composite components have resulted in several innovative manufacturing
techniques currently being used in the composites industry. It is obvious, especially for
composites, that the improvement in manufacturing technology alone is not enough to
overcome the cost hurdle. It is essential that there be an integrated effort in design,
material, process, tooling, quality assurance, manufacturing, and even program
management for composites to become competitive with metals. The composites
industry has begun to recognize that the commercial applications of composites
promise to offer much larger business opportunities than the aerospace sector due to
the sheer size of transportation industry. Thus the shift of composite applications from
aircraft to other commercial uses has become prominent in recent years.
Increasingly enabled by the introduction of newer polymer resin matrix materials and high
performance reinforcement fibers of glass, carbon and aramid, the penetration of these
advanced materials has witnessed a steady expansion in uses and volume. The increased
volume has resulted in an expected reduction in costs. High performance FRP can now be found
in such diverse applications as composite armoring designed to resist explosive impacts, fuel
cylinders for natural gas vehicles, windmill blades, industrial drive shafts, support beams of
highway bridges and even paper making rollers. For certain applications, the use of composites
rather than metals has in fact resulted in savings of both cost and weight. Some examples are
cascades for engines, curved fairing
Page 12
Page 13
The increasing demand for lightweight, inexpensive, energy saving, stiff and
strong materials in aircraft, space, defense and automotive applications have
stimulated steadily growing efforts to develop composite materials. Lightweight
composites are attracting a great deal of attention due to the possibility of
weight saving in industrial applications. Automobile weight reduction can directly
translate into reduced fuel consumption. Reduction in the weight of aircraft and
marine vessels can lead to increased loading capacity.
Page 14
Page 15
Polymer Matrix
Metal Matrix
Thermoplastics
Thermo sets
Light metals
& alloys(Al,
Mg, Li & Ti)
Refractory
metals
Ceramic Matrix
Ceramics
Carbon
Glass
Reinforcing Material
Particulate reinforced
Large particles
Dispersoids
Fiber reinforced
Continuous fibers
Discontinues
(short)
Aligned or
random
Structural composites
Laminates
Sandwich
panels
Page 16
Page 17
`
Figure 3.3 Schematic Presentation of Three Shapes of Metal Matrix Composite
Materials
Page 18
3. Cermets are also used as nuclear reactor fuel element and control rods.
Page 19
Page 20
Page 21
Page 22
in
the
melt
and
subsequently
during
solidification.
In
Page 23
phases
added
as
reinforcements
to
improve
the
properties.
The
reinforcements can be in the form of fibers, whiskers and particulates. Properties of the
metal matrix composites can be tailored by varying the nature of constituents and their
volume fraction. They offer superior combination of properties in such a manner that
today no existing monolithic material can rival and hence are increasingly being used in
the aerospace and automobile industries. The principal advantage MMCs enjoy over
other materials lies in the improved strength and hardness on a unit weight basis.
Page 24
Page 25
The main contribution to the strengthening of PRAMCs is particle addition, which affects most of
the mechanical properties of PRAMCs. Several particle parameters, which are
Page 26
3.7 Examples
Continuous carbon fiber reinforced Al alloy likewise has been used in most
structures (vertical support structures) in the Hubble telescope.
SiC continuous fiber reinforced Al alloy has been used vertical section of
advanced fighter aircrafts.
SiC continuous fiber reinforced Ti alloy has been used for hypersonic aircraft.
Precision components of missile guidance system demand very high dimensional
stability i.e. geometries should not change with temperature excursions during use.
Al alloy with 20% SiC continuous fiber satisfy this requirement.
Discontinuous SiC fibers 1 to 3mm in diameter and 50 to 200mm long are mixed
with Al powders consolidated by hot pressing and then extruded or forged to the
desired shape. With 20% SiC whiskers, the tensile strength increased from 310Mpa
to 480Mpa and the tensile modulus can be increased from 69 to 115 Gpa.
Hybrid composites of 12% by volume fraction of alumina particles (for high strength)
and 9% volume fraction of graphite fibers (for self lubrication) in alloys have been
developed by Honda for Engine blocks, connecting rods, piston rods etc., for
automobiles, which helps in reducing weight of automobile and enhanced engine
life. SiC coated on inter-metallic compound Ti3Al fibers in Ti alloy matrix have been
found to be very effective for high temperatures resistance. These composites find
Page 27
Non-flammability.
Better capability to withstand compression and shear loading.
Disadvantages
Higher densities as compared to PMCs.
MMCs demand higher processing temperatures.
Processing methods are expensive.
Page 28
CHAPTER 4
SELECTION OF MATERIALS
Cast Al356 is one of the most widely used commercial Al-Si-Mg alloys in the aircraft
and automotive industries due to its good castability and the fact that it can be
strengthened by artificial aging. However, the mechanical properties of Al356 are
significantly affected by micro structural features such as microporosity, intermetallics,
eutectic silicon particles and heat treatments. Aluminium Metal matrix composites
(AMMC), where hard ceramic particles are distributed in a relatively ductile matrix, have
widespread applications in aerospace, automobiles and other engineering industries
because of their excellent physical, mechanical and tribological properties.
Page 29
Element
Wt%
Si
Fe
Cu
Mn
Mg
Ni
Zn
Ti
Pb
Aluminium
Rem
Density(*1000 Kg/m3 )
2.685
Poissons ratio
0.33
228
165
Elongation (%)
3.5%
180
151
Melting Temperature
5550C
Fatigue Strength(MPa)
60
Page 30
density
High strength
Page 31
and
moving
turbine
Page 32
High hardness
Zircon Sand
M.P. (0C)
2500
1870
Hardness
7.5
Density (g/cm3)
4.5-4.70
0
4.5
Crystal structure
Tetragonal
Page 33
CHAPTER 5
FABRICATION OF COMPOSITES
Flow chart of composite fabrication is as shown in figure 5.1
Aluminium
matirx (Al356)
Metal matrix composite
Al356-Sic-ZrSio4
Reinforcement
(Silicon Carbide+
Zirconium Silicate)
Matrix
Furnace
Degassing+
Scum powder
Stir
Reinforce
Pouring
Casting
Fig 5.1 Flow chart of fabrication of Composite
Page 34
Page 35
Page 36
Slag removal.
After 10 mins titanium dioxide was added to remove the entrapped gases
(degasification) and Stirrer was introduced.
Stirrer was rotated at a speed of 0 to 300 rpm to create a vortex in the liquid metal.
Reinforcement material Sic and ZrSiO4 powder was added according to the
Page 37
Fig 5.7 Pre heating of reinforcement Fig 5.8 Poured molten metal in mould box
Page 38
Samples
1
Al356 (kg)
3
Sic (%)
-
ZrSio4 (%)
8
The composition of the matrix metal and the reinforcement in different wt%
ratios is shown in the above table. The casting samples with different wt%
reinforcements were prepared respectively as shown below.
Casting 1: Al356+0%SiC+8%ZrSiO4
Casting 2: Al356+6%SiC+2%ZrSiO4
Casting 3: Al356+2%SiC+6%ZrSiO4
Casting 4: Al356+4%SiC+4%ZrSiO4
Casting 5: Al356+8%SiC+0%ZrSiO4
Page 39
CHAPTER 6
EXPERIMENTAL DETAILS
6.1 Fracture Toughness
The measurement of valid plane strain fracture toughness, (KIC) values for
particulate reinforced metal matrix composites is an important step in the
process of developing useful products from these materials and increasing
confidence in their properties and performance.
Fracture toughness is a material property that characterizes the materials resistance to
crack propagation when under load or stress. In more precise terms, it refers to the
resistance of a preexisting crack to extend either under unstable (i.e., brittle fracture) or
by stable tearing means (i.e., ductile fracture). Experimental methods for characterizing
fracture toughness play a critical role in applying fracture mechanics to integrity
assessment, fitness-for-service evaluation, and limit state analyses for a wide variety of
engineering structures. Fracture toughness properties are frequently used as a basis
for material selection, material qualification programs, and quality assurance for critical
structures such as high-pressure gas and liquid transmission pipelines, pressure
vessels, nuclear reactor components, petrochemical processing vessels, and aircraft.
Fracture toughness is a quantitative way of expressing a material's resistance to brittle
fracture when a crack is present. If a material has much fracture toughness it will
probably undergo ductile fracture. Brittle fracture is very characteristic of materials with
less fracture toughness. Fracture mechanics, which leads to the concept of fracture
toughness, was broadly based on the work of A. A. Griffith who, among other things,
studied the behavior of cracks in brittle materials.
The measurement procedure of fracture toughness is based on the principle of linearelastic fracture mechanics (LEFM) and contains three main steps: generation of cracks
in the test specimen, measurement of the load at failure stress respectively, and crack
depth. In the case of ideally brittle materials, the fracture toughness is independent of
the crack extension. The crack growth resistance increases with the increasing crack
extension. Some structural ceramics show an increase of fracture resistance with crack
extension under stable crack growth. The Single-Edge-Notched Beam (SENB) method
was developed as a simple and inexpensive alternative, but the results can be
influenced by the tip radius of the sawed notch.
Page 40
ASTM Code
Span length
(mm)
(mm)
1
ASTM-D790
Flexural
127 x 13 x 6
65
Table 6.1 ASTM codes for mechanical test and sample dimensions
Page 41
--------------- (1)
Where
--------------- (2)
The KIC parameter denotes mode I fracture in which crack formation occurs in
tensile mode due to bending.
Page 42
Yield stress
By considering the stress-strain curve beyond the elastic portion, if the tensile loading
continues, yielding occurs at the beginning of plastic deformation. The yield stress, can be
obtained by dividing the load at yielding (Py) by the original cross-sectional area of the
equation below.
Ductility
Ductility can be expressed either in terms of percent elongation or percent
reduction in area as expressed in the equations below
Page 44
Testing Machine
The average cross section of the specimen was determined using the
micrometer.
2. Firmly grip the upper end of the specimen in the fixed head
of universal testing machine using fixing shackles.
3. The computer controlled testing machine was adjusted to
read zero.
4. Strain rate was selected as per standard 2mm/ min.
5. Applied load until the specimen was broken.
6. Remove the broken specimen from testing machine and
observe for the failure characteristics. The dimension of
smallest section was measured, the parts were held
together and measure gauge length and length between
the shoulders, and diameters.
Brinell hardness number (BHN) is expressed as the ratio of applied load to surface
area of the spherical indentation mode. In this process of hardness determination
when the metal is indented by a spherical tip. The tip first overcomes the resistance
of the metal to elastic deformation and then a small amount of plastic deformation
upon deeper indentation of the tip. It overcomes large deformation.
For the Brinell hardness test, the surface of the specimen on which the impression is to
be made, should be smooth, clear, dry and free from oxides and scales to permit
accurate measurement. For ferrous metals the load ranges P = 30 d should be used,
2
for non-ferrous metals like brass and aluminium load range P= 5 D , should be used.
Page 46
Wait till handle on left side comes to rest and allow the load to act for 30 seconds.
5.
Handle was pressed to release the load and to bring objective back in to position.
6.
Page 47
6.7 Microstructure
The optical metallurgical microscope (model: NIKON Epiphot 200) was used for
microstructure characterization of the Al356 matrix alloy reinforced with SiC and
ZrSio4 to study the effect of reinforcement on the matrix.
The specimens for optical microscopy were prepared according to ASTM E3 standards. The
samples were first subjected to grinding and polishing followed by etching. Grinding and
polishing after usual grinding and machining, the specimens were rough polished using 100,
200, 400, 600, 800 and 1200 grit silicon carbide papers. These papers are less susceptible to
loading than emery papers. The specimens were held firmly in hand and rubbed smoothly
against the SiC papers, exercising sufficient care to avoid any deep scratches since the Al alloys
are comparatively soft. Excessive heat formation during polishing was avoided as Al alloys
contain many metastable phases. Fine polishing was performed using magnesium oxide paste
followed by diamond paste using polishing machine shown in Fig. 4.4. The platform was covered
with billiard cloth. Separate platforms were used for magnesium oxide and diamond polishing.
During fine polishing
Page 48
6.8 Etching
The most useful etchant for microscopic examination of Al and Al alloys is the aqueous solutions
of chromic acid to which sodium sulphate has been added. Etchant composition is as follows:
200gm chromic acid, 15gm sodium sulphate and 1000 ml water.
The specimen surface was first cleaned in alcohol, then in running water and etched while wet.
To avoid staining after etching, it was immediately rinsed in a solution of 200 gm chromic acid in
1000 ml of water. Etching duration was 4 to 5 sec, followed by rinsing in water. The samples
were dipped in alcohol and dried in a stream of clean warm air.
Page 49
Page 50
Page 51
CHAPTER 7
RESULTS AND DISCUSSIONS
7.1 Fracture toughness results
Peak load
Al356+
Al356+
Al356+
Al356+
Al356+
0%Sic+
6%Sic+
2%Sic+
4%Sic+
8%Sic+
8%Zrsio4
2%Zrsio4
6%Zrsio4
4%Zrsio4
0%Zrsio4
660
720
780
780
660
15.27
16.67
18.05
18.05
15.27
(N)
Fracture
toughness
(MPa m1/2)
Page 53
18
17.5
17
16.5
16
15.5
15
14.5
14
13.5
1
Reinforcement in wt%
1. Al356+0%Sic+8%ZrSio4
2. Al356+6%Sic+2%ZrSio4
3. Al356+2%Sic+6%ZrSio4
4. Al356+4%Sic+4%ZrSio4
5. Al356+8%Sic+0%ZrSio4
Fracture
toughness
(experimental)
Fracture
toughness
(FEA)
Al356+
Al356+
Al356+
Al356+
Al356+
0%Sic+
0%Sic+
0%Sic+
0%Sic+
0%Sic+
8%Zrsio4
15.27
8%Zrsio4
16.67
8%Zrsio4
18.05
8%Zrsio4
18.05
8%Zrsio4
15.27
14.13
15.28
16.89
16.89
14.13
Page 54
Al356+
Al356+
Al356+
Al356+
0%Sic+
6%Sic+
2%Sic+
4%Sic+
8%Sic+
8%Zrsio4
2%Zrsio4
6%Zrsio4
4%Zrsio4
0%Zrsio4
18.30
17.70
17.80
17
Displacement at 10
13
12.6
12.2
13.1
12
15.50
14.90
15.70
14.50
97.93
126.49
125.18
127.92
119.28
149.34
148.70
145.03
139.85
4.60
5.78
4.40
3.32
peak (mm)
Load at yield
(KN)
Yield Stress
N/mm2)
Tensile strength 119.15
2
(N/mm )
% Elongation
2.90
Page 55
Strength (N/mm2)
160
140
120
100
80
UT
S
60
YS
40
20
0
1
Reinforcement ratios
Hardness (BHN)
Al356+0%SiC+8%ZrSiO4
52
Al356+6%SiC+2%ZrSiO4
52.6
Al356+2%SiC+6%ZrSiO4
56.6
Al356+4%SiC+4%ZrSiO4
56.6
Al356+8%SiC+0%ZrSiO4
55.6
Page 57
Hardness (BHN)
55
54
53
52
51
50
49
1
Reinforcement in wt%
Page 58
Al356+
Al356+
Al356+
Al356+
Al356+
0%Sic+
6%Sic+
2%Sic+
4%Sic+
8%Sic+
8%Zrsio4
2%Zrsio4
6%Zrsio4
4%Zrsio4
0%Zrsio4
22093.17 22656.05
22019.75
22313.43 20306.63
14
16.5
12.8
13.6
56.23
56.43
56.12
54.91
Displacement at 11.5
Peak (mm)
Compression
56.97
2
Strength(Kg/mm )
Table 7.4 Variation of compression strength with different wt% reinforcement
The compression strength of the matrix alloy reinforced with SiC and ZrSiO 4 is
shown in Fig 7.4. It can be observed from the fig below that the composition
with 0%SiC+8%ZrSiO4 and 2%SiC+6%ZrSiO4 have high compression strength.
57.5
57
56.5
56
55.5
55
54.5
54
53.5
1
Reinforcement in wt%
Fig7.4 Compression strength for different wt% reinforcement
Page 59
7.6 Microstructure
The optical metallurgical microscope (model: NIKON Epiphot 200) was
used for analyzing the distribution of the reinforcement in the matrix alloy.
100X
500X
Fig7.5 Microstructure of Al356+0%SiC+8%ZrSiO 4
100X
500X
Fig7.6 Microstructure of Al356+6%SiC+2%ZrSiO 4
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100X
500X
Fig 7.7 Microstructure of Al356+2%SiC+6%ZrSiO 4
100X
500X
Fig 7.8 Microstructure of Al356+6%SiC+2%ZrSiO 4
Page 61
100X
500X
Fig 7.9 Microstructure of Al356+8%SiC+0%ZrSiO 4
The specimens for microscopic observations were prepared by the standard technique
of grinding with SiC abrasive papers and polishing with a diamond suspension solution.
In the microstructure of the composite, agglomerates of the reinforcement particles are
clearly visible as shown in figures above. From the above figures it can be observed
that there is a reasonably homogenous distribution of the reinforcement particles in the
cast composite. It was found that the particles showed a strong tendency to accumulate
in the colonies which froze in the last stage of solidification. During the distributive
mixing, the rotation of the stirrer generates a vortex through which the reinforcement
particles are drawn into the melt. Once the particles are transferred into the liquid, the
distribution is strongly affected by certain flow transitions. The axial flow causes lifting
of particles due to momentum transfer and radial flow prevents particle settling.
Page 62
CHAPTER 8
CONCLUSION
Aluminum based metal matrix composites are the most promising materials for
the future automotive, aerospace and other applications. Al 356 alloy matrix
hybrid composites reinforced with Zirconium Silicate and Silicon Carbide
particles has been successfully synthesized by the stir casting method.
1. The results from the study reveal that there is considerable increase in the fracture
Page 63
CHAPTER 9
SCOPE FOR FUTURE WORK
1. The amount of reinforcement in metal matrix composite used in the present
study is limited to 8 weight percentage. Further studies can be carried out
by varying the weight percentage of the reinforcement.
2. Single Edge Notch Bend specimen is used in the present study to evaluate
the Fracture Toughness. Similar studies can be carried out using the
compact tension specimen.
3. In the present study mechanical properties have been evaluated. Further
tribological properties like friction, corrosion and wear test can be evaluated.
4. The microstructure was analyzed by metallurgical microscope. To analyze
the microstructure SEM and EDAX can be used.
5. The mechanical properties can also be evaluated after the heat treatment of
the composite.
Page 64
REFERENCES
1. K.K. Alaneme, A.O. Aluko, Fracture toughness (K1C ) and tensile properties
of as-cast and age-hardened aluminium (6063)silicon carbide particulate
composites. Federal University of Technology, Akure, PMB 704, Nigeria.
2. Mohan Vanarotti, SA Kori, BR Sridhar, Shrishail B.Padasalgi, Synthesis and
Characterization of Aluminium Alloy A356 and Silicon Carbide Metal Matrix
Composite IPCSIT vol. 49 (2012) (2012) IACSIT Press, Singapore.
Page 65
Composites
of
12. Shuyi Qin, Guoding Zhang and Wenlong Wang, Fracture Toughness of
Structural SiCp-6061Al/6061Al Composite State Key Lab. of MMCs,
Shanghai Jiao Tong University, Shanghai 200030, China.
13. Atta ur Rehman Shah, Dong-woo Lee, Sang-jin Kim, Abdul Wasy, Yi-Qi
Wang,
Effect
of
wt%
of
ATH
on
Mechanical
Strength
of
of
thermal
sprayed
Metal-Matrix
Composites,
High
Performance Composites for the 1990s, eds. S.K.Das, C.P. Ballard and
F. Marikar, TMS-New Jersey, 1990, p 195.
19. J. Zhang, R.J. Perez, M. N. Gungor and E.J.Lavernia, Damping
Characteristics of Graphite Particulate Reinforced Aluminium Composites,
Developments in Ceramics and Metal Matrix Composites. Kamleshwar
Upadhya, ed., Warrendale, PA: TMS Publication, 1992, pp 203-217.
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