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3.1
IN T R O D U C T IO N
3.2 M A T R IX MODEL
Size range 1 in Table 3-1 is the maximum size and the (n + l)th size range
refers to the residue, that is, to the particles which pass the finest screen in a
nest o f screens.
During a grinding process, particles in all size ranges have some probability
o f being broken and the products o f breakage may fall in that size interval
and in any smaller size interval. It? will be noted that a particle may uiiSergo
minor breakage or chipping which is insufficient to ensure that all fragments
are smaller than the original lower size o f the size range. Consequently, a
mass balance o f a grinding process may be written as shown in Table 3-II.
Column 1 in the product refers to the products o f breakage o f the top size
range, in the feed, column 2 to the second size range, etc.. The elements in
the product have been written in the form p itj where i refers to the size range
in which the element occurs and j refers to the size o f the feed particle from
which it came.
The following points will be noted about this array o f elements which
represent the product.
(1)
The product size may be determined by summing the elements in suc
cessive rows o f the array.
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T A B L E 3-II
Mass balance for a size-reduction process
(2) >2 ft represents the total feed mass F. The particles falling in the residue,
i
that is, size range n + 1, may always be calculated for both feed and product
by subtracting the cumulative weight retained on size n from F. The feed
and product may be represented by arrays containing n by 1 elements.
The element p itj in the array representing products o f breakage may also
be written: p itj = X {j fj where X itj represents the mass fraction o f the par
ticles in the jth size range in the feed which fall in the ith size range in the
product. The product array may be re-written as shown in Table 3-III.
T A B L E 3-III
The produ ct from a size-reduction process expressed in terms o f the feed
If the feed and product size distributions are now written as n by 1 matrices
and the X array as an n by n matrix, the size-reduction process may be repre
sented by the matrix equation shown in Table 3-1V. Consequently, the sim
ple matrix equation:
p = X f
(3-1)
TABLE 3-IV
The development of the general matrix equation of breakage
32
than the discharge gap are retained within the jaws for further crushing. The
same type o f process occurs within gyratory and roll crushers and, as will be
seen, it is a particular feature o f the operation o f rod mills. There are indi
cations that it occurs in almost all type o f industrial grinding units though, in
some cases, the occurrence may be small.
(3-7)
gave a convenient form for the distribution o f particles after breakage. The
function B (x y) represents the proportion o f particles initially o f size y which
appear in size ranges smaller than x after breakage. The important concept
em bodied in this description o f particle breakage is that the distribution
obtained after breakage o f a mineral particle, relative to the initial size, is
independent o f the initial size o f the particle.
was obtained for sizes less than 590 micrometres where n took values from
0.90 to 0.95. At sizes above 590 micrometres, the test results showed
increasing deviations from the relative form . However, Kelsall attributes this
to other assumptions built into the m odel rather than indicating that the
breakage function is dependent on initial size.
The use o f tracers has also involved the removal o f a size fraction o f
natural feed to the mill and tagging this size fraction by irradiation, for
instance, Gaudin et al. (1951), M oore (1964), Bush (1967). The radioactive
fraction was then returned to the feed material and ground in a batch ball
mill. The radioactive content o f individual size fractions o f product material
was then used to follow the m ovement o f tracer. The advantage o f the use o f
the irradiated material is that the tracer material has the same breakage
properties as the host material, and consequently allows the grinding to take
place in a natural environment. The results o f the work o f these authors indi
cated that the breakage function B can be approximated by a step matrix,
that is, the breakage o f a rrffheral particle is independent o f original size.
However, it was found that because o f the nature o f the m odel used, the
breakage function B and the function defining the probability o f breakage S
(called the selection function), were not uniquely determined. Therefore,
many combinations o f B and S exist, each yielding a satisfactory prediction
o f ball mill performance.
The tw o definitions o f the breakage function given above differ only in
relation to defining when a mineral particle is broken. Kelsalls definition
considers a particle to be broken only if none o f it reappears in the parent
size range. Particles remaining in the parent size range are considered
unbroken. The Broadbent-Callcott definition allows the distribution o f pro
ducts o f breakage into the same size range as the parent material. For pur
poses o f the use o f the mathematical models o f particle breakage, this differ
ence in definition is n ot important.
I
35
The breakage function which has been discussed in this section refers to
crushing breakage. In some breakage processes, particles are broken by
abrasion and another type o f function must be considered. This will be dis
cussed in a later section.
3.2.5 Repetitive breakage
Most breakage machines operate so that sequential breakage events occur
while the particles are in the machines. If u events occur and each is denoted
by X, the products from consecutive events may be written:
where Xj is the breakage event occurring during the jth cycle. A cycle may
be related to some aspect o f operation o f the machine, for instance, in the
case o f a tumbling mill, it may be one revolution or a unit o f time. Incom
plete cycles may occur and may readily be handled mathematically. If the
events are identical, the process may be described by the equation:
3 .3 K IN E T IC M O D E L
where W(D) = weight o f particles o f size D, and k(Z)) = rate constant for size
D.
.
By defining the breakage function as the continuous function B(D, D 0)
36
and writing the mass balance for the size fraction W(D, t)6.D (where W(D, t)
represents the oyerall size distribution at time t), Loveday obtained the
integro-differential equation:
to describe the time rate o f change o f sizing o f the contents o f a batch mill.
In this description o f the breakage process, the functions k(.D), W(D), and
B(D, D 0) are all continuous distributions with respect to size D. Loveday
notes that the major problem associated with eq. 3-12 is the com plexity o f
its solution and derives an approximate analytic solution. Other solutions to
the batch grinding equation have also been publishedReid (1965), Kapur
(1971 ).
The main difficulty in the application o f the continuous distribution
m odel to practical problems in com m inution is that o f obtaining a satisfac
tory definition o f the continuous function for the distribution o f particle
sizes. Varying curvature in conventional plots o f sizing distributions for
crusher, rod mill and ball mill products, requires that a multiparameter distri
bution be employed*- Loveday has compared a number o f possible distri
butions and concludes that at least a three-parameter distribution is required.
-r> Because o f the problem o f determining suitable equations to represent
particle-size distribution, it has been convenient to use size-discretized forms
o f the grinding equations. When the batch grinding equation is discretized
with respect to size, the net rate o f change o f material x in a size range i may
be obtained by a simple mass balance and, for the case o f the batch mill, has
been given by Horst and Freeh (1970) as:
The kt- values in these equations are the first-order breakage rate constants
and the elements atj are the inter-size flow coefficients. Horst and Freeh note
that this equation may be written in matrix form as:
where the inter-size flow coefficients A and the rate constants K perform
similar functions to the breakage matrix B^ and selection matrix S in the
matrix model. X is the size distribution.
3 .4
C O N T IN U O U S F L O W S Y S T E M S
describe the- mixing and flow characteristics o f the system. Again, these
characteristics o f the system can be represented either by continuous distri
butions or by a discretized form . The continuous and discretized distribution
models are also sometimes referred to as distributed and lum ped param
eter models, respectively.
The description o f mixing and flow involves a description o f the longitudi
nal and transverse m ovement o f the pulp within the mill. The transverse
movement o f the pulp is usually considered relatively unimportant in a
description o f the flow characteristics since this movement has no direct
effect on the residence time o f the pulp in the mill. Residence time is
important and should be considered in conjunction with the axial movement
o f the pulp in the mill.
Descriptions o f the mixing characteristics can be obtained as a continuous
function o f mill length. However, it is generally convenient to consider a
more convenient lum ped -parameter form o f the model. In these models,
the mixing characteristics o f the system are usually approximated by the
com bination o f a pure delay and a certain number o f perfectly mixed seg
ments connected in series. Varying flow characteristics o f real systems can
then be reproduced by varying the number o f perfectly mixed segments
used, and by variation o f the degree o f mixing between adjacent segments.
Models o f this type have been used by Kelsall et al. (1968) and by Horst and
Freeh (1970). The latter authors also considered the possibility o f a sizedependent diffusion coefficien t to describe the transport o f material in the
axial direction o f the mill. In lumped-parameter_form this diffusion co e f
ficient is equivalent to a classification effect at the end o f each perfectly
mixed segment, and is synonym ous with the classification function used by
Callcott and Lynch (1964) in the rod mill model. If no classification exists,
then the diffusion coefficien t is independent o f size and becomes a single
value describing the mass rate o f discharge o f pulp from the segment.
3 .5
P E R F E C T M IX I N G M O D E L
38
The matrices A, R and D are the appearance, breakage-rate and dischargerate functions. They are essentially the breakage, selection and size-dependent
diffusion (or classification) functions, respectively, used by other authors.
The perfect mixing m odel is particularly appropriate for some comminution
operations and use o f a different set o f symbols for essentially the same
functions avoids confusion between models.
Whiten showed that the model is particularly easy to manipulate using
simple matrix methods for simulation and for the calculation o f the model
parameters. These may be obtained by examining the solution at steady state
which gives:
3 .6
O T H E R A P P R O A C H E S T O S IZ E -R E D U C T I O N M O D E L L IN G
and the expression for the rate function or selection function which is used
in grinding kinetics. Further studies in the com bination o f both the energy
size-reduction relationship and kinetic approach may produce a better overall
m odel since a knowledge o f the energy consumed in grinding is still very
important, particularly in mill design.
Empirical studies o f grinding-mill behaviour have also been carried out, for
example, by Kelly (1970). These studies generally utilise a statistical
approach which involves the collection o f a series o f data values planned
according to a factorial design. These data are then analysed using standard
regression and analysis o f variance techniques to determine those variables
which have a significant effect on performance criteria. The empirical
approach is o f limited value in m ost applications for two reasons. Firstly,
models developed on an empirical basis do not usually have very satisfactory
extrapolation behaviour.' This means, for example, that an empirical model
developed on a pilot-plant-scale mill may not generally be used to predict
the performance o f full-scale mills. Secondly, while an empirical model
developed on the full-scale mill could be validly applied, it is not generally
possible to implement a series o f experiments which constitute an exper
imental design. This is because large-scale ball mills are invariably operated in
closed circuit with :;ome form o f classifier, so that the feed conditions to the
mill are determined by classifier characteristics and are not available for inde
pendent manipulation.
40
N U M E R IC A L E X A M P L E S
The numerical exam ples given refer to the matrix m o d e l since this is the m odel which
is m o st co m m o n ly used in the remainder o f the text.
E x a m p le 3 -1 . In the equ ation for a breakage process p X f, the values o f the breakage
matrix X and the feed size distribution f are show n in Table 3 -V I.
T A B L E 3 -V I
Num erical values in the breakage m atrix and feed size distribution
W hat will be the size distribution o f the product fro m the process?
<0 2 .0
"
41
T A B L E 3 -V II
M ethod o f calculation for a process involving bo th selection and breakage
TABLE 3-IX
Product from a breakage process which includes classification
43
Equilibrium is reached w hen the mass discharged for increm ents o f time equals the mass
entering, that is, equals 1 0 0 units. T h e build-up o f ore in the coarse size fractions due to
internal classication m ay be calculated in this manner.
I f the ore becom es harder or softer, B will vary and change will occur in the mass
retained.
CHAPTER 4
Breakage within any com m inution unit may be described by the equation:
4 .1 C O N E C R U S H E R S
47
model and the internal flows between them are shown in Fig. 4-1. The vec
tors f, x and p give the mass flow rates in each size fraction. The lower tri
angular matrix, B, gives the relative distribution o f the particles after break
age and the diagonal matrix, C, gives the proportion o f particles in any given
size fraction which enter the breakage zone. Several more complicated
models may be proposed for the con e crusher. However, it is considered that
this model provides an adequate description o f cone-crusher behaviour and
that the data which are available or may be obtained from industrial oper
ations would not be sufficient to calculate parameters for a more com plex
model.
Mass balances at the nodes in Fig. 4-1 give the equations:
which relates the product from the cone crusher to the cone-crusher feed.
Adding eqs. 4-1 and 4-2 gives:
and this equation shows how the total breakage occurring in the crusher,
that is, f p, is related to the vector C -x.
This m odel will be discussed with reference to data obtained from a series
o f tests which were carried out in the crushing plant o f Mount Isa Mines
Limited, (MIM), the flowsheet o f which is given in Fig. 4-2. During these
tests, crusher performance was studied at different feed size distributions,
48
feed rates and closed side settings. These changes also produced changes in
the current drawn by the crusher and a relationship was developed to pre
dict the current fo r a wide range o f operating conditions. The values o f the
parameters were determined by least squares and spline regression techniques
so that the best fit between predicted and observed performance was obtained
over the range o f operating conditions studied.
Subsequent to the development o f the m odel, data have been obtained for
both the secondary and tertiary crushing operations at Bougainville Copper
Limited. The data obtained at Mount Isa Mines Limited indicated that it
was necessary for the m odel to incorporate separate distributions describing
the coarse and fine portions o f the crusher product. This has been confirmed
by the data collected at Bougainville Copper Limited and the same form o f
the model has been successfully used to describe these crushing operations.
4.1.2 The breakage matrix
The observed data on the cone crusher was best explained by proposing
that two modes o f breakage occur in a cone crusher. In the first breakage
m ode particles are caught between the opposing liners o f the crusher and
fracture catastrophically into a small number o f relatively large particles.
These particles may or may not re-enter the breakage zone o f the crusher
m odel. A step matrix Bj which gives the product size distribution relative
to the size o f the original particle was used to predict the products o f this
breakage m ode. It is calculated from the distribution:
49
where x' is a size such that a very significant portion o f the product which
is less than this size was produced by fine breakage. In the calculation, this
distribution is altered so that the material predicted above the size o f the
original particle appears after breakage at the original particle size. This
amount is generally small. The values calculated for the parameters in this
distribution for the MIM crusher are: x = 3.05 0.51 mm; v 1.25 0.14.
The total breakage matrix, B, may be calculated by adding the two com
ponent matrices as follow s:
It was found that the value o f a could be predicted from the closed side
setting o f the crusher:
Fig. 4 -3 . Probability C (s) o f a particle entering the breakage stage (see eq. 4 -1 0 ) .
The values o f the C matrix can be obtained as the mean values o f the
function C(s) in the appropriate size range, that is:
where st and si+1 are the lower and upper limits o f the size interval for the
zth size fraction.
The tw o parameters k L and k 2 were predicted for the MIM crusher by the
equations:
where q is the fraction plus 25.4 mm in the feed. The effect o f feed tonnage
on k2 is shown in Fig. 4-4. The relation for k x is as would be expected. The
relation between k2 and closed side setting is reasonable and the remaining
terms in the equation appear, to relate to the ease o f flow through the
crusher, that is, large particles and low tonnages flow through the crusher
m ore rapidly.
4.1.4 Crusher current
It has been seen (eq. 4-5) that the total breakage occurring in the crusher
is related to the vector C - x . Now this vector contains no material which
does not enter the breakage stage o f the crusher, and the current drawn by
' the crusher has been calculated using this vector. A parameter, a, which is
dependent upon the size distribution o f the feed to the crusher, is calculated
as follow s:
where , is the zth element o f C x, and sh s{+1 are the lower and upper limits
o f the zth size fraction. For the fine-size fractions tt equals zero. The crusher
current, A , is then predicted b y :