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KEMAMAN TERENGGANU
LABORATORY REPORT
DPV 1012 CHEMISTRY
OBJECTIVE
-To identify saturated and unsaturated hydrocarbons using properties and reactions.
PROCEDURE
1.Dry the filter disk in the oven at 103C to 105C for 1 hour,cool in a desiccators and weigh.
2.Assemble filtering apparatus and filter and begin suction.Wet the filter with a small volume
of distilled water to seat it.
3.Pipette 50 mL of water sample (mixed to ensure homogeneity) onto centre of filter disk in a
Buchner flask, using gentle suction (under vacuum).
4.Wash filter with three successive 10 mL volumes of distrille water, allowing complete
drainage between washing, and continue suction for about 3 min after filteration is complete.
5.Carefully remove filter from filteration apparatus and transfer to aluminium weighing
dish/crucible dish as a support.
6.Dry at least 1 hour at 103C to 105C in an oven, cool in a dessicator to balance
temperature, and weigh.
7.Repeat the cycle of drying, cooling, dessicating, and weighing until a constant weight is
obtained.
RESULT
Sample
(different
sources)
Plain water
Weight of filter,
mg
Net weight, mg
TSS, mg/L
776.3
Weight of filter +
dried residue,
mg
778.1
1.8
36
Pond water
771.2
875.0
103.8
2076
Drain water
771.5
779.8
8.3
166
Plain water
Drain water
Pond water
DISCUSSION
1) Calculate the Total Suspended Solids (TSS) in the water and wastewater
samples using the following equation:
Mg TSS/L = (A-B)1000
Sample volume, Ml
where;
A=weight of filter+dried residue,mg
B=weight of filter
Soil Erosion
Soil erosion is caused by disturbance of a land surface. Soil erosion can be
caused by Building and Road Construction, Forest Fires,
Logging, and Mining. The eroded soil particles can be carried by
stormwater to surface water. This will increase the TSS of the water body.