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INTRODUCTION
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METHODOLOGY
Materials
The experiment made use of two setups namely the sublimation set-up and the
melting point set-up.
Methods
Sublimation set-up
Five (5) grams of impure benzoic
acid was placed in an evaporating dish and
covered with perforated filter paper. An
inverted pre-weighed watch glass was
placed on top and sealed with masking tape,
carefully making sure that no spaces were
left unsealed. A moistened tissue paper was
placed on top of the watch glass. The set-up
was placed on a hot plate and allowed to
heat for ten to fifteen (10-15) minutes until
most of the sample has vaporized and was
then cooled. The pre-weighed watch glass
was inverted and the sample was collected
and weighed. This allowed the percentage
yield to be calculated.
Initial
Temperature
124C
Final
Temperature
128C
104C
110C
Figure 2. Sublimate
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% recovery =
Weight of
pure
from
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x 100
Weight of impure
% recovery= 1.1 g
x 100
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5g
% recovery= 22%
This indicates that the percentage of
pure benzoic acid in 5 grams of impure
benzoic acid is 22%.
In conclusion, the sublimate
collected was not pure since its melting
point (110C ) was too far from the pure
benzoic acid (122.5C).
REFERENCES
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[3]
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