Method: Pelat Ins 2015

Page

Date: 12/21/2015 3:52:13 PM

====================================================================================================

Sequence No.: 1
Sample ID: Calib Blank 1
Analyst:
Logged In Analyst (Original) : HP
Initial Sample Wt:
Dilution:

Autosampler Location:
Date Collected: 12/21/2015 12:45:46 PM
Data Type: Reprocessed on 12/21/2015 3:52:06 PM
Initial Sample Vol:
Sample Prep Vol:

----------------------------------------------------------------------------------------------------

Replicate Data: Calib Blank 1

Repl# Analyte
1
1
1
1
1
1
1
1
1
1
1
1
1

Cu 324.752
Cr 283.563
Fe 259.939
K 766.490
Cd 228.802
Pb 283.306
Ca 393.366
Na 588.995
Mg 279.553
Ni 341.476
Mn 257.610
Zn 213.857
Co 228.616

Net
Intensity

Corrected
Intensity

2516.7
1604.0
412.9
68690.7
131.5
299.5
409940.5
-25164.6
90896.4
-99.1
325.6
3364.2
3.7

2516.7
1604.0
412.9
68690.7
131.5
299.5
409940.5
-25164.6
90896.4
-99.1
325.6
3364.2
3.7

Calib.
Conc. Units
[0.00]
[0.00]
[0.00]
[0.00]
[0.00]
[0.00]
[0.00]
[0.00]
[0.00]
[0.00]
[0.00]
[0.00]
[0.00]

mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L

Analysis
Time
12:46:55
12:46:55
12:46:55
12:46:49
12:46:55
12:46:55
12:46:49
12:46:49
12:46:49
12:46:55
12:46:55
12:46:55
12:46:55

PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM

----------------------------------------------------------------------------------------------------

Mean Data: Calib Blank 1

Mean Corrected
Analyte
Intensity
Cu 324.752
Cr 283.563
Fe 259.939
K 766.490
Cd 228.802
Pb 283.306
Ca 393.366
Na 588.995
Mg 279.553
Ni 341.476
Mn 257.610
Zn 213.857
Co 228.616

Std.Dev.

2516.7
1604.0
412.9
68690.7
131.5
299.5
409940.5
-25164.6
90896.4
-99.1
325.6
3364.2
3.7

RSD

Calib
Conc. Units
[0.00]
[0.00]
[0.00]
[0.00]
[0.00]
[0.00]
[0.00]
[0.00]
[0.00]
[0.00]
[0.00]
[0.00]
[0.00]

mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L

====================================================================================================

Sequence No.: 2
Sample ID: Std 1a
Analyst:
Logged In Analyst (Original) : HP
Initial Sample Wt:
Dilution:

Autosampler Location:
Date Collected: 12/21/2015 12:51:09 PM
Data Type: Reprocessed on 12/21/2015 3:52:06 PM
Initial Sample Vol:
Sample Prep Vol:

----------------------------------------------------------------------------------------------------

Replicate Data: Std 1a

Repl# Analyte
1
1
1
1
1
1
1
1
1
1

Cu 324.752
Cr 283.563
Fe 259.939
K 766.490
Cd 228.802
Pb 283.306
Ca 393.366
Na 588.995
Mg 279.553
Ni 341.476

Net
Intensity

Corrected
Intensity

2820636.4
1495852.2
976.3
165323.3
161.9
-136.4
6884743.7
376896.6
543163.4
19.9

2818119.7
1494248.1
563.4
96632.6
30.4
-435.9
6474803.1
402061.2
452266.9
118.9

Calib.
Conc. Units
[10]
[10]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]

mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L

Analysis
Time
12:51:24
12:51:24
12:51:30
12:51:24
12:51:30
12:51:30
12:51:23
12:51:24
12:51:24
12:51:30

PM
PM
PM
PM
PM
PM
PM
PM
PM
PM

Method: Pelat Ins 2015

1
1
2
2
2
2
2
2
2
2
2
2
2
2

Mn 257.610
Zn 213.857
Cu 324.752
Cr 283.563
Fe 259.939
K 766.490
Cd 228.802
Pb 283.306
Ca 393.366
Na 588.995
Mg 279.553
Ni 341.476
Mn 257.610
Zn 213.857

Page
4426.2
10703.8
2848397.9
1510808.8
1047.4
167193.4
152.2
-129.3
6751088.2
387306.5
542454.1
-48.8
4260.8
10645.3

4100.6
7339.7
2845881.2
1509204.8
634.5
98502.7
20.6
-428.8
6341147.7
412471.1
451557.7
50.2
3935.2
7281.2

Date: 12/21/2015 3:52:13 PM

[0]
[0]
[10]
[10]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]

mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L

12:51:30
12:51:30
12:51:32
12:51:32
12:51:38
12:51:32
12:51:38
12:51:38
12:51:31
12:51:32
12:51:32
12:51:38
12:51:38
12:51:38

PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM

----------------------------------------------------------------------------------------------------

Mean Data: Std 1a

Mean Corrected
Intensity

Analyte
Cu 324.752
Standard
Cr 283.563
Standard
Fe 259.939
Standard
K 766.490
Standard
Cd 228.802
Standard
Pb 283.306
Standard
Ca 393.366
Standard
Na 588.995
Standard
Mg 279.553
Standard
Ni 341.476
Standard
Mn 257.610
Standard
Zn 213.857
Standard

Std.Dev.

RSD

2832000.4
19630.33
0.69%
intensity and concentration values are not
1501726.5
10575.95
0.70%
intensity and concentration values are not
599.0
50.28
8.39%
intensity and concentration values are not
97567.7
1322.38
1.36%
intensity and concentration values are not
25.5
6.89 27.03%
intensity and concentration values are not
-432.4
5.05
1.17%
intensity and concentration values are not
6407975.4
94508.69
1.47%
intensity and concentration values are not
407266.1
7360.92
1.81%
intensity and concentration values are not
451912.3
501.52
0.11%
intensity and concentration values are not
84.6
48.57 57.43%
intensity and concentration values are not
4017.9
116.95
2.91%
intensity and concentration values are not
7310.4
41.38
0.57%
intensity and concentration values are not

Calib
Conc. Units
[10] mg/L
in the same order.
[10] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.

====================================================================================================

Sequence No.: 3
Sample ID: Std 1b
Analyst:
Logged In Analyst (Original) : HP
Initial Sample Wt:
Dilution:

Autosampler Location:
Date Collected: 12/21/2015 12:52:32 PM
Data Type: Reprocessed on 12/21/2015 3:52:06 PM
Initial Sample Vol:
Sample Prep Vol:

----------------------------------------------------------------------------------------------------

Replicate Data: Std 1b

Repl# Analyte
1
1
1
1
1
1
1
1
1
1
1

Cu 324.752
Cr 283.563
Fe 259.939
K 766.490
Cd 228.802
Pb 283.306
Ca 393.366
Na 588.995
Mg 279.553
Ni 341.476
Mn 257.610

Net
Intensity

Corrected
Intensity

8428234.9
4636313.3
2472.6
308255.1
125.2
-1015.5
18986147.9
934087.4
1689741.8
-13.1
99716.7

8425718.2
4634709.2
2059.7
239564.4
-6.3
-1315.0
18576207.4
959252.0
1598845.4
85.9
99391.1

Calib.
Conc. Units
[30]
[30]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]

mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L

Analysis
Time
12:52:40
12:52:41
12:52:49
12:52:43
12:52:49
12:52:49
12:52:40
12:52:41
12:52:41
12:52:49
12:52:43

PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM

Method: Pelat Ins 2015

1
2
2
2
2
2
2
2
2
2
2
2
2

Zn 213.857
Cu 324.752
Cr 283.563
Fe 259.939
K 766.490
Cd 228.802
Pb 283.306
Ca 393.366
Na 588.995
Mg 279.553
Ni 341.476
Mn 257.610
Zn 213.857

Page
39632.9
8546047.3
4614877.5
2052.9
286545.3
109.8
-930.1
19137450.9
930926.9
1681272.0
-65.4
98494.1
39712.5

36268.7
8543530.6
4613273.5
1640.1
217854.6
-21.7
-1229.6
18727510.4
956091.5
1590375.6
33.7
98168.5
36348.4

Date: 12/21/2015 3:52:13 PM

[0]
[30]
[30]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]

mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L

12:52:49
12:52:51
12:52:52
12:52:59
12:52:53
12:52:59
12:52:59
12:52:51
12:52:52
12:52:52
12:52:59
12:52:53
12:52:59

PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM

----------------------------------------------------------------------------------------------------

Mean Data: Std 1b

Mean Corrected
Intensity

Analyte
Cu 324.752
Standard
Cr 283.563
Standard
Fe 259.939
Standard
K 766.490
Standard
Cd 228.802
Standard
Pb 283.306
Standard
Ca 393.366
Standard
Na 588.995
Standard
Mg 279.553
Standard
Ni 341.476
Standard
Mn 257.610
Standard
Zn 213.857
Standard

Std.Dev.

RSD

8484624.4
83305.96
0.98%
intensity and concentration values are not
4623991.4
15157.35
0.33%
intensity and concentration values are not
1849.9
296.76 16.04%
intensity and concentration values are not
228709.5
15351.17
6.71%
intensity and concentration values are not
-14.0
10.93 77.92%
intensity and concentration values are not
-1272.3
60.41
4.75%
intensity and concentration values are not
18651858.9
106987.41
0.57%
intensity and concentration values are not
957671.8
2234.76
0.23%
intensity and concentration values are not
1594610.5
5989.05
0.38%
intensity and concentration values are not
59.8
36.98 61.84%
intensity and concentration values are not
98779.8
864.51
0.88%
intensity and concentration values are not
36308.5
56.29
0.16%
intensity and concentration values are not

Calib
Conc. Units
[30] mg/L
in the same order.
[30] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.

====================================================================================================

Sequence No.: 4
Sample ID: Std 1c
Analyst:
Logged In Analyst (Original) : HP
Initial Sample Wt:
Dilution:

Autosampler Location:
Date Collected: 12/21/2015 12:54:00 PM
Data Type: Reprocessed on 12/21/2015 3:52:06 PM
Initial Sample Vol:
Sample Prep Vol:

----------------------------------------------------------------------------------------------------

Replicate Data: Std 1c

Repl# Analyte
1
1
1
1
1
1
1
1
1
1
1
1

Cu 324.752
Cr 283.563
Fe 259.939
K 766.490
Cd 228.802
Pb 283.306
Ca 393.366
Na 588.995
Mg 279.553
Ni 341.476
Mn 257.610
Zn 213.857

Net
Intensity

Corrected
Intensity

14330150.0
7484182.7
4561.0
200395.5
165.4
-1848.6
8331728.8
527026.8
606982.0
-117.9
15931.6
29710.2

14327633.3
7482578.7
4148.1
131704.8
33.9
-2148.1
7921788.2
552191.4
516085.6
-18.8
15606.0
26346.0

Calib.
Conc. Units
[50]
[50]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]

mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L

Analysis
Time
12:54:07
12:54:07
12:54:14
12:54:08
12:54:14
12:54:14
12:54:07
12:54:08
12:54:08
12:54:14
12:54:14
12:54:14

PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM

Method: Pelat Ins 2015

2
2
2
2
2
2
2
2
2
2
2
2

Cu 324.752
Cr 283.563
Fe 259.939
K 766.490
Cd 228.802
Pb 283.306
Ca 393.366
Na 588.995
Mg 279.553
Ni 341.476
Mn 257.610
Zn 213.857

Page
14370731.0
7497194.7
4627.2
203130.8
146.0
-1840.3
8453751.6
553908.4
608703.3
-12.3
15948.9
29785.9

14368214.3
7495590.7
4214.3
134440.1
14.5
-2139.8
8043811.1
579073.0
517806.9
86.8
15623.3
26421.7

Date: 12/21/2015 3:52:13 PM

[50]
[50]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]

mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L

12:54:15
12:54:15
12:54:22
12:54:16
12:54:22
12:54:22
12:54:15
12:54:16
12:54:16
12:54:22
12:54:22
12:54:22

PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM

----------------------------------------------------------------------------------------------------

Mean Data: Std 1c

Mean Corrected
Intensity

Analyte
Cu 324.752
Standard
Cr 283.563
Standard
Fe 259.939
Standard
K 766.490
Standard
Cd 228.802
Standard
Pb 283.306
Standard
Ca 393.366
Standard
Na 588.995
Standard
Mg 279.553
Standard
Ni 341.476
Standard
Mn 257.610
Standard
Zn 213.857
Standard

Std.Dev.

RSD

14347923.8
28695.09
0.20%
intensity and concentration values are not
7489084.7
9200.90
0.12%
intensity and concentration values are not
4181.2
46.78
1.12%
intensity and concentration values are not
133072.4
1934.15
1.45%
intensity and concentration values are not
24.2
13.70 56.66%
intensity and concentration values are not
-2144.0
5.88
0.27%
intensity and concentration values are not
7982799.7
86283.18
1.08%
intensity and concentration values are not
565632.2
19008.15
3.36%
intensity and concentration values are not
516946.2
1217.17
0.24%
intensity and concentration values are not
34.0
74.67 219.90%
intensity and concentration values are not
15614.6
12.24
0.08%
intensity and concentration values are not
26383.9
53.51
0.20%
intensity and concentration values are not

Calib
Conc. Units
[50] mg/L
in the same order.
[50] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.

====================================================================================================

Sequence No.: 5
Sample ID: Std 2a
Analyst:
Logged In Analyst (Original) : HP
Initial Sample Wt:
Dilution:

Autosampler Location:
Date Collected: 12/21/2015 12:56:25 PM
Data Type: Reprocessed on 12/21/2015 3:52:07 PM
Initial Sample Vol:
Sample Prep Vol:

----------------------------------------------------------------------------------------------------

Replicate Data: Std 2a

Repl# Analyte
1
1
1
1
1
1
1
1
1
1
1
1
2

Cu 324.752
Cr 283.563
Fe 259.939
K 766.490
Cd 228.802
Pb 283.306
Ca 393.366
Na 588.995
Mg 279.553
Ni 341.476
Mn 257.610
Zn 213.857
Cu 324.752

Net
Intensity

Corrected
Intensity

44426.4
3122271.7
3621416.4
111479.5
137.6
-389.6
9955146.9
465163.4
694735.6
-15.5
56146.9
9961.3
27096.2

41909.7
3120667.7
3621003.6
42788.8
6.0
-689.1
9545206.3
490328.0
603839.2
83.5
55821.2
6597.2
24579.4

Calib.
Conc. Units
[0]
[20]
[20]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]

mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L

Analysis
Time
12:56:40
12:56:40
12:56:40
12:56:40
12:56:46
12:56:46
12:56:39
12:56:40
12:56:40
12:56:46
12:56:40
12:56:46
12:56:49

PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM

Method: Pelat Ins 2015

2
2
2
2
2
2
2
2
2
2
2

Cr 283.563
Fe 259.939
K 766.490
Cd 228.802
Pb 283.306
Ca 393.366
Na 588.995
Mg 279.553
Ni 341.476
Mn 257.610
Zn 213.857

Page
3106863.3
3766926.4
114844.8
192.8
-402.7
9893078.0
441078.8
686970.2
18.9
55686.3
9977.4

3105259.2
3766513.6
46154.1
61.2
-702.2
9483137.4
466243.4
596073.8
117.9
55360.7
6613.2

Date: 12/21/2015 3:52:13 PM

[20]
[20]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]

mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L

12:56:49
12:56:49
12:56:49
12:56:55
12:56:55
12:56:48
12:56:49
12:56:49
12:56:55
12:56:49
12:56:55

PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM

----------------------------------------------------------------------------------------------------

Mean Data: Std 2a

Mean Corrected
Intensity

Analyte
Cu 324.752
Standard
Cr 283.563
Standard
Fe 259.939
Standard
K 766.490
Standard
Cd 228.802
Standard
Pb 283.306
Standard
Ca 393.366
Standard
Na 588.995
Standard
Mg 279.553
Standard
Ni 341.476
Standard
Mn 257.610
Standard
Zn 213.857
Standard

Std.Dev.

RSD

33244.6
12254.34 36.86%
intensity and concentration values are not
3112963.4
10895.40
0.35%
intensity and concentration values are not
3693758.6
102891.11
2.79%
intensity and concentration values are not
44471.5
2379.60
5.35%
intensity and concentration values are not
33.6
39.03 116.00%
intensity and concentration values are not
-695.6
9.25
1.33%
intensity and concentration values are not
9514171.9
43889.35
0.46%
intensity and concentration values are not
478285.7
17030.41
3.56%
intensity and concentration values are not
599956.5
5490.96
0.92%
intensity and concentration values are not
100.7
24.35 24.18%
intensity and concentration values are not
55590.9
325.66
0.59%
intensity and concentration values are not
6605.2
11.32
0.17%
intensity and concentration values are not

Calib
Conc. Units
[0] mg/L
in the same order.
[20] mg/L
in the same order.
[20] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.

====================================================================================================

Sequence No.: 6
Sample ID: Std 2b
Analyst:
Logged In Analyst (Original) : HP
Initial Sample Wt:
Dilution:

Autosampler Location:
Date Collected: 12/21/2015 12:57:45 PM
Data Type: Reprocessed on 12/21/2015 3:52:07 PM
Initial Sample Vol:
Sample Prep Vol:

----------------------------------------------------------------------------------------------------

Replicate Data: Std 2b

Repl# Analyte
1
1
1
1
1
1
1
1
1
1
1
1
2
2

Cu 324.752
Cr 283.563
Fe 259.939
K 766.490
Cd 228.802
Pb 283.306
Ca 393.366
Na 588.995
Mg 279.553
Ni 341.476
Mn 257.610
Zn 213.857
Cu 324.752
Cr 283.563

Net
Intensity

Corrected
Intensity

16382.1
5999016.3
7618860.3
126754.8
213.0
-1113.9
11243435.1
506692.1
900065.1
-69.4
1941.6
13591.6
9967.2
6046425.7

13865.4
5997412.3
7618447.4
58064.1
81.5
-1413.4
10833494.6
531856.7
809168.6
29.7
1616.0
10227.4
7450.5
6044821.6

Calib.
Conc. Units
[0]
[40]
[40]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[40]

mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L

Analysis
Time
12:58:02
12:57:55
12:57:55
12:57:56
12:58:02
12:58:02
12:57:54
12:57:55
12:57:55
12:58:02
12:57:56
12:58:02
12:58:12
12:58:05

PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM

Method: Pelat Ins 2015

2
2
2
2
2
2
2
2
2
2

Fe 259.939
K 766.490
Cd 228.802
Pb 283.306
Ca 393.366
Na 588.995
Mg 279.553
Ni 341.476
Mn 257.610
Zn 213.857

Page
7881738.1
151207.3
180.8
-1136.9
11181073.7
500367.2
903829.9
-95.8
1885.4
12749.0

7881325.2
82516.6
49.2
-1436.4
10771133.2
525531.8
812933.5
3.3
1559.7
9384.8

Date: 12/21/2015 3:52:13 PM

[40]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]

mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L

12:58:05
12:58:06
12:58:12
12:58:12
12:58:04
12:58:05
12:58:05
12:58:12
12:58:06
12:58:12

PM
PM
PM
PM
PM
PM
PM
PM
PM
PM

----------------------------------------------------------------------------------------------------

Mean Data: Std 2b

Mean Corrected
Intensity

Analyte
Cu 324.752
Standard
Cr 283.563
Standard
Fe 259.939
Standard
K 766.490
Standard
Cd 228.802
Standard
Pb 283.306
Standard
Ca 393.366
Standard
Na 588.995
Standard
Mg 279.553
Standard
Ni 341.476
Standard
Mn 257.610
Standard
Zn 213.857
Standard

Std.Dev.

RSD

10658.0
4536.00 42.56%
intensity and concentration values are not
6021117.0
33523.50
0.56%
intensity and concentration values are not
7749886.3
185882.64
2.40%
intensity and concentration values are not
70290.3
17290.52 24.60%
intensity and concentration values are not
65.4
22.82 34.90%
intensity and concentration values are not
-1424.9
16.26
1.14%
intensity and concentration values are not
10802313.9
44096.16
0.41%
intensity and concentration values are not
528694.2
4472.38
0.85%
intensity and concentration values are not
811051.1
2662.14
0.33%
intensity and concentration values are not
16.5
18.70 113.42%
intensity and concentration values are not
1587.8
39.77
2.50%
intensity and concentration values are not
9806.1
595.81
6.08%
intensity and concentration values are not

Calib
Conc. Units
[0] mg/L
in the same order.
[40] mg/L
in the same order.
[40] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.

====================================================================================================

Sequence No.: 7
Sample ID: Std 2c
Analyst:
Logged In Analyst (Original) : HP
Initial Sample Wt:
Dilution:

Autosampler Location:
Date Collected: 12/21/2015 12:58:57 PM
Data Type: Reprocessed on 12/21/2015 3:52:07 PM
Initial Sample Vol:
Sample Prep Vol:

----------------------------------------------------------------------------------------------------

Replicate Data: Std 2c

Repl# Analyte
1
1
1
1
1
1
1
1
1
1
1
1
2
2
2

Cu 324.752
Cr 283.563
Fe 259.939
K 766.490
Cd 228.802
Pb 283.306
Ca 393.366
Na 588.995
Mg 279.553
Ni 341.476
Mn 257.610
Zn 213.857
Cu 324.752
Cr 283.563
Fe 259.939

Net
Intensity

Corrected
Intensity

9182.0
8633016.1
11096727.7
150456.1
218.1
-1867.1
47047075.1
525017.0
984215.3
-66.3
2161.7
18075.3
8160.1
8687973.5
11333690.3

6665.3
8631412.1
11096314.8
81765.4
86.6
-2166.6
46637134.6
550181.6
893318.9
32.7
1836.1
14711.1
5643.4
8686369.5
11333277.4

Calib.
Conc. Units
[0]
[60]
[60]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[60]
[60]

mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L

Analysis
Time
12:59:13
12:59:06
12:59:06
12:59:07
12:59:13
12:59:13
12:59:06
12:59:07
12:59:07
12:59:13
12:59:07
12:59:13
12:59:24
12:59:16
12:59:16

PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM

Method: Pelat Ins 2015

2
2
2
2
2
2
2
2
2

K 766.490
Cd 228.802
Pb 283.306
Ca 393.366
Na 588.995
Mg 279.553
Ni 341.476
Mn 257.610
Zn 213.857

Page
156778.2
232.5
-1704.8
47352163.3
563459.1
994455.4
-107.6
2254.9
18172.2

88087.5
100.9
-2004.3
46942222.8
588623.7
903559.0
-8.6
1929.3
14808.0

Date: 12/21/2015 3:52:13 PM

[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]

mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L

12:59:18
12:59:24
12:59:24
12:59:16
12:59:18
12:59:18
12:59:24
12:59:18
12:59:24

PM
PM
PM
PM
PM
PM
PM
PM
PM

----------------------------------------------------------------------------------------------------

Mean Data: Std 2c

Mean Corrected
Intensity

Analyte
Cu 324.752
Standard
Cr 283.563
Standard
Fe 259.939
Standard
K 766.490
Standard
Cd 228.802
Standard
Pb 283.306
Standard
Ca 393.366
Standard
Na 588.995
Standard
Mg 279.553
Standard
Ni 341.476
Standard
Mn 257.610
Standard
Zn 213.857
Standard

Std.Dev.

RSD

6154.3
722.59 11.74%
intensity and concentration values are not
8658890.8
38860.71
0.45%
intensity and concentration values are not
11214796.1
167557.86
1.49%
intensity and concentration values are not
84926.5
4470.37
5.26%
intensity and concentration values are not
93.8
10.13 10.81%
intensity and concentration values are not
-2085.5
114.77
5.50%
intensity and concentration values are not
46789678.7
215729.93
0.46%
intensity and concentration values are not
569402.7
27182.68
4.77%
intensity and concentration values are not
898438.9
7240.84
0.81%
intensity and concentration values are not
12.1
29.19 241.46%
intensity and concentration values are not
1882.7
65.89
3.50%
intensity and concentration values are not
14759.6
68.51
0.46%
intensity and concentration values are not

Calib
Conc. Units
[0] mg/L
in the same order.
[60] mg/L
in the same order.
[60] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.

====================================================================================================

Sequence No.: 8
Sample ID: Std 3a
Analyst:
Logged In Analyst (Original) : HP
Initial Sample Wt:
Dilution:

Autosampler Location:
Date Collected: 12/21/2015 1:01:13 PM
Data Type: Reprocessed on 12/21/2015 3:52:07 PM
Initial Sample Vol:
Sample Prep Vol:

----------------------------------------------------------------------------------------------------

Replicate Data: Std 3a

Repl# Analyte
1
1
1
1
1
1
1
1
1
1
1
1
2
2
2
2

Cu 324.752
Cr 283.563
Fe 259.939
K 766.490
Cd 228.802
Pb 283.306
Ca 393.366
Na 588.995
Mg 279.553
Ni 341.476
Mn 257.610
Zn 213.857
Cu 324.752
Cr 283.563
Fe 259.939
K 766.490

Net
Intensity

Corrected
Intensity

6091.6
5616.1
880983.2
3120526.2
143.6
374.4
34399921.7
1707861.7
1456754.7
142.5
4405.3
10119.9
5662.6
4808.7
878915.3
3199870.6

3574.8
4012.0
880570.3
3051835.5
12.1
74.9
33989981.2
1733026.3
1365858.2
241.5
4079.7
6755.7
3145.9
3204.7
878502.4
3131179.9

Calib.
Conc. Units
[0]
[0]
[10]
[10]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[10]
[10]

mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L

Analysis
Time
1:01:28
1:01:28
1:01:22
1:01:22
1:01:28
1:01:28
1:01:21
1:01:22
1:01:22
1:01:28
1:01:28
1:01:28
1:01:38
1:01:38
1:01:32
1:01:32

PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM

Method: Pelat Ins 2015

2
2
2
2
2
2
2
2

Cd
Pb
Ca
Na
Mg
Ni
Mn
Zn

228.802
283.306
393.366
588.995
279.553
341.476
257.610
213.857

Page
161.8
395.6
34059730.2
1714024.4
1450021.6
78.7
4381.5
10407.7

30.3
96.1
33649789.6
1739189.0
1359125.2
177.7
4055.8
7043.6

Date: 12/21/2015 3:52:13 PM

[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]

mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L

1:01:38
1:01:38
1:01:30
1:01:32
1:01:32
1:01:38
1:01:38
1:01:38

PM
PM
PM
PM
PM
PM
PM
PM

----------------------------------------------------------------------------------------------------

Mean Data: Std 3a

Mean Corrected
Intensity

Analyte
Cu 324.752
Standard
Cr 283.563
Standard
Fe 259.939
Standard
K 766.490
Standard
Cd 228.802
Standard
Pb 283.306
Standard
Ca 393.366
Standard
Na 588.995
Standard
Mg 279.553
Standard
Ni 341.476
Standard
Mn 257.610
Standard
Zn 213.857
Standard

Std.Dev.

RSD

3360.4
303.30
9.03%
intensity and concentration values are not
3608.4
570.86 15.82%
intensity and concentration values are not
879536.4
1462.18
0.17%
intensity and concentration values are not
3091507.7
56104.97
1.81%
intensity and concentration values are not
21.2
12.84 60.61%
intensity and concentration values are not
85.5
14.95 17.49%
intensity and concentration values are not
33819885.4
240551.76
0.71%
intensity and concentration values are not
1736107.6
4357.67
0.25%
intensity and concentration values are not
1362491.7
4761.00
0.35%
intensity and concentration values are not
209.6
45.14 21.53%
intensity and concentration values are not
4067.8
16.89
0.42%
intensity and concentration values are not
6899.6
203.56
2.95%
intensity and concentration values are not

Calib
Conc. Units
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[10] mg/L
in the same order.
[10] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.

====================================================================================================

Sequence No.: 9
Sample ID: Std 3b
Analyst:
Logged In Analyst (Original) : HP
Initial Sample Wt:
Dilution:

Autosampler Location:
Date Collected: 12/21/2015 1:02:34 PM
Data Type: Reprocessed on 12/21/2015 3:52:07 PM
Initial Sample Vol:
Sample Prep Vol:

----------------------------------------------------------------------------------------------------

Replicate Data: Std 3b

Net
Intensity

Corrected
Intensity

Cu 324.752
6436.2
Cr 283.563
9299.3
Fe 259.939
4156489.4
K 766.490
8755667.0
Cd 228.802
190.0
Pb 283.306
529.5
Ca 393.366
Saturated3
Saturated in preshot (code 3)
1
Na 588.995
2316670.7
1
Mg 279.553
2210594.1
1
Ni 341.476
26.3
1
Mn 257.610
11105.8
1
Zn 213.857
10801.1
2
Cu 324.752
5845.3
2
Cr 283.563
8931.9
2
Fe 259.939
4260381.2
2
K 766.490
9268187.1

3919.4
7695.2
4156076.5
8686976.3
58.5
230.0
Saturated3

[0]
[0]
[30]
[30]
[0]
[0]

mg/L
mg/L
mg/L
mg/L
mg/L
mg/L

1:02:49
1:02:49
1:02:42
1:02:41
1:02:49
1:02:49
1:02:49

PM
PM
PM
PM
PM
PM
PM

2341835.3
2119697.7
125.3
10780.1
7437.0
3328.5
7327.8
4259968.4
9199496.4

[0]
[0]
[0]
[0]
[0]
[0]
[0]
[30]
[30]

mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L

1:02:42
1:02:42
1:02:49
1:02:43
1:02:49
1:02:59
1:02:59
1:02:52
1:02:51

PM
PM
PM
PM
PM
PM
PM
PM
PM

Repl# Analyte
1
1
1
1
1
1
1

Calib.
Conc. Units

Analysis
Time

Method: Pelat Ins 2015

Page

2
2
2

Cd 228.802
180.6
Pb 283.306
580.4
Ca 393.366
Saturated3
Saturated in preshot (code 3)
2
Na 588.995
2348847.1
2
Mg 279.553
2199611.4
2
Ni 341.476
-38.1
2
Mn 257.610
11257.8
2
Zn 213.857
11027.7

49.0
280.9
Saturated3
2374011.7
2108715.0
61.0
10932.1
7663.5

Date: 12/21/2015 3:52:13 PM

[0] mg/L
[0] mg/L

1:02:59 PM
1:02:59 PM
1:02:59 PM

[0]
[0]
[0]
[0]
[0]

1:02:52
1:02:52
1:02:59
1:02:53
1:02:59

mg/L
mg/L
mg/L
mg/L
mg/L

PM
PM
PM
PM
PM

----------------------------------------------------------------------------------------------------

Mean Data: Std 3b

Mean Corrected
Intensity

Analyte
Cu 324.752
Standard
Cr 283.563
Standard
Fe 259.939
Standard
K 766.490
Standard
Cd 228.802
Standard
Pb 283.306
Standard
Ca 393.366
Na 588.995
Standard
Mg 279.553
Standard
Ni 341.476
Standard
Mn 257.610
Standard
Zn 213.857
Standard

Std.Dev.

RSD

3624.0
417.82 11.53%
intensity and concentration values are not
7511.5
259.81
3.46%
intensity and concentration values are not
4208022.4
73462.62
1.75%
intensity and concentration values are not
8943236.3
362406.41
4.05%
intensity and concentration values are not
53.8
6.67 12.41%
intensity and concentration values are not
255.5
36.00 14.09%
intensity and concentration values are not
Saturated3
2357923.5
22752.15
0.96%
intensity and concentration values are not
2114206.3
7765.95
0.37%
intensity and concentration values are not
93.2
45.50 48.85%
intensity and concentration values are not
10856.1
107.50
0.99%
intensity and concentration values are not
7550.2
160.20
2.12%
intensity and concentration values are not

Calib
Conc. Units
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[30] mg/L
in the same order.
[30] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.

====================================================================================================

Sequence No.: 10
Sample ID: Std 3c
Analyst:
Logged In Analyst (Original) : HP
Initial Sample Wt:
Dilution:

Autosampler Location:
Date Collected: 12/21/2015 1:03:48 PM
Data Type: Reprocessed on 12/21/2015 3:52:07 PM
Initial Sample Vol:
Sample Prep Vol:

----------------------------------------------------------------------------------------------------

Replicate Data: Std 3c

Repl# Analyte
1
1
1
1
1
1
1
1
1
1
1
1
2
2
2
2
2

Cu 324.752
Cr 283.563
Fe 259.939
K 766.490
Cd 228.802
Pb 283.306
Ca 393.366
Na 588.995
Mg 279.553
Ni 341.476
Mn 257.610
Zn 213.857
Cu 324.752
Cr 283.563
Fe 259.939
K 766.490
Cd 228.802

Net
Intensity

Corrected
Intensity

15965.8
15219.8
8550560.6
15922366.6
221.2
733.1
50107412.1
1963380.8
2022366.3
-3.1
13291.9
12342.2
15755.0
15143.2
8616498.2
16118182.3
184.2

13449.1
13615.7
8550147.7
15853675.9
89.7
433.6
49697471.6
1988545.5
1931469.8
96.0
12966.2
8978.0
13238.3
13539.1
8616085.3
16049491.6
52.6

Calib.
Conc. Units
[0]
[0]
[50]
[50]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[50]
[50]
[0]

mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L

Analysis
Time
1:04:12
1:04:12
1:04:04
1:04:04
1:04:12
1:04:12
1:04:04
1:04:05
1:04:05
1:04:12
1:04:06
1:04:12
1:04:23
1:04:23
1:04:15
1:04:15
1:04:23

PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM

Method: Pelat Ins 2015

2
2
2
2
2
2
2

Pb
Ca
Na
Mg
Ni
Mn
Zn

283.306
393.366
588.995
279.553
341.476
257.610
213.857

Page
750.2
50041207.0
2096411.0
2043309.9
-16.7
13347.3
12248.7

450.7
49631266.5
2121575.6
1952413.5
82.3
13021.7
8884.6

10

Date: 12/21/2015 3:52:13 PM

[0]
[0]
[0]
[0]
[0]
[0]
[0]

mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L

1:04:23
1:04:15
1:04:16
1:04:16
1:04:23
1:04:17
1:04:23

PM
PM
PM
PM
PM
PM
PM

----------------------------------------------------------------------------------------------------

Mean Data: Std 3c

Mean Corrected
Intensity

Analyte
Cu 324.752
Standard
Cr 283.563
Standard
Fe 259.939
Standard
K 766.490
Standard
Cd 228.802
Standard
Pb 283.306
Standard
Ca 393.366
Standard
Na 588.995
Standard
Mg 279.553
Standard
Ni 341.476
Standard
Mn 257.610
Standard
Zn 213.857
Standard

Std.Dev.

RSD

13343.7
149.09
1.12%
intensity and concentration values are not
13577.4
54.16
0.40%
intensity and concentration values are not
8583116.5
46624.91
0.54%
intensity and concentration values are not
15951583.8
138462.58
0.87%
intensity and concentration values are not
71.1
26.19 36.82%
intensity and concentration values are not
442.2
12.07
2.73%
intensity and concentration values are not
49664369.0
46814.09
0.09%
intensity and concentration values are not
2055060.5
94066.51
4.58%
intensity and concentration values are not
1941941.6
14809.39
0.76%
intensity and concentration values are not
89.2
9.65 10.82%
intensity and concentration values are not
12994.0
39.21
0.30%
intensity and concentration values are not
8931.3
66.06
0.74%
intensity and concentration values are not

Calib
Conc. Units
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[50] mg/L
in the same order.
[50] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.

====================================================================================================

Sequence No.: 11
Sample ID: Std 4a
Analyst:
Logged In Analyst (Original) : HP
Initial Sample Wt:
Dilution:

Autosampler Location:
Date Collected: 12/21/2015 1:05:55 PM
Data Type: Reprocessed on 12/21/2015 3:52:07 PM
Initial Sample Vol:
Sample Prep Vol:

----------------------------------------------------------------------------------------------------

Replicate Data: Std 4a

Repl# Analyte
1
1
1
1
1
1
1
1
1
1
1
1
2
2
2
2
2
2

Cu 324.752
Cr 283.563
Fe 259.939
K 766.490
Cd 228.802
Pb 283.306
Ca 393.366
Na 588.995
Mg 279.553
Ni 341.476
Mn 257.610
Zn 213.857
Cu 324.752
Cr 283.563
Fe 259.939
K 766.490
Cd 228.802
Pb 283.306

Net
Intensity

Corrected
Intensity

3889.8
1686.5
3608.5
5475314.1
129.8
24176.3
21917325.9
1054041.9
1102504.9
38.5
2542.5
13583.3
3759.1
1616.4
3164.9
5354874.9
144.7
25054.0

1373.1
82.5
3195.6
5406623.4
-1.7
23876.7
21507385.3
1079206.5
1011608.5
137.6
2216.9
10219.2
1242.4
12.3
2752.0
5286184.2
13.2
24754.5

Calib.
Conc. Units
[0]
[0]
[0]
[20]
[20]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[20]
[20]
[0]

mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L

Analysis
Time
1:06:16
1:06:16
1:06:16
1:06:09
1:06:16
1:06:16
1:06:09
1:06:10
1:06:10
1:06:16
1:06:16
1:06:16
1:06:25
1:06:25
1:06:25
1:06:18
1:06:25
1:06:25

PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM

Method: Pelat Ins 2015

2
2
2
2
2
2

Ca
Na
Mg
Ni
Mn
Zn

393.366
588.995
279.553
341.476
257.610
213.857

Page
21503001.8
1081204.7
1080155.3
-70.6
2514.7
13558.4

21093061.3
1106369.3
989258.9
28.5
2189.0
10194.2

11

Date: 12/21/2015 3:52:13 PM

[0]
[0]
[0]
[0]
[0]
[0]

mg/L
mg/L
mg/L
mg/L
mg/L
mg/L

1:06:18
1:06:19
1:06:19
1:06:25
1:06:25
1:06:25

PM
PM
PM
PM
PM
PM

----------------------------------------------------------------------------------------------------

Mean Data: Std 4a

Mean Corrected
Intensity

Analyte
Cu 324.752
Standard
Cr 283.563
Standard
Fe 259.939
Standard
K 766.490
Standard
Cd 228.802
Standard
Pb 283.306
Standard
Ca 393.366
Standard
Na 588.995
Standard
Mg 279.553
Standard
Ni 341.476
Standard
Mn 257.610
Standard
Zn 213.857
Standard

Std.Dev.

RSD

1307.8
92.40
7.07%
intensity and concentration values are not
47.4
49.60 104.64%
intensity and concentration values are not
2973.8
313.64 10.55%
intensity and concentration values are not
5346403.8
85163.34
1.59%
intensity and concentration values are not
5.7
10.53 184.70%
intensity and concentration values are not
24315.6
620.69
2.55%
intensity and concentration values are not
21300223.3
292971.36
1.38%
intensity and concentration values are not
1092787.9
19206.97
1.76%
intensity and concentration values are not
1000433.7
15803.53
1.58%
intensity and concentration values are not
83.0
77.13 92.92%
intensity and concentration values are not
2203.0
19.70
0.89%
intensity and concentration values are not
10206.7
17.62
0.17%
intensity and concentration values are not

Calib
Conc. Units
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[20] mg/L
in the same order.
[20] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.

====================================================================================================

Sequence No.: 12
Sample ID: Std 4b
Analyst:
Logged In Analyst (Original) : HP
Initial Sample Wt:
Dilution:

Autosampler Location:
Date Collected: 12/21/2015 1:07:44 PM
Data Type: Reprocessed on 12/21/2015 3:52:08 PM
Initial Sample Vol:
Sample Prep Vol:

----------------------------------------------------------------------------------------------------

Replicate Data: Std 4b

Repl# Analyte
1
1
1
1
1
1
1
1
1
1
1
1
2
2
2
2
2
2
2

Cu 324.752
Cr 283.563
Fe 259.939
K 766.490
Cd 228.802
Pb 283.306
Ca 393.366
Na 588.995
Mg 279.553
Ni 341.476
Mn 257.610
Zn 213.857
Cu 324.752
Cr 283.563
Fe 259.939
K 766.490
Cd 228.802
Pb 283.306
Ca 393.366

Net
Intensity

Corrected
Intensity

4054.9
1705.3
2676.7
10532573.1
118.2
89712.1
28531681.5
1196755.3
1402048.5
-48.1
3616.1
7329.4
3793.9
1623.8
2965.7
10802826.6
155.6
92270.6
28516312.4

1538.1
101.2
2263.9
10463882.4
-13.3
89412.6
28121741.0
1221919.9
1311152.0
50.9
3290.5
3965.2
1277.1
19.7
2552.8
10734135.9
24.1
91971.0
28106371.9

Calib.
Conc. Units
[0]
[0]
[0]
[40]
[40]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[40]
[40]
[0]
[0]

mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L

Analysis
Time
1:08:01
1:08:01
1:08:01
1:07:53
1:08:01
1:07:55
1:07:53
1:07:54
1:07:54
1:08:01
1:08:01
1:08:01
1:08:12
1:08:12
1:08:12
1:08:03
1:08:12
1:08:06
1:08:03

PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM

Method: Pelat Ins 2015

2
2
2
2
2

Na
Mg
Ni
Mn
Zn

588.995
279.553
341.476
257.610
213.857

Page
1285579.8
1426725.8
-105.1
3538.2
7405.5

1310744.4
1335829.4
-6.1
3212.6
4041.4

12

Date: 12/21/2015 3:52:13 PM

[0]
[0]
[0]
[0]
[0]

mg/L
mg/L
mg/L
mg/L
mg/L

1:08:05
1:08:05
1:08:12
1:08:12
1:08:12

PM
PM
PM
PM
PM

----------------------------------------------------------------------------------------------------

Mean Data: Std 4b

Mean Corrected
Intensity

Analyte
Cu 324.752
Standard
Cr 283.563
Standard
Fe 259.939
Standard
K 766.490
Standard
Cd 228.802
Standard
Pb 283.306
Standard
Ca 393.366
Standard
Na 588.995
Standard
Mg 279.553
Standard
Ni 341.476
Standard
Mn 257.610
Standard
Zn 213.857
Standard

Std.Dev.

RSD

1407.6
184.55 13.11%
intensity and concentration values are not
60.5
57.63 95.31%
intensity and concentration values are not
2408.3
204.32
8.48%
intensity and concentration values are not
10599009.1
191098.10
1.80%
intensity and concentration values are not
5.4
26.44 488.87%
intensity and concentration values are not
90691.8
1809.09
1.99%
intensity and concentration values are not
28114056.4
10867.63
0.04%
intensity and concentration values are not
1266332.2
62808.40
4.96%
intensity and concentration values are not
1323490.7
17449.52
1.32%
intensity and concentration values are not
22.4
40.30 179.70%
intensity and concentration values are not
3251.5
55.09
1.69%
intensity and concentration values are not
4003.3
53.86
1.35%
intensity and concentration values are not

Calib
Conc. Units
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[40] mg/L
in the same order.
[40] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.

====================================================================================================

Sequence No.: 13
Sample ID: Std 4c
Analyst:
Logged In Analyst (Original) : HP
Initial Sample Wt:
Dilution:

Autosampler Location:
Date Collected: 12/21/2015 1:09:31 PM
Data Type: Reprocessed on 12/21/2015 3:52:08 PM
Initial Sample Vol:
Sample Prep Vol:

----------------------------------------------------------------------------------------------------

Replicate Data: Std 4c

Repl# Analyte
1
1
1
1
1
1
1
1
1
1
1
1
2
2
2
2
2
2
2
2

Cu 324.752
Cr 283.563
Fe 259.939
K 766.490
Cd 228.802
Pb 283.306
Ca 393.366
Na 588.995
Mg 279.553
Ni 341.476
Mn 257.610
Zn 213.857
Cu 324.752
Cr 283.563
Fe 259.939
K 766.490
Cd 228.802
Pb 283.306
Ca 393.366
Na 588.995

Net
Intensity

Corrected
Intensity

3576.8
1598.1
2519.3
15543883.3
126.1
160223.5
33272780.6
1498772.0
1579014.3
-30.7
4315.0
9095.6
3471.8
1565.2
2291.4
15344801.7
129.1
157612.4
32934798.1
1458245.4

1060.0
-6.0
2106.4
15475192.6
-5.4
159924.0
32862840.1
1523936.6
1488117.9
68.3
3989.4
5731.4
955.1
-38.8
1878.5
15276111.0
-2.4
157312.9
32524857.6
1483410.0

Calib.
Conc. Units
[0]
[0]
[0]
[60]
[60]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[0]
[60]
[60]
[0]
[0]
[0]

mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L

Analysis
Time
1:09:54
1:09:54
1:09:54
1:09:46
1:09:54
1:09:48
1:09:46
1:09:47
1:09:47
1:09:54
1:09:54
1:09:54
1:10:05
1:10:05
1:10:05
1:09:56
1:10:05
1:09:59
1:09:56
1:09:58

PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM
PM

Method: Pelat Ins 2015

2
2
2
2

Mg
Ni
Mn
Zn

279.553
341.476
257.610
213.857

Page
1557705.1
-41.6
4235.1
9036.5

1466808.7
57.5
3909.4
5672.3

13

Date: 12/21/2015 3:52:13 PM

[0]
[0]
[0]
[0]

mg/L
mg/L
mg/L
mg/L

1:09:58
1:10:05
1:10:05
1:10:05

PM
PM
PM
PM

----------------------------------------------------------------------------------------------------

Mean Data: Std 4c

Analyte
Cu 324.752
Standard
Cr 283.563
Standard
Fe 259.939
Standard
K 766.490
Standard
Cd 228.802
Standard
Pb 283.306
Standard
Ca 393.366
Standard
Na 588.995
Standard
Mg 279.553
Standard
Ni 341.476
Standard
Mn 257.610
Standard
Zn 213.857
Standard

Mean Corrected
Intensity

Std.Dev.

RSD

1007.6
74.22
7.37%
intensity and concentration values are not
-22.4
23.24 103.73%
intensity and concentration values are not
1992.4
161.12
8.09%
intensity and concentration values are not
15375651.8
140771.96
0.92%
intensity and concentration values are not
-3.9
2.14 54.37%
intensity and concentration values are not
158618.5
1846.34
1.16%
intensity and concentration values are not
32693848.8
238989.73
0.73%
intensity and concentration values are not
1503673.3
28656.63
1.91%
intensity and concentration values are not
1477463.3
15067.87
1.02%
intensity and concentration values are not
62.9
7.67 12.19%
intensity and concentration values are not
3949.4
56.53
1.43%
intensity and concentration values are not
5701.9
41.80
0.73%
intensity and concentration values are not

Calib
Conc. Units
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[60] mg/L
in the same order.
[60] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.
[0] mg/L
in the same order.