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Deep Earth Energy Research Lab, Department of Civil Engineering, Monash University, Building 60, Melbourne, Victoria 3800, Australia
Department of Mechanical & Aerospace Engineering, Monash University, Building 36, Melbourne, Victoria 3800, Australia
a r t i c l e
i n f o
Article history:
Received 1 October 2012
Accepted 25 November 2014
Available online 13 January 2015
Keywords:
Geothermal
Granite
Brittleplastic
High temperature
a b s t r a c t
The effect of temperature on the mechanical behaviour of Strathbogie granite (ne-grained) was studied under unconned stress conditions. Fracturing behaviour of test specimens was studied using an
acoustic emission (AE) detection system and some crack propagation was also performed using electron microscopy scanning (SEM). The stressstrain curves showed plastic and post-peak behaviour for
temperatures above 800 C and the brittleplastic transition was observed to occur between 600 and
800 C for the uniaxially tested Strathbogie granite at a strain rate of 0.1 mm/min and room humidity.
Specimens were heated at a rate of 5 C/min with a 1 h holding period before testing. The AE results
showed that the increasing temperature reduces the stress thresholds for crack initiation and crack damage and extends the duration of stable crack propagation. Prevalence of ductile properties with increasing
temperature was also observed from AE results. The stressstrain and AE results reveal that the failure
modes of Strathbogie granite specimens changed from brittle fracturing to quasi-brittle shear fracturing
and eventually to ductile failure with increasing temperature. Temperature was observed to inuence the
colour of granite, and the initial white/grey colour changed to an oxidated reddish colour with increasing
temperature. The stressstrain data of tested specimens were incorporated into a nite element model
(ABAQUS 6.7.1), so that both plastic and ductile behaviour of the Strathbogie granite could be predicted
over a wide range of temperatures.
2014 Elsevier Ltd. All rights reserved.
1. Introduction
Geothermal heat is now a recommended renewable energy
resource on the time-scales of both technological and societal systems, with cost, reliability and environmental advantages
over conventional energy resources (Rybach, 2003; Gallup, 2009;
Axelsson, 2010). Exploration of geothermal resources has posed
new challenges for engineers and geologists to counter rock engineering problems at high temperatures. Laboratory testing is an
important aspect of rock mechanics, which provides essential input
data for the design of engineering structures in the Earths crust
and mantle subjected to tectonic forces. Since the 1970s, a large
number of laboratory studies have been carried out to investigate the effect of temperature on the physical and mechanical
Corresponding author at: Deep Earth Energy Research Lab, Civil Engineering
Department, Clayton Campus, Monash University, VIC 3800, Australia.
Tel.: +61 3 99054982; fax: +61 3 99054944.
E-mail address: ranjith.pg@monash.edu (P.G. Ranjith).
http://dx.doi.org/10.1016/j.geothermics.2014.11.005
0375-6505/ 2014 Elsevier Ltd. All rights reserved.
97
Fig. 1. Stressstrain curves of granite after high temperature (Xu et al., 2008a,b).
98
Fig. 2. Summation of counts vs. axial stress of single fractured rock (Ranjith et al., 2004).
A number of previous studies used the acoustic emission technique to study crack growth in brittle material (Shield, 1997;
Eberhardt et al., 1998; Rudajev et al., 2000; Cai et al., 2007). Eberhardt used a combination of AE technology and stressstrain curve
measurement data in their experimental study (Eberhardt et al.,
1999). Chang and Lee (2004) studied the cracking and damage
mechanisms of Korean Hwang-deung granite and Yeo-san marble under triaxial compression using acoustic emissions. These
researchers have divided the process of crack development into ve
different stages: crack closure, crack initiation, secondary cracking,
crack coalescence and crack damage, which mirror the divisions
established by Hoek and Bieniawski (1965) based on stressstrain
behaviour. A similar type of division of stress threshold has been
carried out by Ranjith et al. (2008) in their experimental studies
on fractured rock under uniaxial compression. They used the characteristics of the curve of cumulative AE count versus axial stress
to dene the stress thresholds for different fracture development
stages. The crack initiation stress threshold ( ci ) has been dened
as the point where the curve of cumulative AE counts marks the
initial lift-off (Fig. 2). The region, which sustains a linear increase
of cumulative AE counts with increasing stress, is termed stable
crack propagation. When the curve starts exhibiting an exponential growth, the corresponding stress is called the crack damage
stress threshold ( cd ) and the region between crack damage and
failure is dened as unstable crack growth.
2. Experimental work
2.1. Specimen preparation
The tested rock specimens were produced from one macroscopically homogeneous Strathbogie granite block. The Strathbogie
granite is a high-level, discordant, composite granitoid intrusion in
south-eastern Australia. It is ne-grained and white grey and dark
brown in colour with a tested porosity of 0.463%. It contains magmatic garnet, and cordierite and biotite predominate in the bothlith
(Neil Phillips et al., 1981). Grain size (which is measured from the
thin section of rock samples) ranges from 0 mm to 200 m, with
a few grains larger than 300 mm (Fig. 3). An optical microscopy
image of Strathbogie granite is presented in Fig. 4. At room temperature, Strathbogie granite showed a bulk density of 1805.7 kg/m3 ,
peak compressive strength of 215.97 MPa and elastic modulus of
8.97 GPa.
99
Table 1
Mechanical properties of Strathbogie granite at different test temperatures (averaged results).
Temperature,
Peak strength,
MPa
Elastic
modulus, GPa
Failure strain, %
23
100
200
400
600
800
900
1000
1100
215.98
190.64
234.02
203.67
119.56
96.01
39.63
37.07
5.29
8.98
8.28
8.48
7.95
5.78
3.72
1.71
1.34
0.23
2.70
2.60
3.15
2.95
2.55
4.05
5.75
5.75
7.45
100
Fig. 5. Two testing devices used for experiments (a) servo-controlled Instron machine with a loading capacity of 100 kN and environmental furnace; (b) universal testing
machine with loading capacity of 500 kN and cylindrical furnace.
Table 2
Average and normalized values of compressive strength, elastic modulus and strain at failure.
T ( C)
Average c (MPa)
Normalized c
Average E (GPa)
Normalized E
Average
Normalized
23
100
200
400
600
800
900
1000
1100
215.97
190.63
234.02
203.66
119.56
96.01
38.53
37.07
5.29
1
0.883
1.084
0.943
0.554
0.445
0.178
0.172
0.024
8.97
8.28
8.48
7.94
5.77
3.72
1.71
1.34
0.23
1
0.923
0.945
0.885
0.644
0.415
0.190
0.150
0.026
0.027
0.026
0.032
0.030
0.026
0.040
0.058
0.057
0.075
1
0.966
1.172
1.103
0.952
1.500
2.142
2.134
2.775
101
Fig. 7. (a) Peak strength of Strathbogie granite at different test temperatures; (b) elastic modulus of Strathbogie granite at different test temperatures; (c) failure strain at
peak load of Strathbogie granite at different test temperatures. The dashed line indicates the melting point (600 C) of quartz, K-feldspar, Na-plagioclase and micas.
characteristics. For the specimens tested at 900 C and 1000 C, failure occurred along only a few failure planes and closely resembled
shear failure. Specimens tested at 1100 C showed a very different failure mode, in which the failure took place in a more ductile
manner. The overall trend of the failure mechanisms clearly shows
that increasing temperature inuences the failure mechanisms of
Strathbogie granite in such a way that the ductile properties are
dominant at higher temperatures.
The micro-structural changes which occur with increasing
temperature in granite inuence the variation of failure mechanisms for different temperatures. Scanning electron microscopic
(SEM) images of granite thin sections are provided in Fig. 10, and
indicate that cracks developed and opened up with increasing
Fig. 8. Normalized compressive strength vs. test temperature curves for the present study and previous studies.
102
Fig. 9. Normalized elastic modulus vs. test temperature curves for the present study and previous studies.
Fig. 10. SEM images of negrained Strathbogie granite: (a) thin section at room temperature; (b) thin section heated to 400 C; (c) thin section heated to 800 C.
between mineral grains, as a result of differential thermal expansion between grains with different thermo-elastic moduli and
thermal conductivities (Dmitriyev et al., 1972; Heard and Page,
1982; Kranz, 1983).
Micro-cracking patterns and the distribution of inter- and intragranular micro-cracks in granites have been studied previously
(Kudo et al., 1992; Nasseri et al., 2005) and after being affected by
high temperature (Nasseri et al., 2007). Mineralogy is known to play
an important role in granite thermal degradation. As David et al.
(2012) reported, the crack density of La Peyratte granite is increased
from 0.2 at room temperature to 4.4 at 600 C temperature. They
further stated that differences of thermal expansion between different minerals cause crack nucleation, and the dramatic increase
of crack density of La Peyratte granite between 500 C and 600 C
is a result of transition of quartz, which occurs at 576 C. Even
with a temperature increase below the transition threshold, the
high and anisotropic thermal expansion leads to the fact that with
the variation of quartz content a different deterioration is expected
upon the same temperature changes. Especially in crystalline rock,
the amount of quartz has a signicant effect on thermally induced
micro-cracks because of the complexity of its thermal expansivity. It is reasonable to state that when the temperature increases
103
Table 3
Post-failure images of tested specimens.
Gf5 at 23 C
Gf7 at 100 C
Gf8 at 200 C
Gf12 at 400 C
Gf13 at 600 C
Gf19 at 800 C
Gf23 at 900 C
Gf20 at 1000 C
Gf24 at 1100 C
Fig. 11. Cumulative AE events vs. axial stress at room temperature 23 C (Gf6).
Fig. 12. Cumulative AE events vs. axial stress at temperature 100 C (Gf7).
Fig. 13. Cumulative AE events vs. axial stress at temperature 200 C (Gf10).
Fig. 14. Cumulative AE events vs. axial stress at temperature 400 C (Gf12).
Table 4
Different colours observed at different temperatures for the tested specimens.
T ( C)
23
100
200
400
600
800
900
1000
1100
Colour
Reddish
Reddish
Pink
104
Fig. 15. Cumulative AE events vs. axial stress at temperature 600 C (Gf14).
Table 5
Stress thresholds for different fracturing stages.
T ( C)
ci , MPa
ci2 , MPa
cd , MPa
peak , MPa
23
100
200
200
400
400
600
600
200
135.8
209
232.4
190
169.5
31.6
35.900
202
140.8
214.7
235
194
182.8
203
165.5
217.8
238.7
197
190
96.8
115.8
214.467
181.989
228.074
239.975
203.198
204.128
117.321
121.804
Fig. 16. Crack initiation and crack damage stress thresholds and peak compressive
strength for different temperatures.
Table 6
Normalized values of crack initiation and crack damage for different temperatures.
Temperature ( C)
23
100
200
200
400
400
600
600
ci / peak
cd / peak
0.93
0.95
0.75
0.91
0.92
0.95
0.97
0.99
0.94
0.97
0.83
0.93
0.27
0.82
0.29
0.95
Fig. 17. Normalized stress for crack initiation and crack damage at different temperatures.
inuences the crack initiation stress thresholds of Strathbogie granite and increasing temperature allows crack initiation to happen
earlier. The early occurrence of crack initiation as temperature is
increased indicates the domination of ductile properties at elevated
temperature. This correlation is consistent with the prevalence of
ductile failure at higher temperatures (Table 3).
However, the normalized stress values for crack damage do not
show any important scatter with increasing temperature for Strathbogie granite, suggesting that crack damage occurs very close to
failure during uniaxial loading, but independent of the temperature.
3. Finite element modelling
Conducting a rigorous laboratory testing programme is usually time-consuming, labour-intensive and expensive. Validating a
numerical model using few experimental results and then extending the models for many other scenarios is a far more efcient
approach, and the availability of sophisticated and user-friendly
software packages has made this task much easier. This approach
is extremely useful, since results can be obtained even under
test conditions that the experimental approach fails to simulate.
In addition, some critical insights, such as stress/strain distribution within model specimens, such as the distribution of plastic
strain, can be comprehensively obtained from numerical simulations. Therefore, the experimental results of this study were rst
used to validate a nite element numerical model and then some
105
Table 7
Temperature-dependent mechanical properties of Strathbogie granite.
T ( C)
c (MPa)
E (GPa)
23
100
200
400
600
800
900
1000
1100
215.97
190.63
234.02
203.66
119.56
96.01
38.53
37.07
5.29
0.027
0.026
0.032
0.030
0.026
0.040
0.058
0.057
0.075
8.97
8.28
8.48
7.94
5.77
3.72
1.71
1.34
0.23
Table 8
Temperature-dependent plastic properties of Strathbogie granite.
T ( C)
800
800
900
900
1000
1000
1100
1100
82.51
26
38
25
31
7.11
7.65
Plastic strain
0
0.0125
0
0.0149
0
0.0140
0
0.0100
Fig. 18. Geometry of model specimen (a) specimen and the platens of the testing apparatus (the shaded area is the portion of the specimen that was modelled
by ABAQUS) and (b) the two-dimensional axis-symmetric model of the uniaxial
compression test.
106
Fig. 19. Experimental results vs. values predicted by FEM (red squares) for different test temperatures.
107
Fig. 20. Predicted compressive strength of Strathbogie granite using FEM (red squares) for (a) 500 C and (b) 700 C.
Fig. 21. The distribution of plastic strain in the specimen deformed at 800 C (a) strain = 0.0251, (b) strain = 0.0343 and (c) strain = 0.0457.
108
Acknowledgement
The authors acknowledge the use of facilities within the Monash
Centre for Electron Microscopy.
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