Professional Documents
Culture Documents
Water and
Environmental (LEAP)
Proficiency Testing
Programme
2016
Contents
Who We Are
10
11
13
13
14
15
16
16
17
18
19
19
20
23
24
25
26
26
27
27
Ordering Information
28
Technical Information
29
Protocols
29
29
ISO Accreditation
29
Agent Information
12
30
Who We Are
Fapas is the leading global provider of proficiency testing schemes, quality control
samples and reference materials in the food sector, offering products throughout the
year.
Proficiency testing in an independent check of your laboratory procedures providing you
with a completely confidential assessment of your capability. Not only does participation
in the relevant testing schemes allow you to demonstrate your systems and the technical
ability of your staff, it will also help you gain and maintain ISO/17025 accreditation.
Established in 1990, we are an experienced, accredited provider of proficiency tests for the food and
water, environmental chemistry and microbiology sectors. Taking part in our proficiency tests provides
you with the confidence in your laboratory equipment, methods and staff, and assurance that you are
delivering the quality results required by your customers.
We provide our participants with a confidential service that allows you to participate at a level that suits
you; there is no minimum number of proficiency tests that you must take part in each year. Our system
provides an easy reporting facility via our website and our comprehensive reports, which receive
rigorous statistical analysis, contain method comparisons.
We also offer quality control samples and reference materials from selected food chemistry proficiency
tests which can be purchased easily through our website throughout the year.
Our four Fapas proficiency testing schemes cover food chemistry, food microbiology, GM and water
and environmental analysis.
Participation can be at a level that suits your business from taking part in one of our scheduled tests,
through to company-specific closed tests.
Results from each proficiency test receive rigorous statistical analysis, ensuring you have clear feedback
on your performance. Comprehensive reports provide information on analytical methods used by other
participants. We can provide problem-solving consultancy on your laboratory procedures if required.
Participation in Fapas is easy. Arrangements can be made through our network of agents, or via our
website, www.fapas.com. Fapas Food Chemistry follows international guidelines for proficiency testing
and is accredited by UKAS to ISO/IEC 17043.
Analytes
Water Type
Concentration Ranges
(approx, after dilution)
Volume
Supplied
(approx)
sodium
potassium
chloride
calcium
magnesium
alkalinity
total hardness
total phosphorus
fluoride
sulphate
5.0 50 mg/l
0.3 3.0 mg/l
6.0 50 mg/l
10 150 mg/l
1.0 15 mg/l
30 300 mg HCO3/l
30 130 mg Ca/l
100 3000 g P/l
150 1800 g/l
8.0 100 mg/l
nitrite
nitrate
ammonium
TOC
PI
colour (filtered)
SR phosphate
pH
turbidity
0
conductivity @ 20 C
cadmium
lead
iron
manganese
aluminium
copper
zinc
nickel
chromium
1 litre
2
Routine
Components
3
Routine Metals
500 ml
Water Type
Concentration Ranges
(approx, after dilution)
Volume
Supplied
(approx)
mercury
barium
boron
arsenic
selenium
antimony
silver
strontium
lithium
cobalt
vanadium
molybdenum
tin
beryllium
Standard
concentrates or
standard solutions
in ultra-pure water
500 ml
5
Inorganic
Disinfection Byproducts
bromide
bromate
chlorite
chlorate
Standard solution in
ultra-pure water
5 200 g/l
1.0 20 g/l
1.0 200 g/l
1.0 1000 g/l
125 ml
6
Trihalomethanes
/Chlorinated
Solvents
chloroform
dichloromethane
bromodichloromethane
dibromochloromethane
bromoform
trichloroethene
tetrachloroethene
carbon tetrachloride
1,2-dichloroethane
1,2,3-trichlorobenzene
1,2,4-trichlorobenzene
1,3,5-trichlorobenzene
hexachlorobutadiene
1,1,1-trichloroethane
Ultra-pure water +
spiking concentrate
in methanol
1 litre
anthracene
fluoranthene
benzo (b) fluoranthene
benzo (k) fluoranthene,
naphthalene
benzo (a) pyrene
benzo (ghi) perylene
indeno (1,2,3-cd) pyrene
1 litre
7
Polycyclic
Aromatic
Hydrocarbons
Analytes
9
Acid Herbicides
Analytes
Water Type
Concentration Ranges
(approx, after dilution)
Volume
Supplied
(approx)
alachlor
azinphos-ethyl
azinphos-methyl
dichlorvos
fenitrothion
malathion
mevinphos
chlorofenvinphos
chlorpyrifos
diazinon
fenthion
parathion-ethyl
parathion-methyl
cypermethrin
propetamphos
1 litre
MCPA
MCPB
2,4-D
dichlorprop
dicamba,
2,4-DB
bentazone
mecoprop
propyzamide
ioxynil
bromoxynil
triclopyr
clopyralid
fluroxypyr
2,3,6-TBA
2,4,5-T
dichlobenil
bromacil
metazachlor
propachlor
benazolin
metaldehyde
1 litre
11
BTEX
12
Chlorine
Analytes
Water Type
Concentration Ranges
(approx, after dilution)
Volume
Supplied
(approx)
1 litre
endrin
dieldrin
Aldrin
p,p DDT
o,p-DDT
p,p-DDE
o,p-DDE
p,p-DDD
o,p-DDD (TDE)
hexachlorocyclohexane
(alpha)
hexachlorocyclohexane
(beta)
hexachlorocyclohexane
(delta)
lindane (gamma HCH)
trifluralin
alpha endosulphan
beta endosulphan
Hexachlorobenzene
heptachlor
heptachlor epoxide (total),
pentachlorobenzene
pendimethalin
benzene
toluene
ethylbenzene
styrene
o-xylene
m-xylene
p-xylene
m+p xylene
total xylene
1 litre
Concentrate for
dilution up to 1 litre
3 ml
16
Total Cyanide
Analytes
Water Type
Concentration Ranges
(approx, after dilution)
Volume
Supplied
(approx)
isoproturon
diuron
linuron
chlortoluron
monuron
methabenzthiazuron
diflufenican
metamitron
simazine
atrazine
propazine
cyanazine
trietazine
prometryn
terbutryn
ametryn
carbetamide
pirimicarb
1 litre
total cyanide
Concentrate for
dilution up to 1 litre
3 ml
10
11/01/2016
date
C1235
C1236
C0536
C0399
C0299
C0199
21/03/2016
CHEM 171
Closing date for registrations for Group 12 is four weeks before the start dates for these tests.
Closing date for registrations for Groups 9 & 15 is five weeks before the start dates for these tests.
Closing date for registrations for all other groups is two weeks before the start date of these tests
Group 15
C1504
C1136
Group 11
Group 12
C1036
Group 10
C0836
Group 8
C0936
C0736
Group 7
Group 9
C0636
07/03/2016
CHEM 170
Group 6
Group 5
C0535
C0398
C0397
Group 3
C0436
C0298
C0297
Group 2
Group 4
C0198
08/02/2016
CHEM 169
C0197
18/01/2016
CHEM 168
Group 1
2015-16
analyte group
CHEM 167
distribution
11
12/04/2016
date
DWC1602
DWC1202
Closing date for registrations for Group 12 is four weeks before the start dates for these tests.
Closing date for registrations for Groups 9 & 15 is five weeks before the start dates for these tests.
Closing date for registrations for all other groups is two weeks before the start date of these tests.
Group 16
Group 15
DWC1501
DWC1102
DWC1101
Group 11
Group 12
DWC1003
DWC1002
DWC1001
Group 10
DWC1103
DWC0902
21/11/2016
DWC009
DWC0901
DWC0802
DWC0801
Group 8
DWC0502
DWC0304
DWC0204
DWC0104
14/11/2016
DWC008
Group 9
DWC0702
DWC0701
Group 7
27/09/2016
DWC007
DWC0602
DWC1201
DWC0402
DWC0303
DWC0203
DWC0103
19/09/2016
DWC006
DWC0601
02/08/2016
DWC005
Group 6
DWC1601
DWC0401
Group 4
DWC0501
DWC0302
DWC0301
Group 3
Group 5
DWC0202
DWC0201
Group 2
11/07/2016
DWC004
DWC0102
07/06/2016
DWC003
DWC0101
17/05/2016
DWC002
Group 1
2015-16
analyte group
DWC001
distribution
DWC0803
DWC0703
DWC0603
05/12/2016
DWC010
LEAP
Fapas Water and Environmental
For Total Coliforms & Escherichia coli, this sample contains Escherichia coli and another
coliform organism.
Sample B:
Sample C:
Organism Identification:
12
This is a nutrient agar slope, which has been inoculated with a Gram negative
rod-shaped organism but please note, occasionally a Gram positive organism
may be used. The organism chosen is one which is routinely recovered from
water. This sample requires no preparation.
LEAP
Fapas Water and Environmental
MICRO 98
MICRO 99
DWM001
DWM002
Test
12/01/2016
16/02/2016
15/03/2016
19/04/2016
10/05/2016
Y0197
Y0198
Y0199
DWM0101
DWM0102
Y0297
Y0298
Y0299
DWM0201
DWM0202
Y0297
Y0298
Y0299
DWM0201
DWM0202
Enterococci
Y0467
Y0468
Y0469
DWM0301
DWM0302
Clostridium perfringens
Y0467
DWM0301
DWM0302
Y0469
Y0468
Pseudomonas aeruginosa
Y0735
Organism Identification
Y0736
Closing date for registrations is five weeks before the start date of these tests
DWM004
DWM005
DWM006
DWM007
DWM008
Test
14/06/2016
19/07/2016
13/09/2016
11/10/2016
08/11/2016
06/12/2016
DWM0103
DWM0104
DWM0105
DWM0106
DWM0107
DWM0108
DWM0203
DWM0204
DWM0205
DWM0206
DWM0207
DWM0208
DWM0203
DWM0204
DWM0205
DWM0206
DWM0207
DWM0208
Enterococci
DWM0303
DWM0304
DWM0305
DWM0306
DWM0307
DWM0308
Clostridium perfringens
DWM0303
DWM0304
Pseudomonas aeruginosa
Organism Identification
DWM0306
DWM0401
DWM0305
DWM0307
DWM0402
Closing date for registrations is five weeks before the start date of these tests
13
DWM0308
LEAP
Fapas Water and Environmental
What methods were used to detect the taste and odour contaminant(s)?
Results must be e-mailed or faxed to Fapas. The closing date for submission of results will be 3 weeks
from the start date for the exercise.
Once per year a Discussion Forum is held at Fera, York, to discuss the outcomes of each taste and
odour contamination test. The meeting is an important opportunity for participants to share information
on detecting the contaminant(s) present. The cost for participating in the meeting is included in the price
for participation in this test, with a maximum of 2 people per organisation attending. Chatham House
Rules apply at these discussion forums.
14
LEAP
Fapas Water and Environmental
distribution number
test
08/09/2016
TOCHEM05
Closing date for registrations is two weeks before the start date for this test
Contaminated Potable Water Samples, labelled TASTE & ODOUR CHEMICAL CONTAMINATION:
NB participants should not undertake any taste (organoleptic) testing on this sample
Blank Water Samples, labelled BLANK:
NB participants should not undertake any taste (organoleptic) testing on this sample
15
LEAP
Fapas Water and Environmental
PARA 54
DWP001
DWP002
DWP003
DWP004
Tests
12/01/2016
15/03/2016
10/05/2016
19/07/2016
13/09/2016
08/11/2016
Suspension A
P0153
P0154
DWP0101
DWP0102
DWP0103
DWP0104
Suspension B
P0253
P0254
DWP0201
DWP0202
DWP0203
DWP0204
Filter A
P0353
P0354
Closing date for registrations is two weeks before the start date of these tests
16
LEAP
Fapas Water and Environmental
Do you have any analytical information that you feel would help the water company to decide if
this water could be safely used for non-drinking purposes (e.g. bathing, washing, laundry etc.)
Results must be e-mailed or faxed to Fapas. The closing date for submission of results is 7 days from
the start date for the exercise.
Laboratories will be informed by e-mail within 1 day of the closing date of the list of contaminants
knowingly added to the test samples.
Once per year a Discussion Forum is held at Fera, York, to discuss the outcomes of each emergency
test. The meeting is an important opportunity for participants to share information on detecting the
contaminants present. The cost for participating in the meeting is included in the price for participation in
these tests, maximum of 2 people per organisation attending. Chatham House Rules apply at these
discussion forums.
17
LEAP
Fapas Water and Environmental
distribution number
test
April 2016
EMY32
Contamination Incident
October 2016
EMY33
Contamination Incident
Closing date for registrations is two weeks before the start date of these tests
Contaminated Drinking Water Samples, labelled CONTAMINATION INCIDENT:
18
1 x 500 ml PET bottle only to be tested for gross alpha and beta levels at above 1bq/litre. NB this
sample is acidified (0.1M nitric acid)
LEAP
Fapas Water and Environmental
Environmental Legionella
Two solid tablets which require reconstitution with laboratories own sterile deionised (or distilled) water to
1litre before analysis. Participants are required to report results qualitatively, indicating whether
Legionella spp. is detected or not detected and identify the species present. Quantitative results are
requested to be expressed in cfu/l.
19/04/2016
11/10/2016
Legionella spp
LG0101
LG0102
Closing date for registrations is five weeks before the start date of these tests
19
LEAP
Fapas Water and Environmental
20
Analytes
Concentration Ranges
(approx, after dilution)
Volume
Supplied
Dilution
Required
(approx)
BOD 5-day
COD
TOC
50 ml
x20
Dissolved Solids
Suspended Solids
Total Solids
Settled COD
100 ml
x20
Nitrate (N)
Nitrite (N)
Ammonia (N)
Chloride
Orthophosphate (P)
Sulphate (SO4)
Total Phosphorus (P)
Kjeldahl Nitrogen (N)
Total Nitrogen (N)
0.5 50 mg/l
0.2 10 mg/l
0.2 20 mg/l
10.0 500 mg/l
1.0 100 mg/l
10.0 500 mg/l
0.2 5 mg/l
2.0 50 mg/l
2.0 50 mg/l
4 x 60ml
x20
pH
o
Electrical Conductivity @ 25 C
2 x 125 ml
no dilution
required
LEAP
Fapas Water and Environmental
21
Analytes
Concentration Ranges
(approx, after dilution)
Volume
Supplied
Dilution
Required
(approx)
5
Trace Metals 1
Aluminium
Arsenic
Beryllium
Cadmium
Chromium (Total)
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Nickel
Selenium
Vanadium
Zinc
20 ml
to 1 l
6
Trace Metals 2
Antimony
Barium
Boron
Molybdenum
Silver
Strontium
Thallium
95 900 g/l
100 2500
800 2000
60 600
26 600
30 300
60 900
20 ml
to 1 l
Hexavalent Chromium
45 880 g/l
20 ml
to 1 l
Alkalinity
Calcium
Total Hardness
Magnesium
Potassium
Sodium
2 x 20 ml
to 1 l
Bromide
Fluoride
1 10 mg/l
0.3 4
20 ml
to 1 l
10
10 100 mg/l
2 ml
to 1 l
11
Cyanide (Total)
0.1 to 1 mg/l
2 ml
to 1 l
12
Total Sulphide
1 10 mg/l
20 ml
to 1 l
13
Settleable Solids
(Volumetric test using Imhoff cone)
5 100 ml/l
25 g
to 1 l
14
Dissolved Oxygen
Dissolved Oxygen (Winkler)
2 ml
to 1 l
LEAP
Fapas Water and Environmental
15
VOC 1
22
Analytes
Benzene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Ethylbenzene
Methyl tert-butyl ether (MTBE)
Naphthalene
Toluene
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
m+p-Xylene
o-xylene
Total Xylene
Concentration Ranges
(approx, after dilution)
8 120 g/l
8 100
9 125
8 115
9 100
15 100
8 190
7 100
8 100
8 100
8 300
8 300
20 300
Volume
Supplied
(approx)
Dilution
Required
1.5 ml
to 100 ml
LEAP
Fapas Water and Environmental
WW001
WW002
WW003
date
25/04/2016
25/07/2016
24/10/2016
Group 1
WW0101
WW0102
WW0103
Group 2
WW0201
WW0202
WW0203
Group 3
WW0301
WW0302
WW0303
Group 4
WW0401
WW0402
WW0403
Group 5
WW0501
WW0502
WW0503
Group 6
WW0601
WW0602
WW0603
Group 7
WW0701
WW0702
WW0703
Group 8
WW0801
WW0802
WW0803
Group 9
WW0901
WW0902
WW0903
Group 10
WW1001
WW1002
WW1003
Group 11
WW1101
WW1102
WW1103
Group 12
WW1201
WW1202
WW1203
Group 13
WW1301
WW1302
WW1303
Group 14
WW1401
WW1402
WW1403
Group 15
WW1501
WW1502
WW1503
Closing date for registrations is two weeks (for Groups 1-4) and four weeks (for Groups 5-15) before the start date
of these tests.
23
LEAP
Fapas Water and Environmental
Concentration Ranges
Volume Supplied
(approx)
(approx)
1.5-35 mg/L
1.5-35 mg/l
0.5-10 mg/l
500 ml
Ammonia as N
Nitrate as N
Nitrate+nitrite as N
Nitrite as N
Orthophosphate as P
0.650-19.0 mg/l
0.250-40.0 mg/l
0.250-40.0mg/l
0.400-4.00 mg/l
0.500-5.50 mg/l
500 ml
Calcium, Ca
Magnesium, Mg
Potassium, K
Alkalinity as CaCO3
Conductivity (25C)
Hardness, total as CaCO3
pH
25-110 mg/l
2-40 mg/l
4-40 mg/l
10-100000 mg/l
0.00-100 S/cm
8.7-275 mg/l
5-10 units
500 ml
4
Trace Metals 1
Aluminium
Arsenic
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Mercury
Nickel
Selenium
0-10000 g/l
0-10000 g/l
0-10000 g/l
0-10000 g/l
0-10000 g/l
0-10000 g/l
0-10000 g/l
0-10000 g/l
0-10000 g/l
0-10000 g/l
0-10000 g/l
0-10000 g/l
0-10000 g/l
500 ml
5
Trace Metals 2
Antimony, Sb
Barium, Ba
Boron, B
Molybdenum, Mo
Silver, Ag
Strontium, Sr
Thallium, Tl
Tin, Sn
Titanium, Ti
95-900 g/l
100-2500 g/l
800-2000 g/l
60-600 g/l
26-600 g/l
30-300 g/l
60-900 g/l
1000-5000 g/l
80-300 g/l
500 ml
1
Complex
Nutrients
2
Simple Nutrients
3
Minerals
24
Analytes
LEAP
Fapas Water and Environmental
HS002
HS003
date
28/06/2016
01/11/2016
Group 1
HS0102
HS0103
Group 2
HS0202
HS0203
Group 3
HS0302
HS0303
Group 4
HS0402
HS0403
Group 5
HS0502
HS0503
Closing date for registrations is four weeks before the start date of these tests
25
LEAP
Fapas Water and Environmental
Cadmium
Lead
Chromium
Arsenic
Barium
Nickel
Copper
Zinc
Mercury
Concentration Ranges
Volume Supplied
(approx)
Dilution
Required
68g
no dilution required
distribution number
test
11/05/2016
SL001
SL0101
17/08/2016
SL002
SL0102
01/12/2016
SL003
SL0103
Closing date for registrations is four weeks before the start date of these tests
26
LEAP
Fapas Water and Environmental
1
Major Inorganic
Components
Analytes
Water Type
surface water
surface water
3
Metals
(in 0.5% Nitric Acid)
surface water
500 ml +
spiking
conc
4
Toxic Metals
(in 0.5% Nitric Acid)
surface water
500 ml +
spiking
conc
2
Routine Components
SW001
SW002
date
21/06/2016
17/10/2016
Group 1
SW0101
SW0102
Group 2
SW0201
SW0202
Group 3
SW0301
SW0302
Group 4
SW0401
SW0402
Closing date for registrations is two weeks before the start date of these tests.
27
Volume
Supplied
(approx)
1 litre +
spiking
conc
LEAP
Fapas Water and Environmental
Ordering Information
Notes:
a)
b)
c)
d)
e)
f)
The dispatch date shown is our planned dispatch date. You will be notified by email if any of the tests
you order are delayed or cancelled for any reason. The majority of test close dates are 2-4 weeks after
dispatch.
Closing dates for registrations for proficiency tests in the Fapas Programme are located with the
timetables.
Indicate a contact name and email address against each test you order, otherwise the name given will be
used.
The approximate quantity of test material we will supply is given for each test. If your method needs more
material please indicate the number of extra test materials you require. There is a charge for additional
test materials.
The purchase of extra test materials does not entitle you to receive an extra performance assessment.
You must place multiple orders for the test if you require this service.
Test materials are dispatched by normal post unless courier service is requested. Please contact Fapas
for prices of sending test materials by courier.
Additional notes:
i. Dispatch
a)
b)
c)
d)
Please contact us if your postal or economy courier dispatch has not arrived within 10 working days, or
your courier dispatch has not arrived within 4 working days.
The tracking number of your courier consignment will be sent to the email address given for the sample
contact and the delivery contact for that test. The message will indicate how to track the consignment.
Airway Bill Numbers are also available from the participants secure pages on the Fapas website.
It is the responsibility of a participant to monitor the progress of their courier dispatch.
We are not responsible for damage or loss of test materials due to problems in customs or for import
fees.
If you require special import permits for importing certain types of test material into your country please
inform us at least 3 weeks prior to dispatch date. There is a charge for this service.
Phytosanitary certificates can be provided for plant based products where appropriate. There is a charge
for this service.
iii. Results
a)
b)
Participants generally have 2-4 weeks to return results after a test material is dispatched, except Fapas
drinking water chemical emergency.
Result submission will only be allowed via the Fapas website.
iv. Reports
a)
b)
c)
28
The cost of the test includes access to an electronic copy of the report for the person placing the order
and designated sample contact.
Reports are normally available on our website within 25 days of the closing date of the test.
The reports are in PDF format and are secured by a digital signature. Adobe Reader version 7 or greater
is required to open these files.
LEAP
Fapas Water and Environmental
Technical Information
Protocols
Example Report
ISO Accreditation
The Fapas proficiency testing schemes are accredited by UKAS, Proficiency Testing Provider
No. 0009.
This accreditation confirms that we comply with the requirements of International Standard
ISO/IEC 17043:2010.
In addition, Fera is accredited by other external bodies to other internationally recognised
standards including ISO 9001:2008.
Fapas (and other proficiency testing schemes) does not award accreditation. That is the
responsibility of national accreditation bodies. A list of national and international accreditation
bodies can be found at www.fasor.com/iso25. Results of proficiency testing are used by
laboratory accreditation bodies as part of the process to assess the ability of laboratories to
perform analytical tests for which accreditation is required.
29
LEAP
Fapas Water and Environmental
Agent Information
Fapas has a network of Agents to help you locally. Please contact your nearest office:
Argentina
Phone: +5411-4701-6262
E-mail: c.daiutolo@rbiopharmlat.com.ar
Armenia
Phone: +7 495 707 28 68
E-mail: pt@stylab.ru
30
Indonesia
Phone: +62 811824811
E-mail: marketing@rnd.co.id
Israel
Phone: +972572400503
E-mail: assafy@eldan.biz
Spain
Phone: +34 91.504.66.02
E-mail: info@setelsl.com
Switzerland
Phone: +49 40 49294 2930
E-mail: fapas@eurofins.de
Austria
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UK
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