Kattedan Industrial Area Remediation Plan

Andhra Pradesh Pollution Control
Board - APPCB
Kadam
En vironmental
Consultants
Consultancy Services for

Remediation of Noor Mohammed
Kunta, Kattedan Industrial Area
(KIE) in Rangareddy District,
Andhra Pradhesh
Sampling Protocol (final)
April 2012

Board - APPCB
Kadam
En vironmental
Consultants
Consultancy Services for

Remediation of Noor Mohammed
Kunta, Kattedan Industrial Area
(KIE) in Rangareddy District,
Andhra Pradhesh
Sampling Protocol (final)
April 2012
reference
project code
status
IND50-1/berr9/066
IND50-1
final version
project manager
project director
date
M. van der Wijk BSc
W. Hendriks MSc
April 11, 2011
authorisation
name
initials
approved
M. van der Wijk BSc
Witteveen+Bos India
Level 1, Midtown Building
Road No. 1, Banjara Hills
Hyderabad - 500 034
India
The Quality management system of Witteveen+Bos has been approved based on ISO 9001.
telephone +91 40 4433 4140

fax message +91 40 4433 4444
www.witteveenbos.com
Witteveen+Bos
No part of this publication may be reproduced or published by means of printing,
photocopying, microfilming or by any other means, without the prior permission of
Witteveen+Bos Consulting engineers, nor without such permission, may it be used for any
other purpose than that for which it was produced.
INDEX
P.
1. INTRODUCTION
1.1. Background
1.2. General objective of the Sampling Protocol
1.3. Time frame
1.4. Scope of the Sampling Protocol
1.5. Used guidelines
1.6. Set-up of the report
1.7. Quality system
1
1
1
2
2
2
3
3
2. GENERAL SITE DESCRIPTION

2.1. Introduction
2.2. Site description
2.2.1.
Lake NMK
2.2.2.
KIE
2.2.3.
Plains downstream
2.2.4.
STP HMD (including collector)
2.3. Geological and (geo)hydrological description
2.4. History of the site
2.5. Draft conceptual site model
5
5
5
5
6
8
8
9
11
11
3. INVESTIGATION STRATEGY
3.1. International guidelines
3.2. Handbook Soil, Groundwater and Aquatic Sediment Survey
3.3. Step by step process
15
15
15
16
4. FIELD WORK PLAN

4.1. Introduction
4.2. Inventories
4.2.1.
Present wells in the investigated area
4.2.2.
Open drains in KIE
4.2.3.
Polluting sources open areas in KIE
4.2.4.
Polluting activities at the industrial plots at KIE
4.3. Topographic survey
4.4. Field work investigation at KIE
4.4.1.
Open drains
4.4.2.
Open areas
4.4.3.
Industrial plots
4.5. Field work plan at Lake NMK
4.5.1.
Sediment Lake NMK
4.5.2.
Surface water
4.5.3.
Drillings
4.5.4.
Groundwater
4.5.5.
In- and outlets
4.5.6.
Covered dumpsite at the south western part of Lake NMK
4.6. Field work investigation at plains downstream
4.6.1.
Sediments
4.6.2.
Surface water
4.6.3.
Groundwater
4.7. Investigation carried out by APPCB
4.7.1.
Water quality of inlets Lake NMK
4.7.2.
Bio monitoring
17
17
17
17
17
18
18
19
19
19
19
20
21
21
23
23
23
24
24
24
24
24
24
25
25
25
4.8.
4.9.
Handling of samples
Field work gear
25
26
5. LABORATORY PLAN
5.1. Introduction
5.2. Laboratories
5.3. Analytical program
29
29
29
30
6. DETAILED SAMPLING AND ANALYSIS PROGRAMME
31
7. HEALTH & SAFETY PLAN

7.1. Standard procedures
7.1.1.
Introduction
7.1.2.
Training
7.1.3.
Toolbox meetings
7.1.4.
Job safety analysis - JSA
7.2. Health & Safety risks
7.3. Health & Safety gear
7.3.1.
Introduction
7.3.2.
Standard personal safety gear and hygiene
7.3.3.
Specific safety gear and hygiene
7.3.4.
Respiratory protection
7.4. Emergency plan
7.4.1.
Emergency calls
7.4.2.
Hospitals and ANGR Agricultural University
7.4.3.
First aid kit
7.5. Registration
41
41
41
41
41
41
41
45
45
45
45
45
45
45
46
46
47
8. WORK SCHEDULE AND PEOPLE INVOLVED

8.1. Time schedule
8.2. List of persons involved
49
49
49
last page
49
APPENDICES
I
Checklist site assessment for industrial sites at KIE
II
Certificates sub contractors
III
Inventory maps
IV
Sampling maps
V
Checklist field work equipment
VI
Field work forms
VII
Health & Safety forms
VIII
Additional information Health & Safety
List of abbreviations
Countries and Government institutions/structures
APPCB
Andhra Pradesh Pollution Control Board
APIIC
Andhra Pradesh Industrial Infrastructure Corporation
CPCB
Central Pollution Control Board
GoI
Government of India
HMDA
Hyderabad Metropolitan Development Authority
IMD
India Meteorological Department
MoEF
Ministry of Environment & Forests
NGRI
National Geophysical Research Institute
NPRPS
National Program for Rehabilitation of Polluted Sites
SPCS
State Pollution Control Board
Other abbreviations
CoC
Compounds of Concern
DNAPL
Dense non-aqueous phase liquid
EPA
Environmental Protection Agency
FTL
Full Tank Level
H&S
Health & Safety
m-bgl
meters below ground level
m-swl
meters below surface water level
KIA
Kattedan Industrial Area
KIE
Kattedan Industrial Estate
MLD
Million Liters per Day
NEN
Nederlandse Norm - Dutch guidelines
NMK
Noor Mohammed Kunta
OCP
Organochloro pesticides
PAH
Polycyclic Aromatic Hydrocarbons
PCB
Polychlorinated biphenyls
PSI
Preliminary site investigation
RoP
Request of Proposal
STP
Sewage Treatment Plant
SQGL
Soil Quality Guidelines Level
TDS
Total Dissolve Solids
THV
Treshold Value
TPH
Total Petroleum Hydrocarbons
VOC
Volatile organic carbons
WWTP
Wastewater Treatment Plant
1.
INTRODUCTION
1.1.
Background
General
The Ministry of Environment & Forests ([MoEF), Government of India (GoI) has received a
loan from the International Bank of Reconstruction and Development for the World Bank
aided Capacity Building for Industrial Pollution Management Project (CBIPMP) for
strengthening the environment management capacity of Central and State level regulatory
authorities with emphasis on rehabilitation of polluted sites. The Andhra Pradesh Pollution
Control Board (APPCB) which is the implementing agency for the State of Andhra Pradesh
intends to apply part of the proceeds of this loan to payment under the contract for
providing consulting services for Assessment of Contamination, Design of Remediation
Plan and Supervision of Remediation Activities for Noor Mohammed Kunta Site at
Hyderabad.
Andhra Pradesh
The APPCB has sanctioned a 2 to 3 years pilot project funded by the World Bank for two
areas, Noor Mohammed Kunta Lake (Lake NMK) in Hyderabad and a municipal dumpsite
in Ukkayapalli, Kadapa. The earlier conducted Environment and Social Assessment study
in these areas with the assistance of the ministry of environment has revealed the following
facts for the Noor Mohammed Kunta site:
- Both surface and ground water quality has deteriorated due to discharge of untreated
industrial effluents.
- Quantities of hazardous wastes are illegally dumped outside industrial estates, on
abandoned public lands, and within privately owned lands.
- There are no estimates available with the SPCB regarding the quantity and nature of
the hazardous wastes in such dumps.
- Lakes, industrial cluster areas, municipal dumping yards, and bio-medical waste sites
are considered to be the dirtiest places.
- Environmentalists and health experts say it is not an easy task to clean up the highly
polluted areas as the ground and surface water are highly contaminated as is the soil
and sediment in the lake.
- Total Dissolve Solids (TDS) in ground water samples was way above the permissible
limit of 2,000 mg/l.
- The hardness of the ground water sample was significantly higher than the desirable
limit of 300 mg/l and the permissible limit of 500 mg/l.
- Chlorides and sulphates in the ground water were in excess of the desired limits.
- The APPCB found various heavy metals in the lake water.
- Cadmium concentration exceeded desirable limits and lead and copper levels were
high.
- Bore well water in the monsoon season showed significant concentration of lead and
soil samples showed high levels of heavy metals.
1.2.
General objective of the Sampling Protocol

Based on the results of the submitted Inception Report (final) with reference IND501/berr9/065 dated 30 March 2012 and the Preliminary Site Assessment Report (final) with
reference IND50-1/berr9/067 dated 11 April 2012 this report describes the protocol and
plan elaborated during task 2 of the project towards achieving the objective as written in the
ToR:
Witteveen+Bos, IND50-1/berr9/066 final version dated April 11, 2011, Consultancy Services for Remediation of Noor Mohammed Kunta,
Kattedan Industrial Area (KIE) in Rangareddy District, Andhra Pradhesh
A detailed sampling protocol aimed at assessing the contamination level of the site and to
establish the baseline environmental status of the project area, shall be developed. The
protocol shall include parameters for analysis, sampling frequency (number of seasons),
number of samples, etc and shall be submitted for approval by APPCB.
The sampling protocol will include appropriate Health & Safety (H&S) measures. The
protocol will be the basis for Consultants activities performed during task 3 (Assessment of
Site Contamination Levels).
In addition to this protocol the Consultant will elaborate in a separate document Standard
Operational Procedures (SOPs). Those procedures will clearly present the criteria for
sampling, the methods of sampling, methods of preservation and transport to the lab and
analytical procedures / techniques to be adopted. Aforementioned procedures are based
on the below mentioned guidelines.
1.3.
Time frame
This report presents the sampling protocol for the post monsoon period
(November 2011 and January 2012). In November 2011 a major part of the proposed
sampling activities in this protocol were carried out. The remaining activities will be
conducted during the January 2012 sampling period. Were appropriate additional sampling
activities will be identified on the basis of new information and the first analytical results.
This additional activities will be discussed with the Client before actual execution and will
be reported in a separate memorandum once approved by the Client.
In a later stage, an addendum to the report will be prepared for the specific activities during
the pre monsoon period, which is foreseen to be carried out around April 2012 (addendum
II).
1.4.
Scope of the Sampling Protocol

The Sampling Protocol for the post monsoon period will in general cover the following
activities:
- Inventory of the open drains and wells at the investigated area.
- Inventory of polluting sources at the open areas of the KIE.
- Assessment of the contamination level at Lake NMK.
- Assessment of the contamination level at the open areas of the KIE.
- Assessment of the contamination level at industrial plots of the KIE.
- Assessment of the contamination level at the downstream plains.
The following activities will be included in the aforementioned addendum:
- Complete site assessment industrial plots at KIE.
- Field investigations phase January-February 2012.
- Pre monsoon field investigations (April 2012): based on the results of the investigation
during the post monsoon period.
1.5.
Used guidelines
This document is elaborated based on Dutch, Belgian and EPA/US guidelines for
environmental investigation of soil and groundwater quality, as well as for investigation of
aquatic sediments.
1.6.
Set-up of the report

Relevant data of the location (based on the results of task 0 and task 1) are summarized in
chapter 2. Chapter 3 gives an overview of the field work activities (including objectives,
sample plans and equipment). Chapter 4 describes the laboratory activities. Chapter 5
deals with H&S aspects. And finally in Chapter 6 a time schedule and resource overview in
is presented.
1.7.
Quality system
This project has been carried out by the quality system of Witteveen+Bos (as lead company
of the associated Consultants) that is ISO 9001:2000 certified.
2.
GENERAL SITE DESCRIPTION
2.1.
Introduction
In this chapter a short resume of the site description is presented based on the submitted
draft Inception Report and draft Preliminary Site Assessment Report. This preliminary
assessment in turn, is the starting point for the proposed field work and laboratory activities
in chapters 3 and 4 Necessary H&S measures are discussed in Chapter 5.
2.2.
Site description
The site can be divided into three areas:
1. KIE
2. Lake NMK
3. plains (including surrounding lakes) to the west of Lake NMK
In figure 2.1 the site is shown. In the following sections for each area a general description
is presented.
Figure 2.1.
Location
1. KIE
2. Lake NMK
3. Plains
4. Railway line (Secundarabad - Kurnool)
5. Hyderabad-Bangalore National Highway NH-7
6. Sewage Treatment Plant STP (HMDA)
2.2.1.
Lake NMK
Lake NMK is a small surface water body located in Katedan Industrial area of
Rajendranagar municipality adjoining Hyderabad city. Geographically, the lake is situated
close to the southern suburbs of Hyderabad City (7826 East longitude and 171845
North latitude). Its surface is approximately 6.2 ha and the lake has a present water depth
of 2 - 3 m (shallow).
Figure 2.2.
Lake Noor Mohammed Kunta
In topographic maps from the Survey of India (SoI), the water-spread area is measured as
8.3 ha in 1975, which is reduced to 7.6 ha as reported in 2002. However the area of the
lake is also reported as about 13.6 ha in one of the other available reports. The depth of the
lake ranges from 0.5 m in the edges to 3.5-4 m in the deepest part. Based on the
hydrographic survey conducted by APERL, the area of the water spread in 1997 has been
estimated as 7.95 ha with a maximum depth of 3.9 m, a water elevation of +98.30 and
lowest river bed level at RL +94.40. The total capacity of the lake at RL +98.30 has been
estimated as 0.1626 MCM (5.75 MCFT).
A single-lane broad railway line (Secundarabad-Kurnool) forms the eastern boundary of the
lake, whereas the western boundary of the lake is the Hyderabad-Bangalore National
Highway NH-7. On the northern boundary of the lake is a big hillock, whereas open lands
with sparse habitation form the southern boundary of the lake. The Budwel railway station
is the nearest railway station about 200 m to the south-eastern side of the lake.
The areas to the south and south-east of the lake form the catchment of Lake NMK. The
lake catchment forms part of the catchment area of the Musi River. Lake NMK has two
feeder channels. The channel running from southern-south-eastern side and joining the
lake on the eastern side is the main feeder channel. The approximate length of this stream
is about 1.6 km. The other channel joins the lake in the southern side and the length of the
stream is approximately 1.4 km. The two feeder channels separately enter the lake through
culverts under the railway at the eastern and southern sides.
2.2.2.
KIE
The lake lies in the KIE. The KIE is set up to accommodate small/medium scale industrial
units by the Andhra Pradesh Industrial Infrastructure Corporation (APIIC). There is no
public water supply in the area and the industries meet their water demand through
individual arrangements. The land use of KIE is dominated by industrial, residential,
commercial and institutional activities. In Figure 2.3 an overview of Katedan Industrial
Estate is presented.
Figure 2.3.
General view Katedan Industrial Area
In total approximately 550 industries are present in the KIE. Most of these are in smallmidscale sector and are indicated as green industries. The majority of contaminating
factories (especially textile factories and lead extraction factories) were moved away in the
90s. Most of the industries at the KIE discharge their effluent into nearby open ditches,
drains and streams (see figure 2.4). Solid waste is randomly dumped on open land along
roads and lakes (see figure 2.5). The industrial effluents contain appreciable amounts of
inorganic and organic chemicals.
Figure 2.4.
Open drains at the KIE collecting the waste water of the different
factories
Figure 2.5.
2.2.3.
Uncontrolled solid waste
Plains downstream
The western boundary of Lake NMK is the Hyderabad-Bangalore National Highway NH-7.
At the other side of this highway plains are encountered. A canal flows from the lake under
the highway towards the plains. Visually the plains consist of alluvium. At several places
bedrock appears at the surface. Figure 2.6 shows the plains at the Westside of Lake NMK.
Figure 2.6.
Plains downstream
The plains stretch in western direction until the Devullama Cheruvu, Chilan Lake and Mir
Alam tank.
2.2.4.
STP HMD (including collector)

The domestic waste water originating from the residential areas in the surroundings passes
by a pipeline to the Sewage Treatment Plant (STP) (see Figure 2.7) located next to Lake
NMK. The plant has a capacity of 4 MLD and HMDA operates the plant. It is estimated by
the Consultant and other stakeholders that between 25 and 50 % of this capacity is
currently used.
After treatment, the water is discharged into the lake. Available analysis indicate that the
contaminants in the discharged water do not exceed the permissible discharge limits put in
place for this plant (source: APPCB).
Figure 2.7.
STP - HMDA
At the eastern boundary of Lake NMK a collector (with a pump station) is situated for
domestic waste water from the residential areas. Next to the collector a highly
contaminated area with stagnant water is situated. (contaminated with heavy metals,
organics, inorganics and TPH) The area is fed by open drains containing waste water from
the KIE and incidentally also with overflow water from the collector itself.
Figure 2.8.
2.3.
Flooded area hotspot (highly contaminated) next to the collector
Geological and (geo)hydrological description

In general lithologic sections show topsoil followed by weathered rock and fractured rock
underlain by bedrock (see figure 2.10). Weathered zone thickness varies from ground level
until 10-15 m. The fracture zone has a maximum thickness of 35 m.
The groundwater occurs under phreatic conditions in the shallow weathered zone and
under semi confined to confined conditions in the fractured and sheared zones at deeper
levels.
The groundwater level measured at the existing wells is at an average of approximately 810 m-bgl. Groundwater level contours show a predominant groundwater direction towards
the Mir Alam Tank (north east, see figure 2.9). It should be mentioned that the ground
water levels and direction are influenced by local pumping conditions.
Analyses of sediments samples taken at other lakes in the surroundings (e.g.
Patercheruvu, Nallacheruvu and Peddacheruvu) show that the combined silt and clay
percentage is about 85-90 % at the bed level and 70-75 % with increase in clay content at
0.9 m. The permeability of the lakebed sediments has been found to be varying between
5.110-4 and 9.010-4 m/day.
Figure 2.9.
10
Mir Alam Tank Watershed (including ground water and cross section
A-A)
Figure 2.10.
2.4.
Geological cross section A-A
History of the site

The KIE was developed by the APIIC during the 1980s. There is no information of earlier
industrial pollution of Lake NMK and the surrounding environment (groundwater). Upon the
start of industrial activities in the KIE, pollution of surface and groundwater was observed.
The Agricultural University (located immediately downstream of Lake NMK) started
observing problems with germination and development of some of the crops on their
research fields. They started measuring water quality and concluded that considerable
pollution levels were present in the lake and groundwater, and since then filed several
complaints in order to force a solution. The KIE then consisted of various types of
industries, both polluting and non-polluting1, including lead extraction facilities and textile
industries. During the first decade of this century, APIIC commenced a re-location of
polluting industries to other industrial areas, and this resulted in a slight reduction of
general pollution levels over the last few years. At the moment it is claimed by industries as
well as APIIC that there are no polluting industries anymore operational in the KIE.
Nonetheless, illegal waste dumping and uncontrolled discharge of polluted water still can
be observed. Once these uncontrolled and illegal activities have been stopped, the project
will be foremost concerned with a remediation of historical contaminations.
2.5.
Draft conceptual site model

Based on the site visits and the gathered documents a draft conceptual site model is
elaborated using the source-pathway-receptor approach. This approach is used to identify
the possible risks of the observed contamination at Lake NMK and the KIE. Based on the
conceptual site model, the Sampling Protocol is elaborated. This Sampling Protocol will be
used for the Assessment of Site Contamination Levels (task 3).
Below, the source of the pollution, the different pathways along which the contamination
can migrate and the potential impact on the receptors are listed. Figure 2.11 shows a
general cross section of the conceptual site model for the area (1. KIE; 2. Lake NMK and 3.
downstream plains).
Although these terms are commonly used, there is no formal definition of a polluting or a non-polluting industry.
11
Figure 2.11.
12
General cross section of the conceptual site model for the area
Witteveen+Bos, IND50-1/berr9/066 final version dated April 11, 2011, Consultancy Services for Remediation of Noor Mohammed Kunta, Kattedan Industrial Area (KIE) in Rangareddy District, Andhra Pradhesh
Source
The source of the pollution is identified and described. All hazardous substances present
on site are considered as the source of pollution. The prime sources of pollution are:
- Activities at KIE
- (Solid) Waste dump site (illegal)
- Waste water
- Secondary sources of pollution
Pathways
The potential routes along which the compounds off concern can migrate from the source
of pollution to the different receptors are considered as the pathways of pollution. To
determinate potential pathways, baseline data were collected that give information about
the migration of the pollution into soil, water and air. The pollution dispersion pathways are:
- Air (smoke and dust) dispersion;
- Surface water
- Storm water - run-off
- Water collectors drains
- Groundwater
- Erosion of soil
- Plant uptake
Receptor
The potential impact on receptors is evaluated. Receptors can be defined as functions,
organisms or water bodies that could be harmed by the pollutant. In this case the impact on
receiving water bodies (surface and ground water), humans, and ecology is evaluated and
assessed. If in addition to the above mentioned receptors other relevant receptors are
present the potential impact of the pollution on these additional receptors is also evaluated
and assessed. Examples of other relevant receptors are among others archaeological
sites, historical buildings and sites important for tourism. (Re)development activities can
also introduce new receptors in the coming years. When (re)development plans are know
the impact on future receptors will be also addressed. Human and environmental receptors
are:
- Human population and domestic animals of the area and wider regional area
- Local flora and fauna
- Lake NMK, regional water and river systems
- Wind blown affected areas
Witteveen+Bos, IND50-1 draft version 01 dated November 1, 2011, Development of Sampling Protocol, Consultancy SerVIces for Remediation
of Noor Mohammad Kunta, Kattedan Industrial Area (KIE) in Rangareddy District, Andhra Pradesh
13
14
3.
INVESTIGATION STRATEGY
3.1.
International guidelines
To elaborate the sampling protocol and the investigation strategy several guidelines are
used which are presented in table 3.1.
Table 3.1.
Overview guidelines sampling protocol and investigation strategy
country
code
title
the Netherlands
NEN5720
Investigation of the environmental quality of sediments.
NEN5717
Strategy for preliminary investigation prior to sediment

investigation.
NEN5740
Investigation of the environmental quality of soil and soil

lots.
NEN5725
Strategy for preliminary investigation prior to exploratory

and main survey.
Belgium
Investigation of the environmental quality of sediments.
Decree on soil remediation and soil protection (October

11th, 2006).
Investigation of the environmental quality of soil and
groundwater.
USA
Contaminated
Sediment
Remediation
Guidance
for
Hazardous Waste Sites - EPA.
EPA/600/R-92/12
Preparation
of
Soil
Sampling
Protocols:
Sampling
Techniques and Strategies.
3.2.
Handbook Soil, Groundwater and Aquatic Sediment Survey

In a separate handbook the Standard Operational Procedures (SOPs) for Soil,
Groundwater & Aquatic Sediment Surveys are presented. This document is elaborated on
the basis of Dutch, Belgian and EPA/US guidelines for environmental investigation of soil
and groundwater quality, as well as for investigation of aquatic sediments.
Aforementioned handbook is set-up in such a way that it can be expanded to cover an
increasing number of aspects of environmental, soil, groundwater and sediment
investigations. It is therefore a living document that can be expanded and amended, based
on experiences gained during both projects.
This separate handbook provides technical guidance for the Consultants field staff, the
APPCB and other relevant Authorities in order to: (a) ensure quality of sampling, (b) ensure
uniformity, and (c) to allow for effective assessment of fieldwork quality.
15
Oktober November 2011
Main input:
Preliminary site assessment &
Inception report
January-February 2012
Step by step process
Main input:
CoCs, Inventory of wells, surface
drains and common areas in the
KIE
Premonsoon - April 2012
3.3.
Main input:
Pollution sources, site
assessments & selection of
possible hotspots
INITIAL INVESTIGATION
Main output:
Determine the critical
parameters; the Compounds of
Concern (CoCs)
INVESTIGATION PHASE I
Main output:
Determine the main sources of
pollution and pollution levels
INVESTIGATION PHASE II
Main output:
Detailed assessment of pollution
sources
Direct input for:

(1) Final overall CSM for the KIE and Lake NMK and downstream plains &
(2) CSMs for selected hotspots &
(3) Basis for remediation strategy and KIE management plan
16
4.
FIELD WORK PLAN
4.1.
Introduction
Based on the international guidelines and the conceptual site model presented in chapter 2,
a Sampling Protocol is elaborated to obtain more information on the different sources of
contamination, the different pathways present and finally the most important receptors
within the investigated area. Chapter 4 presents the field work activities (for the post
monsoon period) and chapter 5 the analytical tests of the Sampling Protocol.
The field work activities start with a first set of sampling. After these preliminary samples
have been analysed, the Sampling Protocol will be finalised and further executed. The
basic plan is described in this chapter. Sections 4.4 till 4.6 describe the field work activities
whereas in chapter 6 a detailed overview is given of the field work activities in a table
format.
Further, the sampling gear that will be used during the field investigation is explained. At
this stage of the project only manual sampling gear will be used. Based on the results of
the activities in November 2011, it will be decided if mechanical gear is required.
4.2.
Inventories
Before starting the field work activities, the following inventories have to be carried out:
- Present wells in the investigated area
- Open drains in KIE
- Polluting sources open areas in KIE
- Polluting activities at the industrial plots in KIE
4.2.1.
Present wells in the investigated area

The preliminary site investigation showed 119 registered wells to be present within the
project area:
- 98 bore wells equipped with electric submergible pumps
- 14 bore wells equipped with hand pumps
- 7 dug wells
Most of the wells equipped with submergible pumps are mainly used for industrial purpose,
but some are also used for domestic purposes except the wells at the Agricultural
University campus. All wells equipped with hand pumps and dug wells are for domestic
purposes. These wells will be used to investigate the groundwater levels and the
groundwater contamination in the area. Appendix III presents an inventory map for the
available wells.
4.2.2.
Open drains in KIE

In KIE several open drains are present containing waste water from industrial and other
activities at the estate. The following aspects of the open drains will be evaluated during the
inventory:
- Exact location
- Design and length
- Flow direction of the water
- Type of drain
- Visual contamination
17
Based on the inventory of the open drains at KIE, surface water and sediments of the open
drains will be investigated (see paragraph 4.3). Appendix III presents an inventory map for
the open drains in the estate. This map is based on the inventory map of the open drains
received by the APIIC during task 1.
4.2.3.
Polluting sources open areas in KIE

Several polluting sources are identified within the open (public) areas of KIE. During the
site visits of task 1. solid waste was found at many locations. Electrical transformers that
may be a source of PCB contamination are present as well at KIE.
The aforementioned polluting sources will be inventorised on the following aspects:
- Type of polluting source
- Type of contamination
- The exact location
- The amount of contamination
Based on the inventory of the polluting sources at KIE, a specific drilling program will be
performed (see paragraph 4.3). Appendix III presents an inventory map for this.
4.2.4.
Polluting activities at the industrial plots at KIE

Approximately 550 plots are present at KIE. They have various kinds of activities. A list of
these activities is submitted in the Preliminary Site Assessment report.
The Consultant will train staff members of APPCB to perform site assessments of individual
plots, as part of the capacity building program. The staff will be trained how to gather data,
perform a site inspection and report the results. Furthermore, staff will be trained in
assessing and evaluating the reported data for individual plots. Finally, staff will be trained
in site comparison and development of a priority list.
In November 2011 the staff will receive the training in site assessment methodology and
approach. In Appendix I a format of the checklist for site assessment of industrial sites at
KIE is presented.
Per site, a short report will be prepared containing the results of the site assessment and
evaluation. The standard field inspection report will be attached to this report.
A representative of the Consultant will perform a review of the site assessment progress in
the earlier stages of the work.
Once reports for the assessed plots are available, the Consultant will perform a final check
on a number of plots in the field. After this final check, senior staff members will compare
site assessment results and propose the final category and priority for each site (site
comparison and development of a priority list). Aspects as historical and current activities,
type of pollutant and amount of pollutant will form the criteria in order to prioritise the
industrial plots. As a result of the investigations the Client and the Consultant will be able to
prepare a priority list of individual plots, resulting in a shortlist of plots where further
investigation or remediation is deemed necessary.
18
Based on the shortlist, several plots will be selected for which a sampling plan will be
elaborated and implemented. These sampling plans are not yet included in this sampling
protocol and will be submitted in an addendum.
During the inception visit already two plots have been selected in consultation with APPCB.
Based on the historical activities at KIE, the main polluting activities were textile factories
and lead extraction factories. The factories were moved away and the sites are now either
abandoned or used as storage place. Because of the historical aspects the two following
representative sites haven been selected in consultation with APPCB to be included in this
sampling protocol and the subsequent field investigation:
- Plot nr. 44: former lead extraction factory
- Plot nr. 46: former textile factory
A specific drilling program will be performed at these plots (see paragraph 4.4.3). In
Appendix IV site investigation maps are submitted for both plots.
4.3.
Topographic survey
During the field work activities at each drilling point, the X, Y, Z coordinates will be
determined by GPS. Based on these data the elevation at the investigated area will be
determined.
At the moment of writing of this report the Consultant is verifying the licenses in order to
execute the topographic survey with an unmanned airplane, using a digital camera and
software to generate an ortho photo of the site and a digital terrain model.
4.4.
Field work investigation at KIE

In this section a description is given of the field work activities at KIE. In chapter 6 a
detailed overview of the field work activities at the KIE is presented. Appendix IV presents
the sampling plan.
4.4.1.
Open drains
After the inventory of the open drains in KIE (see paragraph 4.2), a selection will be made
of the open drains that will be investigated based on following criteria:
- Direction flow: flowing to Lake NMK
- Level of contamination (visually)
- Representativeness for KIE
In total approximately ten open drains will be selected where following investigation will be
performed:
- Sampling surface water
- Sampling sediments
4.4.2.
Open areas
Public areas along the roads, hillocks and open spaces
During the inventory (see paragraph 4.2) of the open areas, at several locations top soil
samples will be collected (approximately 0.5 m-bgl) along the roads, hillocks and open
spaces. The exact locations of the drillings will depend on the results of the inventory, but
the focus will be directed towards the visually contaminated sources.
19
After the inventory of the existing deep wells, in total four representative wells will be
selected for groundwater sampling at the first aquifer. In order to assess the ground water
flow direction, the ground water level at the first aquifer will be measured. These deep wells
will be representative for the whole KIE area.
Stagnant water is present at the biggest hillock. A sample of this surface water will be
taken.
Pool with stagnant waste water bordering the Collector pump unit
Nearby the Collector a low laying area with stagnant waste water is present. This stagnant
water is highly contaminated (visual monitoring). Based on the preliminary sampling, also
the sediment is highly contaminated with heavy metals, organics and TPH. At the pool with
stagnant water, the following activities will be performed in order to assess the level of
contamination:
- Sampling surface water
- Sampling sediments
- Sampling plant material (plant uptake of pollutants - especially heavy metals
- Installation of two piezometers and subsequent ground water sampling: in order to
assess the level of contamination in the ground water
When during field investigation visually contaminated samples are encountered, the
visually contaminated sample will not be mixed in the mixed sample, but will be separately
investigated.
Downstream, along the border of Lake NMK four shallow piezometers will be placed in
order to verify if pollution is flowing from KIE to Lake NMK.
4.4.3.
Industrial plots
As mentioned in paragraph 4.4. the investigation at the industrial plots is not included in this
Sampling Protocol. Before investigation of the industrial plots, a site assessment will be
executed by APPCB as part of the capacity building. A training program will be elaborated
by the Consultant, for field investigations at the following selected locations:
- Plot nr. 44: former lead extraction factory
- Plot nr. 46: former textile factory
Former lead extraction factory
In order to assess the level of contamination, drillings will be performed at the former lead
extraction factory. Due to the former activities it is to be expected that especially heavy
metals are the pollutants of concern and will be present in the topsoil. In appendix IV a
sampling map is presented.
The sampling strategy is based on the NEN5740 (Dutch guidelines): location expected to
be contaminated, contamination homogenous. Because of very site specific conditions
(shallow soil layer above rock layers) the amount of drillings, depth and the exact location
of the drillings are adapted to those conditions.
Former textile factory
In order to assess the level of contamination a number of topsoil drillings (0.5 m-bgl) ( (in
total 7) will be performed at the former textile factory. The field investigation will especially
focus at the former waste water treatment plant. Three drillings until 0.5 m-bgl (topsoil) will
be placed here.
20
The sampling strategy is based on the NEN5740 (Dutch guidelines): location expected to
be contaminated, contamination heterogenous. Because of very site specific conditions
(shallow soil layer above rock layers) the amount of drillings, depth and the exact location
of the drillings are adapted to those conditions.
Due to the former activities it is to be expected that especially chlorinated solvents and
heavy metals are the pollutants of concern. Based on the characteristics of these pollutants
of concern, it is expected that the heavy metals will be present in the top soil and in the
groundwater. Based on the characteristics of chlorinated solvents, it is expected that they
are mainly present in the groundwater and in the soil air (highly volatile). Regarding the
groundwater the chlorinated solvents have the tendency to migrate to the deeper
groundwater layers due to their high specific density and can form there DNAPLs (dense
non aqueous phase liquids). In order to assess the ground water contamination at this
stage one existing deep well will be selected and sampled. The obtained groundwater
sample will be analysed. When during drilling chlorinated volatiles are detected, a soil air
sample will be taken. In appendix IV a sampling map is presented.
4.5.
Field work plan at Lake NMK

In this chapter a description is given of the field work activities at Lake NMK. In Chapter 6 a
detailed overview is given of the field work activities at Lake NMK. In appendix IV the
sampling plan is shown.
4.5.1.
Sediment Lake NMK

Sampling strategy sediments
The most important aspects that have to be determined during the field investigation of
sediments are:
- The amount of samples to be sampled and the amount of mixed samples
- The thickness of the layer(s) to be sampled
- The sampling density
- The Compounds of Concern (CoCs) to be analysed
The sampling strategy depends on the objective of the investigation, the type of waterbody
and the investigation effort. These aspects are determined during phase 1.
As well as a variety of water bodies and its different characteristics, there is a variety of
sampling strategies described in international guidelines. For Lake NMK the sampling
strategy water bodies, non-linear and normal investigation effort is applicable (table 4.1.Dutch guideline NEN5720). In table 4.2. the sampling strategy is submitted for sediment
sampling at Lake NMK.
Table 4.1.
Sampling strategy waterbodies, non-linear and normal investigation

effort (e.g. Lake)
Strategy
Amount of subarea
Activities
a)
am = 2 x A
where:
A the total surface area of the location in ha
am the amount of subarea
Amount of drillings
6 per subarea
21
Strategy
Activities
Maximum length of the subarea
Not applicable
Layer to be sampled
The layer to be dredged;
Contaminated sediment layer;
The non-contaminated layer (approximately until 50 cm below the

contaminated sediment layer)
Compounds of Concern - CoCs
b)
Dry matter
Organic matter
Clay fraction
TPH
PAH
Heavy metals
PCBs (polychlorinated biphenyls) and OCPs

(organochloropesticides)
a)
For each subarea minimum 1 mixed sample for analysis
b)
Applicable in the Netherlands, Belgium and USA, for Indian sediment investigations the CoCs still have to be
determined
Table 4.2.
Sampling strategy Lake Noor Mohammed (total surface area of 6.6 ha)
Strategy
Activities
Amount of subarea
am = 2 x 6.6
where:
A the total surface area of the location in ha
am the amount of subarea
am = 5.13
Amount of drillings
6 per subarea: 6 x 5.13 32 drillings
Maximum length of the subarea
Not applicable
Layer to be sampled
Based on the available data of the Lake NMK sampling is carried

out at two depths:
-
Sediment (appr. 0-20 cm thickness);
Soil layer below the sediment
Minimum amount of mixed samples
Compounds of Concern - CoCs
Dry matter
Organic matter
Clay fraction
TPH
PAH
Heavy metals
22
Spatial distribution of subareas and drilling points

Before the field work activities, a sampling map has to be elaborated where the locations of
the drilling points are visualised. Before the drilling points are located, the spatial
distribution of the subareas have to be elaborated. Its preferable that the subareas are
equal in size, but this depends on the characteristics of the waterbodies. The drilling points
are placed in a grid with an equal distribution pattern (e.g. cross sections). It is important to
mention that based on the results of the site assessment (see Chapter 2) the positions of
the sampling pattern is finally selected. This means that with motivation the equally
distributed pattern doesnt have to be followed.
Field work activities
By means of a pontoon (see figure 4.3.) and a piston sampler, sediment sampling will be
performed in a grid of approximately 50 m by 50 m. The sampling strategy and the
proposed grid provide a basis to obtain five longitudinal and six latitudal cross sections.
Based on the cross sections, the total volume of (contaminated) sediment present at Lake
NMK will be estimated. In total the lake will be divided in four quadrants based on the site
specific conditions.
Drilling will be performed until about 0.5 m below the contaminated sediment. It is expected
that two consecutive layers are present:
- A contaminated sediment layer formed during the polluting activities in the 1990s.
- The original sediment/soil layer.
These two layers will be sampled and analyzed (including the width of each layer). When
during field investigation visually contaminated samples are encountered, the visually
contaminated sample will not be mixed in the mixed sample, but will be separately
investigated.
Special attention will be given to the area direct downstream of the spot with the stagnant
highly contaminated water in KIE. At the Lake NMK separate samples will be taken to verify
if there is an influence from the stagnant water in KIE on the sediment and water quality of
Lake NMK.
Furthermore it is expected that at the outlet of the STP more sediments will be present than
the rest of Lake NMK, although in minor levels because the STP has been opened in 2009.
4.5.2.
Surface water
At three different places of Lake NMK the surface water will be sampled at two different
depths, at the surface and at a deeper depth just above the sediments.
4.5.3.
Drillings
Along the shores of Lake NMK several drillings will be placed to a depth approximately 2.0
m-bgl in order to assess the level of the contamination at the boundaries of Lake NMK.
4.5.4.
Groundwater
After the inventory of the present deep wells, one representative well will be selected for
ground water sampling at the first aquifer. In order to assess the groundwater flow
direction, the groundwater level at the first aquifer will be measured.
23
At the border with KIE two shallow piezometers will be placed in order to verify if pollution is
flowing from KIE to Lake NMK. At the border with the downstream plains two shallow
piezometers will be placed in order to verify if pollution is flowing from Lake NMK to the
plains downstream. Based on preliminary sampling, the water level is to be estimated at
approximately 1.0 m-bgl.
4.5.5.
In- and outlets

Surface water samples will be taken in order to investigate the water quality of the two
inlets to Lake NMK, one coming from the STP (outlet STP) and one coming from a
residential area. The water quality of the outlet has been already analysed during the
preliminary sampling.
4.5.6.
Covered dumpsite at the south western part of Lake NMK

Estimated amount of solid waste present and level of contamination
In the past a part in the southwest of Lake NMK has been filled by solid waste (uncontrolled
dump site). After the dumping activities, the dumpsite has been covered with a soil layer
and the STP has been constructed. Five drillings will be carried out in order to estimate the
type and quantity of waste and pollution present.
Groundwater
In order to investigate the influence of the covered dump site on the water quality of Lake
NMK, a piezometer will be placed between the waste dump and the lake in order to identify
the groundwater quality.
4.6.
Field work investigation at plains downstream

An open drain originating from Lake NMK passes the plains downstream. This open drain
is the main pathway towards the plains downstream and will be at this stage investigated.
4.6.1.
Sediments
By means of a piston sampler, sediment sampling in the open drain will be performed at
four different locations. Drilling will be performed until at least 0.5 m below the
contaminated sediment. It is expected that three consecutive layers are present:
- A highly contaminated sediment layer formed during the polluting activities in the
1990s.
- The original sediment/soil layer.
These two layers will be sampled and analyzed (including the width of each layer).
4.6.2.
Surface water
At four different places in the open drain, the surface water will be sampled and analysed to
verify the water quality and the influence of Lake NMK.
4.6.3.
Groundwater
Four representative wells will be selected for groundwater sampling at the first aquifer. In
order to assess the groundwater flow direction, the groundwater level at the first aquifer will
be measured. These deep wells will be representative for the whole KIE area.
24
At the border with Lake NMK two shallow piezometers will be placed in order to verify if
pollution is flowing from Lake NMK to the plains downstream. Furthermore two shallow
piezometers will be placed along the open drain to assess the potential influence of the
pollutants at the open drain.
4.7.
Investigation carried out by APPCB
4.7.1.
Water quality of inlets Lake NMK

One of the crucial preconditions before carrying out the remediation activities is that the
waste water coming from KIE is collected and treated before discharging the water into
Lake NMK.
As known the STP of HMDA is present and can be used for treatment of the waste water
coming from KIE. In order to design the treatment of the waste water, APPCB will verify the
quality of the waste water coming from the open drains in KIE by analysing the water on
several indicative parameters (pH, Total Suspended Solids, Total Dissolved Solids,
Chlorides, Sulphates, COD, BOD and heavy metals).
APPCB is recommended to assess and evaluate the proper functioning of the STP through
monitoring and measuring.
4.7.2.
Bio monitoring
In order to evaluate the results of the remediation activities (task 6) biological life will be
monitored before and after the remediation. Therefore several plant species,
phytoplankton, crustacean and invertebrates will be monitored carrying out laboratory
activities and ecological studies on site.
4.8.
Handling of samples
In the separate document presenting the SOPs the appropriate handling of samples is
presented.
Soil and sediment samples
Samples which are collected with the piston sampler or the auger will be spread out on
plastic sheets or a plastic gutter where separation of soil or sediments takes place. The
sample will be marked with references to the place where the sample was taken. From
every sample a borehole description will be made according the field work form as shown
in appendix VI. Cross contamination will be prevented by cleaning used equipment after
every sampling with clean tap water from jerry cans.
Other samples
Groundwater, surface water and plant samples will be marked with reference to the place
where the sample was taken. A visual description of each sample will be made. The
samples will be put into bottles or plastic bags.
Storage and transportation
The samples which are collected will be stored and cooled preferably in a refrigerator at
temperatures of 4-8 C. The collected samples in the field will be temporarily stored in cool
boxes for transport to the storage facilities. The samples will be transported to the
laboratory in weekly batches.
25
4.9.
Field work gear

During the field work gear will be used as shown in table 4.3. Figures 4.1 and 4.2. present
the sampling gear for manual drilling is presented (piston sampler and auger). At this stage
only manual drilling will be performed and no mechanical drilling.
Table 4.3.
Field work activities
1. Sampling gear
Auger (manual drilling and soil sampling) (see figure 4.2.)
Piston sampler (sediment sampling) (see figure 4.1.)
Pumping device (ground water sampling)
2. Handling samples
Sediment / soil containers (bags/bottles)
Buckets for mixing samples
Plastic (several m)
Cooling device for samples
Half pipe
3. Measure instruments
Measure device water level Lake NMK
Measure device water level Piezometers/Wells
GPS system
Measuring tape / rule
4. Others
Pontoon (see figure 4.3.)
Figure 4.1.
26
Piston sampler - sediment sampling
Figure 4.2.
Auger shallow drillings
Figure 4.3 presents the pontoon is presented which will be used during the field work
activities at Lake NMK.
Figure 4.3.
Pontoon - investigation Lake NMK
27
28
5.
LABORATORY PLAN
5.1.
Introduction
In this chapter the laboratory activities are described for the post-monsoon period. The
different labs that will be used for the analyses are defined and also when the different
laboratories will be used. The main part of this chapter is dedicated to the analysis program
for KIE, Lake NMK and the downstream plains.
5.2.
Laboratories
The samples will be analysed by different laboratories as presented in table 5.1. The Indian
laboratories are acknowledged by MoEF. The international laboratories are NEN-ENISO/IEC 17025 accredited. In appendix II an overview is given of the certificates for
accreditation of the different laboratories.
Table 5.1.
Overview laboratories
Laboratory
Address
Accreditation
Analysis
Vimta Lab
M/s. Vimta Labs Ltd.
National Accreditation Board for
Heavy metals (Pb, Cd, Cr, Zn, Hg,
142, Industrial
Laboratories
Cu, Ni, As), mineral oil, chlorinated
Development Authority,
MoEF (see appendix II)
solvents, PAH, pH, Conductivity,
Cheralapally
TSS, TDS, Cl, SO4, PO4, NO3,
Hyderabad - 500 051
COD, BOD, DO, oil and grease
Analytico
PO Box 459
NEN-EN-ISO/IEC 17025 (see
Environment
NL-3770 Barneveld
appendix II)
All above mentioned

parameters: cross-verification /
AL -Netherlands
split samples;
-
TerrAttest (see below);
Pesticides, PCBs and OCPs.
Vimta Lab
For the majority of the samples and the parameters either Vimta Lab in Hyderabad or
Eurofins in The Netherlands will be used. Vimta Lab is acknowledged by MoEF as a
gazette laboratory under the Environment Protection Act. Eurofins is a Dutch accredited
laboratory.
Analytico Environment - Eurofins
For the purposes of ensuring cross-verification of selected results, various samples will be
analysed by Analytico Environment (Eurofins) in the Netherlands. Analytico Environment
(Eurofins) is NEN-EN-ISO/IEC 17025 accredited.
Also this laboratory will be used in order to analyse the samples on TerrAttest.
TerrAttesT offers a complete soil research formula, giving the possibility of issuing wellfounded statements concerning the nature and degree of environmental contamination in
soil and water samples. For TerrAttesT the laboratory Eurofins Analytico environmental
research laboratory uses the most advanced analytical techniques for the direct
quantitative measurement of over 200 chemical compounds(characterisation parameters,
metals, aromatic compounds, phenols, PAH, volatile halogenated hydrocarbons,
chlorobenzenes, chlorophenols, PCB, other chlorohydrocarbons, pesticides, herbicides and
fungicides and TPH). Additional testing due to the results of screening parameters is
therefore no longer required.
29
APPCB Central Lab

In agreement with APPCB, the laboratory activities during Task 3 (Field investigation) will
not be performed by APPCB Central Lab (see Inception Report). The APPCB Central Lab
will work independently, collecting samples (also split samples) and analysing these
samples during the field investigation (task 3) in order to verify the results of the
Consortium. Furthermore the APPCB Central Lab will carry out following specific
investigations:
- Water quality inlet 2 - KIE
- Biomonitoring
The results of these investigations will be included in the reports which the Consultant will
prepare in task 3 (Site investigation report) and task 4 (Remediation plan).
5.3.
Analytical program
In chapter 6 an overview is given of the analytical program for the initial investigation phase
(November 2011). The analytical program for the next investigation phases (year 2012) will
be elaborated based on the analytical results of the initial investigation phase.
30
6.
DETAILED SAMPLING AND ANALYSIS PROGRAMME

Coding samples
explanation drilling activity / sampling
code
shallow drilling and soil sampling
piezometer and shallow ground water sampling
(deep)well and first aquifer sampling
DW
sediment sampling
SS
surface water sampling
SW
mixed sample
MS
In this chapter 6 the total overview of the field work activities for the initial phase (November
2011) and for the next phases (year 2012) is submitted.
31
Phase
Zone
Initial
Lake NMK
Investigation
Sampling equipment
Pontoon
Sample bottles (prepared)
Samples
Parameters for analysis
Type
Numbers
Surface water
At two depths:
(Mixed) samples
6x (pH, EC, TSS, TDS, Cl-,
SO4, PO4, NO3, COD, BOD,
SW2-1 till SW2-3
dissolved
(November
oxygen,
heavy
metals, TPH)
2011)
SW2-4
and
SW2-5
(near two inlets)

dissolved
oxygen,
heavy
metals, TPH)
Lake NMK
Manually operated piston

sampler
Pontoon
Sample jars
Aquatic sediment
SS2-1 till SS2-32
See
table
mixed
samples below
8x (heavy metals and As,

PAH, Oil & Grease, volatile
aromatics
clay
(BTEX),
fraction
and
PCBs,
organic
matter, texture, dry matter)

Lake NMK
Mechanically operated auger

drill or
Manually operated Edelmandrill and
Possible piston sampler
Piezometer material
Groundwater
At the dumpsite near
1x (pH, EC, heavy metals,
the STP:
SO4,
P2-1
chlorinated solvents)
At the side of the KIE:
P2-2 and P2-3
SO4,
PO4,
PO4,
NO3,
NO3,
TPH,
TPH,
At
the
downstream
side:
P2-4 and P2-5
SO4,
DW2-1
PO4,
NO3,
TPH,
Lake NMK
Lake NMK
32
Making use of existing wells

and boreholes
drill or
Manually operated Edelmandrill
Groundwater
TPH, chlorinated solvents)

Soil
At the dumpsite near
4x (heavy metals, PAH, TPH,
the STP:
S2-1 till S2-5
2x soil texture + organic
Sample jars
matter
Around
areas;
KIE; common areas; stagnant
KIE;
common
groundwater
water

and boreholes
the
lake
(fringes):
pesticides and PCBs)
S2-6 till S2-10
1x texture
Groundwater
DW1-1 till DW1-3
3x TerrAttest
Surface water
SW1-3

dissolved
oxygen,
heavy
metals, TPH)
KIE; surface water drains

sampler
Sample jars
Aquatic sediment
SS1-4 till SS1-10

2x texture
1x TerrAttest
Surface water
SW1-4 till SW1-10

dissolved
oxygen,
heavy
metals, TPH)
1x TerrAttest
KIE;
surface
water
drains;
nearby the Collector
Surface water

sampler
Sample jars
Aquatic sediment
SW1-1 and SW1-2
6x (pH, TSS, TDS, Cl-, SO4,

COD, BOD, heavy metals,
TPH)
KIE;
surface
water
drains;
SS1-1 till SS1-3
See
table
mixed
samples below
2x (heavy metals and As,

PAH, Oil & Grease, volatile
aromatics
clay
(BTEX),
fraction
and
PCBs,
organic
matter, texture, dry matter)

KIE;
surface
water
drains;

drill or
Groundwater
P1-1 and P1-2

SO4,
PO4,
NO3,
Witteveen+Bos, IND50-1 draft version 01 dated November 1, 2011, Development of Sampling Protocol, Consultancy SerVIces for Remediation of Noor Mohammad Kunta, Kattedan Industrial Area (KIE) in Rangareddy District,
Andhra Pradesh
33
TPH,
Downstream
plains
(at AU
premises)
Piezometer material

Piezometer material
Groundwater
Upstream; at the side
of the NMK:
SO4,
P3-1 and P3-2
Nearby
the
PO4,
NO3,
TPH,
open
drain:
P3-3 and P3-4
Downstream
(at AU
drains (at AU
plains
premises)
Downstream
premises)
Groundwater

and boreholes
sampler
Sample jars
Surface water
DW3-1 and DW3-2

TPH, chlorinated solvents)
Aquatic sediment
SS3-1 till SS3-4

1x granulometry
Downstream
drains (at AU
premises)
SW3-1 till SW3-4

dissolved
oxygen,
heavy
metals, TPH)
Investigation
KIE; common areas
phase I
(January-

drill or
Sample jars
Soil
S1-1 till S1-60
5x TPH
5x dry matter
5x clay and organic matter
4x soil texture
February 2012)
3x PCBs (transformers)
10x heavy metals (8 metals
total) (incl. preparation)
4x TerrAttest
5x PAH
areas;
KIE;
common
groundwater
34
Make use of existing wells and

boreholes
Groundwater
To be determined
Surface water
To be determined
Water
Aquatic sediment
To be determined

sampler
Sample jars
Surface water
To be determined
KIE;
drains;
Surface water
To be determined
drains;
Aquatic sediment
To be determined
drains;

sampler
Sample jars
drill or
Piezometer material
drill or
Sample jars
Groundwater
To be determined
Soil
At textile factory: S1
till S7
surface
water

KIE;
surface
water

KIE;
surface
water
KIE; selected hotspots
2x soil texture and organic

matter
3x
TPH
sampling
analyzing
(in
case
of
soil
on
odour,
air
and
chlorinated
solvents)
At lead factory:
S1 till S3

1x soil texture and organic
matter

drill or
Piezometer material
Groundwater
At textile factory:
1x TerrAttest (incl. chlorinated
DW1-4
solvents)
Andhra Pradesh
35
Downstream
plains
(at AU
plains
(at AU
drains (at AU
lake
premises)
Downstream
premises)
Downstream
premises)
Downstream
Investigation
(at
AU
premises)
KIE; common areas
phase II
(April 2012)
KIE;
common
areas;
groundwater

water
Soil
To be determined
Groundwater
To be determined
Aquatic sediment
To be determined
Aquatic sediment
To be determined

drill or
Sample jars
drill or
Piezometer material
Soil
To be determined
Groundwater
To be determined
Surface water
To be determined
Aquatic sediment
To be determined
Surface water
To be determined

sampler
Sample jars
KIE;
drains;
Surface water
To be determined
drains;
Aquatic sediment
To be determined
drains;

sampler
Sample jars
drill or
Groundwater
To be determined
surface
water

KIE;
surface
water

KIE;
surface
water
36

Sample jars
Piezometer material
sampler
Sample jars
sampler
Pontoon
Sample jars
Downstream
(at AU
(at AU
drains (at AU
lake
plains
premises)
Downstream
plains
premises)
Downstream
premises)
Downstream
premises)
(at
AU

Piezometer material
drill or
Sample jars
drill or
Piezometer material
Sample jars
Piezometer material
sampler
Sample jars
sampler
Pontoon
Sample jars
Soil
To be determined
Groundwater
To be determined
Soil
To be determined
Groundwater
To be determined
Aquatic sediment
To be determined
Aquatic sediment
To be determined
Andhra Pradesh
37
Analytical program mixed samples the initial investigation phase (November 2011)
When during field investigation visually contaminated samples are encountered, the visually contaminated sample will not be mixed in the mixed sample,
but will be separately investigated.
Zone
Lake NMK
(Mixed)
Sample
samples
type
MS1
Aquatic
Sample number including depth (m-swl or m-bgl)
Motivation
Parameters for analysis
SS2-2, SS2-7, SS2-13
Mixed sludge sample second quadrant near outlet
Heavy metals and As, PAH, Oil &
STP, water depth 3-4 meter, no distinct layers
Grease, volatile aromatics (BTEX),
observed
PCBs,
sediment
clay
fraction
and
organic
matter, texture, dry matter

MS2
Aquatic
SS2-6, SS2-11, SS2-12
sediment
MS3
Aquatic
SS2-3, SS2-8, SS2-9, SS2-15
sediment
Mixed sludge sample second quadrant near outlet
STP, water depth 1-2 meter, no distinct layers
observed
PCBs, dry matter
Mixed sludge sample first quadrant near outlet
plains downstream, water depth 3-4 meter, no
distinct layers observed
PCBs,
clay
fraction
and
organic

MS4
Aquatic
SS2-5, SS2-10, SS2-14, SS2-16
sediment
MS5
Aquatic
SS2-17, SS2-18, SS2-19
sediment
Mixed sludge sample first quadrant near outlet
plains downstream, water depth 2-3 meter, no
PCBs, dry matter
Mixed sludge sample third quadrant near inlet
southwest corner, water depth 1-2 meter, no
PCBs,
clay
fraction
and
organic

MS6
Aquatic
SS2-24, SS2-25, SS2-29
sediment
MS7
Aquatic
sediment
SS2-21, SS2-22, SS2-27, SS2-32
Mixed sludge sample third quadrant near inlet
southwest corner, water depth 0-1 meter, no
PCBs, dry matter
Mixed sludge sample fourth quadrant near inlet
stagnant water KIE, water depth 2-3 meter, no
PCBs,
clay
fraction
and
38
organic
KIE
MS8
Aquatic
SS1-2, SS1-3
sediment
Mixed sludge sample (first layer) stagnating water
near collector

PCBs, dry matter
MS9
Aquatic
sediment
SS1-2, SS1-3
Mixed sediment sample (second layer) stagnating
water near collector

PCBs, dry matter
clarification layers:
water depth 0-1 m
water depth 1-2 m
water depth 2-3 m
water depth 3-4 m
Andhra Pradesh
39
40
7.
HEALTH & SAFETY PLAN
7.1.
Standard procedures
7.1.1.
Introduction
The safety and hygienic measures will be carried out in accordance with the Dutch safety
guidelines for field work investigation.
7.1.2.
Training
When people first come to the site, they receive information about the site hazards and the
steps that have been taken to control the risks. All employees have to be competent and
trained for the job. They have to use agreed methods to do the work en use suitable and
safe equipment.
Before starting the field work investigation a brief training will be given to each member of
the field team and to the people of the APPCB. A document for the training will be
submitted by the Consultant at the start of the field investigation.
7.1.3.
Toolbox meetings
Before starting each new day of field work, a toolbox meeting will be carried out by the
leader of the survey team. During these toolbox meetings safety procedures will be
explained to each member of the field team. Also discussions will be performed to improve
the health and safety aspects during the field investigation. A format of the toolbox meeting
is shown in appendix VI. Also the format for the register of attendance for each working day
is submitted in appendix VI.
7.1.4.
Job safety analysis - JSA

A Job Safety Analysis (JSA) is a method that is used to identify, analyze and record the
steps involved in performing for the investigation activities, the existing or potential safety
and health hazards associated with the investigation activities, and finally the
recommended action(s)/procedure(s) that will eliminate or reduce these hazards and the
risk of a workplace injury or illness.
7.2.
Health & Safety risks

In table 7.1 a complete overview is given of the most important health and safety risks
which are present at the investigated sites. Subsequently for each health and safety risk,
an overview is given of the preventive and mitigating measures.
41
Table 7.1.
Overview H&S risks and preventive measurements
Item
Comments
Preventive measures during field work activities
Mitigating measures
General risks of
drilling and sampling
The site consists of slopes, (possibility of)
- Set up a drilling plan before implementation
First aid kit, emergency call or
unstable
- Mark dangerous spots on the site
on land and water
presence of animals, etc. with risks of falling,
hospital
soil,
rough
terrain,
vegetation,
slipping, tripping, being hit by equipment
- Awareness is very important. Each toolbox meeting (carried out each day
before starting the field work activities) will be focused on the awareness on
the specific site conditions
- The field worker need to use personal protection equipment (PPE)
Pollutants
several
pollutants, in soil, sediments, ground water
The
site
is
contaminated
with
before starting the field work activities) will be focused on the awareness of
and surface water
the presence of the hazardous waste and pollutants

hospital

- By visible dust: use a protective dust mask
- Youth and pregnant women are not allowed on the site
- Proper cleaning procedure of equipment and clothing
- Good personal hygiene
- Facilities to wash hands and face
- Eating, drinking and health stop after washing hands and face
- Dont smoke
- Treat the samples properly and wear also protective clothing
Field work activities at
The water level at Lake NMK is maximum 4.0
Lake NMK
m (at the deepest point). The investigation at

Lake NMK will be carried out by means of a
pontoon
- The pontoon will be provided with a hard board at the bottom which enables
standing straight in the boat (necessary for sampling)

hospital
- At least three men will be on the dinghy: in case somebody falls in the water,
at least two men will be able to drag the person out of the water
- All men on board will be carrying a life jacket
- During the sampling at least one field worker will be present onshore and keep
eye contact in case of emergency
- In windy conditions the pontoon will be kept in place by placing several poles
Waste
(solid
waste water)
and
At the site on different locations, solid waste is
present and waste water flows into open
drains through the investigation area. During

task 1 e.g. not only municipal solid waste, but
42
Emergency
call
and/or
hospital
the presence of the hazardous waste and pollutants

Item
Comments
Also medical waste.
- Youth and pregnant women are not allowed on the site
Pathogens and
At the site some locations are encountered
bacterias
where sewage water and dead animals is
present. These location are a source for

several pathogens and bacterias
Mitigating measures
Emergency
call
and/or
call
and/or
hospital
the presence of pathogens and bacterias;

- The field worker need to use personal protection equipment (PPE);
- Youth and pregnant women are not allowed on the site.
Diseases
In general several diseases can be present at
- Each disease has its own preventive measures.
Emergency
the investigation area. The most important
Malaria:
hospital
diseases are:
Take an antimalarial drug such as mefloquine, atovaquone/Proguanil, or
- Malaria
doxycycline. Also take measures to prevent against mosquito bites (insect
- Dengue fever
repelent).
- Hepatitis A and B
Dengue fever:
- Typhoid
There aren't any drugs available to prevent the virus. As it's transmitted via
- Tetanus
mosquitoes, wear a strong insect repellent containing DEET to prevent getting

bitten.
Hepatitis A and , Typhoid and Tetanus:
Vaccination.
Flora and fauna
Several snakes and scorpions are present that

are poisonous or dangerous:
- Ptyas mucosus - Rat Snake
- Naja naja - Indian Cobra
- Vipera russelli - Russells Viper
- Bungarus caeruleus - Common Krait
When a field worker has a
bite from a poisonous snake,
the presence of the dangerous animals.
scorpion or other animal, the
- Set up emergency plan (incl. the fastest route to antidote) (see paragraph
5.4.).
hospital
or
Acharya
NG
Ranga Agricultural University

will
be
contacted
(see
- Eryx Conica - Indian Sand Boa (not
Emergency plan paragraph
venomous)
5.4.)
- several scorpions
In order to recognize the poisonous snake
some photos and additional information are
submitted in appendix VIII.
Dust
Wind can occur during the site investigation.

During the dry season this can provoke dust.
- Protection to possible fine dust a cup-shape respirator will be used.

hospital
Andhra Pradesh
43
Item
Comments
Mitigating measures
Climate conditions
The main issue is the sun and the warmth.
During the investigation on Lake NMK, the sun
before starting the field work activities) will be focused on the awareness on
rays will be reflected by the water so the effect
the specific climate conditions
will be enhanced.
hospital
- Sun protection (sun block and a hat)

- The field work activities will start as early as possible (approximately 05.00 06.00 am)
- Sufficient breaks
- Sufficient shade will be provided by placing a refugee
- Drinking water will be present
Language and
awareness
Working with people with multiple nationalities
- Safety instructions translated at least in English
Instruct fiedworkers
- Check if fieldworker understands the given safety information by asking

questions. With safety site-inspections management is able to verify the
working method and the use of needed safety measures and ppe
44
7.3.
Health & Safety gear
7.3.1.
Introduction
Based on the abovementioned health and safety risks in this chapter a brief description of
the health and safety equipment is described to prevent contact with pollutants. This
chapter has the following subdivision:
- Standard personal health and safety gear - PPE
- Specific health and safety gear
7.3.2.
Standard personal safety gear and hygiene

During the field work every team member will be wearing his / her personal protection
equipment (PPE). This personal protection equipment consists of:
- Safety boots / shoes
- Safety glasses
- Safety helmet
- Gloves
- Overall
Water and soap will be on site for hygienic purposes. Everyone who works on the site must
have access to adequate toilet and washing facilities, a place for preparing and consuming
refreshments and somewhere for storing and drying clothing and personal protective
equipment.
Welfare facilities should be easily available to people working on the site. Toilets need to be
easily accessible from where the work is being done. Washing facilities should be as close
as possible to the toilets.
7.3.3.
Specific safety gear and hygiene

During the field work several specific health and safety gear will be present at the site and
will be used when necessary, This equipment consists of:
- Respiratory protection: cup-shape respirator
- Life saving vests: to be used during the investigation at Lake NMK
7.3.4.
Respiratory protection
Wind can occur during the site investigation. During the dry season this can provoke dust.
When blowing of dust is visible the fieldworkers have to wear a cup-shape respirator.
7.4.
Emergency plan
7.4.1.
Emergency calls
In case of emergency during the field work activities, an emergency call will be performed
The 108 Emergency Response Services is a free 24/7 emergency service for providing
integrated medical, police and fire emergency services. The service is provided in Public
Private Partnership between State Government and GVK Emergency Management and
Research Institute.
45
When an emergency is reported through 1-0-8, the call taker gathers the needed basic
information and dispatches appropriate services. Basic information obtained includes:
- Where the call is placed from (District/Mandal/City/Town/exact location/landmark)
- The type of emergency
- The number of people injured and the condition of the injured
- The callers name and contact number for location guidance if required
Emergency help dispatched through this process is expected to reach the site of the
emergency in an average of 18 minutes. Pre-hospital care will be given to patients being
transported to the nearest hospital.
Table 7.2 shows other relevant phone numbers.
Table 7.2.
7.4.2.
Relevant phone numbers in case of an emergency
Police
100 or 2611
Medical
102,1298,108,112,2611
Fire
101 or 2611
Hospitals and ANGR Agricultural University

In the centre of Hyderabad hospital Nizam Institute of Medical Sciences, Erramanzil will be
used in case of mayor injuries. It takes approximately 1 hour to get to the hospital. When a
snake bite occurs, the fastest way to get an antidote is to contact the Acharya NG Ranga
Agricultural University. The University has anti venom and in less then 15 minutes
(depending on the exact location when the investigation takes place) an antidote can be
given.
During the field investigation a route map for evacuation will be present at the site
indicating the fastest way to got to the hospital or the university.
Table 7.3.
Relevant phone numbers hospitals and ANGR Agricultural University
Hospital in Hyderabad city
Nizam Institute of Medical Sciences,

Erramanzil
+91 40-23489000
Care Hospital, Banjara Hills
Sarojinidevi Eye Hospital, Mehadipatnam
+91 40-23608262
Acharya NG Ranga Agricultural University (special for anti

venom)
+91 99 480 43 048 (cell)
- Dr. K. Jeevan Rao;
+91 98 49 28 16 08 (cell)
- Dr. S.A. Hussain.
7.4.3.
First aid kit

During the field investigation a first aid kit will be always present for treatment of minor
injuries. The first aid kit includes adhesive bandages, regular strength pain medication,
gauze and low grade disinfectant.
46
7.5.
Registration
Each day a daily report will be developed with following dates:
- Names of field workers
- Time of start and end of field work investigation
- Climate conditions (like estimated temperature, wind direction and speed)
- Conducted activities
In appendix VI an example of a daily report is enclosed.
47
48
8.
WORK SCHEDULE AND PEOPLE INVOLVED
8.1.
Time schedule
For the initial phase the sampling will start on November 1, 2011. The duration of the
sampling is estimated at 14 working days. For a more detailed time schedule of the initial
phase please see Table 8.1. For the next investigation phases (carried out in 2012) a
detailed time schedule will be submitted to the Client.
Table 8.1.
Time schedule
Working day
Preparations start work
Inventory:
10
11
12
13
14
existing wells
open drains KIE
polluting sources open
areas KIE
Field work investigation KIE
Field work investigation
Lake NMK
Field work investigation
plains downstream
Preparations departure
8.2.
List of persons involved

In the table below the names of persons involved and their function are listed.
Table 8.2.
Sampling team
company
name
Witteveen+Bos
Mr. Jan Jacob Stolte
function
Leader of survey team
Kadam
Mr. Mahendra Jadhav
Chief Field Chemist
Kadam
Mr. Jabir Syed
Field Chemist
Kadam
Mr. Parag Shah
Field Investigator
49
APPENDIX I
CHECKLIST SITE ASSESSMENT FOR INDUSTRIAL SITES AT KIE
Witteveen+Bos, appendix I to report IND50-1/berr9/066 dated April 11, 2011
Witteveen+Bos, appendix I to report IND50-1/berr9/066 dated April 11, 2011

Board - APPCB
Kadam
Environmental
Consultants
Site assessment Checklist for

industrial sites at the Kattedan
Industrial Estate

Board - APPCB
Kadam
Environmental
Consultants
Site assessment Checklist for

industrial sites at the Kattedan
Industrial Estate
reference
project code
status
IND50-1/berr9/043
IND50-1
draft version 01
project manager
project director
date
M. van der Wijk BSc
W. Hendriks Msc
December 8, 2011
authorisation
name
initials
approved
M. van der Wijk BSc
Witteveen+Bos India
Hyderabad - 500 034
India
The Quality management system of Witteveen+Bos has been approved based on ISO 9001.
telephone +91 40 4433 4140
fax message +91 40 4433 4444
Witteveen+Bos
No part of this publication may be reproduced or published by means of printing,
photocopying, microfilming or by any other means, without the prior permission of
Witteveen+Bos Consulting engineers, nor without such permission, may it be used for any
other purpose than that for which it was produced.
INDEX
P.
1. GENERAL INFORMATION
2. SITE DESCRIPTION
3. SOIL AND GROUNDWATER QUALITY
4. MISCELLANEOUS
11
5. SITE PLAN
13
6. DRAFT CONCEPTUAL SITE MODEL
15
7. INITIAL CONCLUSION
17
8. PHOTOGRAPHIC RECORD
19
last page
19
APPENDICES
-
number of pages.
Introduction
This document is a checklist issued by the Consultant to the APPCB in the project
Remediation of Lake Noor Mohammed Kunta in the Kattedan Industrial Estate,
Hyderabad. The answers in this checklist are provided by the assessor. This assessment is
specifically designed to provide a complete overview of soil and groundwater quality
aspects at the industrial site, and to relate these to soil and groundwater issues (risks).
This checklist relates to the site assessment of [name of company on site, site #] in the
Kattedan Industrial Estate (KIE), Hyderabad, India. The assessment was undertaken
through document review, a site visit, and interviews with key personnel of [name of
company on site].
The assessor was [name assessor] and the assessment was completed on [date].
PLEASE NOTE: ALL INFORMATION GATHERED IS CONFIDENTIAL!
Witteveen+Bos, IND50-1/berr9/043 draft version 01 dated December 8, 2011, Site assessment Checklist for industrial sites at the Kattedan
Industrial Estate
Industrial Estate
1.
GENERAL INFORMATION
1.1
1.2
1.3
Site number (cadastral number)

Site name (company name)
Date site visit
Assessor(s)
Assessee(s)/Interviewee(s)
1.4
Site Address & contact details
1.9
1.10
Cadastral number
GPS coordinates
Elevation (by GPS) in m above sea level
Please provide site plans (e.g. site lay-out plan, etc)
Age of plant/site (date current operation commenced)
Total number of years of this operation
Is there still on-site activity?
Name of site owner
Name of previous owner(s)
1.11
1.12
Number of employees working at the site

Past use of site (Give summary of previous owners,
1.5
1.6
1.7
1.8
dates and type of operations, hazardous materials used,

comments; identify previous risky operations at adjacent
properties, if any)
1.13
History of waste disposal, spills or leakage of

materials or waste on-site or inside the
production premises
Industrial Estate
1.14
Current operations on site
(Note: Provide flow charts, briefly describe the process, and list
products, list quantities of produced products, list raw materials used, and indicate period of each
process)
Process/operation
Years
1.15
Discontinued operations and date operations ceased
Date ceased
1.16
Previous soil & groundwater quality investigations

that may have been conducted
1.17
What are the available data / hours to visit the site?
1.18
Are there safety measures required by the owner of

the site? If so, which safety measures? Are there
any known dangers which a visitor should be aware
of like instable buildings and structures, toxic liquids,
holes etc.
1.19
Is there a permission to visit / investigate the whole

site?
Year
Industrial Estate
2.
SITE DESCRIPTION
2.1
Total surface area of the site (m2)
2.2
Built-up area (m2)
2.3
Outdoor pavement type (concrete, asphalt, brick,

concrete blocks or sheets, gravel, etc)
2.4
Non-paved areas (grass, trees, bush, bare soil, other)
2.5
Stressed vegetation observed? (yes/no; elaborate
2.6
Is there information on present underground civil

structures of former facilities or residues of
construction rubble; e.g. concrete foundations,
further on where stressed vegetation was observed)
sewages etc.?
2.7
Are there lay-out maps and flow-chart schemes

of the site available? (if so, attach these)
Is the site easily accessible?
Surroundings of the Industry:
North
East
South
West
2.8
How is the geology (general description)?
2.9
Are there (deep) wells or boreholes present

nearby (e.g. for drink water extraction)?
What are the drainage patterns?
2.10
2.11
In which direction is the flow of groundwater,

surface water, etc.?
2.12
Is there surface water run-off present?
2.13
Groundwater depth (m below ground level)
Industrial Estate
Industrial Estate
3.
SOIL AND GROUNDWATER QUALITY

Expected pollutants on-site
3.1
What are the identified potential

pollutants?
3.2
How are the potential pollutants used,

stored and disposed off (e.g. stock, tanks,
piles, tailings, waste disposal, etc.)?
3.3
What are the sources of pollution? (e.g.

storage tanks, filling points, fuel stations,
transformers, machines, specific plant
components like ovens, degreasing
machines etc.)
3.4
Is there visual evidence of possible risks

for pollutants to infiltrate and percolate into
the soil (threatening the environment; e.g.
groundwater, surface water, etc.)?
3.5
What is the chemical composition of the

potential pollutant or of the mix of potential
pollutants?
3.6
What can be stated regarding the mobility

of the potential pollutant?
What can be stated regarding the toxicity
of the potential pollutant?
3.7
Industrial Estate
3.8
3.9
In what quantity (volume or weight) and in

what form (stored in bags, in tanks, in
drums, in bulk/silage, etc) is the potential
pollutant present on-site?
What is the specific location of the
potential hazard (stock, tanks, piles,
tailings, etc.) on the site? (Indicate on the site
plan if available, or draw a sketch)
3.10
3.11
3.12
Are there any known dumpsites (of

chemical waste, construction waste,
domestic waste, etc) present?
Since when is the potential pollutant
already present at the site?
List the storage tanks present above
ground
3.13
List the storage tanks present below

ground
3.14
Quantity and type of solid waste generated
3.15
Solid waste disposal practices and

mechanisms
3.16
Describe the waste water that is generated

on-site (e.g. domestic or industrial effluent,
approximate quantity, etc)
3.17
Describe the waste water discharge

practices (i.e. how is it disposed off?)
3.18
Are any water or waste water analysis

reports available please indicate
Industrial Estate
Level of contamination observations using senses (sight and smell)

3.19
What is the level (intensity) of visible

contamination on buildings and
infrastructure? (e.g. fresh contamination, light
spots or clear saturation of concrete, etc)
3.20
What is the size (quantity) of visible

contamination on buildings and
infrastructure? (e.g. small spots, whole areas,
square meters, etc.)
3.21
What is the level (intensity) of visible soil

contamination? (e.g. clear signs of significant
pollutions like saturated soils, floating layers on
open / standing water, etc)
3.22
What is the scale of visible soil

contamination? (e.g. small spots, whole areas,
square meters, etc.)
3.23
3.24
3.25
3.26
Are there indications of groundwater

pollution; e.g. smelling wells.
If yes, what is the level (intensity) of
groundwater contamination (if noticable)?
surface water contamination?

aquatic sediment contamination (e.g.
existing ponds, flows, in open drains,
etc.)?
What is the known / noticable (smell) air
quality at the site?
3.27
What is the estimated surface / volume of

the contamination?
3.28
Is the present contamination local (hot

spot) or diffuse?
Industrial Estate
10
Industrial Estate
4.
MISCELLANEOUS
4.1
List any other pending complaints, claims, liabilities, non-compliances, and other relevant
matters related to soil and groundwater pollution aspects
Industrial Estate
11
12
Industrial Estate
5.
SITE PLAN
Please provide a sketch of the sites lay-out (include at least main occurrences and main
sources and pathways of pollution):
Industrial Estate
13
14
Industrial Estate
6.
DRAFT CONCEPTUAL SITE MODEL

Please provide a sketch of the sites Conceptual Site Model:
Industrial Estate
15
16
Industrial Estate
7.
INITIAL CONCLUSION
Please provide your initial conclusions:
Category of the site
(1 non-suspect, 2 suspect,
highly suspect
hotspot):
&
Motivation (base yourself on the information gathered, and motivate in terms of

3 presence and use of potential contaminants, level of on-site waste management, level
potential of treatment of effluents, spilling incidents, obvious signs of pollution, duration of

polluting operations, presence of environmental management practices and
measures, etc):
Motivation (base yourself on the information gathered, and motivate in terms of

Priority of the site
(1 low priority, 2 medium humane risks like contact of sensitive receptors with hazardous substances,
priority, 3 high priority):
ecological risks like spread of pollution via groundwater flows, ongoing pollution or
historic pollution, etc):
Industrial Estate
17
18
Industrial Estate
8.
PHOTOGRAPHIC RECORD
Please include several photos that best illustrate the soil and groundwater quality related
aspects and issues:
Industrial Estate
19
APPENDIX II
CERTIFICATES SUB CONTRACTORS
Witteveen+Bos, appendix II to report IND50-1/berr9/066 dated April 11, 2011
Witteveen+Bos, appendix II to report IND50-1/berr9/066 dated April 11, 2011
Form A - TRP1
01/2004
ISSUED TO:
KADAM ENVIRONMENTAL CONSULTANTS
871/B/3, Near Himalaya Machinery
GIDC Makarpura
KIND ATTN: Mr. JA Rathi General Manager
Sample Particulars:
Report Number
:
Issue Date
: xxxx-xx-xx
Your Ref
: TRF
and Date
: 2011-12-05
13953/11/VLL/000/xxx
WATER SAMPLES
Page2 of 2
Sample Received Date : 2011-12-02

Sample Registration Date: 2011-12-05
xxxx-xx-xx
Analysis Starting date: 2011-12-07
Analysis Completion date:
Sample particulars: Surface Water Samples
Quantity received:
Sample is Coded as : SW-1
& SW-2
Tests required: pH, EC, TSS, TDS, Cl, SO4, PO4, NO3, COD, BOD, DO, O &G, Pb, Cd, Cr, Zn, Hg,Cu, Ni, As, BTEX, Chlorinated Solvents;
SAMPLE TESTED AS RECEIVED
LAB REFERENCE: EC
TEST RESULTS
Sl. No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
Parameter
pH
Electrical Conductivity at 25C
Total Suspended Solids at 105C
Total Suspended Solids at 180C
Chloride as Cl
Sulphate as SO4
Phosphate as PO4
Nitrate as NO3
Chemical Oxygen Demand
Biochemical Oxygen Demand
Dissolved Oxygen
Oil & Grease
Lead as Pb
Cadmium as Cd
Chromium as Cr
Zinc as Zn
Mercury as Hg
Copper as Cu
Nickel as Ni
Arsenic as As
BTEX
Chlorinated Solvents
Unit
s/cm
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Method of Testing
SM 4500 H+ B
SM 2510 B
SM 2540 D
SM 2540 C
SM 4500-Cl
SM 4500-SO4 E
SM 4500-PO4 D
SM 4500-NO3
SM 5220
IS : 3025, Part-44
SM 4500-O-C
SM 5520 B
SM 3125
SM 3125
SM 3125
SM 3125
EPA 200.8
SM 3125
SM 3125
SM 3125
USEPA 8260
USEPA 8260
SW-1
SW-2
Remarks: Instrument used: Inductively Coupled Plasma Mass Spectrometer (ICP-MS) Make: Agilent, GC-MS (Varian) & AAS, Make: Thermo.
E.Shyam Sundar
Vice President - Environment
Form A - TRP1
01/2004
ISSUED TO:
GIDC Makarpura
Sample Particulars:
Report Number
:
Issue Date
: xxxx-xx-xx
Your Ref
: TRF
and Date
: 2011-12-05
13953/11/VLL/000/xxx
WATER SAMPLES
Page2 of 2

xxxx-xx-xx
Sample particulars: Ground Water Samples
Quantity received:
Sample is Coded as : GW-1
& GW-2
Tests required: pH, EC, TSS, TDS, Cl, SO4, PO4, NO3, COD, BOD, DO, O &G, Pb, Cd, Cr, Zn, Hg,Cu, Ni, As, BTEX, Chlorinated Solvents;
LAB REFERENCE: EC
TEST RESULTS
Sl. No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
Parameter
pH
Electrical Conductivity at 25C
Sulphate as SO4
Phosphate as PO4
Nitrate as NO3
Oil & Grease
Lead as Pb
Cadmium as Cd
Chromium as Cr
Zinc as Zn
Mercury as Hg
Copper as Cu
Nickel as Ni
Arsenic as As
BTEX
Unit
s/cm
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Method of Testing
SM 4500 H+ B
SM 2510 B
SM 4500-SO4 E
SM 4500-PO4 D
SM 4500-NO3
SM 5520 B
SM 3125
SM 3125
SM 3125
SM 3125
EPA 200.8
SM 3125
SM 3125
SM 3125
USEPA 8260
USEPA 8260
GW-1
GW-2
Remarks: Instrument used: Inductively Coupled Plasma Mass Spectrometer (ICP-MS) Make: Agilent, GC-MS (Varian) & AAS, Make: Thermo.
E.Shyam Sundar
Form A - TRP1
01/2004
ISSUED TO:
GIDC Makarpura
Sample Particulars:
Report Number
:
Issue Date
: xxxx-xx-xx
Your Ref
: TRF
and Date
: 2011-12-05
13953/11/VLL/000/xxx
SEDIMENT SAMPLES
Page2 of 2

xxxx-xx-xx
Sample particulars: SEDIMENT SAMPLES
Quantity received:
Sample is Coded as : SS-1
Tests required: Pb, Cd, Cr, Zn, Hg,Cu, Ni, As, BTEX,PAH, PCB, Clay fraction, Oil & Grease, Texture and Dry matter;
LAB REFERENCE: EC
TEST RESULTS
Sl. No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Parameter
Lead as Pb
Cadmium as Cd
Chromium as Cr
Zinc as Zn
Mercury as Hg
Copper as Cu
Nickel as Ni
Arsenic as As
BTEX
Polynuclear Aromatic
Hydrocarbons
Polychlorinated Biphenyls
Oil and Grease
Clay Fraction
Texture
Dry Matter
Unit
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Method of Testing
ASTM D 5198
ASTM D 5198
ASTM D 5198
ASTM D 5198
USEPA 3050B
ASTM D 5198
ASTM D 5198
ASTM D 5198
USEPA 8260 B
USEPA 8310
mg/kg
mg/kg
%
USEPA 8082
USEPA 9071 B
SSSA
SSSA
ASTM Method
SS-1
SS-2
Remarks: Instrument used: Inductively Coupled Plasma Atomic Emission Spectrometer (ICP-AES) Make: VARIAN, Model- VISTA
GC-MS ( Varian), GC-MS-MS ( Waters Quatro macro-mass) & AAS, Make : Thermo.
E.Shyam Sundar
Form A - TRP1
01/2004
ISSUED TO:
GIDC Makarpura
Sample Particulars:
Report Number
:
Issue Date
: xxxx-xx-xx
Your Ref
: TRF
and Date
: 2011-12-05
13953/11/VLL/000/xxx
SOIL SAMPLES

Sample particulars: SOIL SAMPLES
Page2 of 2
xxxx-xx-xx
Quantity received:
Sample is Coded as : S-1
& S-2
Tests required: Pb, Cd, Cr, Zn, Hg, Cu, Ni, As, Chlorinated solvents, PAH, PCB, Clay fraction, Oil & Grease, Texture and Dry matter;
LAB REFERENCE: EC
TEST RESULTS
Sl. No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Parameter
Lead as Pb
Cadmium as Cd
Chromium as Cr
Zinc as Zn
Mercury as Hg
Copper as Cu
Nickel as Ni
Arsenic as As
Polynuclear Aromatic
Hydrocarbons
Polychlorinated Biphenyls
Oil and Grease
Clay Fraction
Texture
Dry Matter
Unit
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Method of Testing
ASTM D 5198
ASTM D 5198
ASTM D 5198
ASTM D 5198
USEPA 3050B
ASTM D 5198
ASTM D 5198
ASTM D 5198
USEPA 8260
USEPA 8310
mg/kg
mg/kg
%
USEPA 8082
USEPA 9071 B
As per SSSA
As per SSSA
ASTM Method
Soil-1
Soil-2
Remarks: Instrument used: Inductively Coupled Plasma Atomic Emission Spectrometer (ICP-AES) Make: VARIAN, Model- VISTA
GC-MS ( Varian), GC-MS-MS ( Waters Quatro macro-mass) & AAS, Make : Thermo.
E.Shyam Sundar
Appendix to ISO/IEC 17025 accreditation certificate

number: L 010
of
Eurofins Analytico B.V.

Barneveld
Valid from: 17-05-2011 till 01-04-2013
Nr.
Material or
product
Replaces appendix dated: 01-04-2011
Type of activity / investigation method
Internal
reference number
Inorganic analysis (physical-chemical)

1
Field-moist soil
Determination of dry matter content; gravimetry
W0104
equivalent to NEN-ISO 11465
Sludge and
sediment
Wastewater
Determination of the total residue on evaporation after

drying; gravimetry
W0104
equivalent to NEN-EN 12880
W0113
in accordance with NEN 6499
and in accordance with
NEN-EN 15216
Sediment
Determination of the density; gravimetry
W0114
in house method
Soil and
sediment
Determination of clay content and the particle size

distribution; sieve and pipette
W0105 and W0173
Soil and
sediment
Determination of the particle size distribution; laser

diffraction
W0174
in accordance with ISO 13320-1

(pre-treatment in accordance with
ISO 11277)
Soil and
sediment
Determination of clay content; laser diffraction
W0176
(pre-treatment in accordance with
ISO 11277)
Soil
Wastewater
Determination of organic matter content;

loss-on-ignition method
W0109
Determination of the total residue on evaporation;

W0113
in accordance with
NEN 6499 and NEN-EN 12879
This annex has been approved by:
Ir. J.C. van der Poel

Chief Executive
Page 1 of 38

number: L 010
of

Barneveld
Valid from: 17-05-2011 till 01-04-2013
Nr.
10
11
12
Material or
product
Internal
reference number
Sludge and
sediment
Determination of the total residue on evaporation;

W0109
Soil
Determination of the content of carbonates, expressed as

calcium carbonate (calcite); volumetry
W0177
Determination of clay content; sieve and pipette
W0171
Sand and clay
equivalent to NEN-EN 12879
equivalent to NEN-ISO 10693
equivalent to NEN 5753
13
Drinking water
and surface
water
Determination of the content of suspended solids and its

ignition residue; gravimetry
W0552
NEN 6484
14
Wastewater
and sludge
Determination of the content of suspended solids and its

ignition residue; gravimetry
W0552
and equivalent to NEN 6621
15
16
Wastewater,
drinking water,
groundwater
and surface
water
Determination of the content of suspended solids; gravimetry W0587
Wastewater
Determination of the fat content; gravimetry

NEN-EN 872
W0555
in house method
17
Wastewater
Determination of the amount of settleable solids
and mixtures of
sludge/water
W0558
in accordance with
NEN 6623
Inorganic analysis (classical chemical)

18
19
Wastewater,
drinking water,
groundwater,
water from
boiler plants,
surface water
and seawater
Determination of electrical conductivity; conductometry
Soil and
sediment
W0506
in accordance with
NEN-ISO 7888
W0506
Page 2 of 38

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of

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Valid from: 17-05-2011 till 01-04-2013

Nr.
Material or
product
20
Wastewater,
drinking water,
groundwater,
water from
boiler plants,
surface water
and seawater
Determination of pH; potentiometry
(Sewage)
sludge
21
Internal
reference number
W0524
in accordance with
NEN-ISO 10523
W0524
in accordance with
NEN-EN 12176
22
Soil and
sediment
Determination of pH-CaCl 2 and pH-KCl; potentiometry
W0524
in accordance with
NEN-ISO 10390
23
24
25
26
27
Wastewater,
drinking water
and
groundwater
Determination of the content of fluoride; potentiometry
Wastewater,
groundwater
and
surface water
Determination of biochemical oxygen demand
Wastewater,
drinking water,
groundwater,
water from
boiler plants,
surface water,
seawater and
(sewage)
sludge
Determination of chemical oxygen demand; titrimetry
Drinking water
and water from
boiler plants
Determination of permanganate index; titrimetry
Wastewater
and
groundwater
Determination of permanganate index; titrimetry
W0546
W0556
in accordance with
NEN-EN 1899-1 and
NEN-ISO 5814 (EN 25814)
W0553
in accordance with
NEN 6633 (2006) and
NEN 6633/A1 (2007)
W0508
in accordance with
NEN-EN-ISO 8467
W0508
in house method
(analysis in accordance with
NEN-EN-ISO 8467)
Page 3 of 38

number: L 010
of

Barneveld
Valid from: 17-05-2011 till 01-04-2013

Nr.
28
Material or
product
Water from
boiler plants
Determination of the alkalinity (the P- and M-number);

titrimetry
Internal
reference number
W0545
in accordance with
NEN-EN-ISO 9963-1
29
30
Wastewater
and
groundwater
Determination of the total alkalinity (M-number); titrimetry
Wastewater,
drinking water
and surface
water
Determination of Kjeldahl nitrogen; spectrophotometry
W0545
in accordance with
NEN-EN-ISO 9963-1
W0554
in house method
(mineralization in accordance with
NEN-ISO 5663 and analysis in
accordance with NEN 6604)
31
32
33
34
Wastewater,
groundwater
and water from
boiler plants
Determination of the content of monomeric silicate;

spectrometry
W0561
Wastewater,
drinking water
and
groundwater
Determination of the content of anionic surfactants;

spectrometry
W0578
Wastewater,
drinking water,
groundwater
and surface
water
Determination of the content of total cyanide and free

cyanide; continuous flow analysis and spectrometry
W0517
Soil
Determination of the content of total cyanide and free

cyanide; continuous flow analysis and spectrometry
in accordance with NF T90-007
in accordance with WAC/III/D/040
in accordance with
NEN-EN-ISO 14403
W0117 and W0517

in accordance with
NEN-ISO 17380
35
36
Wastewater,
groundwater,
water from
boiler plants
and surface
water
Determination of the content of sulphate; continuous flow

analysis and spectrometry
Wastewater,
groundwater
and surface
water
Determination of phenol index; continuous flow analysis and

spectrometry
W0522
in accordance with
NEN 6654 (1992)
W0544
in accordance with
NEN-EN-ISO 14402
Page 4 of 38

number: L 010
of

Barneveld
Valid from: 17-05-2011 till 01-04-2013

Nr.
37
Material or
product
Eluates

spectrometry
Internal
reference number
W0544
in accordance with
NEN-EN 13370 and in
accordance with
NEN-EN-ISO 14402
38
Soil and
building
materials

spectrometry
W0544
in house method
NEN-EN-ISO 14402)
39
40
41
42
Wastewater,
drinking water,
groundwater,
water from
boiler plants
and surface
water
Determination of the content of ions; discrete analysis and

spectrometry
Groundwater
Determination of the content of dissolved anions; liquid

chromatography of ions
W0504
chloride, bromide, sulphate, nitrite, nitrate and fluoride
NEN-EN-ISO 10304-1
Determination of the content of dissolved anions; liquid

W0504
chloride, bromide, sulphate and fluoride
NEN-EN-ISO 10304-1
Determination of the content of chromium VI; liquid

W0588
Eluates
Groundwater
and eluates
W0566
ammonium, chloride, nitrate, nitrite and ortho-phosphate
in accordance with
in accordance with
in house method
NEN-EN 15192)
Page 5 of 38

number: L 010
of

Barneveld
Valid from: 17-05-2011 till 01-04-2013

Nr.
Material or
product
Internal
reference number
Inorganic analysis (element determinations)

43
Soil, sediment
and destruates
of solid
matrices
Determination of the content of elements; inductively

coupled plasma with mass spectrometry
W0107, W0420 and

W0423
aluminium, antimony, arsenic, barium, cadmium, calcium, chromium,
in accordance with
phosphor, potassium, cobalt, copper, mercury, lead, magnesium,
NEN-EN-ISO 17294-2
manganese, molybdenum, sodium, nickel, selenium, tin, vanadium, iron and (digestion in accordance with
44
Soil, sediment
and destruates
of solid
matrices
zinc
NEN 6961)

W0107, W0420 and

W0423
titanium and sulphur
in accordance with
NEN-EN-ISO 17294-2
(in house digestion-method)
45
Wastewater
and surface
water

W0108 and W0425
aluminium, antimony, arsenic, barium, beryllium, boron, cadmium, calcium,
NEN-EN-ISO 17294-2
chromium, phosphor, potassium, cobalt, copper, mercury, lead,
digestion in accordance with
in accordance with
magnesium, manganese, molybdenum, sodium, nickel, selenium, strontium, NEN 6961)

tellurium, thallium, tin, vanadium, iron, silver and zinc
46

W0108 and W0425
cerium, titanium and sulphur
NEN-EN-ISO 17294-2
in accordance with
(in house digestion-method)
47
Groundwater
and eluates

W0420 and W0421
aluminium, antimony, arsenic, beryllium, barium, cadmium, calcium,
NEN-EN-ISO 17294-2
in accordance with
chromium, potassium, cobalt, copper, mercury, lead, magnesium,

manganese, molybdenum, sodium, nickel, selenium, tin, titanium,
vanadium, iron and zinc
48
Wastewater,
drinking water,
groundwater,
water from
boiler plants,
surface water,
seawater and
(sewage)
sludge
Determination of the total hardness; inductively coupled

plasma with mass spectrometry
W0108, W0420, W0421

and W0425
in house method
Page 6 of 38

number: L 010
of

Barneveld
Valid from: 17-05-2011 till 01-04-2013

Nr.
Material or
product
Internal
reference number
Organic analysis
49
50
51
52
Soil and
sediment
Determination of the halogen content originated from nonvolatile with acetone and petroleum ether extractable
organohalogen compounds (EOX); microcoulometry
W0120, W0132 and

W0351
Drinking water,
groundwater
and surface
water
Determination of the halogen content derived from nonvolatile, with petroleum ether extractable organohalogen
compounds (EOX); microcoulometry
W0130 and W0351
Wastewater
Determination of the content of petroleum ether extractable

organically bound halogens (EOX-AW); microcoulometry
W0130 and W0351
Determination of the halogen content derived from volatile

organohalogen compounds (VOX); microcoulometry
W0354
Wastewater
and
groundwater
in house method
in house method
in house method
(sample preservation in house
method, analysis in accordance
with NEN 6401)
53
Soil and
sediment
Determination of the hydrocarbon oil index; gas

chromatography with flame-ionisation detection
W0120, W0132 and

W0202
in house method
54
55
Wastewater,
drinking water,
groundwater
and surface
water
Determination of the hydrocarbon oil index; large volume

injection gas chromatography with flame-ionisation
detection
W0123 and W0215

W0123 and W0215
in house method
in accordance with
NEN-EN-ISO 9377-2
56
57
58
Soil
Determination of the content of volatile hydrocarbons

(fraction C6-C12); gas chromatography with flame-ionisation
detection
W0136 and W0216
Wastewater,
drinking water,
groundwater
and surface
water
Determination of the content of volatile hydrocarbons

(fraction C6-C12); gas chromatography with flame-ionisation
detection
W0122 and W0216
Soil
Determination of the aromatic fraction, the aliphatic fraction

and the content of total petroleum hydrocarbons (TPH); gas
W6161 and W6261
in house method
in house method
in house method
Page 7 of 38

number: L 010
of

Barneveld
Valid from: 17-05-2011 till 01-04-2013

Nr.
59
60
Material or
product
Groundwater
Wastewater,
drinking water,
groundwater
and surface
water
Internal
reference number
Determination of the aromatic fraction, the aliphatic fraction

and the content of total petroleum hydrocarbons (TPH); gas
W6162 and W6263
Determination of the content of volatile components; static

headspace gas chromatography with mass spectrometry
W0122 and W0254
dichloromethane, trichloromethane, tetrachloromethane,
NEN-EN-ISO 10301
1,1-dichloroethane, 1,2-dichloroethane, 1,1,1-trichloroethane,
(preservation in accordance with
1,1,2-trichloroethane, 1,1-dichloroethylene, cis-1,2-dichloroethylene,
NEN-EN-ISO 5667-3)
in house method
in accordance with
trans-1,2-dichloroethylene, trichloroethylene, tetrachloroethylene,

monochlorobenzene, 1,2-dichlorobenzene, 1,3-dichlorobenzene and
1,4-dichlorobenzene
61
62
63
Wastewater,
drinking water,
groundwater
and surface
water

W0122 and W0254
benzene, toluene, ethylbenzene, xylenes, naphthalene and styrene
(preservation in accordance with
Wastewater,
drinking water,
groundwater
and surface
water

Soil

W0136, W0132 and

W0254
benzene, toluene, ethylbenzene, xylenes, naphthalene, styrene,
vinyl chloride, dichloromethane, trichloromethane, tetrachloromethane,
(extraction in accordance with
1,1-dichloroethane, 1,2-dichloroethane, 1,1,1-trichloroethane,
NEN 6973)

NEN-EN-ISO 5667-3)
W0122 and W0254

in house method
propylbenzene, 1,2,3-trimethylbenzene, 1,2,4-trimethylbenzene,

1,3,5-trimethylbenzene, vinyl chloride, methyltertiarybutylether (MTBE),
ethyltertiarybutylether (ETBE) and tertiaryamylmethylether (TAME)
1,1,2-trichloroethane, 1,1-dichloroethylene, cis-1,2-dichloroethylene,

trans-1,2-dichloroethylene, trichloroethylene, tetrachloroethylene,
monochlorobenzene, 1,2-dichlorobenzene, 1,3-dichlorobenzene,
1,4-dichlorobenzene, propylbenzene, pentane, hexane, heptane, octane,
1,2,3-trimethylbenzene, 1,2,4-trimethylbenzene, 1,3,5-trimethylbenzene
methyltertiarybutylether (MTBE), ethyltertiarybutylether (ETBE) and
tertiaryamylmethylether (TAME)
Page 8 of 38

number: L 010
of

Barneveld
Valid from: 17-05-2011 till 01-04-2013

Nr.
64
Material or
product
Soil and
sediment
Determination of the content of organochloropesticides and

polychlorinated biphenyls; gas chromatography mass
spectrometry
Internal
reference number
W0120 and W0262
in house method
alpha-HCH, beta-HCH, gamma-HCH, delta-HCH, epsilon-HCH,

pentachlorobenzene, HCB, heptachlor, aldrin, telodrin, isodrin,
heptachloroepoxide, hexachlorobutadiene, alpha-endosulphan,
beta-endosulphan, alpha-chlordane, gamma-chlordane, o,p'-DDE,
p,p'-DDE, o,p'-DDD, p,p'-DDD, dieldrin, endrin, o,p'-DDT, p,p'-DDT,
endosulphansulphate,
PCB 28, PCB 52, PCB 101, PCB 118, PCB 138, PCB 153 and PCB 180
65
Drinking water,
groundwater
and surface
water
Determination of the content of organochloropesticides and

polychlorinated biphenyls; large volume injection gas
chromatography mass spectrometry
W0137 and W0260

in house method
alpha-HCH, beta-HCH, gamma-HCH, delta-HCH, epsilon-HCH,

pentachlorobenzene, HCB, heptachlor, aldrin, telodrin, isodrin,
heptachloroepoxide, hexachlorobutadiene, alpha-endosulphan,
beta-endosulphan, alpha-chlordane, gamma-chlordane, o,p'-DDE,
p,p'-DDE, o,p'-DDD, p,p'-DDD, dieldrin, endrin, o,p'-DDT, p,p'-DDT,
endosulphansulphate,
PCB 28, PCB 52, PCB 101, PCB118, PCB 138, PCB 153 and PCB 180
66
Wastewater,
groundwater
and surface
water
Determination of the content of polycyclic aromatic

hydrocarbons; high performance liquid chromatography with
UV- and fluorescence detection
W0130 and W0301

in house method
naphthalene, acenaphthylene, acenaphthene, fluorene, phenanthrene,

anthracene, fluoranthene, pyrene, benzo(a)anthracene, chrysene,
benzo(b)fluoranthene, benzo(k)fluoranthene, benzo(a)pyrene,
dibenzo(a,h)anthracene, benzo(g,h,i)perylene and
indeno(1,2,3-c,d)pyrene
67
Groundwater

hydrocarbons; on-line solid phase extraction and high
performance liquid chromatography with UV- and
fluorescence detection
W0130 and W0302

in house method

Page 9 of 38

number: L 010
of

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Valid from: 17-05-2011 till 01-04-2013

Nr.
68
Material or
product
Soil and
sediment
Internal
reference number

W0120 and W0301
NEN 6971, cleanup in


Asphalt investigation
69
Asphalt cores
70
Determination of the structure of asphalt layers;

ruler / slide gauge
W0179
Detection of polycyclic aromatic hydrocarbons (PAH);

PAH-detection (PAH-marker)
W0180
in accordance with RAW 152
in accordance with
CROW publication 210
71
Asphalt

W7124 and W0301
naphthalene, phenanthrene, anthracene, fluoranthene,
benzo(a)anthracene, chrysene, benzo(k)fluoranthene, benzo(a)pyrene,
accordance with NEN 6976 and
in house method
benzo(g,h,i)perylene, indeno(1,2,3-c,d)pyrene and the sum of these 10 PAH analysis in accordance with
NEN 6977)
Leaching test
a
Soil and waste

materials
Determination of the leachable fraction by means of a one or W0155

in accordance with
two stage batch test (L/S 10 and L/S 2-8) for materials with
NEN-EN 13370
particle size < 4 mm
NEN-EN 12457-1 to 3
Page 10 of 38

number: L 010
of

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Valid from: 17-05-2011 till 01-04-2013

Nr.
Material or
product
Internal
reference number
Tests forming part of TerrAttesT Soil

72
Soil
W0104
in house method
73
Soil
Determination of clay content; pipette method
W0171
equivalent to NEN 5753
74
75
76
Soil
Soil
Soil
Determination of loss on evaporation after ignition and the

total residue on evaporation after ignition; gravimetry
W0109
Determination of organic matter content as loss-on-ignition;

gravimetry
W0109

W0107 and W0423
aluminium, antimony, arsenic, barium, boron, beryllium, cadmium, calcium,
17294-2
chromium, phosphor, cobalt, copper, mercury, lead, magnesium,
(digestion in accordance with
manganese, molybdenum, nickel, selenium, tin, titanium, vanadium, iron,
NEN 6961)
in accordance with NEN-EN-ISO
silver, zinc and sulphur
77
Soil

detection
W6128, W6237 and

W6330
in house method
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Nr.
78
Material or
product
Soil
Internal
reference number
Determination of organic contaminations; gas

chromatography with mass spectrometry
W6128, W6330 and

W6331
Aromatic compounds
in house method
Monoaromatic hydrocarbons: benzene, ethylbenzene, toluene,

o-xylene, m,p-xylene, styrene, 1,2,4-trimethylbenzene,
1,3,5-trimethylbenzene, n-propylbenzene, isopropylbenzene (cumene),
n-butylbenzene, sec-butylbenzene, tert-butylbenzene and
p-isopropyltoluene
Phenols: phenol, o-cresol, m-cresol, p-cresol, 2,4-dimethylphenol,
2,5-dimethylphenol, 2,6-dimethylphenol, 3,4-dimethylphenol,
o-ethylphenol, m-ethylphenol, thymol, 4-ethyl/2,3- and 3,5-dimethylphenol
Polycyclic aromatic hydrocarbons: naphthalene, acenaphtylene,
acenaphthene, fluorene, phenanthrene, anthracene, fluoranthene, pyrene,
benzo(a)anthracene, chrysene, benzo(b)fluoranthene,
benzo(k)fluoranthene, benzo(a)pyrene, dibenzo(a,h)anthracene,
benzo(g,h,i)perylene and indeno(1,2,3-c,d)pyrene
Halogenated compounds
Volatile halogenated components: tetrachloromethane,
1,2-dichloroethane, 1,1,1-trichloroethane, 1,1,2-trichloroethane,
1,1,1,2-tetrachloroethane, 1,1,2,2-tetrachloroethane, trichloroethylene,
tetrachloroethylene, 1,2-dichloropropane, 1,3-dichloropropane,
1,2,3-trichloropropane, 1,1-dichloropropene, cis-1,3-dichloropropene,
trans-1,3-dichloropropene, dibromomethane, 1,2-dibromoethane,
tribromomethane (bromoform), bromodichloromethane,
dibromochloromethane, 1,2-dibromo-3-chloropropane and bromobenzene
Chlorobenzenes: monochlorobenzene, 1,2-dichlorobenzene,
1,3-dichlorobenzene, 1,4-dichlorobenzene, dichlorobenzenes (sum),
1,2,3-trichlorobenzene, 1,2,4-trichlorobenzene, 1,3,5-trichlorobenzene,
trichlorobenzenes (sum), 1,2,3,4-tetrachlorobenzene,
1,2,3,5/1,2,4,5-tetrachlorobenzene, tetrachlorobenzene (sum),
pentachlorobenzene and hexachlorobenzene
Chlorophenols: 2-chlorophenol, 3-chlorophenol, 4-chlorophenol,
2,3-dichlorophenol, 2,4/2,5-dichlorophenol, 2,6-dichlorophenol,
3,4-dichlorophenol, 3,5-dichlorophenol, 2,3,4-trichlorophenol,
2,3,5-trichlorophenol, 2,3,6-trichlorophenol, 2,4,5-trichlorophenol,
2,4,6-trichlorophenol, 3,4,5-trichlorophenol, 2,3,4,5-tetrachlorophenol,
2,3,4,6/2,3,5,6-tetrachlorophenol, pentachlorophenol and
4-chloro-3-methylphenol
Polychlorinated biphenyls: PCB 28, PCB 52, PCB 101, PCB 118,
PCB 138, PCB 153 and PCB 180
Chloronitrobenzenes: 2/4-chloronitrobenzene, 3-chloronitrobenzene,
2,3-dichloronitrobenzene + 3,4-dichloronitrobenzene,
2,4-dichloronitrobenzene, 2,5-dichloronitrobenzene and
3,5-dichloronitrobenzene
Miscellaneous chlorinated hydrocarbons: 2-chlorotolueen,
4-chlorotolueen and 1-chloronaphthalene
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Nr.
Material or
product
Pesticides
Organic chlorinated pesticides: p,p
-DDE, o,p
-DDE, p,p
-DDT,
p,p
-DDD/o,p
-DDT, o,p
-DDD, aldrin, dieldrin, endrin, alpha-HCH,
beta-HCH, gamma-HCH, alpha-endosulphansulphate,
alpha-chlordane, gamma-chlordane, heptachlor, heptachloroepoxide,
hexachlorobutadiene, isodrin, telodrin and tedion
Organic phosphor pesticides: azinphos-ethyl, azinphos-methyl,
bromophos-ethyl, bromophos-methyl, chloropyrophos-ethyl,
chloropyrophos-methyl, cumaphos, demeton-S/demeton-O, diazinone,
disulphotone, fenitrothion, fenthion, malathion, parathion-ethyl,
parathion-methyl, pyrazophos and triazophos
Organic nitrogen pesticides: ametryn, atrazine, cyanazin, desmetryn,
prometryn, propazine, simazine, terbutylazine and terbutryn
Miscellaneous pesticides: bifenthrine, cypermethrin A, cypermethrin B,
cypermethrin C, cypermethrin D, deltamethrin, permethrin A +
permethrin B, propachlor and trifluralin
Internal
reference number
W6128, W6330 and
W6331
in house method
Miscellaneous organic contaminants

biphenyl, nitrobenzene and dibenzofurane
Phthalates: dimethylphthalate, diethylphthalate, di-isobutylphthalate,
dibutylphthalate, butylbenzylphthalate, bis(2-ethylhexyl)phthalate and
di-n-octylphthalate
Page 13 of 38

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Nr.
Material or
product
Internal
reference number
Tests forming part of TerrAttesT Water

79
80
Drinking water
and
groundwater

detection
W6139 and W6239

W0420 and W0421
antimony, arsenic, barium, beryllium, cadmium, chromium, cobalt, copper,
NEN-EN-ISO 17294-2
in house method
in accordance with
mercury, lead, molybdenum, nickel, selenium, tin, vanadium and zinc
81
W0506
in accordance with NEN-ISO 7888
82
W0524
in accordance with
NEN-ISO 10523
83
Determination of the content of volatile components;

on-line purge and trap - thermic desorption - gas
W6136 and W6225

in accordance with
NEN-EN-ISO 15680
Monoaromatic hydrocarbons
benzene, ethylbenzene, toluene, o-xylene, m-xylene, p-xylene, styrene,
1,2,4-trimethylbenzene, 1,3,5-trimethylbenzene (mesitylene),
n-propylbenzene, isopropylbenzene (cumene), n-butylbenzene,
sec-butylbenzene, tert-butylbenzene and p-isopropyltoluene (p-cymene)
Halogenated hydrocarbons
chloroform (trichloromethane), tetrachloromethane, 1,1-dichloroethane,
1,2-dichloroethane, 1,1,1-trichloroethane, 1,1,2-trichloroethane,
1,1,1,2-tetrachloroethane, 1,1,2,2-tetrachloroethane, trichloroethylene,
tetrachloroethylene, 1,2-dichloropropane, 1,3-dichloropropane,
1,2,3-trichloropropane, 1,1-dichloropropene, cis-1,3-dichloropropene,
trans-1,3-dichloropropene, dibromomethane, 1,2-dibromoethane,
tribromomethane (bromoform), bromodichloromethane,
dibromochloromethane, 1,2-dibromo-3-chloropropane, bromobenzene,
chloromethane, dichloromethane, vinyl chloride (chloroethene),
1,1-dichloroethylene, cis-1,2-dichloroethylene,
trans-1,2-dichloroethylene, 2,2-dichloropropane, hexachlorobutadiene,
2-chlorotoluene, 4-chlorotoluene, trichlorofluormethane, chloroethane,
bromochloromethane and bromomethane
Chlorobenzenes
chlorobenzene, 1,2-dichlorobenzene, 1,3-dichlorobenzene,
1,4-dichlorobenzene, 1,2,3-trichlorobenzene and 1,2,4-trichlorobenzene
Polycyclic aromatic hydrocarbons

naphthalene
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Valid from: 17-05-2011 till 01-04-2013

Nr.
84
Material or
product
Groundwater
Determination of organic contaminations; gas

Aromatic compounds
Internal
reference number
W6136, W6330 and
W6336
in house method
Phenols: phenol, o-cresol, m-cresol, p-cresol, 2,4-dimethylphenol,

2,5-dimethylphenol, 3,4-dimethylphenol, 2-ethylphenol, 3-ethylphenol,
4-ethylphenol/2,3-dimethylphenol, 3,5-dimethylphenol, 2,6-dimethylphenol
and thymol
Polycyclic aromatic hydrocarbons: naphthalene, acenaphtylene,
acenaphthene, fluorene, phenanthrene, anthracene, fluoranthene, pyrene,
benzo(a)anthracene, chrysene, benzo(b+k)fluoranthene, benzo(a)pyrene,
dibenzo(a,h)anthracene, indeno(1,2,3-c,d)pyrene and benzo(g,h,i)perylene
Halogenated compounds
Chlorobenzenes: monochlorobenzene, 1,2-dichlorobenzene,
1,3-dichlorobenzene, 1,4-dichlorobenzene, 1,2,3-trichlorobenzene,
1,2,4-trichlorobenzene, 1,3,5-trichlorobenzene, 1,2,3,4-tetrachlorobenzene,
1,2,3,5/1,2,4,5-tetrachlorobenzene, pentachlorobenzene and
hexachlorobenzene
Chlorophenols: 2-chlorophenol, 3-chlorophenol, 4-chlorophenol,
2,3-dichlorophenol, 2,4/2,5-dichlorophenol, 2,6-dichlorophenol,
3,4-dichlorophenol, 3,5-dichlorophenol, 2,3,4-trichlorophenol,
2,3,5-trichlorophenol, 2,3,6-trichlorophenol, 2,4,5-trichlorophenol,
2,4,6-trichlorophenol, 3,4,5-trichlorophenol, 2,3,4,5-tetrachlorophenol,
2,3,4,6/2,3,5,6-tetrachlorophenol, pentachlorophenol and
4-chloro-3-methylphenol
Polychlorinated biphenyls: PCB 28, PCB 52, PCB 101, PCB 118, PCB 138,
PCB 153 and PCB 180
Chloronitrobenzenes: 2/4-chloronitrobenzene, 3-chloronitrobenzene,
2,3-dichloronitrobenzene, 2,4-dichloronitrobenzene,
2,5-dichloronitrobenzene, 3,4-dichloronitrobenzene and
3,5-dichloronitrobenzene
Miscellaneous halogenated hydrocarbons: 1-chloronaphthalene
Pesticides
Organic chlorinated pesticides: p,p
-DDE, o,p
-DDE, p,p
-DDT,
p,p
-DDD/o,p
-DDT, o,p
-DDD, aldrin, dieldrin, endrin, alpha-HCH,
beta-HCH, gamma-HCH, delta-HCH, alpha-endosulphan,
alpha-endosulphansulphate, alpha-chlorodane, gamma-chlorodane,
heptachlor, heptachloroepoxide, hexachlorobutadiene, isodrin, telodrin and
tedion
Organic phosphor pesticides: azinphos-ethyl, azinphos-methyl, bromophosethyl, bromophos-methyl, chloropyriphos-ethyl, chloropyriphos-methyl,
cumaphos, demeton-S/demeton-O, diazinone, dichlorophos, disulphotone,
fenitrothion, fenthion, malathion, parathion-ethyl, parathion-methyl,
pyrazophos and triazophos
Organic nitrogen pesticides: ametryn, atrazine, cyanazin, desmetryn,
prometryn, propazine, simazine, terbutylazine and terbutryn
Miscellaneous pesticides: bifenthrine, carbaryl, cypermethrin A+B+C+D,
deltamethrin, linuron, permethrin A, permethrin B, propachlor and trifluralin
Miscellaneous organic contaminants

biphenyl, nitrobenzene and dibenzofurane
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Nr.
Material or
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Internal
reference number
AP04-tests, package SG1 (composition of soil) (version 01-Oct-2008); complete package

--
Soil
Sample pre-treatment for AP04-SG1
W7101
in accordance with AP04-V
85
Determination of pH-CaCl 2; potentiometry
W0524
in accordance with AP04-SG-I
86
Field-moist soil
and air-dried
soil
W7104
in accordance with AP04-SG-II
NEN-ISO 11465
87
Soil
Determination of clay content; sieve and pipette
W7173
in accordance with AP04-SG-III
NEN 5753
88
Determination of organic matter content as loss-on-ignition;

gravimetry
W7109
in accordance with AP04-SG-IV
NEN 5754
89
Determination of the content of metals; inductively coupled

W0107 and W0423
antimony, arsenic, barium, cadmium, chromium, cobalt, copper, mercury
(non volatile), lead, molybdenum, nickel, selenium, tin, vanadium and zinc
NEN-EN-ISO 17294-2
in accordance with AP04-SG-V

NEN 6961)
90

hydrocarbons (PAH); high performance liquid
chromatography with UV- and fluorescence detection
W7124 and W0301

in accordance with AP04-SG-IX

NEN 6977
benzo(g,h,i)perylene, indeno(1,2,3-c,d)pyrene and the sum of these 10 PAH
NEN 6971 and cleanup in
91

hydrocarbons (PAH); gas chromatography with mass
spectrometry
W0125 and W0271
NEN-ISO 18287)
in accordance with AP04-SG-IX

and equivalent to

Page 16 of 38

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Valid from: 17-05-2011 till 01-04-2013

Nr.
92
Material or
product
Soil
Internal
reference number
Determination of the content of polychlorinated biphenyls

(PCB); gas chromatography with electron-capture detection
W7124 and W7255
PCB 28 (2,4,4' trichlorobiphenyl),
PCB 52 (2,5 2,5' tetrachlorobiphenyl),
NEN 6980
PCB 101 (2,4,5 2',5' pentachlorobiphenyl),
PCB 138 (2,3,4 2',4',5' hexachlorobiphenyl),
in accordance with AP04-SG-X

PCB 180 (2,3,4,5 2',4',5' heptachlorobiphenyl)
and the sum of these 7 PCB
93

(PCB); gas chromatography with mass spectrometry
W0125 and W0271
and equivalent to NEN 6980
(extraction equivalent to
NEN 6972 and cleanup
equivalent to NEN 6974)
in accordance with AP04-SG-X

94

W7124 and W7203

in accordance with AP04-SG-XI
NEN 6978
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Material or
product
Internal
reference number

--
Soil
W7101
95
Determination of the content of organochloropesticides

(OCP); gas chromatography with electron-capture detection
W7214 and W7255
hexachlorobenzene (HCB), -hexachlorocyclohexane ( -HCH),
-hexachlorocyclohexane ( -HCH), -hexachlorocyclohexane ( -HCH),
in accordance with AP04-SG-XIV

NEN 6980
aldrin, dieldrin, endrin, sum of these three "drin's", o,p'-DDD, p,p'-DDD, sum
of these two DDD's o,p'-DDE, p,p'-DDE, sum of these two DDE's, o,p'-DDT,
p,p'-DDT, sum of these two DDT's, isodrin, telodrin, hexachlorobutadiene,
heptachlor, -endosulfan, cis-heptachlor epoxide, trans-heptachlor epoxide,

sum of these two heptachlor epoxide, cis-chlorodane, trans-chlorodane and
the sum of these two chlorodanes and the sum of organochloropesticides
96
Determination of the content of less volatile chlorobenzenes; W7124 and W7255

gas chromatography with electron-capture detection
in accordance with AP04-SG-XV
sum of these three trichlorobenzenes, 1,2,3,4-tetrachlorobenzene,
1,2,3,5-tetrachlorobenzene, 1,2,4,5-tetrachlorobenzene, sum of these three
tetrachlorobenzenes, pentachlorobenzene and hexachlorobenzene,
sum of chlorobenzenes (see also package AP04-SG3)
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Nr.
Material or
product
Internal
reference number

--
Soil
W7101
97
98
Determination of the content of volatile aromatic and volatile

halogenated hydrocarbons MTBE and ETBE; static
W0132, W0136 and

W0254
volatile aromatic hydrocarbons: benzene, toluene, ethylbenzene,

o-xylene, m-xylene, p-xylene, sum of these three xylenes, styrene and the
sum of aromatic hydrocarbons
volatile halogenated hydrocarbons: chloroethylene (vinyl chloride),
dichloromethane, trichloromethane, tetrachloromethane, trichloroethylene,
tetrachloroethylene, 1,1-dichloroethane, 1,2-dichloroethane, sum of these
two dichloroethanes, 1,1-dichloroethylene, cis-1,2-dichloroethylene,
trans-1,2-dichloroethylene, sum of these three dichloroethylenes,
1,1,1-trichloroethane, 1,1,2-trichloroethane, 1,1-dichloropropane,
1,2-dichloropropane, 1,3-dichloropropane and the sum of these three
dichloropropanes
other volatile compounds: methyltertiarybutylether (MTBE),
ethyltertiarybutylether (ETBE)
Determination of the content of volatile chlorobenzenes;

static headspace gas chromatography with mass
spectrometry
W0132, W0136 and

W0254
in accordance with AP04-SG-VIII

NEN 6981
NEN 6973)
in accordance with AP04-SG-XV

1,4-dichlorobenzene and sum of these three dichlorobenzenes

--
Soil
W7101
99
Determination of the content of cyanides (total-free and

total-complex); continuous flow analysis and spectrometry
W0517
in accordance with AP04-SG-VII
NEN-ISO 17380
100
Determination of the content of chloride;

ion chromatography
W0504
in accordance with AP04-SG-XII
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Material or
product
Internal
reference number
AP04-tests, package SG5 (composition of soil) (version 01-Oct-2008); incomplete package

--
Soil
W7101
101
Determination of the content of organic nitrogen pesticides;

gas chromatography with mass spectrometry
W1124 and W1256
atrazine, propazine, simazine and terbutryn
in accordance with AP04-SG-XVI

VPR C85-17
102

W0107 and W0423
beryllium, tellurium, thallium and silver
in accordance with AP04-SG-V

NEN-EN-ISO 17294-2
NEN 6961)
AP04-tests, package SG7 (composition of soil) (version 01-Oct-2008);

complete package (with structural outsourcing of the determination of fluoride)
--
Soil
W7101
103
Determination of the content of extractable organohalogen

W7124 and W0351

in accordance with AP04-SG-XX
NEN 6979
NEN 6972)
104
Determination of the content of bromide; liquid

W0504
in accordance with AP04-SG-XXI
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Material or
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Internal
reference number
AP04-tests, package SB1 (composition of building materials, soil excluded) (version 01-Oct-2008);
complete package
--
Building
material
Sample pre-treatment for AP04-SB1
W7101
105 Field-moist and Determination of the dry matter content; gravimetry

air-dried
building material
W7104
106 Building
material
(except
bitumen)

W0120 and W0301
NEN 6977
benzo(g,h,i)perylene, indeno(1,2,3-c,d)pyrene and the sum of
these 10 PAH

spectrometry
W0125 and W0271
NEN-ISO 18287)
107
in accordance with AP04-SB-I
in accordance with AP04-SB-III

in accordance with AP04-SB-III

and equivalent to

108 Building
material

(PCB); gas chromatography with electron-capture detection
W7124 and W7255

in accordance with AP04-SB-IV

PCB 180 (2,3,4,5 2',4',5' heptachlorobiphenyl),
and the sum of these seven PCB
109

W0125 and W0271

in accordance with AP04-SB-IV

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Material or
product
110 Building
material

Internal
reference number
W7124 and W7203
in accordance with AP04-SB-V
NEN 6978
complete package
--
111
Building
material
W7101

(OCP); gas chromatography with electron-capture detection
W7124 and W7255

in accordance with AP04-SB-XIII

aldrin, dieldrin, endrin, p,p'-DDE, o,p'-DDD, o,p'-DDT, p,p'-DDD,
o,p'-DDE, p,p'-DDT, isodrin, telodrin, heptachlor, -endosulfan,
cis-heptachlor epoxide, trans-heptachlor epoxide, cis-chlordane,
trans-chlordane and the sum these 21 organochloropesticides
112
Determination of the content of organic nitrogen pesticides

(ONP); gas chromatography with mass spectrometry
W1124 and W1256

in accordance with AP04-SB-XIV
atrazine, propazine, simazine, terbutryn and the sum of pesticides not

containing chloro-organics
113
Determination of the content of organic phosphor pesticides

(OPP); gas chromatography with mass spectrometry
W1124 and W1256
parathion-methyl, parathion-ethyl, malathion, diazinone, disulphotone,
dichlorophos, dimethoate, mevinphos, fenthion, chlorpyriphos-ethyl,
VPR C85-18
in accordance with AP04-SB-XV
chlorpyriphos-methyl, azinphos-ethyl, azinphos-methyl,

bromophos-methyl, bromophos-ethyl and the sum of pesticides not
containing chloro-organics
114
Determination of the content of extractable organohalogen

W7124 and W0351

in accordance with AP04-SB-XVI
NEN 6979 (extraction in
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Nr.
Material or
product
Internal
reference number
complete package
--
Building
material
W7101
115
Determination of the content of volatile aromatic

hydrocarbons (BTEX); static headspace gas
W0132, W0136 and

W0254
in accordance with AP04-SB-II
benzene, toluene, ethylbenzene, o-xylene, m-xylene, p-xylene, sum of

these three xylenes and styrene
AP04-tests, package U1 (leaching test) (version 01-Oct-2008); complete package

--
Soil and
building
materials
Sample pre-treatment for AP04-U1 (and AP04-E)
W7101
Determination of the leaching of inorganic components with

the column test
W0152
in accordance with AP04-U-I and
Associated analyses of eluates are mentioned below in

package E AP04-tests, analysis of eluates
and NEN 7373

--
Building
materials and
monolites
W7101
Determination of the leaching of inorganic components with

the diffusion test
W0153
in accordance with AP04-U-II and

--

Building
materials and
waste materials
Determination of the availability of inorganic components for
leaching
W7101
W0151
in accordance with AP04-U-III

NEN 7371
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product
Internal
reference number
AP04-tests, package E (analysis of eluates) (version 01-Oct-2008)

116 Eluates
W0160
in accordance with AP04-U-IV
o-NEN 6411
117
W0160
in accordance with AP04-U-V and
in accordance with
NEN-ISO 7888
118

W0420 and W0421
antimony, arsenic, barium, cadmium, chromium, potassium, cobalt, copper,
XV and XIX and equivalent to
mercury, lead, molybdenum, sodium, nickel, selenium, tin, vanadium and
NEN 7324 (mercury) and in
zinc
accordance with
in accordance with AP04-E-I to
NEN-EN-ISO 17294-2 (remaining

metals)
119
Determination of the content of cyanides (free and complex); W0517

continuous flow analysis and spectrometry
in accordance with AP04-E-XVI
NEN-EN-ISO 14403
120
Determination of the content of bromide, chloride and

sulphate; liquid chromatography of ions
W0504
in accordance with AP04-E-XVII
NEN-EN-ISO 10304-2
121
W0546
in accordance with AP04-E-XVIII
NEN 6483
AP04-tests, package Bm/Bssa (granular waste materials)

--
122
Granular waste
materials
(version 01-Oct-2008)
Sample pre-treatment for AP04-Bm/Bssa
; complete package
W7101
W7104
in accordance with AP04-SB-I
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Nr.
123
Material or
product
Granular waste Determination of the loss-on-ignition; gravimetry

materials
Internal
reference number
W7109
in accordance with AP04-SB-IX
NEN 6499
124
Determination of the content of total organic carbon (TOC);

infrared detection
W0594
in accordance with AP04-SB-X
NEN-EN 13137
125
W0524
in accordance with AP04-SB-XI
126
Determination of the acid neutralization capacity; titrimetry
W7547
in accordance with AP04-SB-XII
Determination of the leachable fraction by means of a one

stage batch test (L/S 10) for materials with particle size
< 4 mm
W0156
in accordance with AP04-U-VIII
NEN-EN 12457-4
127 Eluates
W0160
in accordance with AP04-U-IV
o-NEN 6411
128
W0160
in accordance with AP04-U-V and
in accordance with
NEN-ISO 7888
129

W0420 and W0421
antimony, arsenic, barium, cadmium, chromium, copper, mercury, lead,
XV and XIX and equivalent to
molybdenum, nickel, selenium and zinc
NEN 7324 (mercury) and in
in accordance with AP04-E-I to
accordance with
NEN-EN-ISO 17294-2 (remaining
metals)
130
Determination of the content of bromide, chloride and

sulphate; liquid chromatography of ions
W0504
in accordance with AP04-E-XVII
NEN-EN-ISO 10304-2
Page 25 of 38

number: L 010
of

Barneveld
Valid from: 17-05-2011 till 01-04-2013

Nr.
Material or
product
131 Eluates
Internal
reference number
W0546
in accordance with AP04-E-XVIII
NEN 6483
132
Determination of dissolved organic carbon (DOC); oxidation

followed by the determination of the content of CO2
W0590
in accordance with AP04-E-XX
NEN-EN 13370 (NEN-EN 1484)
133
Determination of the content of total dissolved solids (TDS);

gravimetry
W0113
in accordance with AP04-E-XXI
NEN-EN 15216
AS3000; package 3010 (Laboratory analysis for soil, sediment and groundwater investigation;
soil basic package)(version 01-Oct-2008); complete package
--
Soil
Sample pre-treatment for package 3010
W0101
in accordance with AS3000 and
134
W0524
in accordance with performance
sheet 3010-1 and in accordance
with NEN-ISO 10390
135
W0104
sheet 3010-2 and equivalent to
NEN-ISO 11465
136
Determination of organic matter content; gravimetry
W0109
with NEN 5754
137
Determination of the clay content; sedimentation
W0105 and W0173

with NEN 5753
138 Sand and clay
Determination of the clay content; sedimentation and density W0171

determination
NEN 5753
Page 26 of 38

number: L 010
of

Barneveld
Valid from: 17-05-2011 till 01-04-2013

Nr.
Material or
product
139 Soil
Internal
reference number

W0107 and W0423
barium, cadmium, cobalt, copper, mercury (non-volatile), lead,
sheet 3010-5 (digestion in
molybdenum, nickel and zinc
accordance with NEN 6961,
analysis in accordance with

NEN-EN-ISO 17294-2)
140

W0120 and W0301


with NEN 6977
141

spectrometry
W0125 and W0271
NEN-ISO 18287)


142

W0120, W0132 and

W0202
with NEN 6978
143

W0120 and W0262
NEN 6980
NEN 6972, cleanup equivalent to
NEN 6974)

Page 27 of 38

number: L 010
of

Barneveld
Valid from: 17-05-2011 till 01-04-2013

Nr.
Material or
product
144 Soil
Internal
reference number

W0125 and W0271
NEN 6980
NEN 6974)

145

W0120 and W0266
NEN 6980
equivalent to NEN 6972, cleanup
in accordance with equivalent to
NEN 6974)

soil complementary I)(version 01-Oct-2008); complete package
--
Soil
W0101
146

(OCP); gas chromatography with mass spectrometry
W0120 and W0262

NEN 6980
aldrin, dieldrin, endrin, sum of these three "drin's", o,p'-DDD, p,p'-DDD, sum
of these two DDD

s, o,p'-DDE, p,p'-DDE, sum of these two DDE
s,
o,p'-DDT, p,p'-DDT, sum of these two DDT

s, heptachlor, -endosulfan,
NEN 6974)
isodrin, telodrin, cis-heptachlor epoxide, trans-heptachlor epoxide, sum of

these two heptachlor epoxides, cis-chlorodane, trans-chlorodane, sum of
these two chlorodanes, sum of organochloropesticides and
hexachlorobutadiene
Page 28 of 38

number: L 010
of

Barneveld
Valid from: 17-05-2011 till 01-04-2013

Nr.
Material or
product
147 Soil
Internal
reference number
Determination of the content of less volatile chlorobenzenes; W0120 and W0262

NEN 6980
tetrachlorobenzenes, pentachlorobenzene and hexachlorobenzene, sum of
chlorobenzenes
NEN 6974)
soil complementary II)(version 01-Oct-2008); complete package
--
Soil
W0101
148

hydrocarbons, volatile halogenated hydrocarbons, MTBE
and ETBE; static headspace gas chromatography with
mass spectrometry
W0132, W0136 and

W0254
volatile aromatic hydrocarbons: benzene, toluene, ethylbenzene, o-xylene,
with NEN 6981
m-xylene, p-xylene, sum of these three xylenes, styrene, sum of aromatic
solvents, naphthalene
NEN 6973)

volatile halogenated hydrocarbons: chloroethylene (vinyl chloride),

tetrachloroethylene, 1,1-dichloroethane, 1,2-dichloroethane,
1,1-dichloroethylene, cis-1,2-dichloroethylene, trans-1,2-dichloroethylene,
sum of these three dichloroethylenes, 1,1,1-trichloroethane,
1,1,2-trichloroethane and the sum of these two trichloroethanes,
1,1-dichloropropane, 1,2-dichloropropane, 1,3-dichloropropane and the sum
of these three dichloropropanes, tribromomethane
other volatile compounds: methyltertiarybutylether (MTBE) and
149 Soil
Determination of the content of volatile chlorobenzenes;

static headspace gas chromatography with mass
spectrometry
W0132, W0136 and

W0254
1,4-dichlorobenzene and the sum of dichlorobenzenes
NEN 6981

NEN 6973)
Page 29 of 38

number: L 010
of

Barneveld
Valid from: 17-05-2011 till 01-04-2013

Nr.
Material or
product
150 Soil
Internal
reference number
Determination of the content of other solvents; static

W0132, W0136 and

W0254
1,2,3-trimethylbenzene, 1,2,4-trimethylbenzene, 1,3,5-trimethylbenzene,
2-ethyltoluene, 3-ethyltoluene, 4-ethyltoluene, isopropylbenzene,
propylbenzene and the sum aromatic solvents
with NEN 6981

NEN 6973)
soil complementary III)(version 01-Oct-2008); complete package
--
W0101
151
Determination of the content of cyanides (free, total and

complex); continuous flow analysis and spectrometry
W0117 and W0517

with NEN-ISO 17380
152
Determination of chloride; liquid chromatography of ions
W0504
sheet 3040-2
VPR C85-06, analysis in
accordance with
NEN-ISO 10304-2 )
(version 01-Oct-2008)
soil complementary IV)
; complete package
--
Soil
W0101
153

W0107 and W0423
antimony, arsenic, chromium, tin, vanadium, beryllium, tellurium, thallium
sheet 3050-1 and -2
and silver
NEN 6961, analysis in

accordance with
NEN-EN-ISO 17294-2)
Page 30 of 38

number: L 010
of

Barneveld
Valid from: 17-05-2011 till 01-04-2013

Nr.
Material or
product
Internal
reference number
groundwater basic package)(version 01-Oct-2008) complete package
154 Groundwater
W0524
with o-NEN 6411
155
W0506
with NEN-ISO 7888
156
157

W0420 and W0421
with NEN-EN-ISO 17294-2

W0130 and W0302

W0123 and W0215

NEN-EN-ISO 17993
158

sheet 3110-5
Page 31 of 38

number: L 010
of

Barneveld
Valid from: 17-05-2011 till 01-04-2013

Nr.
Material or
product
Internal
reference number
groundwater complementary I)(version 01-Oct-2008); complete package
159 Groundwater

(PCB) and organochloropesticides (OCP);
W0137 and W0260
NEN-EN-ISO 6468


PCB 180 (2,3,4,5 2',4',5' heptachlorobiphenyl),
sum of these seven PCB,
sum of these four HCH's, aldrin, dieldrin, endrin, sum of these three "drin's",
p,p'-DDE, o,p'-DDD, o,p'-DDT, p,p'-DDD, o,p'-DDE, p,p'-DDT, sum of these
six DD's, heptachlor, -endosulfan, cis-heptachlor epoxide,
trans-heptachlor epoxide, sum of these two heptachlor epoxides,
cis-chlorodane, trans-chlorodane and sum of these two chlorodanes
160
Determination of the content of tri- and tetrachlorobenzenes, W0137 and W0260

penta- and hexachlorobenzene; gas chromatography with
mass spectrometry
1,2,3-trichlorobenzene, 1,2,4-trichlorobenzene, 1,3,5-trichlorobenzene, sum
NEN-EN-ISO 6468
of these three trichlorobenzenes, 1,2,3,4-tetrachlorobenzene,

tetrachlorobenzenes, pentachlorobenzene and hexachlorobenzene
Page 32 of 38

number: L 010
of

Barneveld
Valid from: 17-05-2011 till 01-04-2013

Nr.
Material or
product
Internal
reference number
groundwater complementary II)(version 01-Oct-2008); complete package
161 Groundwater

hydrocarbons and volatile halogenated hydrocarbons; static
W0122 and W0254
volatile aromatic hydrocarbons: benzene, toluene, ethylbenzene, o-xylene,
NEN-EN-ISO 15680

m-xylene, p-xylene, sum of these three xylenes, styrene and naphthalene

volatile halogenated hydrocarbons: chloroethylene (vinyl chloride)
tetrachloroethylene, 1,1-dichloroethane, 1,2-dichloroethane,
1,1-dichloroethylene, cis-1,2-dichloroethylene, trans-1,2-dichloroethylene,
sum of these three dichloroethylenes, 1,1,1-trichloroethane,
1,1,2-trichloroethane, 1,1-dichoropropane, 1,2-dichoropropane,
1,3-dichoropropane, the sum of these three dichloropropanes and
tribromomethane
other volatile compounds: methyltertiarybutylether (MTBE) and
162
Determination of the content of monochlorobenzene and

dichlorobenzenes; static headspace gas chromatography
with mass spectrometry
W0122 and W0254
NEN-EN-ISO 15680

1,4-dichlorobenzene and the sum of these three dichlorobenzenes
groundwater complementary III)(version 01-Oct-2008); complete package
163 Groundwater
Determination of the content of cyanide (free, total and

W0517
with NEN-EN-ISO 14403
164
Determination of the content of anions; liquid

W0504
chloride, nitrate and sulphate

165
Determination of the content of anions; discrete analysis and W0566

spectrometry
chloride, nitrate, ortho-phosphate and sulphate

with NEN 6604
Page 33 of 38

number: L 010
of

Barneveld
Valid from: 17-05-2011 till 01-04-2013

Nr.
Material or
product
Internal
reference number
groundwater complementary IV)(version 01-Oct-2008); complete package
166 Groundwater

W0420 and W0421
antimony, arsenic, chromium, tin, vanadium, beryllium, tellurium, thallium
sheet 3150-1 and -2 and in
and silver
accordance with
NEN-EN-ISO 17294-2
sediment basic package)(version 25-Jun-2008) complete package
--
Sediment
W0101
167
W0104
with NEN-EN 12880
168
Determination of organic matter content; gravimetry
W0109
sheet 3210-2a and in accordance
with NEN 5754
169
Determination of the total residue on evaporation; gravimetry W0109

sheet 3210-2b and in accordance
with NEN 5754
170
Determination of the particle size fractions; sedimentation
W0173
< 2 m (clay) and < 16 m

with NEN 5753
171

W0107 and W0423

NEN 6961)
Page 34 of 38

number: L 010
of

Barneveld
Valid from: 17-05-2011 till 01-04-2013

Nr.
Material or
product
172 Sediment

Internal
reference number
W0120, W0132 and
W0301

with NEN 6977
173

W0120, W0132 and

W0202
with NEN 6978
174

W0120, W0132 and

W0262
NEN 6980
NEN 6974)

Page 35 of 38

number: L 010
of

Barneveld
Valid from: 17-05-2011 till 01-04-2013

Nr.
Material or
product
Internal
reference number
sediment complementary I)(version 25-Jun-2008); complete package
--
Sediment
W0101
175

(OCP); gas chromatography with mass spectrometry
W0120, W0132 and

W0262
hexachlorobutadiene, pentachlorobenzene, hexachlorobenzene, the sum of
chlorobenzenes, -HCH, -HCH, -HCH, the sum of these three
HCH-compounds, aldrin, dieldrin, endrin, isodrin, telodrin, the sum of these
NEN 6980
five drin's, o,p'-DDD, p,p'-DDD, the sum of these two DDD

s, o,p'-DDE,
p,p'-DDE, the sum of these two DDE

s, o,p'-DDT, p,p'-DDT, the sum of
these two DDT

s, the sum of these DD
s, heptachlor, -endosulfan,
NEN 6974)
cis-heptachlor epoxide, trans-heptachlor epoxide, the sum of these two

heptachlor epoxides, cis-chlorodane, trans-chlorodane and the sum of
these two chlorodanes
Determination of the content of miscellaneous

organochloropesticides (OCP); gas chromatography with
mass spectrometry
176
-HCH, the sum of the HCH-compounds and endosulphansulphate
W0120, W0132 and

W0262
NEN 6980
NEN 6974)
(version 25-Jun-2008)
sediment complementary II)
; complete package
--
Sediment
W0101
177
Determination of the content of monochlorobenzene and

dichlorobenzenes; static headspace gas chromatography
with mass spectrometry
W0132, W0136 and

W0254
1,4-dichlorobenzene and the sum of these three dichlorobenzenes
with NEN 6981

NEN 6973)
Page 36 of 38

number: L 010
of

Barneveld
Valid from: 17-05-2011 till 01-04-2013

Nr.
Material or
product
178 Sediment
Internal
reference number
Determination of the content of tri- and tetrachlorobenzenes; W0120, W0132 and

W0262
1,2,3,5-tetrachlorobenzene, 1,2,4,5-tetrachlorobenzene, the sum of these
NEN 6980
three tetrachlorobenzenes and the sum of the chlorobenzenes
NEN 6974)
sediment complementary III)(version 25-Jun-2008); complete package
--
Sediment
W0101
179
Determination of the content of cyanide (free, total and

W0117 and W0517

with NEN-ISO 17380
180
Determination of the content of chloride; liquid

W0504
with NEN-ISO 10304-2 (analysis)
Determination of pH-H2O; potentiometry
181
W0524
with NEN-ISO 10390
sediment complementary IV)(version 25-Jun-2008); complete package
--
Sediment
W0101
182

W0107 and W0423
antimony, arsenic, chromium, tin and vanadium

NEN 6961)
Page 37 of 38

number: L 010
of

Barneveld
Valid from: 17-05-2011 till 01-04-2013

Nr.
Material or
product
Internal
reference number
sediment complementary V)(version 25-Jun-2008); complete package
--
Sediment
W0101
183
Determination of the content of pentachlorophenol; gas

W0139 and W0267

NEN-ISO 14154
184
Determination of the content of organotin compounds; gas

W0140 and W0268
tributyltin compounds (TBT), triphenyltin compounds (TPhT) and the sum of
these organotin compounds
with ISO/DIS 23161
Page 38 of 38
APPENDIX III
INVENTORY MAPS
Witteveen+Bos, appendix III to report IND50-1/berr9/066 dated April 11, 2011
Present wells
Open drains at KIE
Open area sources pollution (solid waste, transformers etc) at KIE
71
76 77
44
I NN
42
43
ER
21
68 66
20
16
RI N
41
GR
OA
D
NH
-7
64
12
13
8
5 6
10
27
22
28
48
24
26
23
47
63
46
62
AFTER INVENTORISATION WELL :

5 DEEP WELL SAMPLES WILL BE TAKEN
DW1-1 TILL DW1-5
PROJECT
ANDHRA PRADESH POLLUTION CONTROL BOARD
Consultancy Services for Remediation of

NMK, Kattedan Industrial Area (KIE) in
Rangareddy District, Andhra Pradesh
REVISION : 0
DRAWN BY : KK
SCALE : N.T.S.
CHD BY :
DATE : 21/10/2011
APPROVED BY :
DRAWING NO:
SOURCE : Enhence Version of Google Earth Dated: Dec/2007
142
5101
TO SHADNAGAR
24
141
2985
133/A
143/A
2067
48/61
82
135
4324
144/A
2151
144/B
2115
48/59
"
'-0
129
4787
146
4210.90
60'-0"
1050
E
8
MOSQUE
129
1530
91/A
2058
92/B
1908
W
E
9
126
716
1471
4629
E
E
11
937.5
I D
E
10
2620
937.5
E
12
E
38
149/A
E
40
E
34
E
27
125/D
2811
E
26
E
33
E
39
94
2397
73/D
4611
160
8875.39
937.5
E
15
E
16
D
40'-0" WIDE ROA
214/A
1600
48/54
HILLOCK
OPEN SPACE
124 & 125
HANUMAN
TEMPLE
48/56
150
4825.61
99
2988
48/55
OPEN SPACE
B.W. 14
121
3106
BW.9
122
2333
WELL
BW.8
156/H
3196
118
3975.34
119/A
3933.33
119/C
3936.33
100/A
1339
119/B
2680.46
151
4625
53/C
152
3642
114
4945
153
4222
A D
ID
154
3882.38
106
4835
N O. 25
83
1452
4
23
7
TO 0
21
24
TO
3
22
1
11
TO
5
11
3
ID
"
14
N
O.
15
O.
19
31/A
105/A
2783
102
4256
16/A
2470
16
2081.20
60
"
'-0
W
I
D
D
E
E
O
R
O
N
.
O
50000 Gallons
Hill Side Reservoir
N
O
.
HILLOCK
48/29
OPEN SPACE
48/28
48/16
48/21
ABAD
156/D
1859
48/34
156/C
1809
101/A
1348
103
4784.44
104
4768.89
156/B
1806
TO HYDER
16/C
1250
101/B
1400
156/A
1778
48/35
31/C
48/33
29
1605
2
O.
16/B
1250
48/32
30
1452
ID
15
2420
48/30
1
4730.98
1/A
5494
5/E
5567
Distribuation Pump
2
3723.90
14
2822.22
16/O
2081.20
3
18
TO
7
18
"
4
2924
164
907
3
2689.44
48/31
' -0
9
16
TO
TO
155
3637.20
105/B
1969
107
5829.13
108
4604.33
31/B
20
32
1961.60
TO
D
19
20
9
15
TO
18
13
4840
5/C
1570
30
16/E
7260
ID
.8
5/B
2000
5/A
1200
IV
3
D
TO
1
13
TO
7
1
13
12
TO
0
13
17
2420
12
4395.40
'-0
15
TO
24
30
TO
14
35
TO
43
D
R
III
D6
5/D
2990
II
D
D5
5/D
2311
O.
10
97
TO
/B
34 0.4
/A 72
34 8
88
"
25
TO
34
ID
18
4691.80
11
2421
'-0
60
3968.80
100
3032.78
30
N O.
48/37
/C
34
3
83
64
TO
89
63
TO
67
30
49
TO
62
28
2420
48/40
IX
"
'- 0
30
.6
O
I
VI
48/42
.
O
"
'-0
60
VI
E
I D
1
23
TO 5
23
115
5033
R O
48/36
113/A
3037
110
2640
58/C
58/E
73
TO
77
"
'-0
30
II
35
12100
VI
48/41
.8
O
G 8/A
1048
TO23
2
D4
ID
5/G
2699
F7
G 6/B
1043
8/D
ID
59
3630
D
ROA
IDR
" W
113/B
3301
116
4991
W I D
E
60/A
1312.27
67
4340
27/A
4062.81
27/B
3607
F6
F9
8/A
8/C
836
F8
8/B
580
20
1263
TO 2
11
.1
O
36
600
48/39
61
2546.84
38
7540
11
ID
F5
37
1000
56
2546.84
11
26
4191
111
3325.22
40'-0
48/38
112/A
117
5084.54
60'-0"
55
3337.72
R 20/A
1025.51
F4
W
TO
21
ID
3
20
TO 6
21
48/43
A
E
39/B
2000
ID
F3
"
97
TO 4
13
5
14 O
T
4
15
O
O
F2
'-0
12
TO 7
-0"
3 0'
"
25
2835.33
'-0
F1
30
13
"
56
"
3
19
TO 2
20
'-0
69
TO 2
18
23
TO 2
19
D3
"
R
D
54
2420
62
5632.16
100/B
2808
120
5844
100/C
1521
53
2420
BW 2882.40
ID
30
21
1790.80
3
16 33
18
'-0
TO 1
6
4
12
11
TO
AD
RO
39
2420
"
'-0
52
2143
48/50
51
2331.36
50/D
/B 5
50 34
19
60
"
'-0
24
665
.2
O
30
40
2420
48/49
41
664
48/48
11
13
30
39
TO 3
4
"
'-0
E
ID
63/B
300 BW
B.6
50/C
70/A
10562.80
N O. 1
7
73
10658
48/51
63/A
756
63
2480
50/A
TO 6
9
TO 2
7
59
TO 3
5
60
D
69
1605
64
2420
123
LOW LAYING AREA

WITH STAGANATION
OF WATER
98
3444
R O
A D
71
1843.80
68
2516.80
65
2224.80
8924.20
ID
W
"
'- 0
30 48 & 49
42
2430
BW
INDIAN MEDICINE
PHARMACY
/B 4
43 2.6
3
23
TEMPLE
44
3897.48
87
TO 6
8
49
25
TO 1
3
D2
'-0
ID
72
1740
67
2420
66
2371.60
.1
NO
W
A
W I
D E
97
99/A 99/B 96
1420
1189 127 1180
N O. 25
148/A 149/B 696

1730 1055
48/57
A D
937.5
E
14
E
25
937.5
E
21
E
24
E
32
48/53
E
20
E
31
E
19
E
13
937.5
R O
148
3125
937.5
E
18
E
23
E
30
E
37
93
1124
72/A
9378
30'-0"
48/52
3.5 Laksh Capacity

Hill Side Reservoir
HILLOCK
OPEN SPACE
92/D
1950
E
36
AD
40'-0" WIDE RO
E
117
E
29
E
22
OPEN SPACE
89/E
2399.82
E
35
E
28
127
1356.40
9121.50
92/N
2017
92/C
2443.97
89/D
2519.43
89/B1
1635
48/65
73/C
268
"
89/C
92/A
1908
N O. 26
OPEN SPACE
E
7
937.50
91/B
2106
OPEN
90/M
2133.83
90/L
2805.55
90/A
76
500
75
4840
/A
43 273
2
BW
73
WELL
30
30
48/45
48/60
145
4096
130
4881
O A
91/C
3044
80/A
2648.35
W
48/58
77
500
"
'-0
'-0
/D
90 .11
1
61
/C
90 .76
8
92
78
8360.75
47
9680
60
30
O
A
NO
.2
2
74
2265
73/A
43
10164
23
6050
22
6808.60
48/46
TO 0
1
D1
"
'-0
30
40
81
9285.50
80/B
3017
131
4779
132
4665
143/B
2031
I D
134
4717
133
4591
48/62
40'-0"
48/64
83/C
1055.30
83/B
1823.00
83/A
1857.20
79
9719.02
48/66
R
86
2000
PW
D.
48/67
73/D
1560
46
9680
48/47
TO
4806
Pro
p
o se
d
ComComm
plex ercia
l
RO
AD
CH
AN
DR
AY
AN
GU
TT
O A D
R
E
I D
W
60'-0"
140
5263
139
4667
137
5867
48/63
136
3289
83/D
53382.20
84/A
1432.30
84/B
1346
84/C
1964
-7
85
7482
NH
EX
IS
TI
NG
87
4333.33
162 BW 3
344.67
88
2202.30
48/68
HOTSOPT-1
FORMER TEXTILE FACTORY
HOTSOPT-2
FORMER LEAD EXTRACTION
48/15
48/22
PERMIT NO: 14280/83 LETTER NO: 14280/ MP2/HUDA/83

LAYOUT IS RELEASED SUBJECT TO CONDICTION
MENTIONED IN LETTER NO: 14280/MP2 PL 5-4-88
SD/5-4-88
FOR VICE CHARMAN
HYDERABAD URBAN DEVELOPMENT
A. P. I. I. C. LTD, HYDERABAD REVISED

LAYOUT PLAN OF S E C KATTEDAN
PHASE I & II.
HYDERABAD A.P.
REFERENCE
SITE BOUDARY
350
67.47%
16.68%
14.20%
1.67%
A. C. 245.00
799950.36 Sq.Yds
197747.88 Sq.Yds
168432.00 Sq.Yds
19747.20 Sq.Yds
100.00%
PROPOSED
NO. OF PLOTS
TOTAL AREA
PLOTTED AREA
ROADS AREA
OPEN AREA
AMENITIES
185829.00 Sq.Yds
LANDUSE ANALYSIS
TOTAL AREA
SCALE = 1"' : 100'
Sd/IN NOTE FILE

ON 29-3-88
VICE CHIRMAN
Dy - CHIEF ENGINEER
A. P. I. I. C. Ltd
Hyderabad
LEGEND :-
- STORM WATER DRAIN
- ROAD WAY
- OPEN AREA/
COMMON FACILITIES
DRAWN BY : KK
M-2
DRAWING NO:

CHD BY :
INVENTORISATION OF OPEN AREA

SOURCE POLLUTANTS
(SOLID WASTES, TRANSFORMERS ETC.)
REVISION : 0
APPROVED BY :
SOURCE :
SCALE : As Shown
PROJECT
DATE : 21/10/2011
TITLE
HR
OA
D
OA
C
PR
AP
N O. 31
ROAD
40'-0" W I D R
N O. 29
R
E
I D
W
60'-0"
R O
A D
R
ID
O A D
RO
AD
DR
" W
I
'-0
30
28
O.
N
W
ROAD
W I
D E
"
9
14 0/B
31
60'-0"
30
'-0
GL
SR
TO
17 90/H
73
.70
23 90/I
33
.95
30 90/J
78
.46
19 90/G
67
.90
SP
AC
E
OP
EN
9
20 0/B
32
.29
161
213.85
8
99 9/A2
3.6
3
89
/A
1
RO
AD
AP
PR
OC
H
30'-0" W I D R
NO
.1
2
D
A
O
R
E
ID
W
E
60
'-0
"
I
W
40
'-0
"
8
17 9/B2
01
.23
17 90/E
08
.66
D
IDE ROA
60'-0" W
142
5101
133/A
143/A
2067
48/61
134
4717
133
4591
48/62
O
.
TO SHADNAGAR
24
141
2985
140
5263
139
4667
40'-0"
135
4324
82
144/A
2151
131
4779
132
4665
143/B
2031
80/B
3017
144/B
2115
48/59
"
146
4210.90
60'-0"
E
8
1050
MOSQUE
129
1530
91/A
2058
92/B
1908
W
E
9
126
716
1471
4629
I
E
10
E
937.5
E
11
2620
937.5
E
12
E
31
E
24
E
19
E
13
937.5
148
3125
937.5
E
18
E
23
E
30
E
37
48/57
149/A
E
39
E
40
E
34
94
2397
160
8875.39
937.5
E
15
E
16
40'-0" WIDE ROA

214/A
1600
48/54
OPEN SPACE
124 & 125
HILLOCK
HANUMAN
TEMPLE
I D
E
48/56
150
4825.61
99
2988
48/55
OPEN SPACE
121
3106
BW.9
122
2333
B.W. 14
WELL
BW.8
100/A
1339
156/H
3196
118
3975.34
119/A
3933.33
119/C
3936.33
119/B
2680.46
151
4625
153
4222
A D
60
3968.80
154
3882.38
106
4835
N O. 25
83
1452
4
23 O
7
T 0
21
24
TO
3
22
"
A
D
N
O.
N
3
D
IV
105/A
2783
29
1605
156/D
1859
48/34
156/C
1809
E
I D
'-0
60
'-0
60
"
W
"
W
I
D
R
O
R
O
N
.
O
N
.
O
HILLOCK
50000 Gallons
Hill Side Reservoir
48/29
OPEN SPACE
48/28
48/16
48/21
TO HYDERA
BAD
156/B
1806
104
4768.89
101/A
1348
103
4784.44
102
4256
16
2081.20
16/A
2470
101/B
1400
156/A
1778
16/C
1250
2
O.
16/B
1250
48/32
30
1452
16/O
2081.20
ID
15
2420
48/30
1
4730.98
1/A
5494
5/E
5567
Distribuation Pump
2
3723.90
14
2822.22
48/35
31/C
48/33
31/A
155
3637.20
105/B
1969
107
5829.13
108
4604.33
31/B
4
2924
164
907
3
2689.44
48/31
"
'-0
3
18
TO
7
18
1
O.
32
1961.60
13
4840
5/B
2000
5/C
1570
30
16/E
7260
9
16
TO
3
20
TO
3
19
TO
2
20
ID
.8
O
9
15
TO
5
14
3
18
TO
0
15
1
13
TO
7
1
13
12
TO
0
13
'-0
15
TO
24
D
5/D
2311
5/A
1200
5/D
2990
35
17
2420
12
4395.40
III
D6
O.
O
R
30
TO
14
TO
43
ID
1
11
TO
5
11
/B
34 0.4
/A 72
34 8
88
97
TO
3
10
II
.
O
0"
63
TO
67
"
'-0
25
TO
34
ID
11
2421
18
4691.80
"
'-0
.6
O
D5
ID
30
3
64
/C
34
ID
100
3032.78
30
N O.
48/37
114
4945
W
83
TO
89
49
30
TO
62
28
2420
48/40
IX
I
VI
48/42
D4
48/43
30'-
II
VI
VI
115
5033
R O
48/36
113/A
3037
152
3642
I D E
116
4991
113/B
3301
110
2640
58/C
58/E
"
'-0
73
TO
77
30
35
12100
48/41
.8
O
G
G 8/A
1048
59
3630
D
ROA
IDR
" W
53/C
111
3325.22
67
4340
2
.1
O
48/39
36
600
27/A
4062.81
27/B
3607
F7
G 6/B
1043
8/D
D3
38
7540
37
1000
56
2546.84
61
2546.84
60/A
1312.27
40'-0
48/38
112/A
117
5084.54
60'-0"
55
3337.72
11
.
O
F6
F9
A
8/C
836
F8
8/B
580
20
1263
8/A
39/B
2000
F5
ID
1
11
TO 2
11
TO 0
11
F4
26
4191
1025.51
O
R
R 20/A
F3
97
ID
3
20
TO 6
21
3
19
TO 2
20
1
23
TO 5
23
TO23
2
7
21
54
2420
62
5632.16
100/B
2808
120
5844
100/C
1521
53
2420
ID
25
2835.33
F2
"
'-0
ID
A
48/50
BW 2882.40
"
'-0
F1
30
O
D
52
2143
"
'- 0
60
51
2331.36
/B 5
50 34
19
ID
39
2420
30
21
1790.80
3
16 33
18
1
12
TO 4
2
13
13
TO 7
13
5
14 O
T
4
15
56
TO 1
6
"
'-0
D2
5/G
2699
R
A
63/B
300 BW
50/D
B.6
70/A
10562.80
N O. 17
48/51
73
10658
63/A
756
63
2480
R
50/A
50/C
"
'-0
24
665
.2
O
30
40
2420
48/49
41
664
48/48
"
'- 0
60
69
1605
64
2420
123
LOW LAYING AREA

WITH STAGANATION
OF WATER
98
3444
R O
A D
71
1843.80
68
2516.80
65
2224.80
8924.20
ID
W
"
'-0
30 48 & 49
INDIAN MEDICINE
PHARMACY
BW
42
2430
59
30
"
'-0
69
TO 2
18
23
TO 2
19
D1
ID
72
1740
67
2420
66
2371.60
13
.
NO
/B 4
43 2.6
3
23
TEMPLE
44
3897.48
87
TO 6
9
TO 6
8
TO 2
7
11
TO 4
12
30
"
'-0
AD
RO
A
73/D
4611
97
99/A 99/B 96
1420
1189 127 1180
N O. 25
148/A 149/B 696

1730 1055
A
937.5
E
38
E
27
125/D
2811
E
33
E
26
937.5
E
21
E
32
48/53
E
25
E
20
E
14
93
1124
72/A
9378
30'-0"
48/52
47
9680
E
ID
48/65
3.5 Laksh Capacity

Hill Side Reservoir
HILLOCK
OPEN SPACE
92/D
1950
E
36
D
40'-0" WIDE ROA
117
E
29
E
22
OPEN SPACE
89/E
2399.82
E
35
E
28
127
1356.40
9121.50
92/N
2017
89/D
2519.43
92/C
2443.97
89/B1
1635
73/C
268
W
89/C
92/A
1908
N O. 26
OPEN SPACE
E
7
937.50
91/B
2106
OPEN
90/M
2133.83
90/L
2805.55
90/A
76
500
75
4840
/A
43 273
2
BW
73
49
TO 3
5
39
TO 3
4
25
TO 1
3
TO 0
1
30
"
48/60
145
4096
130
4881
129
4787
O
91/C
3044
80/A
2648.35
W
48/58
77
500
22
73/D
1560
"
"
/D
90 .11
1
61
/C
90 .76
8
92
78
8360.75
A
NO
.
73/A
'-0
60
' -0
30
O
D
74
2265
46
9680
23
6050
WELL
1
GU
TT
A
48/45
'-0
30
'-0
40
81
9285.50
86
2000
48/66
79
9719.02
IN
G
48/67
48/68
43
10164
48/46
22
6808.60
TO
4806
Pro
pose
dC
Com omm
ple ercia
x
l
OA
D
CH
AN
DR
AY
AN
DETAIL-2
FORMER LEAD EXTRACTION
O A D
R
E
D
I
W
60'-0"
N O. 31
ROAD
40'-0" W I D R
N O. 29
R O
E
28
O.
N
I D
E
W
60'-0"
D
I
W
60'-0"
48/63
136
3289
83/B
1823.00
48/64
83/C
1055.30
83/A
1857.20
EX
IS
T
87
4333.33
162 BW 3
344.67
88
2202.30
48/47
ROAD
137
5867
83/D
53382.20
84/A
1432.30
84/B
1346
84/C
1964
85
7482
N
H7
PW
D.
19 90/G
67
.90
17 90/H
73
.70
DETAIL-1
48/15
48/22
PERMIT NO: 14280/83 LETTER NO: 14280/ MP2/HUDA/83

LAYOUT IS RELEASED SUBJECT TO CONDICTION
MENTIONED IN LETTER NO: 14280/MP2 PL 5-4-88
SD/5-4-88
FOR VICE CHARMAN
HYDERABAD URBAN DEVELOPMENT
A. P. I. I. C. LTD, HYDERABAD REVISED

LAYOUT PLAN OF S E C KATTEDAN
PHASE I & II.
HYDERABAD A.P.
REFERENCE
SITE BOUDARY
350
799950.36 Sq.Yds
197747.88 Sq.Yds
168432.00 Sq.Yds
19747.20 Sq.Yds
100.00%
67.47%
16.68%
14.20%
1.67%
A. C. 245.00
185829.00 Sq.Yds
PROPOSED
NO. OF PLOTS
TOTAL AREA
PLOTTED AREA
ROADS AREA
OPEN AREA
AMENITIES
LANDUSE ANALYSIS
TOTAL AREA
SCALE = 1"' : 100'
Sd/IN NOTE FILE

ON 29-3-88
VICE CHIRMAN
Dy - CHIEF ENGINEER
A. P. I. I. C. Ltd
Hyderabad
- STORM WATER DRAIN
LEGEND :-
- ROAD WAY
- OPEN AREA/
COMMON FACILITIES

KATTEDAN INDUSTRIAL
REVISION : 0
APPROVED BY :
CHD BY :
DRAWN BY : KK
DRAWING NO:
MAP INVENTARISATION OPEN DRAINS
SCALE : As Shown
SOURCE :
DATE : 21/10/2011
TITLE OWNER PROJECT
RO
AD
RO
AC
H
AP
P
23 90/I
33
.95
30 90/J
78
.46
A D
RO
AD
" W
IDR
'-0
30
GL
SR
TO
9
14 0/B
31
R O
A D
ID
W
30
'-0
"
E
D
I
161
213.85
8
99 9/A2
3.6
3
89
/A
1
RO
AD
PR
OC
H
30'-0" W I D R
NO
.1
2
D
A
O
R
E
ID
W
"
60
'-0
W
40
'-0
"
89
17 /B2
01
.23
AP
17 90/E
08
.66
SP
AC
E
OP
EN
9
20 0/B
32
.29
DE ROAD
60'-0" WI
APPENDIX IV
SAMPLING MAPS
Witteveen+Bos, appendix IV to report IND50-1/berr9/066 dated April 11, 2011
KIE (include investigation map Former Textile factory and former lead extraction factory
Lake NMK
Plains downstream
LEGEND
PROPOSED BLOCK
2
E
S
ROAD
HABITATION
INDUSTRY
AGRICULTURE
SS3-6
LAND WITHOUT SCRUBS
Lake
LAND WITH SCRUBS
Adarsh Nagar
SS3-5
WATER BODY
SAMPLING LOCATION
DW3-4
DW3-5
P3-4
8
- SEDIMENT SAMPLING
DW3-3
SW3-4
- TOPSOIL DRILLING
- PIEZOMETER
SS3-4
- SURFACE WATER
DW3-2
SS3-3
SW3-3
DW3-1
- (DEEP) WELL
SCALE
SW3-2
2
3SS
1
3SS
SW3-1
100
200
300
400M
P3
-2
10
3
3-
NH
-7
11
P3
-1
14
PROJECT
13

TITLE
12
Sampling Map
REVISION : 01
DRAWN BY : KK
SCALE : As Shown
CHD BY :
DATE : 21/10/2011
APPROVED BY :
DRAWING NO:
SOURCE : Enhence Version of Google Earth Dated: Jan/2011
LEGEND
N
PROPOSED BLOCK
W
S
ROAD
INDUSTRY
HY
DE
RA
BA
D
WATER BODY
SAMPLING LOCATION
- SEDIMENT SAMPLING
- TOPSOIL DRILLING
- PIEZOMETER
- SURFACE WATER
NMK Pond
SCALE
-3
STP
200
300M
PROJECT

TITLE
SW
24
SH
AD
NA
GA
R
TO
-4
S2
100
S2
-2
S2
S2
-1
NH 7
P2
-1
SW
2- SS
5
2-
S2
-6
P2
-4
LAND WITH SCRUBS
TO
P3
-1
P3
SS
S2
-2
SS
2SS
-7
6
222
11 S
SS
S2
P2
2-1
SS
SS
-5
1
2
SW
S2
7
2
2
-5
-3
-7
2SS
3
SS
2SS
SS
18
2213
S2
2- SS
SW
23
8
2-8
2
4
S
-1
SS
S2
SS
SS
S
2
-1
S2
-2
2P2
29
4
-9
14
5
-2 S
2SS
SS
SS
SS
9
222210
15
25
P1
20
SS
-1
SS
2
SS
SS
SW
-1
26
2221
226
29
2
SS
SS
2SS
22
2230
27
SS
SS
228
231
SS
S2
2-1
32
0
P2
-3
P1
-2
LAND WITHOUT SCRUBS
Sampling Map Lake NMK
REVISION : 01
DRAWN BY : KK
SCALE : As Shown
CHD BY :
DATE : 21/10/2011
APPROVED BY :
DRAWING NO:
DE
RA
BA
D
E
S
TO
HY
LEGEND
S1-14
S1-15
PROPOSED BLOCK
ROAD
S1-13
S1-11
P1-2
S1-8
SW1-2
SW1-1
SS1-2
SS1-3
12
S1-2
14
S1-49
S1-42
S1-33 S1-34
S1-4
S1-35
S1-30
S1-52
- TOPSOIL DRILLING
- PIEZOMETER
S1-53
- SURFACE WATER
S1-43
S1-57
S1-45
S1-36
KATTEDAN INDUSTRIAL AREA
S1-1
- SEDIMENT SAMPLING
S1-54
S1-47
S1-29
SAMPLING LOCATION
S1-55
S1-48
S1-28 S1-40 S1-39
WATER BODY
S1-56
S1-25
S1-27
S1-6
AR
SH
AD
NA
G
TO
S1-50
S1-46
S1-44
SCALE
S1-37
SW1-3
S1-38
N
-7
H
100
200
300
400M
S1-60
S1-31
S1-32
13
LAND WITH SCRUBS
S1-41
S1-5
S1-3
S1-21
S1-24
S1-10
S1-7
INDUSTRY
S1-51
LAND WITHOUT SCRUBS

S1-22
S1-23
S1-9
P1-1
S1-12
S1-20
S1-58
S1-59
PROJECT
SS1-1
11
S1-18
S1-16 S1-17
RAILWAY LINE
TITLE
10
S1-19

Map showing Landuse/Sampling Locations
in the Block Area
REVISION : 01
DRAWN BY : KK
SCALE : As Shown
CHD BY :
DATE : 21/10/2011
APPROVED BY :
DRAWING NO:
ROA
S2
S1
S3
- TOPSOIL DRILLING
FORMER LEAD EXTRACTION FACTORY

SCHEMATIC OVERVIEW
TITLE OWNER PROJECT
SAMPLING LOCATION
KATTEDAN INDUSTRIAL
REVISION : 0
DRAWN BY : KK
SCALE : N.T.S.
CHD BY :
DATE : 21/10/2011
APPROVED BY :
SOURCE :
DRAWING NO:
S2
O
A
S5
S6
M
ai
n
- TOPSOIL DRILLING
SAMPLING LOCATION

SCHEMATIC OVERVIEW
try
En
Storage Place
S4
S1
Former
Textile Factory
S7
S3
Former
Waste Water
Treatment Plant

FORMER TEXTILE FACTORY SCHEMATIC

OVERVIEW
REVISION : 0
APPROVED BY :
CHD BY :
DRAWN BY : KK
DRAWING NO:
SITE LOCATION PLAN
SCALE : N.T.S.
SOURCE :
DATE : 21/10/2011
TITLE OWNER PROJECT
APPENDIX V
CHECKLIST FIELD WORK EQUIPMENT
Witteveen+Bos, appendix V to report IND50-1/berr9/066 dated April 11, 2011
Witteveen+Bos, appendix V to report IND50-1/berr9/066 dated April 11, 2011
CHECKLIST FIELDWORK NMK

Description
1. Sampling equipment
Slib / soil containers (bags/bottles)
Buckets for mixing samples
Plastic (several m)
Auger
Piston sampler / vaccuumsampler
Measure device water level
Measure device water level Piezometers/Wells
Dinghy/ boat/ raft / ponton
Motor
Half pipe
GPS system
Measuring tape / rule
Cooling device for samples
2. Personal safety gear & hygiene

Water for hygienic purposes /Jerry cans
Soap
Overall / appropriate clothing
safety shoes /boots
Gloves
Helmet
Safety glasses
Goggles
Cup-shape respirator
Wading boots
Life jackets / vest (with whistle)
Whistle
Eye cleaner
First aid kit
Protection against the sun
3. Others
Knife
Scissors
Spade
Mobile phone
APPENDIX VI
FIELD WORK FORMS
Witteveen+Bos, appendix VI to report IND50-1/berr9/066 dated April 11, 2011
Bore hole description

Location sampling points (X, Y, Z)
Daily reports
Bore hole description

Witteveen+Bos India
Kadam
Hyderabad - 500 034
Environmental
Consultants
India
telephone +91 40 4433 4140
fax message +91 40 4433 4444
subject
client
project code
Bore hole description fieldwork lake NMK

IND50-1
location
date
Sample code
Water depth (m)
Sample depth (m-swl)
Soil type
Color
Comments
Location sample
points
Witteveen+Bos India
Hyderabad - 500 034
Kadam
India
Environmental
Consultants
telephone +91 40 4433 4140

fax message +91 40 4433 4444
subject
client
project code
Location sample points fieldwork lake NMK

IND50-1
location
date
Reference point
Sample code
X-axis
Y-axis
Z-axis
Daily report
Witteveen+Bos India
Hyderabad - 500 034
Kadam
India
Environmental
Consultants
telephone +91 40 4433 4140

fax message +91 40 4433 4444
subject
client
project code
Daily report fieldwork lake NMK

IND50-1
location
date
1. Persons
Name
Field work team
J.J. Stolte
Company
Function
Time in
W+B
Kadam
Kadam
Kadam
leader of survey team

field assistant
field assistant
field assistant
Time out
Others
2. Weather conditions
Weather conditions
Temperature
3. Activities carried out (soil /sludge samples)
Wind velocity
Wind direction
Bore Log
Kadam
Environmental
Consultants
Boringnumber /
wellnumber:
Coordinates
Date:
X=
GPS -instrument:
Y=
Fieldtechnician:
page..of
groundwaterlevel (cm-gl) 1):
Color (4)
Sample description
samplenumber
(6):
Barcode
3= much
other (5):
1= little
3= much
1= little
0 = none
oilperceptions
3= much
1= little
course
moderate/solid
fine/watery
0 = none
organic matter
Sand
Clay
/water/
Depth (from-till m- slush
gl)
(3)
additionals:
0 = none
Soildiscription (2)
other remarks
well length (cm -top):

top (+/-) groundlevel:
diameter (cm):
screenlength:
1) fill in cm below groundlevel or - (not found)
2) choose between Sand (fine, moderate or course) or Clay and fill in organic matter (0, 1,2 or 3)
3) fill in water or slush in case of investigation of sediments
4) fill in DR (dark) or BR (brown), YE (Yellow), BL (Black) etc
5) fill in additionals from human recources (waste, debris, etc)
6) fill in numer boring plus number sample (1-1, 1-2 etc)
Open Drains Log
K a da m
En vi ro n m e n t a l
C o n s u l ta n t s
Open Drain Log
page 1 off.
Project code
Date:
Fieldtechnician
GPS type
Number of the drain (mark on map):

length
(m)
total length (m):
width
(m)
picture
(number)
drawing number (1)
section 1
section 2
.
flowdirection (mark on map)

location (coordinates and
mark on map)
begin
x=
Y=
end
x=
Y=
number
position individual inflow

points (coordinates and
mark on map):
visual contamination
Number drain or individual
inflow point
description
picture remarks
Other remarks
1) add a drawing per drain or section
4. Discussion points
Witteveen+Bos, dated October 20, 2011
Well-inspection log
K adam
En v i r o n m e n t a l
C o n s u l ta n t s
Project code
Date:
Fieldtechnician
Number:
Type:
Coordinates
GPS-type
A=
B=
C=
D=
Picture:
Well / Deepwell / Deepwell with pump/other:
X=
Y=
Z=
cm
cm
cm
cm
D
A
groundlevel
C
B
groundwater
level
A=
top of well relative to groundlevel
B=
bottom of well
C=
groundwaterlevel relative to top of well
D=
diameter well
Visual observations
Is there any groundwater pumped?
Are there any ditches present on or around the location (mark on map)
What is the condition of the terrain on and around the location. Are there signs of waste dump,
or leakage of oil or other pollutants?
Wich activities are taken place on and around the location:
Other remarks
APPENDIX VII HEALTH & SAFETY FORMS
Witteveen+Bos, appendix VII to report IND50-1/berr9/066 dated April 11, 2011
Formal toolbox meeting

Format register of attendance
Format job safety analysis
Register of
attendance and
toolbox meeting
Witteveen+Bos India
Kadam
Environmental
Consultants
Hyderabad - 500 034

India
telephone +91 40 4433 4140
fax message +91 40 4433 4444
subject
client
project code
Register of attendance and toolbox meeting

IND50-1
1. Register of attendance field work team and others

name
company
function
date
location
signature
name
company
function
date
location
signature
Witteveen+Bos India, IND50-1 register of attendance and toolbox meeting
name
company
function
Witteveen+Bos India, IND50-1 Register of attendance and toolbox meeting
date
location
signature
name
company
function
date
location
signature
Witteveen+Bos India, IND50-1 register of attendance and toolbox meeting
Job Safety Analysis

Control No.: 1
JSA Type:
Office
Transport
Construction
Operations & Startup
Investigation
Co:- APPCB
Fabricator or
Field work &
Department:- NMK project
Work Type: Environmental survey
Date:
20-10-2011
Location: NMK
Work Activity: Soil, sludge, ground water and

surface water sampling
Personal Protective
Equipment (PPE):
Lifeline/Body
Harness
Cup shaped
respirator
Life Vest
Goggles
Hearing
Protection
Air Purifying
Respirator
Other: appropriate
clothing / overall
Hard Hat/Helmet
Welding/Pipe
Clothing
Face Shields
Safety Glasses
Safety Shoes
/Boots
Development Team
P. Van den bossche (Peter)
J.J Stolte (Jan Jacob)
New
Revised
Job Activities
Gloves
Welding
Mask/Goggles
Position/Title
Reviewed By
Position/Title
Leader of
survey team
Environmental
Supervisor
Date
20-102011
20-102011
Potential Hazards
Critical Actions
1.
Conduct pre-start meeting

including JSA PTW
review & equipment
check
Personnel not aware of hazards &

controls
2.
Load/Unload & prepare

equipment sampling
gear & PPE
Manual handling risks

Sharp objects & pinch points
Equipment not available
3.
Take required samples
Unbalanced body position to operate

auger
Contaminated material
4.
Mixing soil sample into

bucket / bottle / plastic
bag
5.
Clean equipment &

prepare samples for
transport to storage
location
Contaminated/soiled equipment
6.
Store soil / sludge
Unclean external surfaces of bottles /
Discuss risks, use coordinated lifting

technique, ensure adequate labor to
assist with manual activity
Identify pinch point hazards &
communicate with work crew, use
gloves & supervise activity
Develop equipment list & cross check
Work slowly & safely no rush
approach
First aid kit & trained first aider
Develop communication system (eg.
Use radio, hand signals, walky talky,
whistle etc)
Use correct PPE to prevent
contamination
Discuss & coordinate procedure to
ensure that auger is handled carefully
Take care not to unnecessarily spill
contaminated material on PPE
Minimize contact with contaminated
material
Use dust mask & goggles to prevent
contamination
Emergency response plan
Use correct PPE to prevent
contamination
Minimize contact with contaminated
material
Provide adequate water supply to
thoroughly rinse personnel &
equipment
Provide barrier protection if
transporting material inside vehicles
(e.g. tarp/plastic)
Ensure all bottles / plastic bags are
Organize & conduct pre-start meeting

Provide Russian translation
General Permit to Work
Equipment checklist
Responsible
Party
Peter & Jan Jacob
Peter & Jan Jacob

each member of survey team
Peter & Jan Jacob

Peter & Jan Jacob

Peter & Jan Jacob

Peter
samples in refrigerated
storage
plastic bags
7.
Reorganize equipment for

next day
Manual handling risks

Sharp objects & pinch points
Equipment not available/lost
8.
Prepare transport of soil /

sludge samples to
laboratory
Unclean external surfaces of bottles /

plastic bags
9.
General risk (1)
Ramadan observance is respected

however it could place personnel at
risk if they are required to work for
extended in hot or cold conditions
12. General risk (2)
Tiredness / sickness / feeling of

being unwell during field work
activities
clean & ready for storage

Ensure contaminated material is
appropriately segregated from other
materials
Discuss risks, use coordinated lifting
technique, ensure adequate labor to
assist with manual activity
Identify pinch point hazards &
communicate with work crew, use
gloves & supervise activity
Use correct PPE to protect hands etc.
Develop equipment list & cross check
Ensure all bottles / plastic bags are
clean & ready for storage and
transportation by train
Ensure contaminated material is
appropriately segregated from other
materials during transportation
Provide barrier protection during
transportation (e.g. plastic)
Ensure personnel are aware of the
hazards & risks
Instruct personnel that they are to
communicate when they are getting
tired or need a break
Ensure regular breaks & a shaded
place to rest
Instruct personnel that they are to
communicate when they are getting
tired or need a break
Ensure regular breaks
In case of emergency: stop activities,
emergency response plan
Peter
Peter & Jan Jacob

laboratory specialist
Peter
Peter & Jan Jacob

JSA Sign Off

Name
Position
Company
Signature
APPENDIX VIII
ADDITIONAL INFORMATION HEALTH & SAFETY
Witteveen+Bos, appendix VIII to report IND50-1/berr9/066 dated April 11, 2011
SNAKES
1. Common Krait - Bungarus caeruleus
The common krait (Bungarus caeruleus) is a type of krait that is found in the jungles of the
Indian subcontinent. This snake is highly venomous, and is one of the "big four" snakes in
India.
Description
The body colour varies from a dark steely blue-black to a pale faded bluish grey. The
average length is 1 m (39 in.). Subcaudal scales after the anal plate are not divided. It has
large hexagonal scales running down its spine. The narrow white cross bands are more
prominent near the tail region. The male is larger than the female and also has a longer tail.
Geographic range
Peninsular India from Sindh (Pakistan), to the West Bengal plains. It occurs throughout
South India and Sri Lanka.
Habitat
Inhabits a wide variety of habitat in its range. It is found in fields, low scrub jungle as well as
inhabited areas. They are known to take up residence in termite mounds, brick piles, rat
holes and also inside houses. It is fond of water and is frequently found in it or within
proximity to a water source.
Feeding
These snakes prey on other snakes, lizards, frogs, rats, and mice. They will devour their
young being cannibalistic in nature. Young are known to eat arthropods. As per Daniels,
the common krait feeds primarily on other snakes, including "blind worms" (snakes of the
genus Typhlops) and other kraits, and also feeds on frogs and lizards and small mammals.
This snake is nocturnal. It is very active and agile at night. It often hides in rodent holes,
loose soil or beneath debris, so it is rarely seen during day.
Behavior
Behavioral differences during day and nighttime have been reported in Bungarus
caeruleus. During the day it is sluggish and rolls its body into a loose coiled ball, keeping its
head well-concealed. In balled condition, the snake allows considerable handling, however,
over handling often instigates bites. At night the snake is very active, escapes by hissing
loudly, or keeping still, occasionally biting the source of the annoyance. When agitated, it
will coil up with head concealed, body flattened, and makes jerky movements. May also lift
its tail. Reluctant to bite, but when it does bite, it typically bites and holds on for awhile,
which enables it to inject considerable amounts of venom. Generally docile and
unaggressive during the day, it may become aggressive at night. The untreated mortality
rate from its bites can be very high. This snake is regarded as one of the most dangerous
Bungarus species.
Venom
The Indian krait's venom consists of neurotoxic which induces muscle paralysis. Clinically,
their venom contains pre-synaptic neurotoxins. These neurotoxins generally affect the
nerve endings near the synaptic gap of the brain. Kraits are nocturnal and seldom
encounter humans during daylight hours, so incidents are rare. There is frequently little or
no pain from a krait bite and this can provide false reassurance to the victim. Typically,
victims complain of severe abdominal cramps, accompanied by progressive paralysis.
Once bitten, the absorption of the venom into the victim can be considerably delayed by
applying a pressure bandage to the bite site (using about the same tension as one uses for
a sprained ankle) and immobilising the area. This allow for gentle transport to medical
facilities, where the venom can be treated when the bandage is removed. As there are no
local symptoms, a patient should be carefully observed for signs of paralysis (e.g., the
onset of ptosis) and treated urgently with antivenin. It is also possible to support bite victims
via mechanical ventilation, using equipment of the type generally available at hospitals.
Such support should be provided until the venom is metabolised and the Victim can
breathe unaided. If death occurs it takes place approximately 6-8 hours after the krait bite.
Cause of death is general respiratory failure, i.e., suffocation. Often in rainy season the
snakes come out of their hiding places and find refuge on dry places inside a house. If
bitten by it in sleep the victim seldom comes to know as the bite feels more like an ant bite
or a mosquito bite. The victim can well be dead before he even wakes up.
2. Indian cobra, Naja naja
Naja naja or the Indian cobra is a species of highly venomous snake found in the Indian
subcontinent. It is one of the "big four", species inflicting the most snakebites in India. This
snake is revered in Indian mythology and culture, and is often seen with snake charmers. It
is now protected in India under the Indian Wildlife Protection Act (1972).
Description
On the rear of the snake's hood are two circular ocelli patterns connected by a curved line,
evoking the image of spectacles. Hindus believe them to be the footmarks of Krishna, who
danced on Kliy snake's head. An average cobra is about 1.9 meters (6 feet) in length and
rarely as long as 2.4 meters (nearly 8 feet). The spectacle pattern on the hood varies
greatly, as does the overall colour of the snake.
The Oriental Ratsnake Ptyas mucosus is often mistaken for the cobra; however this snake
is much longer and can easily be distinguished by the more prominent ridged appearance
of its body. Other snakes that resemble Naja naja are the Banded Racer Argyrogena
fasciolata and the Indian Smooth Snake Coronella brachyura.
The genus name Naja comes from Indian Languages. The Indian Cobra or Spectacled
Cobra, being common in South Asia, is referred to by a number of local names deriving
from the root of Naag (Hindi, Sanskrit, Oriya, Marathi), Moorkan (Malayalam), Naya
(Singhalese), Naaga Pamu (Telugu), Nagara Haavu (Kannada), Nalla pambu or Naja
Pambu (Tamil) and Gokhra (Bengali). The most distinctive and impressive characteristic of
the Indian cobra is the hood, which it forms by raising the anterior portion of the body and
spreading some of the ribs in its neck region when it is threatened.
Lifecycle
The Indian cobra is native to the Indian subcontinent which includes present day Pakistan,
India, Bangladesh and Sri Lanka. It can be found in plains, jungles, open fields and the
regions heavily populated by people. Its distribution ranges from sea-level up to 2000m.
Cobras normally feed on rodents, toads, frogs, birds and other snakes. Its diet of rats leads
it to areas inhabited by humans including farms and outskirts of urban areas. Indian cobras
are oviparous and lay their eggs between the months of April and July. The female snake
usually lies from 10 to 30 eggs in rat holes or termite mounds and the eggs hatch 48 to 69
days later. Newborn cobras measure between 8 and 12 inches (2030 cm). The young
when hatched are exact replicas of the parents and have fully functional venom glands.
Indian Cobra outside a home in Yelandur, Karnataka, South India.
Venom
The Indian cobra's venom contains a powerful post-synaptic neurotoxin. The venom acts
on the synaptic gaps of the nerves, thereby paralyzing muscles, and in severe bites leading
to respiratory failure or cardiac arrest. The venom components include enzymes such as
hyaluronidase that cause lysis and increase the spread of the venom. The toxicity of its
venom is similar to that of the Chinese cobra and it is one of the most venomous Naja
species based on LD50 value in mice. Symptoms of cobra envenomation can begin from
15 minutes to two hours after the bite, and can be fatal in less than an hour.
The Indian Cobra is one of the Big four and a polyvalent serum is available for treating
snakebites by these snakes. Zedoary, a local spice with a reputation for being effective
against snakebite, has shown promise in experiments testing its activity against cobra
venom.
The venom of young cobras has been used as a substance of abuse in India, with cases of
snake charmers being paid for providing bites from their snakes. Though this practice is
now seen as outdated, symptoms of such abuse include loss of consciousness, euphoria,
and sedation.

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Andhra Pradesh Pollution Control

Consultancy Services for

Andhra Pradesh Pollution Control

Consultancy Services for

M. van der Wijk BSc

April 11, 2011

M. van der Wijk BSc

telephone +91 40 4433 4140

2. GENERAL SITE DESCRIPTION

4. FIELD WORK PLAN

6. DETAILED SAMPLING AND ANALYSIS PROGRAMME

7. HEALTH & SAFETY PLAN

8. WORK SCHEDULE AND PEOPLE INVOLVED

Andhra Pradesh Pollution Control Board

Andhra Pradesh Industrial Infrastructure Corporation

Central Pollution Control Board

Hyderabad Metropolitan Development Authority

India Meteorological Department

Ministry of Environment & Forests

National Geophysical Research Institute

National Program for Rehabilitation of Polluted Sites

State Pollution Control Board

Dense non-aqueous phase liquid

Environmental Protection Agency

Full Tank Level

Health & Safety

meters below ground level

meters below surface water level

Kattedan Industrial Area

Kattedan Industrial Estate

Million Liters per Day

Nederlandse Norm - Dutch guidelines

Noor Mohammed Kunta

Polycyclic Aromatic Hydrocarbons

Preliminary site investigation

Sewage Treatment Plant

Soil Quality Guidelines Level

Total Dissolve Solids

Total Petroleum Hydrocarbons

Volatile organic carbons

Wastewater Treatment Plant

General objective of the Sampling Protocol

Scope of the Sampling Protocol

Set-up of the report

GENERAL SITE DESCRIPTION

Lake Noor Mohammed Kunta

General view Katedan Industrial Area

Uncontrolled solid waste

STP HMD (including collector)

Flooded area hotspot (highly contaminated) next to the collector

Geological and (geo)hydrological description

Geological cross section A-A

History of the site

Draft conceptual site model

Overview guidelines sampling protocol and investigation strategy

Investigation of the environmental quality of sediments.

Strategy for preliminary investigation prior to sediment

Investigation of the environmental quality of soil and soil

Strategy for preliminary investigation prior to exploratory

Investigation of the environmental quality of sediments.

Decree on soil remediation and soil protection (October

Hazardous Waste Sites - EPA.

Techniques and Strategies.

Handbook Soil, Groundwater and Aquatic Sediment Survey