Professional Documents
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Michael et al.
(54)
HYDROPHOBIC SILICA
(*)
Notice:
(65)
(63)
6,124,392 A
9/2000
6,193,795 B1
(DE)
11/2001
Troll et al.
524/492
106/484
............... .. 427/220
0 010 655
0 280 851
0 808 880 A2
2 225 570
55-51714
63-054485
63-209715
6-087609
JP
06-087609
6-503048
2000-256008 A
WO92/13694
5/1980
9/1988
11/1997
6/1990
4/1980
3/1988
8/1988
3/1994
*
3/1994
4/1994
9/2000
8/1992
OTHER PUBLICATIONS
O?ice,
http://WWWl9.ipdl.ncipi.go.jp/PAl/cgi-bin/PAlINDEX
Int. Cl.
B01] 2/30
C01B 33/145
C01B 33/159
(2006.01)
(2006.01)
(2006.01)
* cited by examiner
(52)
(58)
516/100
428/405
423/335
523/213
(30)
(51)
10/1991
(60)
5,057,151 A *
JP
JP
WO
Feb. 5, 2004
5,429,873 A
5,686,054 A
5,959,005 A
6,316,050 B1
US 7,282,236 B2
(57)
ABSTRACT
References Cited
1/1975
1/1976
4,877,595 A
7/1987
Burger
. ... .. ... ..
524/268
23/293 R
. . . . ..
of dispersions.
424/47
1 Claim, No Drawings
US 7,282,236 B2
1
HYDROPHOBIC SILICA
REFERENCE TO RELATED APPLICATIONS
Huls AG.
20
folloWing advantages:
30
50
unchanged.
ppm.
55
60
EXAMPLE 1
(CH3)3
Aerosil R 202, Aerosil MS 202, Aerosil MS 202, Aerosil R
106 or Aerosil R 104 having the group
pared.
US 7,282, 236 B2
4
3
The following de?nitions apply:
CF =
VV 60 =
VV 90 =
1O
1.
15
PA
444701
444702
444703
444704
444705
444706
444707
444708
AER
AER
AER
AER
AER
AER
AER
AER
444709
444710
444711
202
202
202
202
805
805
805
805
AER812
AER812
AER812
CF
CF
W60
W90
bulk
CF
W60
W90
bulk
CF
VV60
459
456
382
430
190
185
178
39
43
Test method
0330
0335
0340
Thickening action
11.7
13.3
11.5
0410
127
102
92
0420
Methanol Wetability
45
44
50
0701
Tamped density
0920
Agglemerate strength
54.4
54.7
45
49.4
52. 8
50
51
75
11
20
18
181
42
41.7
44
62
55
68
15
15
20
0930
24
27
36
19
0955
Elfectiveness
258
274
203
266
235
260
236
258
166
185
169
0965
Elfectiveness(UT)
280
290
226
295
271
281
270
288
197
213
209
0975
$ettling(effectiveness)
15
15
15
10
15
10
13
15
444712
444713
444714
444715
444716
AER
AER
AER
AER
AER
444717
444718
444719
444720
444721
444722
444723
812
812$
812$
812$
812$
U$202
U$202
U$202
U$204
U$204
U$204
U$204
VV90
bulk
CF
W60
W90
bulk
CF
VV60
bulk
CF
W60
W90
350.4
377.6
380.8
379.2
350.4
358.4
368
50.7
45.9
45.3
49.9
47
52.6
39
50
67
44
45
57
71
10
15
16
23
PA
Test method
0330
Viscosity, epoxy
before cure
0335
0340
Thickening action
11.1
17.3
0410
77
93
110
110
0420
Methanol Wetability
49
50
58
17.3
18.2
50.7
17
100
0701
Tamped density
73
0920
Agglemerate strength
22
75
0930
12
27
36
20
0955
Elfectiveness
159
168
169
187
209
320
304
320
186
193
192
201
0965
Elfectiveness(UT)
225
201
200
216
235
336
327
346
223
225
225
230
0975
$ettling(effectiveness)
15
10
10
10
10
10
28
US 7,282,236 B2
5
EXAMPLE 2
g/l
Effectiveness, ethanol
AB R 812,
AB R 812,
AB R 812,
compacted
compacted
uncom-
RHE
RHE
pacted
UB 3847-1
UB 3847-2
(4)
UB 3847-3
(5)
10 kg
sack
15 kg
sack
20 kg
sack
50
87
106
approx.
50
184
214
209
216 1)
218
260
290
236 1)
10
AB R 812
RHE
speci?c.
(0955)
Effectiveness (UT),
ethanol (0965)
Settling
vol. %
1)
(effectiveness, high
speed mixer)
5 rpm
50 rpm
in days
[mPa*s]
(mPa*s)
T.I.
16600
80-85 11
4460
3.72
50
15100
50-60 11
4060
3.72
4020
3.73
15100
50-60 11
60
sample.
EXAMPLE 3
Applicational Properties.
US 7,282,236 B2
7
AB R 202,
AB R 202,
AB R 812,
compacted
compacted
uncompacted
RHE
RHE
UB 3848-1
2-02024
UB 3848-2
2-01024-
UB 3848-3
2-01024-
10 kg
(2)
(3)
RHE
sack
15 kg sack
20 kg sack
speci?c.
g/l
51
319
346
93
334
365
119
336
373
approx. 60 3)
334 1)
339 1)
vol. %
10
AB R 202