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Single particles
Agglomerates
Contents
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Moisture
Time
Time
3. CFD simulations
Velocities
Temperatures
Moisture
Deposits
Atomization
Different atomization modes
Configurations
Three spray drying configurations
Open-mode design
Feed
Rotary atomizer
In rotary atomization, the feed is centrifugally accelerated to high velocity in the
atomizer wheel before being discharged into the hot drying gas. The degree of
atomization and particle morphology depends upon peripheral speed, feed rate,
liquid properties and atomizer wheel design. Particle size is adjusted by changing
the peripheral speed. The rotary atomizer, considered the most flexible atomizing
device, is suitable for a wide range of products.
Two-fluid nozzle, co-current or fountain mode
Two-fluid nozzle atomization is achieved pneumatically by high-velocity
compressed air/gas impacting the liquid feed. Particle size is controlled by
varying the nozzle flow ratio between atomizing gas and feed. When operating
in co-current mode, the nozzle tip is placed close to the outlet of the ceiling air
disperser. The co-current mode is selected when drying heat-sensitive products.
When coarse particles of a non-heat-sensitive feed are required, the two-fluid
nozzle in fountain mode is appropriate.
Pressure nozzle, co-current or fountain mode
With a pressure nozzle, atomization is the result of the conversion of pressure
energy within the liquid feed into kinetic energy of a moving thin liquid sheet.
Pressure applied to the liquid within the nozzle forces the liquid out of the
orifice creating the atomization. A pressure nozzle can be operated in co-current
mode or in fountain mode. Particle size is adjusted by changing the feed pressure
and nozzle size. Pressure nozzles will generally deliver a narrower particle size
distribution and coarser particles than other atomizer types. Selection of nozzle
type depends on the feed properties and powder specification.
Heater
Inlet air
Drying
chamber
Outlet gas
Fan
Feed
Rotary atomizer
Main powder
fraction
Dust
Frequency
Frequency
Particle size (m)
40
80
Co-current nozzle
Drying
chamber
Combi-nozzle
Combi-nozzle
Atomization options
Dust
Fines return
Fountain nozzle
3-chamber
integrated
fluid bed
Inlet air
Main powder
fraction
Closed-cycle design
Feed
Heater
Fan
Cyclone
N2 in
Bag filter
N2 out
Atomization options
Condenser
80
Fan
Inlet air
Drying
chamber
Bag filter
COMBI-NOZZLE
Cyclone
Feed
Atomization options
Bag filter
Cyclone
Drying
chamber
Inlet air
Filter
Cooling
medium
in/out
Main powder
fraction
Dust
Solvent
The GEA Niro MOBILE MINOR is the perfect choice for carrying out test
work and exploring the possibilities of spray drying. It meets the demand
for both R&D where a larger capacity is required and for small-volume
The MOBILE MINOR is available in different versions to cater for different
requirements.
utilise the same modules and configurations for different capacity levels
and product requirements. With several modules and options available,
they can be designed to meet almost every customer requirement.
Key figures
MOBILE MINOR
Nominal main process gas flow (kg/h)
80
Water evaporation capacity (kg/h)
0.5 - 6
Typical mean particle size (m)
5 - 80
Space requirements, LxWxH (m)
2.5 x 2 x 2.3
15
10
5
100 150 200 250 300 350
Water
Water
evaporation
evaporation
(kg/h)
(kg/h)
MOBILE
Two fluidMINOR
nozzle
co-current
atomization
co-current atomization
7
35
30
25
20
15
10
VSD-25
co-current
atomization
Outlet
temperature
80 C
VSD-25
co-current
atomization
120
120
100
100
80
80
60
60
40
40
20
20
50
50
Water
Water
evaporation
evaporation
(kg/h)
(kg/h)
50
20
VERSATILE-SD
, size
12.5
VSD-12.5 co-current
atomization
co-currentco-current
atomization
VSD-12.5
atomization
Organic solvent based
feed
25
Outlet temperature 80 C
Outlet temperature 90 C
Outlet temperature 100 C
Outlet temperature 110 C
250
Outlet temperature 90 C
250
Outlet temperature 100 C
200
200
Outlet temperature 110 C
150
150
100
100
50
50
50
Options
50
Rotary atomizer
Options
Rotary atomizer
Two-fluid nozzle
Feed pump
(manual/automatic)
Pneumatic hammer
Explosion membrane
Explosion suppression system
Flame arrester
Cartridge filter
Bag filter
Wet scrubber
HEPA filter
Extra data logging
CIP systems
Key figures
Nominal main process gas flow (kg/h)
Water evaporation capacity (kg/h)
Typical mean particle size (m)
Space requirements, LxWxH (m)
PRODUCTION MINOR
360
5 - 30
10 - 90
4.4 x 2 x 2.7
VERSATILE-SD
size 6.3
VERSATILE-SD
size 12.5
1250
20 - 110
20 - 140
6.5 x 4 x 6.8
Water
Water
evaporation
evaporation
(kg/h)
(kg/h)
30
50
Water
Water
evaporation
evaporation
(kg/h)
(kg/h)
Aqueous feed
35
PRODUCTION
Two fluid nozzleMINOR
co-current
atomization
co-current atomization
Water evaporation (kg/h)
500
Pressure nozzle
500
Feed pump
400
400
Pneumatic hammer
300
Explosion membrane
300
200
Explosion suppression system
200
Bag filter
100
100
Wet scrubber
HEPA
filter
50 100 150 200 250 300 350
Double
valve
50 100flap
150
200 250
Inlet
temperature
(C) 300 350
Inlet temperature
(C)
Fire extinguishing
equipment
Powder cooling systems
Air broom
JET SWEEP
External fluid bed
Extra data logging
CIP systems
applications, where a melted feed stock is atomized and turned into a freeflowing powder.
To develop the right process and select the ideal size, configuration and
equipment, the GEA Niro test centres are available for process development
and carrying out tests and trial productions.
40
80
20
60
4050
20
250
VSD-25
co-current atomization
200
250
150
The complete range of GEA Niro spray dryers are also available for operating
in closed cycle. This ensures safety, protects the environment and enables
solvent recovery.
A wide range of products suspended or dissolved in organic solvents cannot
200
100
be spray dried in a standard dryer with atmospheric air, due to the risk of an
150
50
MOBILE MINOR
explosion or fire. These products must be spray dried in a plant set up, where
100 150 200 250 300 350
Inlet temperature (C)
VERSATILE-SD
VERSATILE-SD
size 25
size 50
Nominal main process gas flow (kg/h)
2500
5000
Water evaporation capacity (kg/h)
40 - 220
80 - 440
Typical mean particle size (m)
40 - 150
80 - 160
Space requirements, LxWxH (m)
10 x 5 x 9 11 x 6 x 11.7
VERSATILE-SD, size 25
50 100 150 200 250 300 350
VSD-25
co-current
atomization
co-current
atomization
Inlet temperature (C)
100
50
50
Key figures
80
120
60
100
25
35
20
30
15
25
10
20
5
15
0
10
500
300
15
10
5
50
150
200
250
120
100
80
60
40
20
50
200
50
100
100
PRODUCTION MINOR
300
100
20
an inert gas, e.g., nitrogen, is used for eliminating fire and explosion risk.
same type of plant set up can also be used where oxidation degradation of
400
200
25
50
30
Spray dryers in closed-cycle design are available for all capacity requirements
and can also be applied for products that are suspended or dissolved in water
150
200
250
Outlet temperature 80 C
Outlet temperature 90 C
Outlet temperature 100 C
Outlet temperature 110 C
100
100
VSD-12.5
co-current atomization
Water evaporation
Water evaporation
(kg/h)
(kg/h)
Water evaporation
Water evaporation
(kg/h)
(kg/h)
120
250
200
150
100
50
50
100
150
200
250
Options
450
400
350
300
250
200
150
100
50
50
Rotary atomizer/two-fluid
pressure nozzle
Feed pump
Pneumatic hammers
Electrical heater, steam
heater or indirect gas heater
Explosion venting, flame
arrester or suppression system
Double-flap valve or rotary
valve for powder discharge
Bag filter or wet scrubber
HEPA filter
Fire extinguishing equipment
Powder cooling systems
Air broom
JET SWEEP
External fluid bed
Data logging
CIP equipment
100
150
200
250
Methylene chloride
evaporation rate at outlet gas
temperature 40 C
Acetone evaporation rate at
outlet gas temperature 50 C
GEA Niro MOBILE MINOR closed-cycle plant.
Options
Rotary atomizer
Two-fluid nozzle
Pressure nozzle
Feed pump
Pneumatic hammer
Bag filter
Wet scrubber
HEPA filter
Double flap valve
Extra data logging
Powder cooling systems
CIP systems
FSD MINOR
Water evaporation (kg/h)
The GEA Niro Fluidized Spray Dryer, FSD, is an efficient multi-stage dryer
7
6
5
4
system inside the centre fluid bed. The FSD-GRANULATOR also allows
1
50
The FSD-GRANULATOR injects liquid feed into the agglomeration area, which
35
25
20
15
10
5
100 150 200 250 300 350
Cyclone
Feed
30
50
Hot
inlet
air
50
40
Drying
chamber
30
20
10
50
Fines return
Feed
60
40
Main powder
fraction
20
50
3-chamber
integrated
fluid bed
Inlet
air
80
Outlet temperature 80 C
Outlet temperature 90 C
Outlet temperature 100 C
Outlet temperature 110 C
Options
Rotary atomizer/two-fluid pressure
nozzle
Feed pump
Pneumatic hammers
Explosion venting, quenching or
suppression system
Bag filter or wet scrubber
HEPA filter
Fire extinguishing equipment
Powder dosing equipment
10
Key figures
FSD MINOR FSDTM -4.0 FSDTM -6.3 FSDTM -12.5
Nominal main process
gas flow (kg/h)
80
400
630
1250
Water evaporation capacity
(kg/h)
0.5 - 6
5 - 25
10 - 50
20 - 90
Typical mean particle
size (m)
30 - 300
50 - 300
50 - 300
50 - 300
Space requirements,
LxWxH (m)
3 x 2.5 x 3 6 x 4 x 5 8 x 4.5 x 6.5 9 x 4 x 7
11
Process control
Process overview at a glance
Cleaning solutions
Define your requirements
Process control and automation is a vital part of any type of processing plant
Our GEA Niro stand-alone process control system features an integrated touchscreen interface and ensures easy, simple and safe operation of your plant.
Our control systems come in a range of options to suit different requirements,
12
13
with the best solutions on the market. We examine your product and its
and recommend the safety concept that is best suited to your situation.
This means reducing possible powder emissions and noise from process
Safety precautions have to be taken for both aqueous and non-aqueous
feeds, but for different reasons. With aqueous feeds, the powder is liable to
dust explosion. Most inorganic powders are not dust explosive, so no further
plants.
Flame arrester system FIKE.
precautions have to be taken. However, almost all organic powders are liable
Suppression
Nitrogen
Explosion membrane FIKE.
when the powder is suspended in air, this dust cloud can explode.
Plant zoning
One ATEX zone classification is available for gases and one for dust.
The following definitions are used for gas/dust:
Zone 0/20 An explosive mixture is frequently present during
normal operation (often defined as more than 50% of the time).
Zone 1/21 An explosive mixture is occasionally present during
normal operation.
Zone 2/22 An explosive atmosphere is normally not present and, if it is,
Zone 20
Zone 22
Closed-cycle Plant
Zoning:
14
15
GEA Group is a global engineering company with multi-billion euro sales and operations in more than
50countries. Founded in 1881, the company is one of the largest providers of innovative equipment
and process technology. GEA Group is listed in the STOXX Europe 600 Index.