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Abstract
In this practice were made five experiments that deal with melting temperature of solutions, it was carried out with a temperature descents
for different concentrations of naphthalene in acetic acid, then was determinate the melting point of the different concentration solutions,
thus founding that the solute decreases it, being 16,6C [1] for the pure solution of acid. Cryoscopic constant was calculated as 0,8C
0,1C for the experiment with insulation and 0,9C 0,1C without insulation, this explain the experimental data deviation from the
overcooling point.
Keywords:Melting point; Cryoscopic constant; Overcooling point.
Introduccin.
Experimentos.
14.8
15.7
320
15.8
15.7
340
15.7
15.7
360
15.8
15.7
380
15.8
15.7
-6.4
-5.6
-1.8
-5
1.4
-4.1
-3.5
0.9
-2.5
0.9
-2.6
0.9
-2
0.9
-1.7
0.9
-0.9
0.9
-0.2
0.9
0.5
0.9
0.8
0.9
1.1
0.9
1.4
0.9
1.8
0.9
0.8
0.9
0.9
0.9
0.8
0.9
0.8
0.9
Anlisis de resultados.
T1(Con
Chaqueta de
aire 0.1C)
23
T2(Sin
chaqueta
de
aire 0.1C)
23
20
22.2
18.4
40
21.6
15.2
60
20.7
15.6
80
20.1
15.7
100
19.1
15.7
120
19.2
15.7
140
18.6
15.7
160
18.3
15.7
180
17.5
15.7
200
16.8
15.7
220
16.1
15.7
240
15.8
15.7
260
15.5
15.7
SOLUCIN 1
40
TEMPERATURAC
20
0
0
-20
100
200
TIEMPO S
300
400
23
23
20
22.3
18
40
21.9
15
60
20.9
15.5
80
20.2
15.6
100
19.5
15.6
120
19
15.6
140
18.6
15.7
160
17.9
15.6
180
17.2
15.6
200
16.9
15.6
220
16.2
15.6
240
15.8
15.6
260
15.4
15.6
280
15
15.6
300
14.6
15.6
320
14.1
15.6
340
13.7
15.6
360
13.5
15.6
380
13
15.6
400
14.5
15.6
420
15.6
15.6
440
15.6
15.6
460
15.6
15.6
480
15.6
15.6
T2c( 0.2C)
1.1
0.9
1.4
0.9
1.8
0.9
0.8
0.9
0.9
0.9
0.8
0.9
0.8
0.9
SOLUCIN 2
40
TEMPERATURA C
20
0
100
200
300
TIEMPO S
T1
(Con
Chaqueta de
aire 0.1C)
T2
(Sin
chaqueta
de
aire 0.1C)
23
23
20
22.4
18.3
40
21.6
14.9
-6.4
60
21
15.4
-5.6
-1.8
80
20.5
15.4
-5
1.4
100
19.7
15.4
-4.1
120
19.1
15.4
-3.5
0.9
140
18.5
15.4
-2.5
0.9
160
18
15.4
-2.6
0.9
180
17.4
15.4
-2
0.9
200
16.8
15.4
-1.7
0.9
220
16.2
15.4
-0.9
0.9
240
15.7
15.4
-0.2
0.9
260
15.2
15.4
0.5
0.9
280
14.7
15.4
0.9
300
14.2
15.4
320
13.8
15.4
340
14.7
15.4
500
-20
-6.4
0.8
400
600
-6.4
-5.8
-1.7
-5
1.7
-4.4
Tiempo (s)
T1
(Con
Chaqueta de
aire 0.1C)
T2
(Sin
chaqueta
de
aire 0.1C)
1.2
80
20.8
15.2
-3.9
1.2
100
20.3
15.2
-3.1
1.2
120
19.7
15.2
-2.5
1.2
140
19.3
15.2
-1.9
1.2
160
19
15.2
-1.4
1.2
180
18.4
15.2
-0.8
1.2
200
18.1
15.2
-0.2
1.2
220
17.7
15.2
0.4
1.2
240
17.3
15.2
0.9
1.2
260
16.9
15.2
1.4
1.2
280
16.5
15.2
1.9
1.2
300
16.1
15.2
2.4
1.2
320
15.5
15.2
2.8
1.2
340
15.3
15.2
1.9
1.2
360
15.1
15.2
1.2
380
15.1
15.2
400
15.1
15.2
1.2
1.2
1.2
Fuente: Elaboracin propia.
SOLUCIN 3
40
TEMPERATURA C
20
0
0
100
200
-20
300
TIEMPO S
400
500
-6.4
-6.4
-5.5
-0.1
-5.2
4.2
-4.9
1.4
-4.2
1.4
-3.7
1.4
-3.1
1.4
-2.7
1.4
-2.4
1.4
-1.8
1.4
-1.5
1.4
-1.1
1.4
-0.7
1.4
-0.3
1.4
T1
(Con
Chaqueta de
aire 0.1C)
T2
(Sin
chaqueta
de
aire 0.1C)
0.1
1.4
0.5
1.4
23
23
1.1
1.4
20
22.1
16.7
1.3
1.4
40
21.8
12.4
1.5
1.4
60
21.5
15.2
1.5
1.4
1.5
1.4
Tiempo (s)
SOLUCIN 4
40
TEMPERATURA C
540
12.5
15.1
20
Tiempo (s)
T1
(Con
Chaqueta de
aire 0.1C)
T2
(Sin
chaqueta
de
aire 0.1C)
23
23
20
22.5
18.3
40
22.1
14
60
21.6
15
80
21.3
15.1
0
0
100
-20
200
300
400
TIEMPO S
T1 (Con Chaqueta de aire 0.1C)
T2 (Sin chaqueta de aire 0.1C)
T1c( 0.2C)
500
T1
(Con
Chaqueta de
aire 0.1C)
T2
(Sin
chaqueta
de
aire 0.1C)
23
23
20
22.5
18.3
40
22.1
14
60
21.6
15
80
21.3
15.1
100
20.7
15.1
120
20.1
15.1
140
19.7
15.1
160
19.2
15.1
180
18.8
15.1
200
18.4
15.1
220
17.8
15.1
240
17.5
15.1
260
17.1
15.1
280
16.6
15.1
300
16.2
15.1
320
15.7
15.1
340
15.6
15.1
360
15.2
15.1
380
14.8
15.1
400
14.5
15.1
420
14.3
15.1
440
13.8
15.1
460
13.6
15.1
480
13.3
15.1
500
13
15.1
520
12.7
15.1
23
20
22.5
40
22.1
60
21.6
80
21.3
100
20.7
120
20.1
140
19.7
160
19.2
180
18.8
200
18.4
220
17.8
240
17.5
260
17.1
280
16.6
300
16.2
320
15.7
340
15.6
360
15.2
380
14.8
400
14.5
420
14.3
440
13.8
460
13.6
480
13.3
500
13
520
12.7
540
12.5
560
12.1
580
12
600
15
620
15.1
640
15.1
TEMPERATURA C
SOLUCIN 5
40
Conclusiones.
20
0
0
200
-20
400
600
800
TIEMPO S
T1 (Con Chaqueta de aire0.1 C)
T2 (Sin chaqueta de aire 0.1C)
T1c( 0.2C)
T2c( 0.2C)
Discusin.
Recomendaciones.