Professional Documents
Culture Documents
Table of contents
Introduction
Standard equipment
The titrator
4.1
10
10
11
11
12
12
12
13
14
15
15
Installation
5.1
5.2
5.2.1
5.2.2
5.2.3
5.2.4
5.3
5.4
Optional accessories
Technical data
Titrator configuration
16
7.1
7.2
Titrator
Supported devices (periphery)
23
23
25
8.1
8.2
8.3
8.4
Clean casing
Clean measuring cell
Cleaning the generator electrode
Transporting the titrator
26
26
26
26
26
Disposal
27
10
28
11
Declaration of conformity
29
Table of contents
1Introduction
Simple and compact
The devices in METTLER TOLEDO's Titration Compact Line are modern, compact titrators for use in a wide vari
ety of application areas. They can be used, for example, in quality control as well as in research and develop
ment and satisfy the most demanding of requirements.
The titrators in the Titration Compact Line perfectly combine simple, easy-to-understand operation with an
extremely high level of precision and outstanding reliability. Thanks to automatic titrant recognition (Plug &
Play burettes), the titrator independently identifies which titrant is required without intervention from the operator.
Titration Compact devices can either be controlled by touchscreen or by using LabX PC software. The large col
or touchscreen allows intuitive control by the user and flexibility in its adjustment options. All functions can be
activated directly from the home screen via shortcuts which can be freely created, making everyday use
extremely simple. Controlling the titrator by touchscreen and all adjustable parameters are described separately
and in detail in the operating instructions.
This installation information explains all the steps necessary for installing and commissioning your device. The
"Quick Guide" will then guide you through the first titration process using a practical example. If you have any
additional questions, METTLER TOLEDO is always available to assist you.
Introduction
instrument is not gas tight (explosion hazard due to spark formation, corrosion
caused by the ingress of gases).
Risk of explosion
Always test the titration vessel for firm seating in the titration head. If it falls off, you
Risk of corrosion
could injure yourself if working with toxic titrants and solvents or strong acids or
bases.
When using chemicals and solvents, comply with the instructions of the producer
and the general lab safety rules!
All Karl Fischer reagents are readily flammable and toxic.
In the case of skin contact, immediately wash off with copious amounts of water!
If eye contact occurs, rinse intensively with copious amounts of water and consult a
physician!
Measures for your operational safety
Have the instrument serviced only by METTLER TOLEDO Service!
Any spillage should be wiped off immediately! Some solvents might cause corrosion
Caution
of the housing.
Exclude the following environmental influences:
Powerful vibrations,
direct sunlight,
atmospheric humidity greater than 80%,
temperatures below 5 C and above 40 C,
powerful electric or magnetic fields!
3Standard equipment
All parts are specified with their ordering code and quantity in cases where more than one part is included.
When ordering, some parts are only available in a minimum order quantity. In such cases, the corresponding
minimum order quantity is quoted. The standard equipment and optional accessories for auxiliary equipment,
e.g. sample changers, are listed in the appropriate operating instructions.
Description
Order number
51105795
51105567
51108732
51108752
51108741
51108740
Standard equipment
51108753
51107830
51107699
51109183
Holder
23960
51191159
51107492
51105600
Standard equipment
Draining tube
23936
71296
Molecular sieve
250 g
71478
Silicone grease
71300
Syringe
1 mL
Injection needle
80 x 0.8 mm
Standard equipment
4The titrator
4.1Titrator configuration
Part
Description
A
Solvent bottle drying tube 1)
B
Waste bottle drying tube
C
Solvent manager
D
Waste bottle
E
Solvent bottle 2)
F
Titration arm
G
Measuring cell
H
Internal magnetic stirrer
I
On/Off button
J
Indicator light (LED)
K
Touchscreen
L
Generator electrode
M
Double platinum pin electrode
n
Extraction adapter and park sleeve 1)
1) Component of the optionally available reagent changing set.
2)
10
The titrator
5Installation
Installation for all titrator types is described in this chapter. Standard equipment for the various types of titrators
varies and also depends on the optional accessories. For this reason, installation steps may vary.
a) Connect the power supply unit to the "POWER SUPPLY" socket on the rear of the titrator and to the mains
supply.
b) Secure the connection at the titrator by screwing the plug connector firmly into place.
The power supply is suitable for all supply voltages ranging from 100240 VAC 10% and 5060 Hz.
Installation
11
5.2Titration stand
5.2.1Connecting the titration stand
Once you have set up your KF titrator in a suitable location,
mount equipment in the titration stand. The titration arm can be
pivoted in both directions.
a) Slide the magnetic stirring rod carefully into the measuring
cell.
b) Place the cell in the titration stand and fasten with the mount
ing bolt.
c) Lightly grease microsections with the silicone grease sup
plied.
d) Place stopper with septum in the opening of the cell.
e) Place the measuring electrode in the cell openings.
f) Place the generator electrode in the cell openings.
g) Fill the drying tube with desiccant and place in the generator
electrode.
h) Use the holder for the tip of the extraction tube.
Part
A
B
C
D
E
F
G
H
I
J
Description
Drying tube
Measuring electrode
Generator electrode
Septum
Stopper
Holder
Measuring cell
Magnetic stirrer bar
Fastening screw
Titration arm
12
Installation
a) Use the triaxial cable with blue plug connector to connect the generator electrode with the "GENERATOR"
socket on the rear of the titrator.
b) Use the triaxial cable with gray plug connector to connect the measuring electrode to the "SENSOR" socket
on the rear of the titrator.
Part
A
B
C
D
E
F
G
H
Description
Extraction tube
Silicone tube (170 mm)
Threaded sleeve
Drying tube
Solvent manager
Connecting cable
Silicone tube (850 mm) only necessary in conjunction
with the reagent changing set
Flat seal
Installation
13
Check all drying tubes and closing points once again for firm seating in order to ensure that the system is leak
tight.
Part
A
B
C
D
E
Description
Drying tube
Threaded sleeve
Screw top
Flat seal
Reagent bottle
a) Push the draining tube of the waste bottle and the dispensing
tube of the reagent bottle through the draining adapter.
The length of the draining tube is adjusted to approx. 100
mm.
The length of the dispensing tube is adjusted to approx.
25 mm.
b) Remove the stopper and place the tubes with the draining
adapter in the opening.
c) Set the height of the waste tube so that it barely touches the
bottom of the cell.
Part
A
B
C
Description
Draining tube
Dispensing tube
Draining adapter
To fill or empty the measuring cell, remove the stopper and place the tubes in the opening with the draining
adapter. If the equipment is not required, you can place it in the park sleeve and insert the stopper again.
Check all drying tubes and closing points once again for firm seating in order to ensure that the system is leak
tight.
14
Installation
a) Switch off the titrator and the Stromboli oven sample changer.
b) Use the cable provided to connect the "TTL/IO port of the oven sample changer to the "TTL-I/O" port on the
rear of the titrator.
Installation
15
6Optional accessories
All parts are specified with their ordering code and quantity in cases where more than one part is included.
When ordering, some parts are only available in a minimum order quantity. In such cases, the corresponding
minimum order quantity is quoted. The standard equipment and optional accessories for auxiliary equipment,
e.g. sample changers, are listed in the appropriate operating instructions.
Description
Order number
Titration software
LabX
51108732
Tempering beaker
51109416
51108752
51108741
51108740
51108751
16
Optional accessories
Die Generatorelektrode darf nur bei Temperaturen unterhalb 80C verwendet werden.
Drying tube, straight
51108733
51107830
51107699
51109183
51109184
51109185
Holder
23960
51191159
51107492
51105606
Optional accessories
17
51105600
18
Optional accessories
Molecular sieve
250 g
71478
Silicone grease
71300
Draining tube
23936
51105581
Silicone tube
170 mm
51105578
23961
51107492
71296
23981
23937
71492
71482
Injection needle
80 x 0.8 mm for 1 ml injections (100 pcs)
80 x 1.2 mm for 10 ml injections) (12 pcs)
71484
71483
DO308
Stromboli
51109259
Stand rod
51107495
51108639
Optional accessories
19
20
Optional accessories
51108761
51190589
11101051
229029
229065
51190363
21901297
21901309
51191880
51105855
51109210
51109862
51109863
LevelSens holder
51109852
51109874
USB-P25
51191926
51105795
Optional accessories
21
51105567
Installation information
- English
- German
- French
- Spanish
- Italian
- Chinese
- Russian
51710625
51710626
51710627
51710628
51710629
51710630
51710631
Quick guide
- English
- German
- French
- Spanish
- Italian
- Chinese
- Russian
51710618
51710619
51710620
51710621
51710622
51710623
51710624
22
Optional accessories
51710633
7Technical data
7.1Titrator
Power supply Input voltage
Input frequency
Primary connection socket
Power consumption
Connected load
Secondary connection plug
CPU Processor
SDRAM
Flash memory
Dimensions Width
Depth
Height
weight
Materials Titrator housing
Cover sheet
Protective cover
Chassis
Titration stand
Dispensing tube / extraction tube
Air tubes
O-ring (screw top)
O-ring (threaded ring)
Sealing ring (bottle)
Seal (dispensing tube / extraction
tube)
Connecting piece
Ambient conditions Ambient temperature
Relative humidity
COM
USB1 / USB2
PC
Ethernet
TTL/IO
CAN OUT
Stirrer / pump
Use
Overvoltage category
Pollution degree
Socket
Configuration
Baud rate
Handshake
Galvanic isolation
ESD stability
Short-circuit protection
USB host
Max. power load
USB client
Socket
Speed
Socket
Inputs
Outputs
Socket
Speed
Voltage
Current
Socket
100240 VAC 10 %
5060 Hz
3 pin, IEC C14
36 VA
24 VDC, 1.5 A
2 pin, DC plug
XScale
64 MB
256 MB (industrial CF card)
210 mm
340 mm
291 mm (with titration stand)
312 mm (ready-to-operate device)
3.3 kg
Crastin PBT
PET
Copolymer
Stainless steel
Crastin PBT
FEP
Silicone
EPDM
FEP / silicone
PTFE / silicone
PTFE
Polypropylene
+5 C 40 C
Max. 80 % (non-condensing) at
31 C, linear fall to 50 % at 40 C
In interior spaces
II
2
9-pin male D-sub
Full-duplex
120019200
X-On / X-Off
No
Min. 1000 V
Yes
USB full/low speed
400 mA (total, both connections)
USB 1.1
RJ45
10/100 MBit/s
9-pin female D-sub
2
4
RJ12
500 kBit/s
24 VDC 10%
Max. 500 mA
5-pin mini-DIN
Technical data
23
Yes
Yes
24 V DC 5 % (max. 400 mA)
0 to 18 V DC 10 % (max. 300
mA)
SENSOR Socket
LEMO triaxial, 9 mm
Current range
0 to 24 A AC
Resolution
0.1 A
Limits of error
1 A
Measuring range
2000 mV
Resolution
0.1 mV
Limits of error
2 mV
GENERATOR Socket
LEMO triaxial, 7 mm
Voltage
Max. 36 V
Limits of error
10 % of selected voltage step
Current steps
100 mA, 200 mA, 300 mA, 400
mA
Limits of error
0.2 % of selected current step
Magnetic stirrer (built-in) Drive
Stepping motor
Max. speed
1050 rpm
Display Technology
Color TFT
Size
5.7"
Resolution
320 x 240 pixels
Backlighting
LED
Brightness control
Per software 50100%
Input Technology
Full-coverage touchscreen
Contains runtime modules from decNumber (c) Copyright IBM Corporation 2001, 2004. All rights reserved.
TTL - I / O Port Pin Assignment
General Socket
GND
Galvanic isolation
Plug & Play support
In Type
Voltage
Current
Out Type
Voltage
Current
Stirrer/Pump Pin Assignment
3
1
24
Technical data
Stirrer +
Stirrer -
4
5
2
5
Pump +
Pump Pump 2 +
Pump 2 -
COM ports
AB-S / PB-S
COM ports
AG / PG / PR
COM ports
AT / MT / UMT
COM ports
AX / MX / UMX
o
COM ports
PG-S
o
COM ports
XP
o
COM ports
XS
o
COM ports
mS
o
COM ports
ML
o
COM ports
Sartorius
Various
COM ports
Standard
o Option
Printer
Printers can be connected to the USB1 or USB2 interface of the titrator. PCL-compatible printers from various
manufacturers are supported. The METTLER TOLEDO USB-P25 is a durable easy-to-operate dot matrix printer
which prints onto standard quality paper. A current list of supported printers can be found on the Internet at:
http://www.mt.com/titration-printers.
Manufacturer
Type
Note
Various
Generic PCL printers
Connection via USB1 or USB2
METTLER TOLEDO
USB-P25
Connection via USB1 or USB2
Sample changer
Manufacturer
METTLER TOLEDO
Type
Stromboli oven sample
changer
Note
Connection via TTL-I/O
Barcode reader
Sample data can be read in via an appropriate barcode. The barcode reader can also be used to enter text in
open input fields. Barcode readers can be connected to the USB1 or USB2 interface of the titrator.
A standard USB hub can be used if more than two devices are to be connected to the USB connections of the
titrator.
Technical data
25
When sending or transporting the titrator over long distances, please use all of the original packaging.
26
9Disposal
In compliance with European Directive 2002/96/EC on Waste Electrical and Electronic
Equipment (WEEE), this instrument must not be disposed of together with domestic
waste. This also applies to countries outside the EU, per their specific requirements.
Please dispose of this product in accordance with local regulations at the collecting
point specified for electrical and electronic equipment.
If you have any questions, please contact the responsible authority or the distributor
from which you purchased this instrument.
Should this instrument be passed on to other parties (for private or professional use),
the content of this regulation must also be related.
Thank you for your contribution to environmental protection.
Disposal
27
Mettler-Toledo AG, Analytical will retain possession of all documents and their reproductions and may wish to
conclude a nondisclosure agreement with those requesting access to these documents.
Schwerzenbach,
September 2009
Chris Radloff
General Manager
Business Unit Analytical
Christian Walter
Manager Business Area
Analytical Chemistry
28
11Declaration of conformity
Declaration of conformity
29
30
Declaration of conformity
Declaration of conformity
31
www.mt.com/titration
For more information
*51710626*