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Indian Standard
METHODSOFTESTFORPETROLEUMAND
ITSPRODUCTS
[P:20]
DETERMINATION
( Second Revision )
ICS
75.080
0 BIS 1998
BUREAU
MANAK
November
1998
OF
BHAVAN,
INDIAN
STANDARDS
9 BAHADUR
SHAH ZAFAR
NEW DELHI 110002
MARG
Price Group
Methods of h4easurement
Committee. PCD 1
Sectional
FOREWORD
This Indian Standard (Second Revision) was adopted by the Bureau of Indian Standards, after the draft finalized
by the Methods of Measurement
and Test for Petroleum, Petroleum Products and Lubricants Sectional
Committee had been approved by the Petroleum, Coal and Related Products Division Council.
This standard was prepared on the basis of IP 170175 and IP 33159 and subsequently revised in 1982. In this
version (second revision), scope has been enlarged and included determination of closed cup flash point of
petroleum products and mixtures to ascertain inflammable vapour below 24C. Positioning and fixing of oil cup,
water bath thermometers into thermometer collar and correction of barometer readings to standard temperature
have been included.
In reporting the results of a test or analysis made in accordance with this standard, if the final value, observed
or calculated, is to be rounded off, it shall be done in accordance with IS 2 : 1960 Rules for rounding off
numerical values (revised).
IS1448[P:20]:1998
Indian Standard
METHODSOFTESTFORPETROLEUMAND
ITSPRODUCTS
[P:20]
DETERMINATION OF FLASH POINT BY ABEL APPARATUS
(
Second Revision )
1 SCOPE
1.1 This method is intended for the determination of
closed-cup flash point of petroleum producti, their
mixtures and other liquids having flash points between
-18C and 7OC.
1.2 Two methods, namely, Method A and Method B
have been prescribed. Method A is for liquids flashing
between -18C and +18SC inclusive; and Method B
is for liquids flashing between
19C and 70C
inclusive.
1.3 This method should be used to measure and
describe the properties of materials, products, or
assemblies
in response to heat and flame under
controlled laboratory conditions, and should not be
used to describe or appraise the fire hazard or fire risk
of materials, products or assemblies under actual fire
conditions. However, results of this test may be used
as elements of a fire risk assessment which takes into
account of all the factors which are pertinent to an
assessment of the fire hazard of a particular end use.
NOTES
1 Flash point is used in shipping, storage, and handling safety
regulations as a classification property to define flammable
and combustible materials. Precise definition of the classes is
given in each particular regulation.
2 Flash point may indicate the possible presence of highly
volatile materials in a relatively non-volatile or non-flammable
material.
3 Since the presence of small propottions of highly volatile
materials need to be detected, this test shall be the first
determination on a received sample.
IS 1448 [ P : 20 ] : 1998
51.1
Title
Methods of test for petroleum
its products
Distillation
[P : 321 : 1992
Density
and relative
(second revision)
Oil Cup
and
(second revision)
density
5.1.2
3 TERMINOLOGY
For the purpose
of this
definitions shall apply.
method,
the following
5 APPARATUS
5.1 The apparatus to be employed shall be the Abel
petroleum
testing apparatus
or Abel apparatus
modified by having an oil cup provided with a stirrer,
constructed
to the dimensions
and tolerances
prescribed
under 5.1.1 to 51.7 and Fig. 1. The
apparatus and thermometers shall bear a test certificate
of the National Physical Laboratory, New Delhi, or
any other institution
authorized
to issue such
certificate. In order to check the performance of the
apparatus, a performance
test is also given
in
Annex B for the guidance of the users.
IS1448[P:20]:1998
pipe also communicate with the water space, through
the top plate and two loop handles are provided
thereon.
Stirrer
Spirit Lamp
Thermometers
Oil
Range
Immersion,
Graduation
-3sT
mm
to +70c
61
0.5Oc
lC and 5C
5C
0.15
Overall length, mm
300 to 320
195
Length of scale range,
mm, Min
300 to 320
164
Bulb, length, mm
Bulb, diameter
7.5 to 10.5
7.5 to 10.5
Stem, diameter, mm
6.0 to 7.0
Distance from bottom
70 to 80
of bulb to lowest
graduation mark, mm
Water Bath
-30 c to +80C
89
0.5Oc
6.0 to 7.0
1OOto 111
a 0.5c
and above 0C
Expansion chamber,
permit heating to
Required
Required
IP 74C
IP 7SC
IS 1448 [ P : 20 ] : 1998
INSIDE DIA OF
SLEEVE TO BE
SUDING FIT ON
-.-._..
SOLDERED
6.30
APPROX
OIL CUP
MATERIAL BRASS
l
3.17
APG
ALL CORNERS TO
OIL CUP
SECTION
__.
Et-
XX
12.9
12.4
7.60
I
STIRRER
MATERIAL BRASS
2.56
PUSH FIT IN THERMOCOVER
AND HEATING
10.28
COVER
MATERIAL BRASS
THERMOMETER
COLLAR
MATERIAL BRASS 2 OFF
+ IT IS RECOMMENDED
THAT IN ORDER TO ACHIEVE INTERCHANGEABILITY
THE
ID OF THE THERMOMETER
SOCKET SHOULD
BE BETWEEN
15.235
h 15.253
AND
THE EXTERNAL DIA OF THE THERMOMETER
COLLAR BETWEEN 15.222
AND 15.232
FIG.
ISl448[P:20]:1998
SLIDE
BRASS
0.91mm
OR TEST
LAMP
OF JET 15 APPROX
JET
AT EN0
WHITE
BEAD
3.6-4.1
SUITABLE
OF
MATERIAL
OIL CUP
SECTlON
THERMOMETER
AA
-69.5-
70.5
MZ.Zr3.9
LONG
CSK
SCREWS
BATH
$VATER
OR ACTUAL
PLAN
VIEW
FUNNEL-j
THERMDHLT~R
POSITION
SiL
OF
INSIDE
OIA
THERMOMETER
SOCKET
lS.G15.0
- OVERFLOW
Sz.i-64.9
IL3-
-7.0
PIPE
-12.0
-EBONrE
OR
RING (EASY
FIT ON CAP]
IL8
FIBRE
TO
-STIRRER
OUTER
JACKET
c-HEATING
VESSEL
- 0.6
COPPER
rid
IO-
-75-11
-_~137-1Lz
IO
162-187
ID
All dimensions
FIG.2
ABEL
THICK
- 0.6
THICK
COPPER
-0.6
THICK
COPPER
in millimetres.
FLASHPOINTAPPARATUSWITHHEATINGJACKET
5
rS1448[P:20]:1998
5.1.6 Other Thermmeters
5.1.7 Metronome
A metronome
is provided, to beat 75 to
minute. Alternatively, a pendulum of 60
length may be used in place of the
counting one beat from one extremity of
the other.
6 PREPARATION
7 PROCEDURE
7.1 Method A
Liquids
flashing
inclusive.
between
-18C
and
+ 18.5C
b)
OF APPARATUS
5.1.6.1
a)
80 beats per
cm effective
metronome,
the swing to
L TUBE PUSH
SHADED AREAS
OF ADHESIVE
IS1448[P:20]:1998
its size to approximately
3.8 mm diameter, and
maintain it at that size throughout the test, comparing
it frequently with the projecting while bead mounted
on the cover of the oil cup.
ing expression:
Corrected flash point = C + 0.25 (101.3-P)
where
C = observed flash point, C; and
P = barometric pressure, kPa.
or
where
M = barometric pressure, mbar; and
H = barometric pressure, mmHg.
This correction is applicable over the range
1.05 x 105 N/m2 or 980 to 1.050 mbar.
NOTE 3 Annex C.
Correction
of barometer
readings
0.98 to
is given in
9 REPORTING
Report the fully corrected result, to the nearest 0.5%
as the Abel flash point.
Liquids flashings
8 CALCULATION
7.2 Method
or
are
between
10 PRECISION
Repeatability
1C
Reproducibility
I .st
IS1448[P:20]:1998
ANNEX
(Clause 1.6)
METHOD FOR THE DETERMINATION OF FLASH POINT
OF SOLID PETROLEUM MIXTURES
A-l.3 The air bath of the testing apparatus shall be
A-l PROCEDURE
A-l.4 The cup shall then be placed in the air bath, and
the temperature of the sample shall be allowed to rise
until the thermometer in the oil cup shows 24C when
the test flame shall be applied.
ANNEX
(CZuuse5.1)
PERFORMANCE TEST FOR THE APPARATUS
B-l The flash point of a standard sample of p-xylene
of the specification
given in Table 1 shall be
determined
five times by the procedure described
under 6 of this standard. The flash point of p-xylene
should be reported to the nearest 0.5C. None of the
results shall deviate by more than lC from the
reported flash point.
ii
Chsracteristic
(1)
(2)
i) Relative density at
Requirement
(3)
0.860to 0.866
Method of Test,
Ref to
PartofIs144a
(4)
[P : 321
15.56i15.5BC
ii) Distillation range
ANNEX
[P : 181
Calculated
from freezing Doint
(Clause 8)
BAROMETER CORRECTIONS
C-3 It is important to note the equation for correcting
temperature readings for barometric pressure in 8 is
entered in kilopascals.
IS1448[P
20 ] : 1998
Barometer
/
940
(11
960
980
Reading,
h
hPa or mhar
\
loo0
1020
1040
(2)
(3)
(4)
(5)
16)
(7)
I 060
(8)
10.0
-1.61
-1.64
-1.68
-1.71
-1.74
-1.77
-1.81
10.5
-1.69
-1.72
-1.76
-1.79
-1.83
-1.86
-1.90
I I.0
113
-1.77
-1.81
-1.84
-1.88
-1.91
-1.95
-1.99
-1.85
-1.89
-1.93
-1.96
-2.00
-2.04
-2.08
12.0
-1.93
-1.97
-2.01
-2.05
-2.09
-2.13
-2.17
12.5
-2.01
-2.05
-2.09
-2.13
-2.18
-2.22
-2.26
13.0
-2.09
-2.13
-2.18
-2.22
-2.26
-2.30
-2.35
13.5
-2.17
-2.22
-2.25
-2.30
-2.35
-2.39
-2.44
14.0
-2.25
-2.30
-2.34
-2.39
-2.44
-2.48
-2.53
14.5
-2.33
-2.38
-2.43
-2.47
-2.52
-2.57
-2.62
15.0
-2.41
-2.46
-2.51
-2.56
-2.61
-2.66
-2.71
IS.5
-2.49
-2.54
-2.59
-2.65
-2.70
-2.75
-2.80
16.0
-2.57
-2.63
-2.68
-2.73
-2.78
-2.83
-2.89
16.5
-2.65
-2.71
-2.76
-2.82
-2.87
-2.92
-2.98
17.0
-2.73
-2.79
-2.84
-2.90
-2.96
-3.01
-3.07
17.5
-2.81
-2.87
-2.93
-2.99
-3.04
-3.10
-3.16
18.0
-2.89
-2.95
-3.01
-3.07
-3.13
-3.19
-3.25
18.5
-2.97
-3.03
-3.10
-3.16
-3.22
-3.28
-3.34
19.0
-3.05
-3.12
-3.18
-3.24
-3.30
-3.36
-3.43
19.5
-3.13
-3.20
-3.26
-3.33
-3.39
-3.45
-3.52
20.0
-3.21
-3.28
-3.35
-3.41
-3.48
-3.54
-3.61
20.5
-3.30
-3.36
-3.43
-3.50
-3.56
-3.63
-3.70
21.0
-3.38
-3.44
-3.51
AS8
-3.65
-3.72
-3.79
21.5
-3.46
-3.53
-3.60
-3.67
-3.14
-3.81
-3.88
22.0
-3.54
-3.61
-3.68
-3.7s
-3.82
c3.89
-3796
22.5
-3.62
-3.69
-3.76
-3.83
-3.91
-3.98
4.0.5
23.0
-3.70
-3.77
-3.85
-3.92
-3.99
-4.07
-4.14
23.5
-3.78
-3.85
-3.93
-4.00
-4.08
-4.16
-4.23
24.0
-3.86
-3.93
-4.01
-4.09
-4.17
-4.2s
-4.32
24.5
-3.94
-4.02
-4.09
-4.17
-4.25
-4.33
-4.41
25.0
-4.01
-4.10
-4.18
-4.26
-4.34
-4.42
-4.50
25.5
-4.10
-4.18
-4.26
-4.34
-4.43
-4.5 1
-4.59
26.0
-4.18
-4.26
A.34
-4.43
-4.51
-4.60
-4.68
26.5
-4.26
-4.34
-4.43
A.51
-4.60
A.69
-4.17
27.0
-4.34
-4.42
-4.51
-4.60
-4.69
A.77
-4.86
27.5
-4.41
-4.50
-4.59
-4.68
A.77
-4.86
-4.95
28.0
-4.49
-4.59
-4.68
-4.77
-4.86
-4.95
-5.04
-s.13
28.5
-4.57
-4.67
-4.16
-4.85
-4.95
-5.04
29.0
-4.6s
-4.75
-4.84
-4.94
-5.03
-S.13
29.9
-4.13
-4.83
-4.93
-5.02
-s:12
-5.2
30.0
-4.81
-491
-5.01
-5.1
-5.20
-5 30
-5 22
-5.31
-5.40
IS 1448 [ P : 20 ] : 1998
Table 3 Correction of Barometer Readings to Standard Temperature OC
( Clauses C-2 and C-4 )
Temperature
Barometer Read@,
hPa or mbar
OC
700
720
740
760
780
800
820
840
860
880
(2)
(3)
(4)
(5)
(6)
(7)
(a)
(9)
(10)
(11)
10.0
-1.14
-1.17
-1.21
-1.24
-1.27
-1.30
-1.34
-1.37
-1.40
-1.44
10.5
-1.20
-1.23
;I.27
-1.30
-1.34
-1.37
-1.40
-1.44
-1.47
-1.51
1I.0
11.5
-I .26
-1.29
-I .33
-1.36
-1.40
-1.44
-1.47
-1.51
-1.54
-1.58
-1.31
-1.35
-1.39
-1.43
-1.46
-1.50
-1.54
-1.58
-1.61
-1.65
12.0
-1.37
-1.41
-1.45
-1.49
-1.53
-1.57
-1.60
-1.64
-1.68
-1.72
12.5
-1.43
-1.47
-1.51
-1.55
-1.59
-1.63
-1.67
-1.71
-1.75
-1.79
13.0
-1.48
-1.53
-1.57
-1.61
-1.65
-1.70
-1.74
-1.78
-1.82
-1.86
13.5
-1.54
-1 sa
-1.63
-1.67
-1.72
-1.76
-1.80
-1.85
-1.89
-1.94
14.0
-1.60
-1.64
-1.69
-1.73
-1.78
-1.83
-1.87
-1.92
-1.96
-2.01
14.5
-1.65
-1.70
-1.75
-1.80
-1.84
-1.89
-1.94
-1.98
-2.03
-2.08
IS.0
-1.71
-1.76
-1.81
-1.86
-1.91
-1.96
-2.00
-2.05
-2.10
-2.15
IS.5
-1.77
-1.82
-1.87
-1.92
-1.97
-2.02
-2.07
-2.12
-2.17
-2.22
16.0
-1.82
-1.88
-1.93
-1.98
-2.03
-2.09
-2.14
-2.19
-2.24
-2.29
16.5
-1.88
-1.94
-1.99
-2.04
-2.10
-2.15
-2.20
-2.26
-2.31
-2.37
17.0
-1.94
-1.99
-2.05
-2.10
-2.16
-2.22
-2.27
-2.33
-2.38
-2.44
17.5
-2.00
-2.05
-2.11
-2.17
-2.22
-2.28
-2.34
-2.39
-2.45
-2.51
18.0
-2.05
-2.11
-2.17
-2.23
-2.29
-2.35
-2.40
-2.46
-2.52
-2.58
18.5
-2.11
-2.17
-2.23
-2.29
-2.35
-2.41
-2.47
-2.53
-2.59
-2.65
19.0
-2.17
-2.23
-2.29
-2.35
-2.41
-2.48
-2.54
-2.60
-2.66
-2.72
19.5
-2.22
-2.29
-2.35
-2.41
-2.48
-2.54
-2.60
-2.67
-2.73
-2.79
20.0
-2.28
-2.34
-2.41
-2.47
-2.54
-2.60
-2.67
-2.74
-2.80
-2.87
20.5
-2.34
-2.40
-2.47
-2.54
-2.60
-2.67
-2.74
-2.80
-2.87
-2.94
21.0
-2.39
-2.46
-2.53
-2.60
-2.67
-2.73
-2.80
-2.87
-2.94
-3.01
21.5
-2.45
-2.52
-2.59
-2.66
-2.73
-2.80
-2.87
-2.94
-3.01
-3.08
22.0
-2.51
-2.58
-2.65
-2.72
-2.79
-2.86
-2.94
-3.01
-3.08
-3.15
22.5
-2.56
-2.64
-2.71
-2.78
-2.86
-2.93
-3.00
-3.08
-3.15
-3.22
23.0
-2.62
-2.69
-2.77
-2.84
-2.92
-2.99
-3.07
-3.14
-3.22
-3.29
23.5
-2.68
-2.75
-2.83
-2.91
-2.98
-3.06
-3.14
-3.21
-3.29
-3.36
24.0
-2.73
-2.81
-2.89
-2.97
-3.05
-3.12
-3.20
-3.28
-3.36
-3.44
24.5
-2.79
-2.87
-2.95
-3.03
-3.11
-3.19
-3.27
-3.35
-3.43
-3.51
2.5.0
-2.85
-2.93
-3.01
-3.09
-3.17
-3.25
-3.33
- 3.42
-3.50
-3.58
25.5
-2.90
-2.99
-3.07
-3.15
-3.24
-3.32
-3.40
-3.48
-3.57
-3.65
26.0
-2.96
-3.04
-3.13
-3.21
-3.30
-3.38
-3.47
-3.55
-3.64
-3.72
26.5
-3.02
-3.10
-3.19
-3.28
-3.36
-3.45
-3.53
-3.62
-3.71
-3.79
27.0
-3.07
-3.16
-3.25
-3.34
-3.42
-3.51
-3.60
-3.69
-3.78
-3.86
21.5
-3.13
-3.22
-3.31
-3.40
-3.49
-3.58
-3.67
-3.76
-3.85
28.0
-3.19
-3.28
-3.37
-3.46
-3.55
-3.64
-3.73
-3.82
-3.9
28.5
-3.24
-3.34
-3.43
-3.52
-3.61
-3.71
-3.80
-3.89
-3.98
-4.08
29.0
-3.30
-3.39
-3.49
-3.58
-3.68
-3.77
-3.87
-3.96
-4.05
-4.15
29.5
-3.36
-3.45
-3.55
-3.64
-3.74
-3.84
-3.93
-4.03
-4.12
-4.22
30.0
-3.41
-3.51
-3.61
-3.71
-3.80
-3.90
-4.00
-4.10
-4.19
-4.29
(1)
-3.93
-4.01
C-4 CORRECTION TO OC
Bureau
of Indian
Standards
BIS is a statutory institution established under the Bureau of Indian Standards Act, 1986 to promote
harmonious development of the activities of standardization, marking and quality certification of goods and
attending to connected matters in the country.
Copyright
BIS has the copyright of all its publications. No part of these publications may be reproduced in any form
without the prior permission in writing of BIS. This does not preclude the free use, in the course of
implementing the standard, of necessary details, such as symbols and sizes, type or grade designations.
Enquiries relating to copyright be addressed to the Director (Publication), BIS.
Review of Indian Standards
Amendments are issued to standards as the need arises on the basis of comments. Standards are also reviewed
periodically; a standard along with amendments is reaffirmed when such review indicates that no changes are
needed; if the review indicates that changes are needed, it is taken up for revision. Users of Indian Standards
should ascertain that they are in possession of the latest amendments or edition by referring to the latest issue
of BIS Handbook and Standards Monthly Additions
This Indian Standard has been developed from Dot: No. PCD I( 1482 ).
Amendments
Date of Issue,
Amend No.
Text Affected
Eastern
Telegrams: Manaksanstha
(Common to all officet)
Telephone
323 76 17,323 38 41
337 84,99,337 85 61
{ 337 86 26,337 9120
60 38 43
{ 60 20 25
235 02 16,235 04142
{ 235 15 19,235 23 15
832 92 95,832 78 58
{ 832 78 91,832 78 92
India