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Abstract
In the past, a lot of experimental studies have been devoted to creep-fatigue interactions in austenitic stainless steels. Tests have
been carried mainly at temperatures of at least 600 C and at high applied strains, which are supposed to be the most damaging.
The present work is dedicated to mechanical tests, TEM observations and lifetime predictions at 550 C which corresponds to
the real industrial temperature in Liquid Metal Fast Breeder Reactors. It is shown that if pure fatigue test results are close to
those performed at 600 C, some of the creep-fatigue results are different, particularly for small applied strains which correspond
once more to the industrial conditions. In the 0.250.3% strain amplitude range, the stress is larger with hold time than without
whatever is the hold time up to 5 h. The numbers of cycles to failure are greatly reduced and no saturation with the hold time is
observed, contrary to higher temperature results. The stressstrain behaviour is discussed considering several high temperature
mechanisms such as ageing, recovery and viscoplasticity and using TEM observations and stress partitioning into kinematic,
isotropic and thermal stresses. Finally, a simple linear damage accumulation model is applied to the 550 C and 600 C tests,
using the measured stresses. The stress dependence on hold time can partly explain the observed failure results on fatigue life.
2004 Elsevier B.V. All rights reserved.
1. Historical background
For the development of structural material for Liquid Metal Fast Breeder Reactors (LMFBR), the creep
fatigue interaction is a very important topic to consider.
Indeed, many structural components are subjected to
repeated thermal stresses as a result of temperature gradients which occur on heating and cooling during startup and shut down cycles or during thermal transient.
For those components working at high temperature in
Corresponding author. Tel.: +33 1 69 08 35 67;
fax: +33 1 69 08 71 67.
E-mail address: sauzay@cea.fr (M. Sauzay).
0029-5493/$ see front matter 2004 Elsevier B.V. All rights reserved.
doi:10.1016/j.nucengdes.2004.05.005
220
Table 1
Chemical composition of the 316LN sheets (wt.%)
C
S
P
Si
Mn
Ni
Cr
Mo
N
B
Co
Cu
SP
SQ
0.021
0.007
0.03
0.4
1.74
12.3
17.2
2.4
0.08
0.0032
0.21
0.15
0.028
0.001
0.023
0.4
1.85
12.31
17.4
2.47
0.074
0.001
0.14
0.17
221
Fig. 1. Evolution of the stress amplitude with respect to the fraction of fatigue life. Pure fatigue, AISI stainless steel 316LN, 550 C.
the annealed alloy cycle by cycle (Fig. 1). After saturation the stressstrain cycles become quite stable, before
a drop of the maximal stress per cycle due to damage
at the end of the lifetime is observed. The maximal
stress continues to increase cycle by cycle until saturation, except for very small applied strains (range under
0.5%) for which no saturation is observed. Fig. 2 compares monotonic and cyclic stress strain (CSS) curves
and shows that the cyclic hardening is large. There is no
significant difference between the CSS curves obtained
Fig. 2. Cyclic and monotonic stressstrain curves. Pure fatigue, AISI stainless steel 316LN, 550 C.
222
Fig. 3. Variations of the tensile stress ratio with respect to the hold time. The maximum tensile stress measured for a given th hold time is divided
by the pure fatigue one (no hold time). Fatigue-relaxation, 600 C.
and for fatigue-relaxation ( tmaxth ) showed that the effect of the hold time on the maximum stress amplitude
is quite large (Fig. 3). For very small hold times (less
than 10 min), there is a stronger cyclic hardening than
without hold time (+7%), but for larger hold times,
there is a reduced hardening. The transition takes
place for hold times of about 10 min. For hold times
greater than 300 min, the reduction of the variation and
maximum tensile stresses is about 1020% of the pure
Fig. 4. Variations of the relaxation stress ratio with respect to the hold time. The relaxed stress measured for a given th hold time is divided by
the maximum stress (measured for the same hold time). Fatigue-relaxation, 600 C.
223
tensile stress increase. At 600 C, in terms of the mechanical behaviour, there is a small difference between
small and large applied strains. But this difference is
much more significant at 550 C.
The complex stressstrain behaviour, which depends on the temperature, on the dwell time and on the
applied strain could influence the damage mechanisms
and the lifetime. The experimental results concerning
lifetime are now described.
3.2. Creep-fatigue damage
The pure fatigue tests at 600 C and 550 C give
similar results (Fig. 8). In this range of temperature,
the MansonCoffin curves are little influenced by the
temperature. It is the same concerning the CSS curves.
The experimental dispersion on the number of cycles to
failure depends on the strain level. For a strain equal to
0.2%, the dispersion factor is about 6. The fatigue life
reduction factors are given in Figs. 9 and 10 (600 C)
and 11 (550 C). They are defined as the ratios between
the fatigue life measured for a given th hold time and
the fatigue life without hold time.
The results concerning the creep-fatigue tests carried at 600 C have already been published (Mottot
et al., 1982; Cailletaud et al., 1984; Levaillant et al.,
1988). The larger is the hold time, the smaller is the
number of cycles to failure. For large applied strains
Fig. 5. Variations of the tensile stress ratio with respect to the hold time. The maximum tensile stress measured for a given th hold time is divided
by the pure fatigue one (no hold time). Fatigue-relaxation, 550 C (compare with Fig. 3).
224
Fig. 6. Variations of the relaxation stress ratio with respect to the hold time. The relaxed stress measured for a given th hold time is divided by
the maximum stress (measured for the same hold time). Fatigue-relaxation, 550 C (compare with Fig. 4).
Fig. 7. Evolution of the stress amplitude for different hold times, with respect to the fraction of fatigue life. Pure fatigue, AISI stainless steel
316LN, 550 C, strain amplitude t = 0.3%.
225
226
Fig. 9. Fatigue life reduction factor with respect to the hold time. Large strains, 600 C. The fatigue life reduction factors are defined as the
ratios between the fatigue life measured for a given th hold time and the fatigue life without hold time.
Fig. 10. Fatigue life reduction factor with respect to the hold time. Small strains (t < 1%), 600 C. The fatigue life reduction factors are
defined as the ratios between the fatigue life measured for a given th hold time and the fatigue life without hold time.
227
Fig. 11. Fatigue life reduction factor with respect to the hold time. Large and small strains, 550 C. The fatigue life reduction factors are defined
as the ratios between the fatigue life measured for a given th hold time and the fatigue life without hold time.
Fig. 12. Multiple planar slip in a grain (TEM). Pure fatigue. AISI stainless steel 316LN, t = 0.6%, 550 C.
228
4. Discussion
4.1. Origin of the hold time inuence on the
mechanical behaviour
4.1.1. Stress partition
Several mechanisms could be involved in the evolution of the stressstrain behaviour with respect to the
hold time. In order to link the physical mechanisms
(1)
(2)
229
Fig. 14. Details of the larger grain shown in Fig. 13 (TEM). AISI stainless steel 316LN, t = 0.6%, 550 C.
cations to escape. If the stress is not large enough, dislocations cannot glide freely. This locking interaction
induces an increase of the isotropic hardening. During
the long hold times, the plastic strain rate decreases
greatly and so does the dislocation gliding speed, which
can induce dislocation locking by solute atoms. These
mechanisms cannot be easily observed but the isotropic
stress increase has been precisely measured using the
stressstrain curves obtained for the fatigue-relaxation
tests with the smallest hold times. Just after the relaxation, the isotropic stress is larger than the pure fatigue
one. But, the isotropic stress measured after the following minimal strain peak is smaller than the pure fatigue
one. This proves that the mean isotropic stress increase
is due to the relaxation time. Sequential tests have been
performed at 550 C and 600 C in order to have a better understanding of what happens for very large hold
times (about one month). First, a cyclic strain is applied
during 300 cycles in order to achieve the saturation of
the behaviour of pure fatigue test. Second, a relaxation
is applied during 15 days. Third, 300 pure fatigue cycles
230
231
Fig. 16. Details of a grain (TEM). Fatigue-relaxation, t = 0.6%, th = 300 min, 550 C. There are less defects than in a pure fatigue specimen
(compare with Fig. 14).
232
Table 2
Number of cycles to failure for pure fatigue tests at 600 C (average
of several tests for each applied strain)
Table 4
Coefficients of the relation between the applied stress and the time
to failure (creep tests at 600 C)
t (%)
N25 ( 103 )
Coefficients
SP
SQ
Krupp
0.4
0.56
0.6
0.7
1.2
1.6
300
12
10
4
0.8
0.4
r
H (min)
9.64
1.63 1028
9.15
6.54 1026
11.21
1.36 1031
tF () =
NF
tF
tFrelax
=1
(3)
N25 ( 103 )
0.4
0.5
0.6
1.2
1.6
860
20
12
1.5
0.45
The comparison between the computed and observed times to failure are given in Tables 6 and 7 for
the two temperatures.
At 600 C, the predictions are quite reliable (Table 6
and Fig. 17). The ratio between predicted and measured values are included in the [1/3,3] range. For large
strains, fatigue and creep damages have the same order
of magnitude. Predictions seem to underestimate the
numbers of cycles to failure. For smaller strains, predictions overestimate them. In this case, the creep damage part becomes larger and the fatigue damage part
smaller. For the smallest applied strain (t = 0.4%),
the fatigue damage is very small (less than 0.03). The
creep damage is larger but remains small too (less than
0.3). The number of cycles to failure is overestimated
by a factor 3 for a 0.4% applied strain variation. It is
difficult to extrapolate the evolution of the lifetime with
hold time increasing.
At 550 C, the predictions are less reliable and depend on the strain level. The agreement between the
model and the experiment is quite good except for the
0.4% applied strain tests and the 1.2% test with the
Table 5
Coefficients of the relation between the applied stress and the time
to failure (creep tests at 550 C)
Coefficients
SP
SQ
r
H (min)
12
4.48 1035
12.6
1.07 1036
233
Table 6
Comparison between the predictions of the linear and the measured numbers of cycles to failure (fatigue-relaxation tests, 600 C)
tmax (MPa)
R (MPa)
NF,comp
NF,exp
t = 1.6% (SP)
th = 90 min
th = 300 min
333
335
88
110
263
194
730
357
t = 1.2%
th = 300 min (SP)
th = 300 min (SQ)
th = 1,440 min (SP)
th = 1,440 min (SQ)
298
290
274
272
82
90
109
93
384
386
440
250
>314 (stopped)
248
398
212
t = 0.7%
th = 300 min (SP)
th = 300 min (SP)
th = 1,440 min (SP)
244
218
240
42
40
66
1,380
1,240
920
1,650
1,133
>100 (stopped)
t = 0.60.56%
th = 720min Krupp
th = 720 min (SQ)
212
198
72
41
2,900
3,100
1,290
>1,550 (stopped)
t = 0.4%
th = 90 min (SQ)
th = 30 min Krupp
187
175
16
11
20,300
36,000
6,500
10,900
The computation concerning the Krupp sheet use the results from its pure fatigue tests specifically. The maximum stress and the relaxed stress
are denoted as tmax , and R , respectively. They are measured at NF /2. The computed and experimental numbers of cycles to failure are denoted
as NF,comp and NF,exp , respectively.
Fig. 17. Experimental and computed numbers of cycles to failure (600 C).
234
Table 7
Comparison between the predictions of the linear and the measured numbers of cycles to failure (fatigue-relaxation tests, 550 C)
tmax (MPa)
R (MPa)
NF,comp
NF,exp
t = 1.2% (SP)
th = 600 min
th = 1,200 min
th = 4,000 min
344
306
310
54
66
95
700
1,140
1,000
360
312
217
t = 0.6% (SQ)
th = 90 min
th = 300 min
th = 300 min
281
270
277
17
15.5
15
2,500
1,300
970
2,250
>1,342 (stopped)
>248 (stopped)
t = 0.5% (SQ)
th = 90 min
th = 300 min
247
256
13.5
13
8,500
2,400
5,000
>317 (stopped)
t = 0.4% (SQ)
th = 30 min
th = 300 min
206
229
10
9
277,000
9,900
13,000
>512 (stopped)
The maximum stress and the relaxed stress are denoted as tmax , and R , respectively. They are measured at NF /2. The computed and experimental
numbers of cycles to failure are denoted as NF,comp and NF,exp , respectively.
Fig. 18. Experimental and computed numbers of cycles to failure (550 C).
largest hold time (4000 min) (Table 7 and Fig. 18). For
these particular tests, the stress level is small during
the largest part of the relaxation time ( 200 MPa,
Table 7). The used creep failure data (Table 5) correspond to larger stress levels. Specific data concerning
small stress levels are needed in order to check the reliability of the linear accumulation rule. The prediction
for 0.4% strain variation is very largely overestimated
(by a factor 20). It could be due to a lack of creep data
or to particular creep-fatigue interaction mechanisms
for small applied strains. Therefore, creep tests with
small applied stresses are needed leading to very long
tests. SEM observations could be useful in order to understand the specific creep-fatigue interaction for small
applied strains. A linear interaction rule and non-linear
pure fatigue (pure creep) damage models could be used
too (Cailletaud et al., 1984). For example the Kachanov
non-linear creep damage law can be used in addition
to a non-linear fatigue damage model (Lemaitre and
Chaboche, 1987). It could permit us to improve predictions at small strain and 550 C. A unified damage
law is used by Sermage et al. (2000). It is simple and
needs only a few material adjustable parameters. But it
seems not sure that the mechanisms of interaction between a fatigue crack and creep damaged grain boundaries near the crack tip are really taken into account
by those phenomenological models (Hales, 1980). It
should be noticed that several phenomenological models have been compared by Cailletaud et al. (1984).
The corresponding tentative extrapolations toward low
strain and long dwell time are scattered depending on
the chosen creep-fatigue damage model.
5. Conclusions
Many results have been obtained from fatiguerelaxation tests carried at 550 C on a 316LN steel. The
effect of small applied strains and long hold times has
been studied. All these test conditions are close to the
real power plant ones and lead to experimental results
which should be partially distinguished from the more
classical laboratory ones (higher temperature, larger
strains, smaller hold times).
The behaviour is affected by the hold time leading for long dwell times to a supplementary hardening
observed at small applied strains and little relaxation
is observed contrary to the results obtained for higher
235
Acknowledgments
Pineau and X. Feaugas are acknowledged for stimulating discussions. This work is supported by the CEA
Program syst`emes du futur for a new generation of
nuclear power plants.
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