Comitt ‘sine se STD-ASTH DLUOL-ENGL 1958 MM 0759520 Ob20564 17) a ap Designation: 0 1401-98 Standard Test Method for Water Separability of Petroleum Oils and Synthetic Fluids‘ his and’ hone spore hy pec of Dene 1, Scope LAI test method covers measuremen of the ailily of petoleun olis or syutkedc dnids to separre Zou water tr: hou deveopayelial ea ol ng sinus 234 oben ste FCs tse canted i tenmnentel hone nce stare becesed 82 2 Teo sil ve wee Ce hint mag of la va ‘uber sk tenpertanes such #8 25°C cana bs ose ‘Fon ctng netsh owe rave Us ae gee thao th rcs cncanged vk bra Sea omy eae he rataen ogee 12 The values stated in ST units aré co be repared at the standard, The values given ib parentheses arc for infeumatior. ony 1.3 This standund does vot purport to address wil of the safisy: concen, of ani, ansactsee with fs use. Ht is The esponvibtin of the wom af ts seacdan! aa exaiticd gpa riave safery ant healt procces avd determine she upelion- Filly of vegulatary Lsiations yirinr besa. Bow spastic precautionary stateraray, s8@ 4.9, 61 2, Reforeneed Dacuments 2. ASTM Standand: 1 668 Tio, Method for Rust 2veventing Characteristics of ahibited Miosrl Oil ix de Presence of Wer? DHL Sprui sation for Subsite Ocean Kates ® D 1193 Specification for Reagem Water DEVI Test Mettod for Dewulsislity Chaucterisis of Lartricating G8 DNS? Practice for Manual Sarupling of Petoleum ane Pouolcnm Predcts* (nr ob ave ay 10 SHE uBlted uber 18S, Cage baited DMT 5 ae aces cin 3 1, ad Boot of ASP San 1: “os nf ASN Sonate NL ILOT “nace AT Sonar NLEE the A ASTM eri e218 2005, fa oe es es 1G erm ey fg A ee A Summary of Tea! Method 3.1 A AGT. sormpls and 40 ml of cisilied wee ‘Nore 8) ae stived for § min at SPC (Note I) ina sredoated cyiusr “The time sequied fur the seqaravion of The emulsion dus foomed is recorded. If cornplete sepuat.on ot emulsion redue- tion te Fre or Tess doer aol uecur alter standing for 39 the volumes oF el fr Maly, wale, and enw romining 4 the time are reported. 4. Sgnidcance and Use ALL This est mead prwides 1 guide for detenninigg De vyater sepwation cha-acterates of oils whigar (© water com Ioinutin ced unbudence, Hs ute Tow apecificaon omen ily and 0 ring of iservize ai, 5. Apparatus 5.1 Cyléwier, WWD ioL, geadvated teem 5 to LOO. mL ie Liem. ivivigns, mile of plas, healowsiniamt glans oe = tsuical eaisalenl, The inside diaueter stil be wo Tey di 2 row ant ne nacre dan 36 rime througout its gts, asirod from the top co « poins 6 ram ficin te bottom of the éylindsr Tae overall height othe egtngee shall 35-225 to 260 rim. The evaduscion shall not he in ceror by nove than 1 mia saty point on Ue sexe 5.2 Heating Baik, sufcienty large and daap w permit te inmersion of scleastrieo reat eslinders im the aath fquid up Deir 85-m) yraioes, The ball shall be eapabe of bes raimicned ata emapersie of Sd = [CONove 1), anal shall be five ida uups sich huld Ree lier iy 3 posion so tha the tnnenuting| Hof the kl eemregponds tn che vertical czrter line of De oslinder deving the stscing operstion. THe, ‘Sur hull ld the eylinder securely hil iy wens une bring strc, 5.3 Sueaeg Fade fie ude of Canuulucplaedl or sululeas spel ne conteming tothe folewsing dimensamns Leng, le} fa Lent Sheveaee mh Tn ft iv mounted ou o vostical shaft of similse mets approst mately 6 on (4 in) in dEameter. cowmecred to 2 drive gehsuis: eh epayes ty paddle un is Yeugitaingl 33s, S06 15 pm. The apparatssis oF such design thet, when theComitt ‘sine se ATDLASTN DLUOL-ENGL 4958 MM 0759570 O620925 O08 Me fh 01401 cylinder is claraped in position und the paddle assembly is foqered ino dae cylinder, a positive stop engages sad hckcls the assembly shen the lower edge ef the paddle is 6 mum from the tottom of the eylinder. Daring the operation of the stincr, he center of the bolton eye ul the ile shall not deviate moe ‘haa 1 en toe she: oF rortion. When ni operalin, Oe pale anreenly can be lifted vertically to lsar tbo lop oF the graduated cylinder & Reagents 6.1 Parity of Reugents Rengew: acvde chemicals shall we uscd in all tests, Unless oherwise indicated. it is intcndod vt all reagent shall conforua lo te specifications of tne Commit tec on Analytica Reageni of the American Chemical Society vwhete such specifications are evaileble.” Otter grades may be teed, provided it is first wwertainal that the reagent is of saficintly high puriy Lo permit is use without lessening the soeurscy of the detestinglton, 6.2 Party of Water—Umess otherwise incicated, reference to war stall be uncerstcad (a meen reagent wacer a8 defined ty Type Win Specificution 11103 16.4 Cleaning Solvents, Ligh-Hydracarbor, such us precip uiton saphtha (Warming Health hazaad) for povlews oi. Use ccher appropriate solvents for dissolving synthesc Hu 64 Acetone, Warning—Health huvard, Flammable 65 Cleaning Reagens, Cleunivy by she: hot NOCHRO MIX! (Warning: Couesive, Heal hazard Oxidizeri, or a Di-hr souk rom leuperilare in MICRO® adutioa gate sccapuble statsticsly oqivilent suns in eonnd-robe kest- ng 1. Sampling 7.1 The testis very scasitive to small ameunts oF contani- ‘ation, Take sample? in socordasce with Prasive D AUS?. 13, Preparation of Apparatus 8, Clean the grafusted eylinder hy removing any Hilt of| cil (or Avid) with cleaning solven: folbwee by a wash fit swith asotone and shen seth tap wast. "The giwssere stl be further cleaned with a suitable. cleaning reagent. Rine thor ‘ughly with lap waler ane thee with ceagent Water Laspect the sylingsrs ‘or any residue. or waler dcplels adhering to the inside walls. Both condiions indicate new fee adioral leaning, §.2 Clean the stirring paldle and shalt with absextent cation ce dave wet with clearing solvent and wir dry. Cure abt bo taken not to boad or misliga Ure paddle assembly during the leaning opezaron, 3, Progudure 9a Het she hath Wiquid w $4 = 19°C (Note 1) and maintain Shear Gina Amarin Gime! Sionty Spuiucion, So Chena Sy, Mating A, Bo sags a Og of eaten [a fy the Area Cocca! Son sce Atal Sands for iborasr ‘heniaty BOM Lily ds, beste UK. sd th ates Seow Phones ed Suro Fen, US amid Convaion (USPC), Rese, * NOCHRONEE salle crm Gates Libingies fe, ENB Ee A, "TRSICRCD esse FoomSrertiomal Pradues Cap, PD. Bor 70, Buringne. the A ASTM beri SRS 2005 it at that tempcratare rouyhout the ws), Add eagent water (Nore 2, ane Noe 3) oe graducted eylinder up to the 40am. imc an! then addon the same cylinder a roprosenative sample of fe oF (or Maid) under test until the cep level of the ail reaches the R0-ml. mark on the cylinder. Place the eslinder 0 the bah and allow the contents lo seach bath temperamre. letling ene may cary sith ape of eqvipinent and ean reach up & Hd min ‘Nore 2H itil volunete mensurements re nse ur eer sean expanron suming athe cbevated fet tempest wl Face B Be conadera. For exuple tere il be tah wun She tod mk at REC. Comet’ teach eo therefor, SI0UM be mde so tht the tal Ie slume eacngs made far sie or dh ote, nd vtonn sees ned enovel 30 TA lesaive prceare which woud i the somec ance is hs ck ce ‘Neve SAU soc elo (ACH slut osmotic eu er (os decried in Spocteatien D LLAL qv Tone Metin D 665, cun heuned inphie oldie tere esting cea ile Fuck usin marine 9:2 Chump the isle in place dectly uncer se stining paallle, Lewer We pulgle wo the cvtinier Und we stop engages at the requitod depth Stat the sir anf a sop watch Simtunspusly nd adj he sive. ss required, toa spe of 1SUD AS qm. Al he a of Sia tp the stozer td oxse ‘herring acon ont itis just cles of the radu. Wipe de pad wilh a poicaues (Not #,alloving the Higa ds rerwoved ly chop hack ve cylinds, Remove che eying froin the retaining clamps and transfor ic warchilly to ater suction ofthe ath, At Sein intervals it the esti cut of the bath, inspect, cad record the volumes ef ths oil Ibid). ‘wate, and emulsion. eye. Neve 4 The plismas shit he mace cf mali sesstat 1 te oil or hd, 10, Report 10.1. Reoaid the tne Cat S-mnin inervas) wnt either (ab the prosnet passes the warcr soparabilily requirements iis being lented agains: oF (b) the west Limie for seater sspambily is ‘esepeded {usually 3-nL emulsion or less for 3U-anin at 51°C and 6D min at 82°2). The maximura volume to be reported ns the oif lover fs 43 ea (Neve 5), For wuifyrmity epoch rest ests In the maaser shown in the following, empl: Ti eomtion rat erate 15 ‘inuson tedioed 9m 29 eee war or. S88 i) Lieto temas inane ate Iebeecb fol, 3 icc water ars cot semeey Luanpateaesotan Joa nt coca ba on ‘lone eiced Sr aries ar 2 s70 ‘tmarpinh ve oan ree er 3 "ni The ert ajar 25 nn beaded ‘Ler esara, O3e-t4or 434 10.2. The appenance of cach kyver may be described ix the following warms. 10.2.1 Off for Oil Rick) Layer 21) Gear. 102.12 Hazy Oot € 10.2.1. Cloudy (ov milky) (Nate 6) 102.04. Combiuasions of 10.2.1.1-10.2STBAASTM DIWOMENGL 1994 Ml 0789520 Ob205hb THY Ww it D 1401 10:22 Miser o Whrer fic Laser 105.1 Welltsined, sare 1922.1 Gear 192 lededned bois Lasy 07 babble: prose, bth 105.3 iMedetved Tac Hazy (Nok 0) 104 Report the test omperaure Ther than S4°C and te 4 Cloudy (eri (Note saya ro Hf obo han dist ae 5 Cooinavong cf 92200324. . erdhon sist as HDS. dase 1 | ose and ey. 2 Cloudy (or milsy) ¢Note > 111 Precision —The previgian of this est method was “5 Croumiy (lke wasynmalsc} (Nate 2) shlaiaed on steam turbine oils hy sites of 2838 10.90 4 Combinsdons of 102,3.1-102.5.3. St tm) AL ADPC and wsng ime fo 5 ent fas ema sion as the tox completion. This precision is expressed graphically in Fig, 1, The graph show's he ragga allssuMe Ueviuion in minutes for cepeatubilty and reproducibility (95 % vocti- dence) ices mar ernutsiues wet vesale For ‘hose ols. may 11. decison and Bias Abe aneneueement of the sn sale: Layee escitily enmplest pron, up ive sl le ee selon Fore ules End the upp ler arn han 13M, ayer sh! cose ‘he smutvun uye, rot he apicabta to other ons or Duis ane 6—Ahazy lyer been astungtiamincwandaccoude ise 1.2 Bias—Tae poceduc inthis test method for meesarig, emp. vente separapalty as no Bits BACAUSe Te value for Yaak ‘Nine 7 pusspd dione here cloudy ard any el cette me el fd pay de ie bar tick cosy ais probly sabe. tnt exusi reutly to fom a ied gash ehieacesmycmuion wll ne, 12s Keywords 1G3 The aprcanmee af the ciVemlsion and wats’ 121 exauision: petroleum oily, steametarbine oils sya- enmalsion imerfares may b> deszribed ia the tallowing tes: ther ids: water sopanibitty eparabtity is defined only in rms ofthe tl tho, C1 repentan ty wean int Reset, min Gert ard outs es poo pis Cane ron ve on ls eau ed abon pall iy 3°88 16“ aps eh he pecerof Sarle—tn ihe mension ot 6-40 (t-n)a 4404 Ew Ty eal LI Kemi InseMaLer More EaNiS 13SEC ae! 28 Tsp wih a eepasta fy aoa Use ie ar Sn f Ine abel of mens ofA absanies FIG. chert‘ Dxtermning Text Precision san Sony ar eta ire kes nope ean ne asses. nooiracton Pear AGS el te ako osprey De ah ebateo Penne stron 384 by epoca trees torrent nla, tO Gorse fovea oie sara tds untae eda setgotrs Sear cre oa oat fhe er {Genncalsonmton none tay nae Mae een our paren ase rau a weary snore sna inoer fens ST Co Cansoncsten 1888 the A ASTM beri SRS 2005 Comitt ‘sine se