Professional Documents
Culture Documents
MODEL 6650SP-XD
UV Fluorescence Analyzer
P/N:M6650SP-A
9/16/2015
DANGER
Toxic gases and or flammable liquids may be present in this monitoring system.
Personal protective equipment may be required when servicing this instrument.
Hazardous voltages exist on certain components internally which may persist for a
time even after the power is turned off and disconnected.
Only authorized personnel should conduct maintenance and/or servicing. Before
conducting any maintenance or servicing, consult with authorized
supervisor/manager.
Model 6650SP-XD
ii
Model 6650SP-XD
Safety Messages
Your safety and the safety of others are very important. We have
provided many important safety messages in this manual. Please read
these messages carefully.
A safety message alerts you to potential hazards that could hurt you
or others. Each safety message is associated with a safety alert symbol.
These symbols are found in the manual and inside the instrument. The
definition of these symbols is described below:
GENERAL WARNING/CAUTION: Refer to the instructions
for details on the specific danger. These cautions warn of
specific procedures which if not followed could cause bodily
Injury and/or damage the instrument.
CAUTION: HOT SURFACE WARNING: This warning is
specific to heated components within the instrument. Failure
to heed the warning could result in serious burns to skin and
underlying tissue.
WARNING: ELECTRICAL SHOCK HAZARD: Dangerous
voltages appear within this instrument. This warning is
specific to an electrical hazard existing at or nearby the
component or procedure under discussion. Failure to heed this
warning could result in injury and/or death from
electrocution.
Technician Symbol: All operations marked with this symbol
are to be performed by qualified maintenance personnel only.
iii
Model 6650SP-XD
iv
Model 6650SP-XD
Table of Contents
Safety Messages .......................................................................... iii
Table of Contents .......................................................................... v
List of Figures ............................................................................. viii
List of Tables ................................................................................ ix
Introduction ................................................................................... 1
1.1 Introduction
1
1.2 Model 6650 Components
1
1.2.1 PX2 Photometric Transmitter
2
1.2.2 Control Unit
4
1.2.3 Xenon UV Source
5
1.2.4 Flourescence Probe
5
1.3 Optional Components
6
1.4 User Interface
7
1.4.1 Displays
7
1.4.2 Control Unit Front Panel
7
1.4.2.1 UP/DOWN Switch
7
1.4.2.2 ESCAPE/ENTER Switch
8
1.5 Equipment Interface
9
1.5.1 Electrical Connector Panel
9
Theory of Operation .................................................................... 11
2.1 Fluorimetry
11
2.2 Filter Based Flurometer Description
12
2.3 Model 6650 Theory and Terminology
12
2.3.1 Excitation Filter
13
2.3.2 Emission Filter
14
2.3.3 Measure Detector
14
2.3.4 Source Reference Detector
14
Model 6650SP-XD
14
14
15
15
15
16
16
16
Installation ................................................................................... 17
3.1 Unpacking and Mounting the Analyzer
17
3.2 Electrical
19
3.2.1 Primary Input Power
20
3.2.2 Fuse Installation
21
3.2.3 Analog Outputs
21
3.2.4 Alarm Relays
23
3.2.5 Digital Remote Cal Inputs
24
3.2.6 Network I/O
25
3.2.7 RS-485
25
3.3 Fiber Optic Cables
26
3.4 Probe Installation
27
3.5 Sample Handling System
27
3.6 First Time Power Up and Initialization
27
3.7 Calibration
27
Setup & Operation ....................................................................... 29
4.1 Interface Panel
29
4.2 Control Unit
30
4.2.1 Mode/Function Selection
31
4.2.1.1 CALC Mode
31
4.2.1.2 Setup Mode
31
4.2.2 Data Entry
33
4.2.2.1 ENTER
33
4.2.2.2 ESCAPE
33
vi
Model 6650SP-XD
34
34
35
36
37
38
38
39
39
39
40
40
40
42
42
43
44
46
47
47
48
48
49
vii
Model 6650SP-XD
List of Figures
viii
Model 6650SP-XD
List of Tables
Table 3-1: Analog Concentration OutputExample ...................... 22
ix
Model 6650SP-XD
DANGER
FLAMMABLE LIQUID USAGE
WARNING
Model 6650SP-XD
Introduction
Introduction
1.1 Introduction
The Model 6650SP-XD UV Fluorescence Analyzer is a
sophisticated instrument designed to measure an oil concentration in
water. It consists of a Control Unit, PX2 Photometric Transmitter, and
an integrated Fluorescence Probe. The Analyzer is housed in an
explosion proof housing with a window providing visual access to the
control unit display. Operational controls are conveniently located on the
outer door of the enclosure so the unit can be operated without having to
open the door.
The PX2 Photometric Transmitter is a dedicated module that
includes a flashed xenon UV light source, detectors and filters plus input
and output connections for the probe. It communicates with the control
unit via a digital RS485 connection. The transmitter is configured at the
factory to produce a highly selective, narrow UV band of radiation to
optically stimulate a target species (the analyate) in a solution. The
excited molecules almost immediately return to a ground state with a
corresponding longer wavelength emission whose signature is
characteristic of the oil species in solution. The Model 6650SP-XD
precisely measures the corresponding fluorescence emission and the
control unit converts signal and displays the concentration in units
convenient to the end user.
The analyzer is equipped with configurable high and low
concentration alarms, a system failure alarm with digital and analog
output signals for process control and measurement. An integral probe
interfaces with the process and transmits optical signals to and from the
sample.
PX2 Transmitter
Introduction
UV Fluorescence Analyzer
Control Unit
Model 6650SP-XD
Introduction
is averaged and passed to the control unit for signal processing and
display through the RS-485 port.
The PX2 Transmitter is carefully configured and tested at the
factory for your specific application. The unit can be reconfigured if
necessary via a USB connection with a remote computer. Contact the
factory for further information on reconfiguring or making changes to
the PX2 setup.
A self-testing routine is installed in the module with multi colored
LEDs indicating status: in test, unit ok, or a fault condition. The
indicators will light up and cycle through a series of colors (blue, red,
green, purple, light green, aqua, and blue) as the unit is supplied with
power. Once the LED has returned to solid blue, the unit is ready for
operation. The PX2 module is shown in Figure 1-2.
The transmitter operates from a dedicated 24VDC power supply
mounted adjacent to the transmitter. See Figure 1-1.
Introduction
UV Fluorescence Analyzer
Model 6650SP-XD
Introduction
No moving parts
Introduction
UV Fluorescence Analyzer
Model 6650SP-XD
Introduction
Z- or X-Purged Enclosure
Ultrasonic Homogenizer
PWD
Logout
Version
Self-Test
Span
Zero
Introduction
UV Fluorescence Analyzer
Alarms
Range
Negative
4-20 Test
Alarm Test
Standby
WARNING:
Enter
Model 6650SP-XD
Introduction
Power Connection
Introduction
UV Fluorescence Analyzer
Analog Outputs
Alarm Connections
USB Port
Remote Valves
Probe Connection
Remote Span/Zero
Calibration Contact
Range ID Contacts
Network I/O
10
Model 6650SP-XD
Theory of Operation
Theory of Operation
2.1 Fluorimetry
The ability to monitor the concentration of an analyte in a process
stream is critical for accurate and reliable process control. There are
many techniques used to determine the analyte concentration of interest.
One of the most sensitive sensing techniques is molecular fluorescence.
Fluorescence occurs when a molecule absorbs light energy, either
ultraviolet or visible, and rapidly emits light, at some longer wavelength.
Fluorescence of this type is referred to as Stokes fluorescence.
Fluorimetry characterizes the excitation and emission properties of the
molecular species. Figure 2-1 shows an example of the excitation and
emission spectrum from a hypothetical fluorophore.
Fluorimetry is concerned with two types of information:
11
Theory of Operation
UV Fluorescence Analyzer
12
Model 6650SP-XD
Theory of Operation
13
Theory of Operation
UV Fluorescence Analyzer
14
Model 6650SP-XD
Theory of Operation
15
Theory of Operation
UV Fluorescence Analyzer
16
Model 6650SP-XD
Installation
Installation
Installation of the Model 6650SP analyzer includes:
1. Unpacking and mounting the analyzer.
2. Making AC power, alarm, and output signal electrical
connections.
3. Optical connection and installing the probe.
4. First time power up and initialization
5. Calibration.
Please follow the outlined sections below as a guideline to
installing the Model 6650SP-XD in your plant environment.
17
Installation
UV Fluorescence Analyzer
18
Model 6650SP-XD
Installation
3.2 Electrical
The Model 6650SP-XD is configured to operate from a standard
110 or 220 VAC 50/60 Hz power source depending on the installation
location. Use the dedicated 3/4 and 1 NPTF feedthroughs for bringing
AC power, signal and alarm connections in and out of the enclosure.
Refer to the Interconnection Diagram in the Appendix for terminal
connections.
Figure 3-3 shows the Electrical Connector Panel. There are
terminal blocks for connecting power, communications, and both digital
and analog concentration outputs.
19
Installation
UV Fluorescence Analyzer
20
Model 6650SP-XD
Installation
21
Installation
UV Fluorescence Analyzer
Voltage Signal
Output (VDC)
0.0
0.1
0.2
0.3
0.4
0.5
0.6
0.7
0.8
Current Signal
Output (mA DC)
4.0
5.6
7.2
8.8
10.4
12.0
13.6
15.2
16.8
22
Model 6650SP-XD
9
10
Installation
0.9
1.0
18.4
20.0
Threshold Alarm 2:
23
Installation
UV Fluorescence Analyzer
System Alarm:
SPAN:
24
Model 6650SP-XD
Installation
25
Installation
UV Fluorescence Analyzer
26
Model 6650SP-XD
Installation
3.7 Calibration
Prior to using the analyzer, the unit must be calibrated. The
calibration procedure is discussed in Sections 4.6 and 5.6. Calibration
requires a familiarity with the operating interfaces of the transmitter and
control unit. Please read Chapter 4 prior to calibrating this instrument.
27
Installation
UV Fluorescence Analyzer
28
Model 6650SP-XD
29
UV Fluorescence Analyzer
30
Model 6650SP-XD
31
UV Fluorescence Analyzer
32
Model 6650SP-XD
Any function can be selected at any time. Just scroll through the
MAIN MENU with the DOWN/UP control to the appropriate function,
and ENTER it. The analyzer will immediately start that function, unless
password restrictions have been assigned. (Password assignment is
explained further on.)
All of these functions are described in greater detail in the
procedures starting in section 4.3. The VFD screen texts used to
illustrate the procedures are reproduced in a Arial Narrow Bold type style.
4.2.2 Data Entry
4.2.2.1 ENTER
33
UV Fluorescence Analyzer
34
Model 6650SP-XD
or
AAAAA
Enter PWD
The screen prompts you to enter the current password. If you are
not using password protection, ENTER to accept TETAI as the default
password. If a password has been previously installed, enter the
password using ENTER to scroll through the letters, and the DOWN/UP
keys to change the letters to the proper password. The last ENTER
enters the password.
If the password is accepted, the screen will indicate that the password
restrictions have been removed and you have clearance to proceed.
PWD Restrictions
Removed
35
UV Fluorescence Analyzer
Change Password?
<ENT>=Yes <ESC>=No
ENTER to change the password (to change either the default TETAI
or the previously assigned password), or ESCAPE to keep the existing
password and move on.
If you choose ENTER to change the password, the password
assignment screen appears.
TETAI
<ENT> To Proceed
or
AAAAA
<ENT> To Proceed
B
L
V
`
j
t
*
4
>
C
M
W
a
k
u
!
+
5
?
D
N
X
b
l
v
"
'
6
@
E
O
Y
c
m
w
#
7
F
P
Z
d
n
x
$
.
8
G
Q
[
e
o
y
%
/
9
H
R
f
p
z
&
0
:
I
S
]
g
q
{
'
1
;
J
T
^
h
r
|
(
2
<
36
Model 6650SP-XD
When you have finished typing the new password, the last ENTER
enters it. A verification screen appears. The screen will prompt you to
retype your password for verification.
AAAAA
Retype PWD To Verify
Wait a moment for the entry (<ENT>) screen. You will be given
clearance to proceed.
AAAAA
<ENT> TO Proceed
Note: If you log off the system using the LOGOUT function in the
MAIN MENU, you will now be required to re-enter the
password to gain access to any of the functions except
password (PWD).
37
UV Fluorescence Analyzer
Then:
RUNNING DIAGNOSTIC
Testing Analog Out
38
Model 6650SP-XD
39
UV Fluorescence Analyzer
40
Model 6650SP-XD
Volume of
Oil
10 ppm
20 ppm
10 l
50 ppm
25 l
100 ppm
50 l
200 ppm
100 l
3. Wipe any excess oil off the outside of the syringe with a
lintless tissue. Be careful not to allow the tissue to wick any
oil out of the syringe.
4. Place the lid on the blender and switch it on to its highest
setting. Lift the lid enough to inject the contents of the
syringe into the water midway between the center of the
vortex and the wall of the blender. Make sure oil injection
happens under water or some of the oil may be thrown
against the wall of the blender
5. Place the lid back on the blender and homogenize for exactly
2 minutes.
6. Discard the contents of the blender into the waste jug. The
blender is now stabilized for accurate preparation of the span
fluid. Repeat steps 2 through 5 and the calibration span fluid
is now ready.
Teledyne Analytical Instruments
41
UV Fluorescence Analyzer
The control unit uses the non-linear 4-20 mA output signal from the
transmitter to report the oil concentration. Control unit calibration
establishes an accurate, linearized correspondence between transmitter
counts and the unit of measure configured at the factory (typically ppm).
It requires setting the control unit zero, half and full span points to the
known concentration of the calibration fluids while the probe is
immersed in the calibration fluid.
Activate the ENTER switch once more to display the next screen:
Getting Zero Values
Please wait . .
42
Model 6650SP-XD
This message will time out in 30 seconds and return to the Analyze
screen or you can use the ENTER switch to immediately return to the
Analyze screen.
At this point the control unit has stored the zero calibration
information and the zero calibration is complete.
Use the ENTER switch again to display the next screen where you
enter the known span concentration:
Span Val: 00060.00
UP/DN Mod <ENT> Done
43
UV Fluorescence Analyzer
The current span value will be blinking. Use the UP/DOWN switch
to modify the value if desired. Then activate the ENTER switch to store
the value in memory. The following screen will display:
Getting Span Values
Please wait . .
Use the ENTER switch to save the calibration and return to the
Analyze screen.
67.4
ppm Anlz
Range: 0 100
44
Model 6650SP-XD
45
UV Fluorescence Analyzer
ppm (oil)
6. Out-of-range direction: HI or LO
7. Defeated? (Yes/No): DftY/N
8. Failsafe? (Yes/No): FsY/N
9. Latching? (Yes/No): LtchY/N.
Once the parameters for the alarm have been set, ENTER the
ALARM function again, and repeat this procedure for next alarm.
Note: In this screen, ENTER moves you through the fields and
ESCAPE takes you back to the previous screen.
46
Model 6650SP-XD
Alarm Test
Upon selecting this function, you are given the choice to test alarm 1 or
alarm 2.
Select Alarm: AL1
47
UV Fluorescence Analyzer
48
Model 6650SP-XD
49
UV Fluorescence Analyzer
50
Model 6650SP-XD
51
UV Fluorescence Analyzer
LEDs that make up the Teledyne logo on the transmitter will turn from
blue to red.
When the Broken Light Path message appears on the display, the
display will not report concentration or allow passage to any other
function until the probe is returned to darkness or the broken path is
corrected.
A second fault message is possible and occurs when the
measurement detector sees a low signal while the reference detector
signal is normal. This will cause a Light Source Failed message to occur
onscreen and the LEDs on the PX2 to flash red. When this occurs, the
display will not report concentration or allow passage to any other
function until the light path is restored and functioning correctly.
52
Model 6650SP-XD
Appendix
Appendix
A.1 Specifications
53
Appendix
UV Fluorescence Analyzer
Outline Diagram
Interconnection Diagram
54