Mirian/Alexa

Normalizacin de sosa
Ensayo
Masa Bif
1
2
3
Promedio
s
%CV
Muestra:
Titulante

Acido
NaOH

V gastado

[NaOH]

Anlisis de muestra des

14
12
10
8

pH

Sulfanlico

6
4
2

V, mL NaOH pH
0
0.5
1
1.5
2
2.5
3
3.5
4
4.5
5
5.5
6
6.5
7
7.5
8
8.5
9
9.5
10
10.5
11
11.5
12
12.5
13
13.5
14

V prom
2.3
2.5
2.6
2.7
2.8
2.9
3
3.1
3.2
3.4
3.6
4
5
9.7
10.6
11
11.2
11.3
11.4
11.5
11.6
11.7
11.7
11.8
11.8
11.8
11.8
11.9
11.9

dpH/dV
0.25
0.75
1.25
1.75
2.25
2.75
3.25
3.75
4.25
4.75
5.25
5.75
6.25
6.75
7.25
7.75
8.25
8.75
9.25
9.75
10.25
10.75
11.25
11.75
12.25
12.75
13.25
13.75

0.4
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.4
0.4
0.8
2
9.4
1.8
0.8
0.4
0.2
0.2
0.2
0.2
0.2
0
0.2
0
0
0
0.2
0

V NaOH
pH

14.5
15

11.9
12

14.25
14.75

0
0.2

Damian/Zayret

Anlisis de muestra desconocida. Mirian/Alexa

Normalizacin de HCl
Ensayo
1
2
3
Promedio
s
%CV

10
9
8
7
6
5
4
3
2

1ra Der

Muestra:
Titulante

1
2

10

V NaOH, mL
pH

dpH/dV

12

14

16

V, mL NaOH
0
0.5
1
1.5
2
2.5
3
3.5
4
4.5
5
5.5
6
6.5
7
7.5
8
8.5
9
9.5
10
10.5
11
11.5
12
12.5
13
13.5
14

14.5
15

mian/Zayret

malizacin de HCl
Masa CarbonaV gastado

[HCl]

Anlisis de muestra desconocida. D

10
9
8

Promedio
s
%CV
Acido
NaOH

7
6

pH

Sulfanlico

5
4
3
2
1
0

pH

V prom
9.2
8.7
8.4
8.2
8
7.9
7.9
7.8
7.7
7.7
7.6
7.5
7.5
7.4
7.4
7.3
7.2
7.1
7
6.8
6.7
6.4
5.8
2.8
2.4
2.3
2.3
2.3
2.2

dpH/dV

10

V NaOH, mL

0.25
0.75
1.25
1.75
2.25
2.75
3.25
3.75
4.25
4.75
5.25
5.75
6.25
6.75
7.25
7.75
8.25
8.75
9.25
9.75
10.25
10.75
11.25
11.75
12.25
12.75
13.25
13.75

-1
-0.6
-0.4
-0.4
-0.2
0
-0.2
-0.2
0
-0.2
-0.2
0
-0.2
0
-0.2
-0.2
-0.2
-0.2
-0.4
-0.2
-0.6
-1.2
-6
-0.8
-0.2
0
0
-0.2

pH

dpH/dV

2.2
2.1

14.25
14.75

0
-0.2

e muestra desconocida. Damian/Zayret

0
-1
-2
-3
-4
-5
-6

10

V NaOH, mL
pH

dpH/dV

12

14

16

-7

1ra Der