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This study was supported by Student Research Grant of the Academy of Prosthodontics.
Associate Professor, Department of Dentistry, Faculty of Medicine and Dentistry.
Private practice, Edmonton, Alberta, Canada.
c
Assistant Professor, Department of Civil and Environmental Engineering.
d
Assistant Professor, Department of Civil and Environmental Engineering.
e
Associate Professor, Head of the Division of Orthodontics and Director of the Orthodontic Graduate Program,
Department of Dentistry, Faculty of Medicine and Dentistry.
a
Nassar et al
173
March 2013
Vinyl polysiloxane (VPS) and polyether (PE) impression materials are
commonly used to produce final impressions in restorative dentistry. VPS
and PE exhibit excellent dimensional
stability under different test and storage conditions.1-6
Differences in the dimensional stability of these 2 materials have been
reported based on the conditions of
the study environment. Unlike VPS,
studies recommended pouring PE
impressions within 1 hour7,8 or within
24 hours9,10 because the loss of volatile substances or absorption of water
contributes to distortion over time.
Although VPS and PE produced
satisfactory dimensional stability
under dry and moist conditions,11
PE produced better surface details
than VPS under moist conditions.
This is in agreement with the conclusion of another study12 which reported that PE impressions should
be used when moisture control is
difficult. Likewise, others13 have
shown that 2 hydrophilic VPS materials were dimensionally accurate
under dry, moist, and wet conditions. The best surface details, however, were obtained only under dry
test conditions.
In 2009, a vinyl polyether silicone product (VPES) (EXAlence; GC
America, Alsip, Ill) was commercially
introduced. This material is available
in a variety of consistencies and setting times. EXAlence is composed of
a combination of VPS and PE and is
promoted as a hydrophilic material
that presumably maintains the stability of the parent products. The manufacturer purports that the pouring of
EXAlence impressions can be delayed
for up to 2 weeks. Currently no research data support this claim. Therefore, the purpose of this study was
to test and compare the dimensional
stability of EXAlence 370 (VPES)
Monophase impression material to
that of Imprint 3 (VPS) Monophase
and Impregum Penta soft (PE) medium-body impression materials.
The null hypothesis was that there
would be no significant difference in
Nassar et al
Type
Manufacturer
Lot Number
GC America Inc
1001051
Monophase
Imprint 3
Alsip, Ill
VPS
Monophase
Impregum
Medium body PE
Metricide 28
3M ESPE AG
70-2011-2495-8
Seefeld, Germany
Type V dental stone
(prepackaged)
Triad Trutray
70-2010-5108-6
Penta soft
Die Keen Green
3M ESPE
D1102028
Dentsply Trubyte
material
York, Pa
Activated 2.5%
Metrex
Glutaraldehyde
Orange, Calif
110113A
70-8120-5
174
2 Cast poured from impression made of metal model. Each cast had
6 measurements of cylinder diameter A/D and B/C, anteroposterior
AB/CD, and cross-arch dimensions BC, DA, and AC/BC as shown.
changes in their properties.14-18 After
the disinfecting procedure, each impression was rinsed thoroughly under
tap water for 30 seconds to remove
disinfectant residues and dried with
a gentle air stream. The impressions
were poured either immediately, after
1 day, after 1 week, or after 2 weeks.
Prepackaged Type V die stone
(Die-Keen; Heraeus, South Bend, Ind)
was used to make the casts. As suggested, 60 grams of powder and 13
mL of distilled water were first mixed
by hand then by vacuum-mixing for
20 seconds. The stone was carefully
vibrated into the impression and
was left for 1 hour. The casts were
removed in the same manner for all
casts by using their distal edges and
were number coded in preparation for
measurements. One person made the
measurements with a digital micrometer
(Mitutoyo IP 54; Mitutoyo Canada
Inc, Mississauga, Canada) (resolution
1 m; instrument error 2 m).
The measurements made on the
240 casts were as follows: the diameter of the 4 cylinders (A, B, C, and D
- the cylinders had known dimensions
(Fig. 1), which provided an optimal
way to compare the measurements
of the casts to the metal model);
anteroposterior measurements (AB
and CD); and cross-arch measurements (BC, DA, AC, and BD) (Fig. 2).
These individual measurements were
paired as follows: cylinders A and D;
RESULTS
The cast measurements at all pour
times had negative values except for
the combined cylinder measurements
A/D in the immediate pour of VPES
(Table II, Fig. 3), which had a mean
dimensional change of 0.04% 0.38%.
Therefore, with the exception of this
measurement, the mean dimensions
of casts were larger than those of the
metal model.
Considering the absolute values
for mean percentage dimensional
changes, all measurements, regardless of the impression material type
or storage time, were below 1% with
the single exception of 1-week PE for
the smaller cylinders B/C. The mean
Nassar et al
175
March 2013
Table II. Mean percentage difference (SD) for all materials, time points,
and measurements
Impression
Materials A/D
Time Point
Immediate casts
VPES
VPS
PE
VPES
1-Day casts
VPS
PE
VPES
1-Week casts
VPS
PE
VPES
2-Week Casts
VPS
PE
B/C AB/CD
BC
DA
AC/BD
0.04
-0.24
-0.23
-0.15
-0.12
-0.10
(0.38)
(0.38)
(0.11)
(0.11)
(0.08)
(0.08)
-0.29
-0.55
-0.35
-0.33
-0.16
-0.22
(0.16)
(0.20)
(0.08)
(0.10)
(0.07)
(0.06)
-0.29
-0.41
-0.25
-0.19
-0.20
-0.13
(0.30)
(0.40)
(0.13)
(0.14)
(0.07)
(0.06)
-0.22
-0.55
-0.34
-0.26
-0.20
-0.18
(0.17)
(0.22)
(0.12)
(0.19)
(0.13)
(0.10)
-0.30
-0.48
-0.35
-0.26
-0.16
-0.19
(0.11)
(0.15)
(0.10)
(0.07)
(0.06)
(0.05)
-0.31
-0.63
-0.46
-0.29
-0.20
-0.18
(0.34)
(0.36)
(0.16)
(0.15)
(0.14)
(0.14)
-0.23
-0.63
-0.23
-0.24
-0.19
-0.17
(0.25)
(0.37)
(0.17)
(0.06)
(0.09)
(0.08)
-0.28
-0.51
-0.32
-0.21
-0.17
-0.19
(0.27)
(0.29)
(0.17)
(0.09)
(0.09)
(0.07)
-0.48
-1.14
-0.36
-0.34
-0.20
-0.17
(0.41)
(0.55)
(0.17)
(0.18)
(0.07)
(0.09)
-0.26
-0.83
-0.31
-0.28
-0.15
-0.15
(0.24)
(0.25)
(0.10)
(0.08)
(0.12)
(0.05)
-0.19
-0.33
-0.26
-0.23
-0.13
-0.16
(0.15)
(0.17)
(0.11)
(0.07)
(0.06)
(0.06)
-0.45
-0.90
-0.37
-0.26
-0.21
-0.18
(0.51)
(0.26)
(0.20)
(0.09)
(0.10)
(0.09)
Immediate Casts
0.6
Mean Percentage
Dimensional Change
0.4
A/D
B/C
AB/CD
BC
DA
AC/BD
0.2
0
-0.2
-0.4
-0.6
-0.8
-1
VPES
VPS
PE
Measurement
3 Mean percentage dimensional change values for measurements from
immediate-pour casts. Error bars represent standard deviation. Statistically
significant differences exist between VPES and VPS for cylinder measurements
A/D (P=.001), B/C (P=.003), anteroposterior measurement AB/CD (P=.001),
cross-arch measurements BC (P<.001), and AC/BD (P<.001) and between
VPES and PE for cylinder measurements A/D (P=.011) and DA (P=.002).
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176
1-Day Casts
A/D
B/C
AB/CD
BC
DA
AC/BD
Mean Percentage
Dimensional Change
0
-0.2
-0.4
-0.6
VPES
-0.8
VPS
PE
-1
-1.2
Measurement
Mean Percentage
Dimensional Change
1-Week Casts
A/D
B/C
AB/CD
BC
DA
AC/BD
-0.2
-0.4
-0.6
-0.8
-1
VPES
-1.2
VPS
-1.4
PE
-1.6
-1.8
Measurement
Mean Percentage
Dimensional Change
2-Week Casts
A/D
B/C
AB/CD
BC
DA
AC/BD
-0.2
-0.4
-0.6
-0.8
VPES
-1
VPS
PE
-1.2
-1.4
Measurement
DISCUSSION
The null hypothesis was not rejected. Casts produced from a disinfected regular set VPES (EXAlence
370 monophase) demonstrated excellent dimensional stability at different pour times and were comparable
to the tested VPS and PE impression
materials.
Considering the dimensional changes of VPES at immediate pour and over
extended periods of time, the results of
this study showed that, similar to the
PE and VPS materials tested, EXAlence
370 monophase had minimal dimensional changes as shown by cast measurements, indicating that the material was accurate and dimensionally
stable. The majority of the specimens
experienced minimal changes (leading
to cast measurement changes equal
to or less than 0.34%) (Figs. 3-6).
VPES was introduced by the manufacturer as a combination of VPS and
PE. The manufacturer reports that it
has 5% to 20% polyether compound,
which is presumably responsible for
enhancing the hydrophilicity of the
impression material. The remainder
of the material, the VPS component,
consists of a combination of vinyldimethylpolysiloxane
(10%-50%),
methylhydrogen dimethylpolysiloxane (3%-10%) and silicon dioxide
(30%-65%). This combination is purported by the manufacturer to provide excellent elastic recovery and
good tear strength. Because of this
unique composition of VPS and PE,
it is reasonable to discuss VPES behavior using the established knowledge on these 2 categories of impression materials.
Nassar et al
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March 2013
Except for one mean measurement, impressions from the 3 materials produced cast measurements that
were slightly larger than the control.
As explained by Wadhwani et al,16
the increased dimensions of the cast
cylinders could result from shrinkage that occurs freely in all directions
toward the center of the mass of the
material. In addition, the tray adhesive and mechanical tray retention
could cause the direction of shrinkage
to be toward the tray wall, in a buccolingual direction. If stone expansion is
considered, 2 comments are relevant.
The first is that the same Type V stone
was used in the same manner for all
impressions so that any expansion in
the casts would be uniform, regardless of impression material. However,
considering a study by Heshmati et
al17 on setting expansion of the Type
V stone, Die-Keen (Heraeus), a 0.35%
expansion of all casts means that the
true polymerization shrinkage of the
materials is in fact much less than the
values obtained in this study, which
means that the materials are more dimensionally stable.
The main reasons for dimensional
contraction in elastomeric materials
are polymerization shrinkage, loss of
volatile components, loss of water,
and lack of elastic recovery.19,20 Continuous evaporation of volatile substances from the polymerized elastomer likely explains the increase in
die size with longer storage periods.
In addition, as the polymerization
process continues, the material may
contract leading to larger cast dimensions.10,21 Because of the PE component of VPES, the absorption of water
from the surrounding environment
and disinfectant likely counteracted
the dimensional contraction for all
VPES measurements. This absorption could explain the combined A/D
cylinder measurements being smaller
than the metal model, resulting in the
positive value for the mean percentage dimensional change mentioned
above.7,10 As can be seen from Figures
3-6, the mean dimensional changes
of the large cylinders A/D are notice-
Nassar et al
ably less than those of the small cylinders B/C; this made their mean dimensional change closer to the metal
model measurements than the values
for B/C at all times and for all materials. While water absorption probably
counteracted the effect of dimensional contraction for all measurements,
it only resulted in a positive value for
cylinders A/D at the immediate time
point when VPES replicated the metal
model accurately.
It is interesting to note that the
cylinder diameter measurements resulted in larger percentage dimensional change values than those of
the anteroposterior and cross-arch
measurements (Figs. 3-6). More specifically, the smaller cylinders (B and
C) with a diameter of approximately
6.35 mm had the highest percentage
dimensional changes. Considering
that polymerization shrinkage affected all parts of the impression equally,
the removal of the metal block could
have caused extra plastic deformation
at the 4 cylinders. As a result, the cylinders, which have small dimensions
showed greater percentage changes
in comparison to the larger measurements. Wadhwani et al16 and Stober
et al22 explained that polymerization
shrinkage in the buccolingual dimension could be exaggerated because of
the use of tray adhesive and the rigid
tray retention. This makes sense in
this investigation since the cylinder diameter was measured buccolingually
in the same manner for all samples.
Another interesting aspect is related to PE, and hence the PE component of VPES. Lawson et al23 showed
that a hybrid material similar to VPES
experienced the least elastic recovery
compared to 5 VPS materials, possibly due to the incorporation of PE,
which was shown to produce lower
elastic recovery.24 Considering these
findings, the graphs in this study show
clearly that the percentage dimensional change decreased with time for
VPS but not for PE or VPES.
For immediate pour casts, VPES
was the most accurate (Fig. 3). However, although the percent dimension-
178
CONCLUSION
Within the limitations of this study
EXAlence 370 monophase impression material demonstrated comparable dimensional stability to the tested VPS and PE materials, and despite
the statistically significant differences
in the dimensions of some of the
cast measurements, its dimensional
changes were minor. Because of the
increased dimensional changes and
the related standard deviation for the
smaller cylinders at the 2-week pour
time, earlier pouring of the impressions should be encouraged whenever
possible.
REFERENCES
1. Corso M, Abanomy A, Di Canzio J,
Zurakowski D, Morgano SM. The effect of
temperature changes on the dimensional
stability of polyvinyl siloxane and polyether
impression materials. J Prosthet Dent
1998;79:626-31.
2. Seyedan K, Sazegara H, Kalalipour M, Alavi
K. Dimensional accuracy of polyether and
poly vinyl siloxane materials for different
implant impression technique. J Applied
Sciences 2008;3:257-63.
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