Yeo Yit Juan

STK 1213 Analytical Chemistry

Assignment 1

1. Quality assurance (QA) is the steps taken during analysis to ensure that the analysis is
under control and that it is properly monitored. One of the most important aspects of QA
is quality control (QC). QC includes specific formal goals (called data quality objectives,
or DQOs), collection of data to assess data quality, and the remedial measures taken
whenever the DQOs are not realized.

2.

a. NH4NO3
b. 2CH3NH2 +

N2O + 2H2O
9
2CO2 + 5H2O + N2
2 O2

c. Cr(OH)3 + 3HClO4
Cr(ClO4)3 + 3H2O
d. CaC2 + 2H2O
Ca(OH)2 + C2H2
e. 2KClO3
2KCl + 3O2

3. Number of mole of FeSO4 =

=

Mass of FeSO 4
Molar mass of FeSO 4
26 g
151.9 g/mol

= 0.1712 mol
Volume of FeSO4 =

Mass of water
Density of water
100 g
1.095 g/ mol

= 109.5 mL
Molarity of FeSO4 =

Number of mole of FeSO 4

Volume of FeSO 4

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0.1712mol
0.1095 L

= 1.5635 mol/ L

4.

B2H6(g) + 3O2(g) 2HBO2(g) + 2H2O(l)

Number of mole of B2H6 =
=

Mass of B 2 H 6
Molar mass of B 2 H 6
2.37 g
27.6 g /mol

= 0.0859 mol
Since 1 mole of B2H6 will produce 2 mole of H2O;
So 0.0859 mol of B2H6 will produce 0.1718 mole of H2O.
Molar mass of H2O= 18 g/mol
Mass of H2O = Number of mole of H2O Molar mass of H2O
= 0.1718 mole 18 g/mol
= 3.0924 g

Mass of piperazine
5. Number of mole of piperazine = Molar mass of piperazine
=

0.05002 g
86.136 g /mol

= 5.807 10-4 mol

Percentage of piperazine = Number of mole of piperazine

-4

= 5.807 10 mol

71.29
100

71.25
100

= 4.140 10-4 %
Mass of piperazine diacetate = Percentage of piperazine Molar mass of piperazine
diacetate

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= 4.140 10-4 % 206.240g/mol
= 0.0854g