Professional Documents
Culture Documents
Operating
Manual
User Guide
VERSION 1.0.
Revision 1.0
June 14
2014 by VINCI Technologies, Inc. All rights reserved.
No part of this publication may be reproduced or used in any form, or by any
mechanical or electrical means, without permission in writing from manufacturer.
ii
At the same time, it is the customers responsibility to allow or not allow that:
Operators,
Technical staff (electrician, chemist...),
Employees,
Non employees (visitors and contract personnel)
Room maintenance staff, etc
Or other people to approach the equipment during operation. As the same way the
customer management is responsible of the authorized working staff.
The equipment, documentation and software are protected under applicable copyright
laws and international treaty provisions.
No part of this manual can be reproduced prior to written permission granted by for the
exact context in which a reference to Vinci Technologies intellectual property is made.
Important: This operating manual is not an exhaustive manual. It has been prepared for
use by trained and experienced operators. Any doubt must be resolved before performing
a test or maintenance. Contact manufacturer if necessary.
iii
TABLE OF CONTENT
1.
INTRODUCTION ......................................................................................................................................... 1
1.1. SYSTEM OVERVIEW ................................................................................................................................................. 1
1.2. INJECTION PUMPS (BENCHTOP DUAL PUMPS S BTDPS 100-10).............................................................................. 1
1.3. ACCUMULATORS ...................................................................................................................................................... 2
1.4. CONFINING SYSTEMS (BTDPS 250 MODULE 1) ....................................................................................................... 2
1.5. HYDROSTATIC CORE HOLDERS ................................................................................................................................ 2
1.6. VISUAL CELL / HPHT SEPARATOR .......................................................................................................................... 3
1.7. HEATING SYSTEMS .................................................................................................................................................. 3
1.8. BACK PRESSURE REGULATOR .................................................................................................................................. 4
1.9. BACK PRESSURE PUMP (BTDPS 250 MODULE 2) .................................................................................................... 4
1.10. WET GAS METER ................................................................................................................................................... 4
1.11. PRESSURE TRANSDUCERS ...................................................................................................................................... 4
1.12. DIFFERENTIAL PRESSURE TRANSDUCERS .............................................................................................................. 5
1.13. ELECTRICAL CONNECTIONS ................................................................................................................................... 5
2.
3.
INSTALLATION ........................................................................................................................................ 16
3.1. UTILITY AND FLOOR SPACE REQUIREMENTS ......................................................................................................... 16
3.2. LOCATION OF THE EQUIPMENT .............................................................................................................................. 16
3.3. INSTALLING THE SYSTEM COMPONENTS ................................................................................................................ 17
3.3.1. The Core Holders...................................................................................................................................... 17
3.3.2. The Accumulators ..................................................................................................................................... 17
3.3.3. The BPR .................................................................................................................................................... 17
3.4. TURNING THE SYSTEM ON ..................................................................................................................................... 18
4.
5.
iv
5.5.3.1.
5.5.3.2.
6.
7.
8.
9.
10.
12.
MANUALS ................................................................................................................................................... 72
vi
TABLE OF FIGURES
FIGURE 1: EXAMPLE OF SLEEVE WITH PRESSURE TAPS ........................................................................................................ 2
FIGURE 2: PID OF THE AUTOFLOOD 700 ............................................................................................................................ 19
FIGURE 3: ILLUSTRATION OF KLINKENBERG EFFECT ......................................................................................................... 27
FIGURE 4: SUMMARY OF EXPERIMENTS CARRIED OUT IN ORDER TO GET RELATIVE PERMEABILITY OF OIL AND BRINE ...... 29
FIGURE 5: A TYPICAL OIL-WATER RELATIVE PERMEABILITY CURVE ................................................................................ 30
FIGURE 6: TYPICAL GAS-LIQUID RELATIVE PERMEABILITY CURVE ................................................................................... 31
FIGURE 7: CLEANING PROCEDURE FOR THE DPT LINE ...................................................................................................... 38
FIGURE 8: FILLING DPT LINE STEP 1 ................................................................................................................................. 39
FIGURE 9: FILLING DPT LINE STEP 2-3 .............................................................................................................................. 40
FIGURE 10: APPLILAB SOFTWARE MAIN WINDOW ............................................................................................................. 56
FIGURE 11: SAMPLE AND FLUIDS INFORMATION ............................................................................................................... 59
FIGURE 12: KMONO WINDOW ........................................................................................................................................... 60
FIGURE 13: TEMPLATE KMONO ......................................................................................................................................... 61
FIGURE 14: DELTAP SELECTION ........................................................................................................................................ 62
FIGURE 15: ACCUMULATOR SELECTION FOR KMONO CALCULATION ................................................................................. 62
FIGURE 16: EXAMPLE OF DELTAP VS Q LINE ..................................................................................................................... 62
FIGURE 17: PICTURE OF THE PRESSURE TRANSDUCER....................................................................................................... 65
FIGURE 18: PICTURE OF THE PINS OF THE TRANSDUCER..................................................................................................... 65
FIGURE 19: PICTURE OF THE INSIDE OF THE HEAD OF THE TRANSDUCER............................................................................ 65
vii
1. Introduction
1.1. System Overview
The Autoflood 700 Sytem is designed to perform tests on core plug samples to aid the
reservoir engineer in determining effective permeability to oil ahead of the flood front,
residual oil content after water flood, and the effective permeability to water behind the
flood front. These data are used with permeability distribution and injection pattern
efficiency to make predictions of reservoir performance.
Some of the tests available with the system include specific liquid permeability, effective
permeability, and relative permeability that involve flowing fluids that are compatible with
the materials of construction. Confining and pore pressure can be up to 700 bars or
10,000 psi maximum. Temperature can be up to 150C or 300F maximum. Note,
however, that the confining pressure must be at least 35 bars or 500 psi higher
than the pore pressure all the time to be able to seal the rubber sleeve around the
core sample. The pore pressure is measured at inlet and outlet ports of the core
sample by using relative and differential pressure transducers. Pressure taps (optional)
may be used to monitor the pressure along the core thanks to differential pressure
transducers. Likewise, the confining pressure is measured with a pressure transducer.
All wetted components are of Stainless Steel 316, Hastelloy C-276 or Titanium TA6V for
chemical compatibility and corrosion resistance.
The pressure control system including oven, pumps, valves, core holder, and
transducers are mounted on specific cabinets. Operation of the system is controlled
through an IBM-compatible computer. The software included with the system is
designed to allow for automated data acquisition and some basic calculations. The
TM
software operates under the Microsoft Windows 8 operating system for multitasking
capability. This gives the user maximum versatility in performing tests. Each of the key
components is discussed in later sections of this manual.
1/72
1.3. Accumulators
The accumulators supplied as part of the system allow you to maintain the test fluids at
reservoir condition during experiment. Accumulators are basically cylinders equipped
with two end plugs and one floating piston, which separates the cylinder into a driving
chamber and a test chamber. The driving chamber contains the driving fluids (water or
hydraulic oil) while the test chamber contains the test fluids. The cylinders are made of
Hastelloy C-276 (Stainless steel SS-316 or Titanium TA6V upon request) for chemical
compatibility and corrosion resistance.
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2. System Capabilities
2.1. Overall System
Max. Pore Press.:
Max. Conf. Press.:
Temp. Range:
Basic Procedures:
Multiple Fluids:
Wetted Material:
Electrical:
Measurement:
Resolution:
Dimensions:
Weight:
Electrical:
XU_SP 1365
150C (300F)
Microprocessor auto-tune Controller (Eurotherm 2416)
Built-in Temperature Limit Switch prevent over-heating
2 type P thermocouples (1 for control, 1 for limit)
0.1C
150 cm W x 120 cm D x 190 cm H
approx. 250 kg
230 VAC, 50/60 Hz, 1-Phase, 3,000 W
The oven is used to heat the core holder and associated parts. Within the oven, full access
to the core holder and valves is provided. A forced air fan and heater is used to heat the
system. A P-type thermocouple and Eurotherm digital temperature controller with a
proportioning solid state relay are used to control oven temperature. All control electronics
are located in the top section of the oven. These include an integral digital-display
microprocessor auto-tune controller for control of the test temperature and a separate
back-up temperature limit switch (see the dedicated manual).
6/72
Injection pump
Model No.:
Delivery Mode:
Max. Pressure:
Flow range:
Wetted Material:
Dimension:
Weight:
Electrical:
BTDPs100-10
Positive Displacement, Constant-Flow or Constant-Pressure
700 bars (10,000 psi)
0 to 50 ml/min (increment by 0.001 ml)
Stainless Steel 316
Panel PC Interfaced for local operation
Computer Interfaced to AppliLab software for remote control
25 cm W x 41 cm D x 76 cm H
43 kg
230 VAC, 50/60 Hz, 1 Phase, 1,000 W
The Injection System consists of an automatic pump BTDPs 100-10 equipped with a
fill/drain system. This is placed on a moveable trolley to provide easy access for
maintenance. Use the constant flow mode of the pump to continuously inject the driving
fluid through the accumulators (see the dedicated manual).
Note that the pump is injecting only silicon oil (or water if under high temperature) through
the accumulators. The supply reservoir is not included in the pump. Please use a glass
beaker or a reservoir made in a resistant plastic as Nalgene. Use a low viscosity, Silicon
oil (or light weight refined oil) in the supply reservoir.
The procedure used for filling and draining the driving fluid from the accumulators is
discussed in the operating procedure section of this manual.
The basic control functions of the injection pump are operated manually (from the local
Panel PC interface user) or automatically from the computer. Automatic valves are used to
isolate or drain the driving section of the accumulators.
A separate operator manual for the BTDPs100-10 pump is included with this manual.
Warning: refer to the BTDPs100-10 dedicated User Guide included with this manual for
descriptions of the available operational details and maintenance.
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2.3.2.
Model No.:
Delivery Mode:
Max. Pressure:
Flow range:
Wetted Material:
Dimension:
Weight:
Electrical:
BTSPs250
Constant-Flow or Constant-Pressure
700 bars (10,000 psi)
0 to 80 ml/min (increment by 0.001 ml)
Stainless Steel 316
Panel PC Interfaced for local operation
Computer Interfaced to AppliLab software for remote control
25 cm W x 41 cm D x 97 cm H
48.5 kg
230 VAC, 50/60 Hz, 1 Phase, 500 W
The BPR Pressurizing System consists of an automatic pump BTSP250 equipped with a
fluid fill/drain system and an inert gas circuitry. This is placed on the back side of the main
oven to provide easy access for maintenance. Note that the use of inert gas is
compulsory in order to have a smooth and precise pressure regulation of the BPR. If the
pressure of inert gas is not enough for the experiment condition, use the constant pressure
mode of the pump to build up the BPR pressure (see the dedicated manual).
The supply reservoir is not included in the pump. Please use a glass beaker or a reservoir
made in a resistant plastic as Nalgene. Use a low viscosity, Silicon oil (or light weight
refined oil) in the supply reservoir. This will allow you to fill about 10cc of oil in order to
protect the piston sealing from the high pressure gas.
The procedure used for filling and draining the inert gas from the BPR is discussed in the
operating procedure section of this manual.
The basic control functions of the BPR pressure pump are operated manually (from the
local Panel PC interface user) or automatically from the computer. Automatic valves are
used to isolate or drain the pressure section of the BPR.
A separate operator manual for the BTSP250 pump is included with this manual.
Warning: refer to the BTSP250 dedicated User Guide included with this manual for
descriptions of the available operational details and maintenance.
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2.3.3.
Model No.:
Delivery Mode:
Max. Pressure:
Flow range:
Wetted Material:
Dimension:
Weight:
Electrical:
BTSPs250
Constant-Flow or Constant-Pressure
700 bars (10,000 psi)
0 to 80 ml/min (increment by 0.001 ml)
Stainless Steel 316
Panel PC Interfaced for local operation
Computer Interfaced to AppliLab software for remote control
25 cm W x 41 cm D x 97 cm H
48.5 kg
230 VAC, 50/60 Hz, 1 Phase, 500 W
9/72
FPA 1000-10
700 bars (10,000 psi)
150C (300F)
C-276 Hastelloy
88 mm,
63 mm
615 mm
13.4 kg
2.6. Accessories
2.6.1.
HP/HT Separator
Model:
Fluid Ports:
Material:
Working Pressure:
Working Temp.:
Sapphire ID:
Sapphire OD:
Sapphire Length:
Visual Length:
Weight:
C-02-002-1
1/8 tube compression fitting
C-276 Hastelloy
10,000 psig
Ambient to 150C
2mm
20mm
70mm
45mm
20.0 kg
10/72
2.6.2.
Model:
Wetted Material:
Flowing Lines:
Pressure Rating:
Temp. Rating:
Dimension:
Weight:
2.6.3.
Vacuum Pump
Model No.:
Ultimate Pressure:
Nominal Pumping:
Oil Capacity:
Dimension:
Weight:
Electrical:
2.6.4.
C06-003-1
C-276 Hastelloy
1/8 outer diameter
700 bars (10,000 psi)
150C (300F)
7 cm Diameter x 14 cm Height
3 kg
2005SD
2x10-3 mbar
5.4 m3/h
0.83 L
42 cm L x 19 cm W x 24 cm H
25 kg
230 VAC, 50/60 Hz, 1 Phase, 500 W
Gas Meter
Model:
Drum Capacity:
Dial Capacity:
Min. Dial Division:
Hourly rate:
Accuracy:
Filling:
Dimension:
Weight:
Electrical:
DM3A
0.5 dm3
0.25 dm3 per rev.
0.005 dm3
50 dm3 (0.1 dm3 to 100 dm3)
< 0.25% of Full Scale
With a shaft encoder of 500 pts per rev.
about 1.2 L
23 cm W x 19 cm D x 24 cm H
3.5 kg
5 VDC
11/72
2.7. Instrumentation
2.7.1.
Pressure Transducers
Manufacturer:
Pressure Range:
Accuracy:
Electrical:
ESI
0 700 bars (0 10,000 psi)
0 7 bars (0 100 psi)
0 1 bar (0 15 psi)
0.25% of Full Scale
With 5-digit Digital Display
24 VCC
The pressure transducers supplied as part of the system are ESI gauge-pressure
transducers with digital displays with an accuracy of +/- 0.25% of full scale. The maximum
full-scale range is 700 bars (10,000 psi) at room temperature. For each system, one
monitors the CONFINING pressure, one monitors the INLET PORE pressure, one
monitors the OUTLET PORE pressure, one monitors the BPR pressure.
2.7.2.
Manufacturer:
Pressure Range:
Line Pressure:
Accuracy:
Electrical:
2.7.3.
Rosemount
+/- 2000 psi, +/-300 psi and +/-9 psi (other range on request)
700 bars (10,000 psi)
0.055% of Full Scale
With 5-digit Digital Display
24 VCC
Temperature Probes
Type:
Resolution:
Electrical:
The temperature probes supplied as part of the system are PT100 type with an accuracy
of +/- 0.1C. They have a full-scale range according to the oven specification. The
temperature probes monitor the core holders, and the oven.
.
12/72
2.7.4.
Temperature Controllers
Manufacturer:
Model:
Resolution:
Electrical:
Eurotherm
2416
5-digit Digital Display
0.1C
230 VAC
This controller is microprocessor based indicator, single loop controller, and profiler
capable of measuring, displaying or controlling process variables such as temperature,
pressure, flow and level from a variety of inputs. Control functions, alarm settings and
other parameters are easily entered through the front keypad or by using the PC based
configuration software. Controller models are easily tuned using the instruments automatic
tuning features. EEPROM technology protects against data or configuration loss during AC
power outages.
Inputs are user configurable for direct connection to thermocouple and RTD probes. Most
models will also accept linear process signal types such as mV DC, VDC or mA DC. If the
instrument is configured with a linear output option module, this output can be scaled to retransmit the process variable or set point to external devices such as data recorders or
PLC.s.
Alarm indication is standard on all instruments; up to three alarms are possible on some
models. The alarm types may be set as process high or low, deviation (active above or
below controller set point), band (active both above and below set point), or control loop
type. Models with a heater current input also have high, low or short circuit heater break
alarms based on control load current. These alarms can be linked to any suitable output.
Alarm status is indicated by an LED and the alarm status screen.
If the instrument is configured with the transmitter power supply option module, an
unregulated 24V DC (22mA) auxiliary output voltage is provided to power external signal
transmitters.
13/72
Flow Lines
The system provides flow lines as normally required for the performance of the system.
Wetted Material:
Flowing Lines:
Fittings:
Low Pressure Rating:
High Pressure Rating:
Temp. Rating:
The low pressure (white and clear plastic) tubing utilized in this system is Teflon made to
withstand the temperature inside the oven. Please do not use nylon or polyethylene tubing
as this may melt or become brittle and break after repeated use in a high temperature
environment. The maximum pressure rating is 10 bars or 145 psi at 150C.
High Pressure Tubing
The high pressure tubing utilized in the pore wetted portion of this system is manufactured
from Hastelloy C-276. The OD is 1/8 (3.18mm) and ID is 0.89mm. Quality assurance
certificates are available to order. The maximum pressure rating is 700 bars or 10,000 psi
at 150C.
2.8.2.
Hand Valves
The system provides hand valves as normally required for the performance of the system.
Wetted Material:
Flowing Lines:
Fittings:
Pressure Rating:
Temp. Rating:
These valves are manufactured by Butech and/or Swagelok. The wetted material of
construction is Stainless steel SS-316 (Hastelloy C-276 or Titanium TA6V upon request).
For more information about these valves, please refer to the Component Manual section at
the end of this manual.
The maximum pressure rating is 700 bars or 10,000 psi at 175C.
14/72
For additional information on any of the components used within the Core Flooding
System, please contact the engineering Department at Vinci Technologies.
15/72
3. Installation
3.1. Utility and Floor Space Requirements
Utility Requirements:
Main oven:
BTDPs100-10/250-10:
Air Supply pressure:
Room Requirements:
Main Oven:
Computer Stand:
Suggested Floor Space:
16/72
Install the core holder on its bracket. Then, bolt the two screws of the claw on the core
holder bracket assembly. Due to its heavy weight, it is not recommended to dismount the
core holder body from the frame.
To install a sample, undo the end closer as explained in this manual but do not dismount
the body. It is recommended to leave the body bolted on its support unless it is necessary
to clean it completely or to change the position to +/-90C.
Reconnect the plumbing (if needed). Be sure to tighten the tubing nuts snugly (do not over
tighten).
3.3.2.
The Accumulators
The piston accumulators have to be mounted in their sanded steel bracket assembly. Slide
the accumulator on the bottom bracket then, clamp the retaining plate in order to hold the
accumulator. The accumulators are equipped with their own handle but they are heavy, so
be careful when handling them.
Reconnect the plumbing (if needed). Be sure to tighten the tubing nuts snugly (do not over
tighten).
3.3.3.
The BPR
Bolt the BPR(s) on its support located under the main oven.
Reconnect the plumbing (if needed). Be sure to tighten the tubing nuts snugly (do not over
tighten).
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5. Theory of Operation
Relative permeability is mathematically defined as the effective permeability to one fluid
divided by a base permeability. The base permeability can be to any fluid of choice;
however, there are certain fluids and sample saturation conditions that are suggested
as the standard base permeability to use for particular relative permeability tests:
Laboratory water flood tests are designed to furnish the effective permeability to oil
ahead of the flood front, residual oil content after water flood, and the effective
permeability to water behind the flood front. These data are used with permeability
distribution and injection pattern efficiency to make predictions of reservoir performance.
Several tests may be run in the laboratory to furnish the required information. These
tests vary in complexity and ease of application from the Basic Flood through Water
Flood Susceptibility (WFS) to water-oil relative permeability (Kw/Ko) measurements.
Water flooding projects normally measure performance relating oil recovery to pore
volumes of injected water and to water-cut. These data are not developed in the Basic
Flood tests, and are reported only for the Water Flood Susceptibility measurements.
This performance data can also be calculated from the K w/Ko data. Basic flood tests can
also be run in addition to a Kw/Ko test as a quality control measure to compare with
Kw/Ko residual oil and to furnish an ultimate residual oil saturation. The RPS system
enables adequate data measurement capability for K w/Ko tests which in turn enable the
calculation of both the WFS and Basic data.
Pore geometry and wettability are two key factors that influence the relative permeability
of a core sample. In some high permeability rock, for example, the pore geometry can
make the relative permeability data appear to be that of an oil-wet rock when it is
actually water wet. If the sample wettability has been altered due to contamination with
surfactants during the coring process or if it is tested with contaminated reservoir fluids,
this can cause pessimistic oil wet characteristics.
Basic flood, Kw/Ko and WFS tests can be made under reservoir conditions of
temperature and pressure using live reservoir oil. This is an improvement over room
condition techniques where tests are made at atmospheric conditions with refined
laboratory oils. Use of the live crude exposes the rock to compounds present in the oil
that might influence wettability and establishes a plug environment as close as possible
to reservoir conditions.
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Flow rates can affect the final saturation values and relative permeability data as a result
of a situation called "capillary end effects". Capillary end effects are the result of a low
viscous to capillary ratio and they result in an excessively high saturation of the wetting
phase at the outlet end of the sample. This results is unrealistic residual oil saturations.
Therefore, special precautions should be taken in both the unsteady-state and steadystate procedures to reduce the possibility of capillary end effect problems. The unsteadystate relative permeability procedure should be undertaken on a sample as long as
possible and should be made at a high flow rate (between 1 and 5 ml/min for plug size
samples). The steady-state relative permeability procedure should also be made on a core
sample as long as possible and the core holder should have either Berea mixing heads or
Archimedes spiral heads to reduce or eliminate the capillary end effect problems within the
core sample itself.
Rock wettability is one of the most important factors concerning the characteristic behavior
of a relative permeability test. As mentioned above in the paragraph discussing saturation
history, there are certain situations and wettability conditions that will help select the most
representative test procedure. Another primary concern of any laboratory planning to
perform reservoir condition relative permeability tests is to obtain uncontaminated cores
and fluids with which to carry out the test procedure. Cores can be contaminated during
the coring procedure if any surface active agents are placed in the drilling mud. These
same surface active agents can also contaminate a fluid sample at the well site. Extreme
care must be observed in the selection and execution of the coring program and fluid
sampling techniques.
Rock pore geometry is also a very important factor concerning the characteristic behavior
of a relative permeability test. Several of the rock properties that will affect the pore
geometry are as follows:
Grain Size
Grain shape
Grain sorting
Grain packing
Grain solution
Grain overgrowths
Grain alteration
Pressure solution effects
Clay (Intergranular)
Clay or shale streaks
Detrital mineral pore fillers
Authigenic mineral pore fillers
22/72
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Monophasic Permeability
Monophasic permeability describes the ability of a single fluid or phase to flow or transmit
through a rock.
In 1856 Henry Darcy studying water injection through a column of sand, found a
relationship between the flow rate and the pressure gradient along the sample:
K P
A
L
Where:
Q is the flow rate in m3.s-1, K the permeability in m, the viscosity in Pa.s, P the
difference between inlet and outlet pressure in Pa, L the core length in m and A the cross
sectional area to flow in m.
24/72
Q
L
24.49593767
P
A
with Q the flow rate in cc/min, K the permeability in mD, the viscosity in cP, P the
difference between inlet and outlet pressure in psi, L the core length in mm and A the
cross sectional area to flow in cm.
Darcys law can be applied under the following assumptions:
The flow is horizontal, steady state and under the laminar regime.
The flow of fluid through the porous medium takes place under viscous regime (i.e.
the rate of flow is sufficiently low so that it is directly proportional to the pressure
differential or the hydraulic gradient).
The flowing fluid does not react with the porous medium because it may alter the
characteristics of the porous medium thereby changing its permeability as flow continues.
25/72
5.5.2.
Gas Permeability
Even though the experimental procedures for permeability measurement using liquids and
gases are basically similar, one major difference exists between liquids and gases in the
approach used for the determination of absolute permeability: the compressible nature of
gases. The original Darcy equation was indeed developed under the assumption of an
incompressible fluid flow.
According to Boyles law, if the temperature is constant:
Q1 P1 Q2 P2 Qavg Pavg
Equation 3: Boyles Law
The Darcy equation can then be expressed in terms of the average gas flow rate to
account for gas expansion in the sample:
Qavg
K ( P1 P2 )
A
With the MFC, the flow rate is reported to atmospheric pressure. Therefore, the previous
equations can be rearranged as:
Q2 P2
K ( P1 P2 )
A
L
P1 P2
2
Equation 5
or
K . A.( P1 P2 )
Q2
2..L.P2
2
Equation 6
Q2 2..L.P2
2
2
A.( P1 P2 )
where Q2 is the outlet flow rate in m3.s-1, K the permeability in m, the viscosity in Pa.s,
P1 the inlet pressure in Pa, P2 the outlet pressure in Pa, L the core length in m and A the
cross sectional area to flow in m.
As for the liquid permeability, a coefficient has to be applied for non S.I units:
24.49593767.
26/72
However, in 1941, Klinkenberg reported that the gas permeability is always higher than the
liquid permeability. His measurements showed a trend of increasing permeability as a
function of increasing reciprocal mean pressure when gas is used. This phenomenon is
due to the gas slippage: the gas does not adhere to the pore walls as liquid does, and the
slippage of gases along the pore walls gives rise to an apparent dependence of
permeability on pressure. This is called the Klinkenberg effect, and it is especially
important in low-permeable rocks.
The following graph represents the Klinkenberg effect for absolute permeability
measurement using gases.
k gas kliquid (1
b
Pmean
Where kgas is the measured gas permeability, Kliquid the equivalent liquid permeability or the
Klinkenberg corrected liquid permeability, b the slippage factor, Pmean the mean pressure.
27/72
5.5.3.
Relative Permeability
While absolute permeability refers to a single fluid, relative permeability is the ability of a
fluid to flow in the presence of another fluid. Relative permeability is helpful in determining
the ratios Kw/Ko, which is used to predict the performance of the reservoir.
The gas, oil and water relative permeabilities are normally denoted by K rg, Kro and Krw,
respectively. Relative permeabilities are usually expressed by the ratio of effective
permeability to absolute permeability. Effective permeability is a relative measure of the
conductance of the porous medium for one fluid phase when the medium is saturated with
multiple fluid phases, i.e. Ko, Kw or Kg. Absolute permeability can be expressed as
monophasic permeability or usually the effective oil permeability at irreducible water
saturation, i.e. Ko(@Swi). You can express relative permeability as follows:
Kro Ko / K
Equation 9: Expression of relative permeability of oil
where Kro is the relative permeability of oil, Ko is the permeability of oil and K=Ko(@Swi) is
the
absolute
permeabily.
The Unsteady State Method for relative permeability is based on the Buckley-Leverett two
phases flow model. (Refer to literature). This model can be applied under the following
assumptions:
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Figure 4: Summary of experiments carried out in order to get relative permeability of oil and brine
From the differential pressure, the flow rate and the cumulative production of injected and
displaced fluids, the model permits to calculate the relative permeability.
In this experiment, the second step is called Drainage and the third one Imbibition.
29/72
5.5.3.1.
At the initial or irreducible water saturation, the oil relative permeability, K ro, always equals
1 if the base permeability used is the effective permeability to oil at S wi. At this point, Krw is
always equal to 0 because water is immobile.
At residual oil saturation Sor, the oil relative permeability, Kro, always equals 0 because the
oil phase is immobile. However, at this saturation water relative permeability is at its
maximum value because water is the only phase that is mobile.
In order to get more details on how to generate these plots, one should read the Operating
Manual of KrLab.
30/72
5.5.3.2.
At 100% liquid saturation, i.e. the irreversible liquid saturation of the sample SL,ir, the oil
relative permeability, Kro, always equals 1 if the base permeability used is the effective
permeability of oil at Swi. At this point, Krg is always equal to 0 because gas is immobile.
At the residual liquid-phase saturation, the oil relative permeability, Kro, always equals 0
because the liquid phase is immobile. However, at this saturation, the gas relative
permeability is at its maximum value because gas is the only phase that is mobile.
Once again, for more detailed information on the method used to get these plots, one
should refer to the Operating Manual of KrLab.
31/72
6.2.1.
1.
Slide the end closer into the nut, then place the anti-friction washer and install the
retainer ring (see the Parts List for help).
2.
Clean the end closer assembly, the end piece and the 1/4" tubing with solvents
and/or distilled water and then blow air through it to remove any residual fluid and
dirt.
3.
Bolt the 1/4 tubing on the end piece by using the specific 1/4 HP fitting (gland and
left thread collar). You may hold the end piece in a wise to properly tight the gland.
4.
Choose a sleeve according to the diameter and/or length of the core sample to be
loaded. Inspect the sleeve and replace if it is obviously cracked and/or deformed.
5.
Inspect all O-Rings and replace it if the O-Rings are obviously worn, torn or are
brittle. Replace all O-Rings that have been exposed to elevated temperatures
(greater than 150C) for more than 24 hours. Always use 75 (or greater) Shore A
Viton O-Ring seals.
6.
Attach the body on its support. The core holder is now ready to be assembled with
a sample.
32/72
6.2.2.
1.
Slide the end closer into the nut then, install the retainer ring (see the Parts List for
help).
2.
Clean the end closer assembly and the body with solvents and/or distilled water and
then blow air through it to remove any residual fluid and dirt.
3.
Inspect all O-Rings and replace it if the O-Rings are obviously worn, torn or are
brittle. Replace all O-Rings that have been exposed to elevated temperatures
(greater than 150C) for more than 24 hours. Always use 75 (or greater) Shore A
Viton O-Ring seals.
4.
Reassemble the accumulators and replace them in their frames. Do not reconnect
the tubing until it has been cleaned.
6.2.3.
1.
Clean the end plug, the piston and the body with solvents and/or distilled water and
then blow air through it to remove any residual fluid and dirt. Particularly, be sure
that the inlet and outlet holes of the body are clean.
2.
Bolt the needle to the piston by using a 5.5mm (7/32) socket wrench. Do not over
tighten.
3.
Clean the sealing washer and inspect it carefully. Replace it if the washer is cracked
and/or the hole is out of specification (diameter greater than 1mm). Install it properly
(see the Parts List for help).
4.
Inspect all O-Rings and replace it if the O-Rings are obviously worn, torn or are
brittle. Replace all O-Rings that have been exposed to elevated temperatures
(greater than 150C) for more than 24 hours. Always use 75 (or greater) Shore A
Viton O-Ring seals.
5.
Reassemble the BPR in that order: piston, end plug and nut. Then, attach it to its
support. Do not reconnect the tubing until it has been cleaned.
6.2.4.
It is recommended to use silicon oil to load the core holder. If silicon oil is not available,
use only oil that can resist to high temperature without smoke and/or explosion in case of
leakage.
Warning:
IF A NEW LIQUID IS TO BE USED IN THE UPCOMING TEST, CLEAN THE PUMPS SUPPLY
RESERVOIR, TUBING AND CYLINDERS FIRST!! It is extremely important that the pump reservoir
is clean and dry prior to filling them with the silicon oil for the upcoming test. If the oil is the
same as was used in the previous test no special cleaning is necessary.
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6.2.5.
Flow solvents and/or distilled water through all flow tubing and valves to clean any
unwanted oil and/or brine from the tubing and valves then, air dry it.
Do not forget to refill the instrumentation piping and the sensors with silicon oil or low
viscosity oil in order to protect it from corrosive fluids. It will also avoid any blockage in the
piping than could occur with crude oil for example.
6.2.6.
2.
3.
4.
Stop the pump when the first drop in flowing out of the line.
5.
Usually, dead volumes are measured at the factory before shipment. However, it is
recommended to check the dead volume again, particularly if tubing or fitting have been
moved, replaced or modified.
Please use the following table to calculate the dead volumes:
Core holder 1
Section
Inlet line
Outlet line
Inlet end closer
End piece + fitting
1/4" HP tubing
Volume (cc/mm)
0.002
0.002
N/A
N/A
0.005
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Length (mm)
Total (cc)
N/A
N/A
100
0.3
0.5
7. Test Procedures
The operation of the system is briefly discussed below. Detailed procedures should be
determined by the user depending on their specific needs and desires.
If live or recombined fluids are to be used, special procedures must be followed after
loading the core sample into the system. Special equipment is also required to charge the
system with live fluids at the required pressures. For more information concerning test
procedures using live fluids, please contact Vinci-Technologies. The following section
describes test procedures using non-pressurized fluids with no gas in solution.
Caution: THE
OPERATOR SHOULD BECOME FAMILIAR WITH THE ENTIRE SYSTEM TO OPERATE THE
EQUIPMENT SAFELY AND EFFECTIVELY.
High-pressure Caution:
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Know the sample dimensions (will the sample fit in the core holder?).
Have at least 500cc (1 liter is recommended) of the liquid to flow through the sample
during the test procedure.
Know the flowing liquid viscosity (cP) at ambient and test temperatures.
Know the pore pressure (psi) required for the test procedure.
Know the effective confining stress (psi) required for the test procedure.
Know the desired flow rate (cc/min) to use during the test procedure.
Know the liquid content (cc or % pore space) in the sample pore space.
If 2 liquids are present, know the initial liquid saturation (%) of pore space.
Insure that all upstream and downstream flow lines are clean and dry.
Insure that the BPR has been rebuilt and is ready for service.
Insure that the accumulators are cleaned and filled with the correct liquid (if used).
Insure the core holder is cleaned, rebuilt and ready to load a core sample.
Store the core sample under the last fluid flowed through the sample until it is ready to
load into the confining sleeve.
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7.2.1.
1.
2.
Have the core holder disassembled with the inlet assembly, downstream end piece,
core sleeve, tubing, nuts and ferrules easily accessible and clean.
Measure the sample weight before loading and record the value. Be sure to wipe
excess liquid off the surface of the sample without wiping liquid out of the pores on
the surface of the rock before weighing it.
Note: normally a core sample is pre-prepared in a separate system before it is loaded into
the Autoflood-700 system. It is recommended that the core is saturated and flushed
outside of the system.
3.
4.
5.
6.
7.
8.
Warning: avoid any gap between the core and the end piece. The gap could occur if the
floating end piece is not pushed in all the way or if the core sample has not square end
faces. Upon pressurizing, a gap will cause the sleeve to extrude and rupture.
9. Connect the confining pressure tubing to the confining port.
10. If present, connect all tubing between the DPTs and the pressure taps ports on the
core holder according to the following drawing (not applicable here).
11. The sample is now loaded into the core holder body and locked in place. Insure that
the temperature probe is in place in the core holder (downstream side).
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7.2.2.
The pressure transducers measure the pressure of the test fluids, which may be corrosive
fluids. In order to avoid any damages to those transducers, the transducers lines must be
filled with silicon (or refined) oil prior to start an experiment. The oil will act as a buffer to
protect the transducers against the corrosive fluids without affecting the pressure
measurement. All transducers are bolted in the instrumentation panel located on the back
side of the main.
Note that all transducers lines are factory filled with silicon (or refined) oil. However, after
replacing any of the transducers lines or the transducers themselves, you may need to
refill the lines with silicon (or refined) oil.
It is not necessary to prime the sensors every time you make a test, particularly if no lines
have been disconnected. However, it is recommended to clean and prime the lines and
sensors every 10 tests. In that case, please follow the procedures described below:
Cleaning Procedure:
1.
Close the 2nd inlet of HV04
and HV12 (connected to the
coreholder)
2.
Connect a vaccum pump to
rd
the 3 inlet of HV04 and open the
3rd inlet of HV12 and open these
valves.
3.
Open the automatic valves
AV11, AV12, AV13, AV14, AV15,
AV16, and AV23.
4.
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Filling Procedure:
1.
First, You need to vacuum the line. Close the 2nd inlet of HV04, which is going to
the coreholder inlet. Connect a vacuum pump to the 3rd port of HV04 that is not
connected. Use a trap full of silicon oil in order to be able to break the vacuum and
fill it with the silicon oil. Open AV11, AV12, AV13, AV14, AV15, AV16 and AV23.
Close all the inlets of HV12. Vacuum the system for at least 30min.
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2.
Break vacuum by disconnecting the hose from the vacuum pump. Oil will fill the
system.
3.
Connect your hand pump to the trap. Inject silicon oil until pressure is increasing for
PT and the different DPTs. Be very careful when filling, it is easy to reach 9psi with
a hand pump, it could damage the deltaP. Make sure that the inlet that goes to the
coreholder of HV04 is closed and that both ways of HV12 are closed.
4.
Your system is now filled with silicon oil. Depending on the type of experiment, it is
possible to open the inlets of HV04 and HV12 in order to fill the lines connected to
the coreholder.
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7.2.3.
1.
Check the liquid level in the pump reservoir. Add additional liquid as required to fill
it. Use only high temperature silicon oil (or suitable refined oil) or water (if no high
Temperature). Check the connections to the core holder to make sure that all
connections are tight. Only pressurize the core holder if a core sample is properly
installed.
2.
Remove the plug located on the top of the core holder. This will allow the air to be
purged from the core holder.
3.
Run the confining pump until some silicon (or refined) oil flows out of the core
holder. You may also use vacuum pump or pour directly the confining oil in the core
holder by using a funnel or use a transfer vessel (option).
4.
Put back the plug located on the top of the core holder and tight it correctly. Run the
pump to pressurize to 1000 psi at first.
Warning: if core holder temperature is increased during or after setting the confining
pressure, the core holder confining pressure will increase, due to thermal expansion of the
fluid. You must carefully monitor this pressure as the core holder heats. Be sure that the
pump is not full to insure pressure regulation.
7.2.4.
You may fill the accumulators by removing the top end closer and pour directly the fluid
into. You may also use a transfer vessel (option) to fill the accumulators as described here:
1.
Open the refilling valve of the accumulator and connect a tubing to recover any
fluids that might come out of the accumulator.
2.
Move the piston of the accumulator up by pressurizing the driving chamber with
compressed air (3bar is usually enough).
3.
Fill the transfer bottle with process fluid. Connect a TeflonTM tube between the valve
of the transfer vessel and the refilling valve of the accumulator.
4.
Fill the accumulator by pressurizing the transfer bottle though the compressed air
regulator (3bar is usually enough). You might have to increase the air pressure
depending on the viscosity of the process fluid.
41/72
7.2.5.
Run the injection pump in order to have the half of each cylinder free of liquid.
2.
Vacuum the injection pump, tubing and driving chamber of the accumulators
through the tank valves of the injection pump. Do not forget to open the process
valves of the injection pump as well. Wait under vacuum for at least 15min.
3.
Close the tank valves, stop the vacuum and reconnect the tank valves to silicon oil
reservoir.
4.
Open the tank valves and wait until the level of oil in the reservoir is stable, which
means that no more oil is entering in the system.
5.
Open the refilling valve of the accumulators and run the injection pump to purge the
process chamber of the accumulators. It is recommended to purge the
accumulators one by one. Inject 50cc minimum into each accumulator.
6.
Purge the tubing all the way between accumulators and the core holder inlet(s).
Warning: the core sample must be loaded into the core holder and the initial confining of
at least 1000 psi must be placed on the core holder prior to vacuum filling any tubing that
connects to the core sample pore system.
Warning: always purge the process chambers of the accumulators by running the injection
pump. If the accumulators are not correctly purged, you may inject air in the system.
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7.2.6.
The injection pump will be used to create pressure in the pore system. Determine what
liquid is the flowing liquid in the core sample and use the pump and accumulator system
with that fluid in it. Open the appropriate valves to connect the correct flow system to the
core sample.
Warning: it is imperative to set all the differential pressure transducers in the SAFETY or
BYPASS position to avoid any damages to them during pore pressurization. Failure to do
this could result in sensors damaging.
The following procedure is described assuming the core sample is 100% saturated with
brine:
1.
Upon raising the confining pressure on the core sample to 1000 psi, insuring that
there are no leaks, vacuum filling and connecting the flow tubing, effluent tubing
and pressure ports to the core holder the pore system can be pressurized.
2.
Using the brine accumulator, run the injection pump at 5cc/min (less or more,
depending on the permeability of the sample) and begin flowing into the core
sample.
3.
Set the BPR to 100 psi initially. Monitor the pump pressure, the upstream and the
downstream pressure while also inspecting for any leaks in the system. The pump
and upstream pressures should remain very close throughout the test procedure.
4.
When the downstream pressure raises to the BPR set pressure and the BPR allows
liquid to flow, that is the time to raise the confining pressure and BPR pressure to
the required pressures.
5.
Check for leaks in the system and fix any found. Upon fixing all leaks the system is
ready to apply heat.
Warning: it is imperative that the confining pressure is always maintained at least 35 bars
(500 psi) above the pore pressure. Failure to do this could result in failure and core sample
contamination.
43/72
7.2.7.
Upon filling and pressurizing the system and fixing any leaks, the operator should set the
temperature of the main oven. Upon doing so the follow steps should be followed:
1.
Set the temperature to the temperature to be used in the upcoming test. To raise the
set temperature, press the up arrow button on the controller. To lower the set point,
press the down arrow button. The temperature controller may display the actual
temperature or the set point (see dedicated manual of temperature controller for
more details). You may also set the temperature remotely from the computer.
Warning: during temperature increase, one should continuously monitor the confining
pressure and pore pressure of the system, even if pressures are automatically controlled.
If the confining pressure ever becomes less than the pore pressure, the core end piece
could be expelled from the core sleeve and the confining fluid could contaminate the core
sample. This would require starting the test over again with another sample.
2.
Monitor the temperature inside the core holder on the computer screen. When the
core holder temperature reaches the preset temperature (within 5 degrees), wait for
an additional 2 hours or more before starting the test.
Note: as the main oven heats up, the liquid and gas in the system will expand. This
expanded volume in the pore system will exit from the BPR at the set point pressure. This
is normal but inspect for leaks frequently.
Remember: the temperature stability will always take a few hours, depending on the
temperature set point and the weight to be heated. Even if pressures are automatically
controlled, it is highly recommended to watch the system during temperature increasing or
decreasing. Never start raising the temperature when leaving the system without watching.
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Note: This procedure assumes that the sample has been saturated with brine outside of
the system before the core sample is loaded into the system.
Set several Flow rates based on the air permeability data measured outside of the
system. The basic things to remember are to attempt to flow between 1 and 5 cc per
minute if the differential pressure required to develop this flow rate is not above the high
differential pressure transducer range. Set the other parameters based on the general
information in the previous section.
Be sure to flow enough brine through the core sample (usually 10 to 20 pore volumes) to
determine the brine permeability.
7.3.2.
Set the Flow rate based on the data measured during the brine permeability
determination. The final oil permeability measured at residual brine saturation will help
determine the rate to perform the water flood. The basic things to remember are to attempt
to flow between 1 and 5 cc per minute if the differential pressure required to develop this
flow rate is not above the high differential pressure transducer range. Set the other
parameters based on the general information in the previous section.
After the Oil Flood procedure has ended, it is standard procedure to flow enough oil
through the core to determine the oil permeability.
Warning: it is important to remember to isolate the crude oil accumulator if live crude oil is
used. Closing the accumulator valves promptly after the test will help insure that the live oil
pressure will remain above the bubble point of the oil enabling the remaining volume of oil
to be used in any forthcoming tests.
45/72
7.3.3.
This requires that several factors are known about the core sample to be tested and the
fluids that will be used to test the core sample. During the sample preparation procedure
an effective permeability to kerosene (dead oil) is measured as the final step. Knowing this
permeability value, the viscosity of the kerosene at ambient temperature and the viscosity
of the crude oil and brine at test temperatures will enable the user to calculate the
expected differential pressure ranges that may be encountered during the relative
permeability test.
The differential pressure transducer ranges should be calculated based on two criteria (i)
viscosity ratio between sample preparation effective permeability and the viscosity of the
crude oil at test temperature and (ii) Scaling Coefficient as described in a paper by
Rapoport and Leas in an AIME paper published in 1953.
a. First, the ratio of oil viscosities used in the sample preparation Ko and the reservoir
condition test will be used to calculate the differential pressure expected during the crude
oil flush and aging process. The equation for this calculation is as follows:
Reservoir_Oil_Viscos ity
46/72
The calculation of this optimum flow rate is based on a "Scaling Coefficient" equation
proposed by Rapoport and Leas must be utilized. The basic form of the equation is as
follows:
Scaling _ Coefficien t
Flow _ Rate
47/72
At the end of the test procedures, the operator should set the temperature of the
oven to 0C to stop the heating.
Warning: the pore and confining pressure will lower as the temperature lowers. The
operator should continuously monitor these pressures to insure that the confining pressure
never drops below the pore pressure during cool down.
2.
Allow the components to cool the room temperature or at least to a temperature that
will not cause any burns when touched.
3.
Upon reaching a cooled state, the backpressure can be lowered followed by the
confining pressure.
Warning: it is imperative that the confining pressure is always maintained at least 35 bars
(500 psi) above the pore pressure. Failure to do this could result in failure and core sample
contamination.
After the test is completed and the temperature is lowered, the operator should lower
the backpressure to zero followed by lowering the confining pressure to zero. It is
best to do this in no more than 100 psi increments.
Warning: if live oil is used, insure that the oil piston accumulator automatic isolation valves
are closed at top and bottom insuring that the oil pressure remains above its bubble point.
Warning: check the level of the liquid in the confining pressure supply reservoir. The liquid
level should not be higher than about 1 cm below the reservoir cap of the pump. If too
much liquid is in the container, it may overflow when liquid is being drained from the core
holder.
2.
After lowering the confining pressure to zero, place a beaker under the lower plug of
the core holder. Then, open the upper plug of the core holder. The core holder will
now begin draining back into the beaker.
Alternative way for drainage: you may also use compressed air to help draining the core
holder. In that case, listen to the sound at the supply reservoir. When air is heard gurgling
into the container, close confining isolation valve. The core holder is now drained of oil in
the confining annulus. It may be advantageous to wait approximately 15 to 30 minutes and
reopen the confining isolation valve to remove any excess oil that may drain off the interior
surfaces with time. After the final draining, close the confining inlet valve and allow the
core holder to vent to atmospheric pressure. This will be verified when no gurgling is heard
at the supply reservoir.
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3.
4.
Disconnect the connector 1/4 MP - 1/8LP and remove the brass nut on the 1/4
tubing.
5.
Check that the anti-friction washer and the external ring are correctly in place, then
remove the retaining nut. Slide the assembly out of the core holder body. Be sure to
push up on the 1/4" tubing while sliding the assembly out of the body. Have a
container or at least a rag under the opening at the end of the core holder to catch
any excess confining oil that is still in the annulus.
After a high temperature test, the sleeve will sometimes mold to the end piece and core
sample making it difficult to slide them out of the sleeve. If this happens, use compressed
air (no more pressure than 15 psi) to help removing everything from the sleeve. If it does
not work, it may be necessary to cut the sleeve off the head with a sharp knife by making a
cut along the length of the sleeve and prying the sleeve away from the end pieces and
core sample. In that case, a new sleeve is needed for a new test.
Upon removing the core sample from the sleeve, immediately wrap it in saran plastic wrap
and foil for short term storage.
The system is now ready for cleaning and rebuilding as described in previous sections.
49/72
8. Data Calculations
Relative Permeability (fraction and ratio) data must be calculated from the data collected
during the test. This can be performed manually or using the supplied calculation program.
A brief history with definitions, introduction to the use of Formation Volume Factors, and
both relative permeability calculation methods are discussed in this section.
Where:
K (h2 h1 )
L
This relationship soon evolved into what became known as Darcy's Law. When the terms
are expressed in suitable units the equation for liquid flow becomes:
( K )( A)( P)
( )( L)(14700)
or
(14700)( )(Q )( L)
( A)( P)
50/72
When one fluid is injected into a sample to displace a fluid with which it is immiscible, the
displacement does not occur in a piston-like manner. The displacing fluid will finger into
the displaced fluid, so that you do not have a solid bank of one fluid followed by a solid
bank of another fluid. The amount of fingering will depend on various factors, primarily the
viscosity ratio of the two fluids and the homogeneity of the sample.
Since this fingering takes place, there is a continually changing saturation profile and we
don't know what the saturation condition is at any point. We also have two fluids flowing
whose rate ratio is changing continually; therefore we cannot determine the specific
permeability directly. We need some form of expression, which will relate the
instantaneous rates of flow and thus, the permeability of each flowing phase to the
saturation of the sample at some point in the sample. The fractional flow of oil is a number,
which can be determined from oil and water production data. Buckley and Leverett took
Darcy's Law and came up with an expression, which related fractional flow to relative
permeability ratio.
Considering a water-oil relative permeability test with oil and water production,
(ko)( A)(P)
qo
( o)( L)14700
fo
(
ko
)(
A
)(
P)
(kw)( A)(P)
qo qw
o w
fo
1
kw o
1
ko w
Where:
fo =
ko =
o =
kw =
w =
51/72
Henry Welge in his paper "A Simplified Method for Computing Oil Recovery by Gas or
Water-Drive" used this relationship and developed mathematically an expression for
determining the instantaneous fraction of oil flowing at the outflow face of a sample. This
relationship is:
fo
dSav
dWi
Where:
Sav = the average saturation of the sample
Wi = the total amount of fluid injected, expressed in the same units
(pore volumes commonly)
This is a calculus expression, but if you are not familiar with it don't let it frighten you. The
equation can be solved graphically by determining the slope of the tangent to a curve. The
instantaneous slope of a curve at any point is equal to the slope of the tangent to the curve
at that point. Mathematically the instantaneous slope is as follows:
dS av
dWi
Using fo and the fractional flow equation, we calculate kw/ko as follows:
fo
1
kw o
1
ko w
ko o
( f o )
w
To obtain the saturation at the outflow face of the core, Welge developed the following
relationship:
52/72
8.2.2.
Johnson, Bossler and Naumann, in their paper "Calculation of Relative Permeability from
Displacement Experiments", reported the development of a procedure for calculating the
individual relative permeability curves. In their derivation, they extended the theory
developed by Welge. Two conditions are assumed, which must be achieved before this
method is applicable:
1)
2)
1
f
(Wi )( I r )
o
1
k ro
d
Wi
fo
1
d
(Wi)( Ir )
1
d
Wi
kro
This again should not frighten you because it simply involves the instantaneous slope of a
curve or the slope of the tangent to the curve (when measured graphically).
In order to calculate the intake capacity at various times during the test, we have to
determine instantaneous rates of flow for the oil stream
(
dVo
)
dT
dVw
)
dT
53/72
Simply make a plot of oil versus time and take the tangent at the times at which we
calculated kw/ko and outflow face saturation and in the same manner that we determined
fractional oil flow. Go through the same process of determining the slope to determine the
instantaneous rate for the water,
Then:
qo qw qt
The intake capacity is calculated from the base permeability and the test pressure using
Darcy's Law:
Qo
(ko)( A)(P)
( o )( L)14700
Then, qt divided by the intake capacity Q at the initiation of the flood is the relative
injectivity:
Ir
qo qw qt
Q
Q
1
kro
d
Wi
Again by plotting
1
versus
(Wi)( Ir )
1
, we can take slopes of the resultant curves to
Wi
1
(Wi )( Ir )
1
d
Wi
Since we have used the same time values for all of our calculations, the fraction curves,
ratio curve and saturations are related to each other.
Gas/oil unsteady-state relative permeability data is treated in the same manner as wateroil relative permeability data, except that gas volumes measured at the outflow pressure
must be converted to gas volumes at the mean pressure of the test.
54/72
for
Steady
State
2-Phase
Relative
The steady state process provides simultaneous flow of displacing and displaced fluids
through the core sample at a number of equilibrium ratios. At each ratio from 100%
displaced phased to 100 % displacing phase an equilibrium condition must be reached at
which the inflow ratio of fluids equals the outflow ratio and at which the pressure gradient
between the inlet and outlet is constant. At such condition the Darcy law equation is
applied to each phase to calculate effective permeability at the given steady state
saturation. Between five and ten stages are usually needed to establish relative
permeability curves.
In the steady state re-circulating flow mode, the fluids are injected through the core sample
using a re-circulating pumping system. The fluids produced from the core sample enter the
separator where they are separated and measured at reservoir conditions by a video
tracker. Then, they return back to the core holder inlet via the re-circulating pumping
system.
The test consists of saturating the core sample with one phase. The two phases are then
injected at different flow rate and the differential pressure along the core (delta P) is
recorded. The level of the two phases in the separator is monitored in order to derive the
saturation of the core sample in phase 1 and 2.
When equilibrium is achieved, and knowing the flow rates of the two phases, the core
saturation and the delta P, the determination of the steady state relative permeability is
straight forward using the Darcy law:
Ko
(14700)( o)(Qo)( L)
( A)( P)
and
Kw
(14700)( w)(Qw)( L)
( A)( P)
f
o
w
Sav
Sout
Wi
V
T
Ir
=
=
=
=
=
=
=
=
=
=
=
=
=
=
=
55/72
9. AppliLab Software
The picture below shows the AppliLab software main window.
Figure 10: AppliLab Software main window
56/72
On this main window we have all the information about our process:
One should note that every value which is in blue can be modified and that every value in
red is either measured or calculated and cannot be changed by clicking on it.
57/72
58/72
In this window, the user can input information about the sample he will use for the test. He
can also input information about the fluid used in the different accumulator. The unit used
for each parameter is given in this window.
59/72
In this window you can select the parameters that will be used for the monophasic
permeability calculation.
The initial flowrate is the flowrate that will be delivered by the injection pump for the first
step.
The final flowrate is the limit flowrate of the macro. It will stop when the flowrate delivered
by the pump is bigger than this value.
The multiplicative factor is the factor that will be applied between the flowrate of step n and
the flowrate of step n+1.
Example: Step 1: QI = 0.5 cc.min-1; multiplicative factor is 2; limit QF= 5 cc.min-1.
You will have Q1=0.5 cc.min-1;Q2=1 cc.min-1;Q3=2 cc.min-1;Q4=4 cc.min-1, and the macro
stops because Q5 would be 8 cc.min-1
You have 2 different options for the monophasic permeability macro: one non automatic
macro and a fully automated one.
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In this window you can select the file name. Both macros will generate an Excel file based on the Template-Kmono.xlsm file.
As we can see on the above picture, all the data about the sample and the fluids will be written. For each flowrate, the
software will write the flowrate applied to the system, and the different DeltaP that can be read: P1-P2, DeltaP500, and
DeltaP8. DeltaPs do not have to be in measure mode to be written in the file. Even if you do not use them in measure, their
value will be written.
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Between each step, the non-auto macro will ask the operator if the deltaP is stabilized
enough. If one clicks OK, then the software will write all DeltaPs and increase the
flowrate to the next step. Once the last step is done, the macro stops and Excel is
quitted.
Note: The files are accessible in the following folder: C/Applilab/Project/32814/Excel.
When the file is opened, one can check the data and select how the monophasic
permeability is calculated. When one clicks under the Select DeltaP mode cell, one
will be able to select which deltaP will be used to calculate Kmono. One can select P1P2, DeltaP500 or DeltaP8.
It is also possible to select which fluid was used to calculate the correct Kmono. Under
the cell Accumulator one will choose between Accu. A, B or C.
Based on these choices, a value of effective permeability will be calculated for each
flowrate using Darcys law.
The plot of DeltaP vs Q is then accessible and gives a precise value of monophasic
permeability in cell M28. This value is based on the regression of the slope, i.e. P/Q,
and Darcys law.
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10.
Key areas of maintenance include transducer and pressure set point calibrations as well
as seal replacement in the core holder, piston accumulator, BPR, fluid separator and air
operated valves to reduce the risk of leaks in the system. Make sure to bleed pressure
from the system before attempting to do any work on either the pore or overburden
pressure systems.
10.1.1.
The following table indicates the default Slope and Offset values to use in the control
program to insure correct engineering units are calculated by the computer and displayed
on the computer screen. The calibration coefficient values are in the control software
under Calibration. The default values in the table below are given in case the system is
tampered with causing the calculated engineering units in the software program to be
incorrect. The values in the table below will result in calculated engineering units that are
close to the correct values. Further calibration will result in accurate operation of the
system.
Transducer
Reference
PT01, 02, 03, 04
DPT01, 02
Default
Slope
1
1
Default
Offset
0
0
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Maximum
Rating (psi)
10,152
+/-0.5; +/-0.8; +/-1.25
Full Scale
Output
4-20 mA
4-20 mA
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Item
Designation
P/N
10
11
12
13
14
15
16
17
18
19
20
21 Ap0002677
22 Ap0012218
23 Ap0012220
24 Ap0017759
25 Ap0018034
26 Ap-299-001-0
27
28 Ap-299-002-0
29 Ap-299-004-0
Humidifier
30 Bh-001-0
Bulkhead H 1/8LP
31 BTs-0710-0
32 BTs-0810-0
33 C02-001-1
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34 C06-003-1
35 FPA-055-0
36 H05-043-0
37 Ov0004902
38 Ov0004904
39 Ov0004965
Window 350x180
40 Ov0005003
41 Ov0005004
42 Ov0005425
43 Ov0006196
44 Ov0006705
45 Ov0006707
46 Ov0006712
47 Ov0006713
48 Ov0006715
External frame
49 Ov0006725
Internal frame
50 Ov0006734
Window corner
51 Ov0006767
Window 350x40
52 Ov0006768
53 Ov0006769
54 Ov0006770
Internal frame
55 Ov0006773
External frame
56 Ov0006776
Window guide
57 Ov0006819
58 Ov0006820
59 Ov0006821
60 Ov0009757
Rail
61 Ov0014412
62 Ov0014413
63 Ov0017707
Oven assembly
64 Ov0017747
Drain pan
65 Ov-903-0
66 Std0000159
67 Std0000170
Long square
68 Std0000175
69 Std0000176
70 Std0000177
71 Std0000245
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72 Std0000313
73 Std0000314
74 Std0000781
75 Std0001107
Flange bottle
76 Std0001109
77 Std0001110
Bottle support
78 Std0001839
79 Std0002369
80 Std0002716
81 Std0003514
82 Std0006397
83 Std0006697
84 Std0007109
85 Std0008618
Lateral support
86 Std0008622
87 Std0008805
Clamping frame
88 Std0008937
89 Std0009170
90 Std0009171
Plate support
91 Std0009717
92 Std0012905
Plug
93 Std0015467
Guiding ring
94 Std0016189
Camera support
95 Std0016195
Plate support
96 Std0016196
97 Std0016468
98 Std0016469
99 Std0016473
100 Std0016483
V support
101 Std0016485
Shaft
102 Std0016488
103 Std0016556
Block bearing
104 Std0016688
Support bearing
105 Std0017640
106 Std0017761
107 Std0017802
Rotating support
108 Std0017804
Articulation support
109 Std0017868
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110 Std-004-0
Eclairage tuve
111 Std-077
112 Std-081
113 Std-095
114 Te-002-0
115 Vn-002-0
116
117 SW02200-HC
118 EXG50c-11012596
Camera
119 LPA2P2L
120 LPF2
Ferrule 1/8LP
121 LPF2-HC
122 LPG2
Gland 1/8LP
123 LPG2
Glang 1/8LP
124 4IN12.00
Rupture disc
125 LPSH2-1/4A
126 LPT2
Tee 1/8LP
127 23-415-8
128 23-411-8
129 16-015-6-12
IMPG63-CN1/4F131 PP10kG-N-O22
132 LM35JC1MS
Objectif
133 3118.06.13
134 0205.10.00
Bouchon 1/8G
135 3805.06.13
136 3175.06.10
137 0674.00.10
Silencieux d'chappement
139 4215-08
140 B72G-2GKQT3-RMN
Filtre dtendeur
141 18-013-989
Manomtre 40
142 4246-52
Manostat
143 4214-51
Quickclamp
144 4214-52
145 2-009-V747-90
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3051S2CD5A3F52A1AE2
146 L8P0Q4Q8 3051S
Delta P serie 3051S 2000psi calibration -2000 to 2000psi
3051S2CD4A3F52A1AE2
147 L8P0Q4Q8 3051S
Delta P serie 3051S 300psi calibration -300 to 300psi
3051S2CD2A3F52A1AE2
148 L8P0Q4Q8 3051S
Delta P serie 3051S 9psi calibration -9 to 9psi
149
0 Rondelle cuivre
156 CV-PIGTAIL-10FT
CV-MAN-12 STA-W/SOL- Manifold base for 12 pneumatic pilot valves 5/2 with
157 AT
solenoids 24VDC
158
0 Ecrou H M6 - inox
159
Ecrou H M8 - inox
160
161
162
163
164
165
166
167
Rondelle M6 - inox
168
169
170
171
172
173
174
175
176
177
178
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179
180
181
182
183
184
185
186
187
188
189
190
191
192
193
194
195
196
197
0 Compteur Gaz
For more information about the spare parts for each equipment please refer to the
dedicated user manual.
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12. Manuals
12.1. Hydrostatic Core Holder H-05-042-0
12.2. Vinci Acquisition 2012 Camera Software
12.3. Zeal Wet Gas Meter
12.4. ESI Sensor Pressure Transducer
12.5. Rosemount Differential Pressure Transducer
12.6. Back Pressure Regulator C-06-003-1
12.7. BenchTop Dual Pump BTDPs100-10
12.8. Benchtop Dual Pump BTDPs250-10
12.9. HP/HT Separator C02-002-1
12.10. Floating Piston Accumulator Hastelloy FPA-1000-10-Hast
12.11. Brooks Mass Flow Controller X-TMF-SLA5800
12.12. Eurotherm 2416
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VINCI TECHNOLOGIES
Parc de lIle 27B rue du Port
92022 NANTERRE CEDEX FRANCE
Tel. +33 1 41 37 9200 Fax. +33 1 41 37 0476
Web site : http://www.vinci-technologies.com