TESTING PROCEDURES AND MATERIAL SPECIFICATION FOR THICK FILM 250 MIL SPECLAD CORROSION PROTECTION SYSTEM FOR TUBESHEETS #STS-10 1.0 Purpose: The purpose of this document is to establish the Surface Preparation Procedures, Coating Application Procedures, Testing Procedures, Materials used in the SPECO SPECLAD Thick Film 250 mil Tube Sheet Cladding Process. 2.0 References: SSPC-SP1, SSPC-SP5, SSPC-VIS 1, and SSPC-SP1. 3.0 Precautions/Limitations: 3.1 Containment: No special containment procedures are required during the surface preparation or coating application of the SPECO SPECLAD system. 3.2 Waste Disposal: Care should be taken to see that all of the spent blasting media is put into drums for proper disposal by the owner. 4.0 Special Tools/Equipment: 4.1 Testex Press-O-Film Replica Tape, or Keene-Tator Anchor Profile Comparator and Micrometer. 4.2 Wet Film Thickness Gauge (WFT) 4.3 Positector 6000 DFT on non-magnetic or non-ferrous tube sheets 4.4 Laboratory triple beam balance 4.5 MEK (Methyl Ethyl Ketone) Solvent 4.6 Non-waxed Paper Cups for mixing materials 4.7 Plastic Sheeting & Duct Tape for masking and dust control 4.8 Miscellaneous items such as clean rags, paper towels, special Speco brushes and hand trowels.
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5.0 Materials Storage/Inventory Control: 5.1 Materials Storage/Inventory Control: SPECLAD, SPEFLEX and SPECURE can be stored for a minimum for 1-2 years at ambient temperature. If the ambient temperature is less than 60F, the material should be stored at 60-70F for at least 24-48 hours prior to use. 6.0 Initial Conditions: 6.1 Work and QC to be done by Speco International, L.L.C. Acceptance will be by owner and Speco International, L.L.C. 6.2 Initial Cleaning: Any coating or lining presently installed shall be completely removed. Residual grease and oil shall be removed in accordance with SSPC-SP1 (if necessary) prior to abrasive blast cleaning. All surfaces to be coated shall be abrasive blast cleaned to the requirements of SSPC-SP5. Other methods of cleaning, e.g., very high-pressure water, may be used to remove any existing coating; however, final surface preparation shall be by abrasive blast cleaning. All sharp edges shall be rounded to 1/8 radius or greater. 6.3 Disposition of Temporary/Removable Tube Plugs: Plugged tubes that have been plugged and coated with a removable temporary epoxy type putty coating shall have the coating removed and the tube sheet crevice will be recleaned and recoated to seal the crevice. 6.4 Existing corrosion to be removed with Kleen Blast. Final profile shall be obtained with Kleen Blast, Aluminum Oxide, or Garnet. 6.5 Tube trimming and/or Tube Flaring: Tubes on the outlet tube sheets will need to be trimmed to a maximum of .25 offset from the tube sheet surface. 6.6 Engineering Hold Point and QC Inspection. 7.0 Surface Preparation: 7.1 Abrasive Material: Abrasive material used for blast cleaning shall develop a fine sharp anchor pattern with a profile of 3.0 mils minimum. Kleen Blast, Garnet, aluminum oxide, or equal are acceptable abrasives. Abrasive blasting shall not reduce the thickness of the substrate to the extent that scoured depressions are evident as a result of the abrasive impinging too long on one spot. 7.2 Air Supply Cleanliness: Compressed air used shall be checked for the presence of oil by wiping a clean white cloth over a clean, smooth metal surface upon which the air stream has been impinged for a period of not less than 2 minutes. The orifice being held not more than 18 away from the surface. Alternatively, the air stream may be
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projected against a square of white blotter taped around its complete periphery to a substantial surface. Sufficient freedom from oil is confirmed if no soiling or discoloration is visible. If air contamination is evidenced, the filters shall be changed or cleaned, traps emptied, after coolers, moisture separators or filters added, the equipment maintained, or such adjustments made as may otherwise be required to achieve clean air. This evaluation shall be done in the shade. The test shall be performed for each compressor used during a given shift, no sooner than one-half hour after starting the compressor. 7.3 Environmental Conditions: The surface should be clean and dry. The surface shall be heated between approximately 75-85F prior to coating. The surface temperature shall be 5 degrees higher than the dew point temperature (minimum) during coating. In no event shall coating begin or continue if there is any visual evidence of the surface turning or corroding after blasting. Ambient temperature 60 - 90F shall be maintained. Ventilation shall be by a Speco Venturi Venting System. 7.4 Degree of Surface Cleanliness: After blasting, traces or accumulations of spent residual abrasives that are evident shall be removed by vacuuming or blown down. If vacuuming is used, the attachments shall be free of oil, grease, or dirt. The surface shall be inspected 15 min. after vacuuming to assure that dust has not resettled on the blasted surfaces. If dust has resettled, vacuuming or blow down shall be repeated until dust is no longer evident. 7.4.1 Discoloration of the surface will also indicate if contamination has occurred. If it is suspected that the moisture separators and after coolers are not removing all the moisture and oil from the compressed air, the abrasive shall be turned off and the airstream from the blast nozzle checked for traces of water or oil. The surface should be heated to between 80 - 90F and may be reheated after the original abrasive blasting, followed by a light touch blasting. 7.5 Inspection Hold Point: All surfaces prepared for lining application during a given shift shall be visually examined for compliance with the requirements of this specification. The degree of surface cleanliness achieved shall be verified to meet the intent of SSPC-SP5. SSPC-VIS 1 visual standards shall be used for comparison. Anchor pattern and profile shall be verified by the use of Testex Press-O-Film Replica Tape, or Keene-Tator Anchor Profile Comparator. Micrometers used in conjunction with the Press-O-Film shall be calibrated.
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8.0 Coating Application 8.1 Setting Plugs for DFT: SPECLAD is applied in a continuous process so that the coating WFT may be checked throughout to verify thickness. Coating thickness during the coating process is also governed and maintained by the height of the plastic plugs used for plugging the condenser tubes. Plugs are set into the tubes at 250 mil height from the tube sheet using a steel plate w/ spacers. After the SPECLAD coating is applied, the system should be allowed to achieve a partial cure overnight or for 8-12 hours. The SPECLAD coating system shall then be sanded to a smooth finish with the plastic plugs left in place. When a smooth planar surface has been achieved the plastic plugs can be removed. The smooth, planar SPECLAD surface will then be given a finish coat of 2-3 mils of SPEFLEX for cosmetic purposes only. After the finish coat has been applied and set, the system shall be allowed to cure for 16 hours at 70F ambient temperature or 24 hours at 60F ambient temperature. 8.2 Environmental Conditions: The surface should be clean and dry. The surface shall be heated between approximately 75-85F prior to coating. The surface temperature shall be 5 degrees higher than the dew point temperature (minimum) during coating. In no event shall coating begin or continue if there is any visual evidence of the surface turning or corroding after blasting. Ambient temperature of 60 - 90F shall be maintained. Ventilation shall be by a Speco Venturi Venting System. 8.3 Mixing and Pot Life: All Speco materials are weighed on laboratory beam balance scales prior to mixing for application. These scales weigh within an accuracy of 1 gram to be sure the correct amount of base material and reactor is placed in the cup for mixing. This assures that, when mixed, all materials will be fully reacted and a homogenous finished coating results. Speco materials are of easily workable consistency that makes possible full mixing contact of reactor and base material molecules. They are not thick pastes which are difficult to mix adequately and where each molecule of the reactor has difficulty moving through the matrix in an effort to attach itself to the base molecules. 8.4 Recoat Window: The coating shall be the SPECO SPECLAD CORROSION PROTECTION SYSTEM applied by employees of Speco International, L.L.C. The mixing of all materials shall be in accordance with Speco instructions. Maximum Recoat time for the material is 15-20 minutes @ 77F. Pot life of the material is 15 minutes at 77F. The first coat
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shall be SPECLAD applied by trowel to a thickness of 250 5 mils. The finish coat (for cosmetic purposes only) shall be SPEFLEX applied by roller on a continuous basis to a thickness of 2-5 mils. In no case shall the total DFT be less than 250 mils. In areas of deep pits, coating thickness may increase to 300+ mils. 8.5 Inspection Hold Point: The coating system shall be visually inspected for pinholes and other coating defects. All pinholes and defects shall be marked and repaired. Repairs shall be done in accordance with Speco International, L.L.C. Bulletin # 9.45A. The DFT shall be measured by using a magnetic gage or Positector. In the case of a non-magnetic or non-ferrous tube sheets, the Positector 6000 will be used. Areas with less than 250 mils coating thickness shall be sanded and recoated to build the thickness to within tolerance. Coating thickness in excess of 250 mils shall not be ground down. All tests shall be conducted in the presence of the assigned inspector from the Owner/ Engineer staff. All documentation shall be completed daily or as required, by the Speco Project Manager. All such documentation shall be done at the site prior to the workdays end. The Speco Project Manager shall ensure that all records are completed daily or as required. After completing the days work, all materials, tools, and equipment shall be properly stored in a protected area or locked tool room so that they will be ready for work the next day and not be subject to damage, contamination, etc., during the time they are in storage. 8.6 The following standards shall apply: SSPC-SP 5 SSPC-VIS 1 9.0 Grinding Excess Build Coat/Coating Continuity: 9.1 In no case shall the DFT be below 250 mils. In areas of deep pits, coating thickness may increase to 300+ mils. After the SPECLAD coating is applied, the system should be allowed to achieve a partial cure overnight or for 8-12 hours. The SPECLAD coating system shall be sanded to a smooth finish with the plastic plugs left in place. 9.2 Coating Plug Removal: When a smooth planar surface has been achieved the plastic plugs are to be removed. The smooth, planar SPECLAD surface will then be given a finish coat of 2-5 mils of SPEFLEX for cosmetic purposes only. After the finish coat has been applied and set, the system shall be allowed to cure for 16 hours at 70F ambient temperature or 24 hours at 60F ambient temperature.
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9.3 Inspection Hold Point: The coating system shall be tested 100% visually for pinholes. Any pinhole shall be marked and repaired. These and such other repairs shall be done in accordance with Speco Bulletin 9.45A or paragraph 10.0. 9.3.1 The DFT shall be measured by using a magnetic gage or Positector. In the case of a non-magnetic or non-ferrous tube sheets, the Positector 6000 will be used. Areas with less than 250 mils coating thickness shall be sanded and recoated to bring the thickness within tolerance. Coating thickness in excess of 250 mils shall not be ground down. 9.3.2 All tests shall be conducted in the presence of the assigned inspector from the Owner/Engineer staff. 9.3.3 All documentation shall be completed daily or as required, by the Speco Project Manager. All such documentation shall be done at the site prior to the workdays end. The Speco Project Manager shall ensure that all records are completed daily or as required. 9.3.4 After completing the days work, all materials, tools, and equipment shall be properly stored in a protected area or locked tool room so that they will be ready for work the next day and not subject to damage, contamination, etc., during the time they are in storage. 9.3.4 The following standards shall apply: SSPC-SP 5 SSPC-VIS 1 10.0 Touch-Up/Minor Repair (Please refer to Bulletin 9.45A): 10.1 SPECLAD is a high-technology protective coating; to repair damaged areas these instructions must be followed carefully. 10.2 To repair damages that have occurred in shipment or are noticed at time of installation, or have occurred during operation. Whatever the cause, it is essential that any damaged areas are repaired as any pinholes or re-coat areas will cause concentrated corrosion or galvanic action. 10.3 Where the coating has been chipped due to a blow or shock, the area around the chip must be probed with a knife and all loose coating must be removed. Cracks that cannot be seen may exist, and the cracked material must be removed with a knife of chisels by prying up the edges of the chip. The coating around the area to be repaired must be adhering firmly to the surface. Dont be afraid to remove a little excess material.
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10.4 For a small area sandpaper the base metal and the surrounding coating. For a larger area, mask off the good coating and sandblast the surrounding material and bare base metal. If oil or grease has gotten on the material around the are to be repaired it must be removed completely. 10.5 For large areas it is essential to heat the base metal to 80-90F to remove all moisture. It is easiest to heat the metal from the rear with a torch or butane space heater. 10.6 Mix SPECLAD and SPEFLEX in accordance with the directions on the label of the can. The patch should be built up to the thickness of the original coating. For small patches use a single coat of SPECLAD followed by a 2-5 mil coat of SPEFLEX. Allow the coating to set for 16 hours at room temperature to fully cure. If it is cold, you can warm the metal to 80-90F for an hour to speed up the curing process. 10.7 Helpful Hints: Mix the materials in a non-waxed paper cup or clean dry tin can. Weigh the materials with a beam balance using 18.6 parts SPECURE to 100 parts SPECLAD or SPEFLEX. Use a putty knife or stiff brush to apply the material. Do not mix too much material as it sets in about 15 minutes at room temperature. If the material gets hot in the container, it has begun setting and should not be applied to the patch. Work the material in with the putty knife or brush to eliminate air bubbles.