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Macarthur Girls High School 3
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Production of Materials
Comparing the reactivity of alkanes and alkenes with bromine
water #01
Introduction:
Alkenes are hydrocarbons which are very reactive. This is because the double
bond between carbons is unstable. Therefore, the double bond breaks and
undergoes addition reaction (chemical reaction). However, alkanes have a single
bond which is not reactive.
Aim:
To investigate and identify the reactivity of alkanes and alkenes in bromine
water.
Materials:
Bromine water
Safety glasses
Test tube
Test rack
Cyclohexane liquid
Cyclohexene liquid
Waste container
Variables:
Independent: type of compound (alkane or alkene)
Dependent: the change in colour
Controlled: amount of each liquid, width of test tube
Method:
1. Wear safety glasses
2. Transfer 1mL of liquid hydrocarbon into the test tube
3. Add a drop of bromine water and shake the test tube laterally.
Observe the results.
4. Continue step 3 until it changes colour. If it does not, then it is an
alkane. If it does, it is alkene.
5. Transfer all the waste into the waste container.
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Risk Assessment:
Liquid Bromine: is very toxic and corrosive as it can cause severe burns to eyes
and skin if it is in contact. To avoid this, wear safety glasses and conduct the
experiment into an air absorbing container. Avoid breathing the fumes of
bromine solution if it is not in the air absorbing container.
Cyclohexane and cyclohexene: is very toxic and flammable as it is very
volatile. It is harmful because it can cause lung damage if swallowed. To avoid
this, wear safety glasses and conduct the experiment into an air absorbing
container.
Results:
Substance What Happened?
Conclusion:
From the results it can be seen that alkenes are more reactive than alkanes.
Discussion:
The experiment was deemed to be a success as it answered the aim. The results
show that alkanes are not reactive as alkenes. This experiment can be deemed
valid as there was only one variable that was changed. This experiment can also
be deemed reliable as the results were same when checked with other groups.
This was not repeated due to time constraints. Moreover, this experiment can be
deemed accurate as all the materials were clean and uncontaminated.
Further improvements to the experiment can include, adding smaller quantities
to the test tube. This will allow for a quicker result which can be more accurate.
However, negatives include a higher percentage error.
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Materials:
Side conical flask
Rubber tube
Delivery tube
Test tube
Glucose
De-ionised water
Yeast
Electronic balance
Limewater
Evaporating dish
Plastic spoon
Stopper
Method:
1. Insert the rubber tube into the long end of the delivery tube. Insert
another side of the rubber tube to the side conical flask.
2. Measure 100mL of glucose solution into measuring cylinder. Pour it
into the side conical flask.
3. Add 3 grams of dry yeast into the evaporating dish. Measure it on
an electronic balance. Pour it into the side conical flask.
4. Close the side conical flask with a stopper.
5. Measure the mass of the conical flask on the electronic balance.
6. Leave it for two days. Record results.
Risk Assessment:
The glassware may break if there is excessive force applied to it. To avoid this,
handle the glassware with care.
Lime water is very dangerous to the skin. It may cause burns if it is in contact
with the skin. To avoid this, wear safety glasses and wipe any spills.
Results:
Mass of glucose dissolved: 5 grams
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= 0.0545
New mole ratio: 0.027:0.054:0.054
Theoretical mass of ethanol produced from glucose:
Mole ratio: 0.02775:0.0555:0.0555
So percentage of theoretical yield is,
0.0545
0.555 x 100 = 98%
Discussion:
This experiment was deemed as successful as the aim was successfully
answered. The hypothesis was correct as seen from the results. The experiment
can be considered accurate as all the apparatus was washed before using to
avoid contaminations. This experiment can also be called reliable as other
groups got similar results to ours. However, this experiment cannot be deemed
valid as there were no independent variables. This is because the aim of the
experiment was to measure the mass changes.
Further improvements to this experiment can include making the glucose
solution from scratch with the powder. This improves the accuracy of the
experiment. Moreover, the electronic balance was accurate to two decimal
places which improve the accuracy. Possible improvements could include tilting
the side conical flask towards the limewater test-tube to allow carbon dioxide to
pass out of the mixture more easily.
Some of the errors in this experiment may have been that the temperature was
not constant across the two days which may affect the rate at which
fermentation occurs. Because carbon dioxide is a fairly dense gas, some of the
carbon dioxide may have remained in the test-tube.
Conclusion: From the results it can be seen that the mass changes when
glucose undergoes fermentation.
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Aim:
To compare the heat of combustion of three alkanols by carrying out the
experiment.
Hypothesis:
Ethanol will have the highest heat of combustion both per mole and per gram.
Materials:
Thermom Wire Retort
eter gauze stand
Measurin Beaker Boss
g cylinder Electronic head
Match balance Clamp
box Ethanol Safety
Spirit 20mL Glasses
burner Water Methanol
Tripod 100mL Propanol
Risk assessment:
Risk Prevention
Method:
1. Gather all the materials needed to conduct the experiment.
2. Pour 100mL of water into a measuring cylinder (100mL) and
transfer it into the beaker.
3. Place a heat proof mat under a spirit burner and place the tripod
and gauze mat.
4. Put the beaker on top of the gauze mat.
5. Attach the boss head and clamp to the retort stand.
6. Gently insert the thermometer into the clamp so that it goes into
the beaker full of water but it does not touch the beaker.
7. Light the spirit burner and leave it for 5 minutes.
8. Repeat steps 1-7 using methanol
9. Repeat steps 1-7 using propanol
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Variables:
Independent: Type of Alkanols (methanol, ethanol, propanol)
Dependent: Heat of combustion of each of the alkanols.
Controlled: amount of water added to each experiment, same amount of height
between the spirit burner and the beaker, same width and size of measuring
cylinder and beaker.
Results:
ETHANOL:
Mass of beaker + ethanol = 228.4g
Mass of beaker + ethanol after burning = 224.3g
Initial temperature = 21C
Final temperature = 61C
CALCULATIONS:
H = mCT
= 100x4.18x40
= 16720J
m
n= Mm
4.1
n= 46.068
= 0.08899887123 moles
HEAT OF COMBUSTION PER MOLE:
16720
=187.87 kJ /mol
0.08899887123
HEAT OF COMBUSTION PER GRAM:
16720
= 4078.05 J / g1
46.068
METHANOL:
Mass of beaker +methanol = 204.9g
Mass of beaker after burning methanol = 203.3g
Initial Temperature = 23.5C
Final Temperature = 41C
CALCULATIONS:
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H = mCT
= 100x4.18x 17.5
=7315J
m
n= Mm
1.6
n=
32.042
0.04993446102 moles
HEAT OF COMBUSTION PER MOLE:
7315
0.04993446102 = 146.49kJ/mol
PROPANOL:
Mass of beaker + propanol = 195.7g
Mass of beaker + propanol after burning= 194.1g
Initial Temperature = 22C
Final Temperature = 50.5C
CALCULATIONS:
H = mCT
= 100x4.18x 28.5
= 11913
m
n= Mm
1.6
n=
60.094
n=0.02662493421
HEAT OF COMBUSTION PER MOLE
11913
0.02662493421 =447.44 kJ/mol
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Discussion:
The hypothesis was proved wrong as propanol has the higher heat of
combustion. The experiment was conducted successfully as it was fairly constant
over time. This experiment can be considered reliable as the results were fairly
consistent across the class when compared. It can also be considered accurate
as the apparatus was cleaned before it was used. This experiment can also be
considered valid as there was only one variable that was changed.
However, errors to this experiment is that the spirit burner containing ethanol
was left to burn for about 10 minutes due to miscommunication. This caused the
change in heat of combustion for ethanol. However overall, this experiment can
be improved by conducting it by one person. This can limit the possible sources
of human error.
Conclusion:
From the results it can be seen that propanol has a higher heat of combustion.
PART 1
Introduction
Reduction and oxidation (redox) reactions occur when electrons are
transferred from the reductant to the oxidant. In 1800, Volta invented an
electrochemical cell where the transferred electrons were channelled into
an external circuit and could be put to use. Voltas original cell was
composed of silver and zinc discs separated by paper soaked in vinegar.
Each of these cells produced 0.76 volts. Volta could not explain the
working of his cell, since electrons and redox reactions were unknown at
this time.
Aim: to identify conditions under which galvanic cell is produced
Materials:
Safety Glasses
Voltmeter
Beaker
Emery paper
Connecting wires(alligator clips)
Zinc, copper and graphite electrodes
50mL distilled water
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50mL NaCl(aq)
150mL H2S04
Risk Assessment:
Acids are corrosive. They may also cause burns on hands if it is not
handled properly. To avoid this, handle the acids with care. If there are
spills, clean it up immediately.
Glassware may break if it is not handled with care. The glass pieces can
hurt and may bleed. To avoid this, hold the glassware properly.
Method:
1. Warning: Wear safety glasses!
2. Warning: 1 mol L1 H2SO4 is corrosive. Avoid skin contact. Clean up
spills immediately.
3. Set up the apparatus shown in the diagram using a small beaker
filled with electrolyte (Z). Connect electrodes (X) and (Y) by wire to a
voltmeter (V).
Perform the trials listed below and observe the cell for signs of chemical
reaction, e.g. gas bubbles, colour changes, voltage reading.
TRIAL ELECTRODE X ELECTRODE Y ELECTROLYTE Z
1 Zn Cu Distilled water
2 Zn Cu 1 mol L1 NaCl
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3 Zn Cu 1 mol L1 H2SO4
4 Cu Cu 1 mol L1 H2SO4
5 Zn C 1 mol L1 H2SO4
4. Electrodes must be rubbed with emery paper, rinsed with water and
dried before each trial cell is connected.
5. Rinse the beaker with water between trials 2 and 3.
6. If the voltmeter reads below zero, reverse the connections
(polarity).
Results:
ELECTRODE X ELECTRODE Y ELECTROLYTE Z VOLTS
Cu Cu 1 mol L1 H2SO4 0V
Discussion:
The aim of this experiment was answered, hence it can be deemed
successful.
Validity: this experiment cannot be called valid as there were no
independent variables in the experiment.
Accuracy: the experiment cannot be called accurate as the metal
electrodes were previously used which may have caused some errors as
they have a high risk of getting contaminated.
Reliability: this experiment can be deemed reliable as the results were
similar to other groups when it was compared to other groups due to time
constraints.
Further improvements: Further improvements to this experiment
includes, using uncontaminated electrodes, beakers, and acid solutions.
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Conclusion:
In conclusion, the conditions under which galvanic cells are produced are
found.
PART 2
Introduction:
In the previous experiment (Galvanic cells (I)), you investigated the essential
conditions necessary for a galvanic cell to operate, and discovered two important
points:
The electrodes must be made of dissimilar conductors.
The electrodes must be immersed in an electrolyte.
Aim:
to measure the difference in potential of different combinations of metals in an
electrolyte solution.
Materials:
1x safety glasses
6x 1 10 cm paper strips* soaked in saturated KNO 3 solution*
1x voltmeter*
2x connecting leads (wires)
1x 150 mL beaker* + Zn electrode + 1 mol L1 ZnSO4
1x 150 mL beaker* + Cu electrode + 1 mol L1 CuSO4
1x 150 mL beaker* + Mg electrode + 1 mol L1 MgSO4
1x 150 mL beaker* + Pb electrode + 1 mol L1 Pb(NO3)2Label:
Toxic
Risk Assessment:
Lead in any form is toxic. If it is in any contact with skin, wash it off with water as
soon as possible. To avoid touching lead, use filter funnel to transfer the solution
from the bottle into the beaker.
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Method:
1 Set up the apparatus using two beakers filled with metallic salt solutions, a
salt bridge and two metal electrodes connected to a voltmeter. For
convenience, the salt bridge used will simply be a strip of filter paper
soaked in saturated KNO3 solution.
Note: To avoid contamination, each trial requires a fresh salt bridge.
2 Record:
athe polarity of the electrodes
b the net voltage (Enet) for each of the trials in the table below:
CE
BEAKER 1 BEAKER 2 NOTES
LL
Zn + 1 mol L1
1 Cu + 1 mol L1 CuSO4
ZnSO4
Zn + 1 mol L1
2 Mg + 1 mol L1 MgSO4
ZnSO4
Zn + 1 mol L1 Pb(NO3)2 is
3 Pb + 1 mol L1 Pb(NO3)2
ZnSO4 toxic
1
Cu + 1 mol L
4 Mg + 1 mol L1 MgSO4
CuSO4
Cu + 1 mol L1 Pb(NO3)2 is
5 Pb + 1 mol L1 Pb(NO3)2
CuSO4 toxic
1
Mg + 1 mol L Pb(NO3)2 is
6 Pb + 1 mol L1 Pb(NO3)2
MgSO4 toxic
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Results:
CEL Observatio
BEAKER 1 BEAKER 2 E0
L ns
Zn + 1 mol L1 No
1 Cu + 1 mol L1 CuSO4 0.2V
ZnSO4
Zn + 1 mol L1 Bubbles
2 Mg + 1 mol L1 MgSO4 0.15V
ZnSO4
Zn + 1 mol L1 Bubbles
3 Pb + 1 mol L1 Pb(NO3)2 0.4V
ZnSO4
Cu + 1 mol L1 No
4 Mg + 1 mol L1 MgSO4 0.025V
CuSO4
Cu + 1 mol L1 No
5 Pb + 1 mol L1 Pb(NO3)2 0.025V
CuSO4
Mg + 1 mol L1 White
6 Pb + 1 mol L1 Pb(NO3)2 0.6V
MgSO4 precipitate
Discussion:
The experiment was conducted successfully as the aim was successfully
answered to the question. It can also be seen that the aim was successfully
done, as seen from the results. However, further improvements to the
experiment includes ensuring accuracy as the glassware may have been
contaminated which can change the potential energy, hence resulting in
inaccuracy in experiments. Furthermore, this experiment cannot be deemed
valid as it the variables were not controlled. But, this experiment can be deemed
reliable as the results were matched with several groups and we got similar
results.
Conclusion:
From the results, it can be seen that the difference in potential difference in
electricity it produces in different solutions.
Acidic Environment
Making a natural indicator using red cabbage & comparing to
universal indicator
Introduction:
Indicators have been used for a long time.Acid/base indicators are compounds
that change colour according to the pH. Indicators are organic compounds and
some, such as litmus, are found naturally in plant pigments like in red cabbage.
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Aim:
To perform a firsthand investigation to measure the pH of substances using a
natural indicator
Hypothesis:
If the natural indicator is prepared correctly, it should show similar colours when
it compared with the universal indicator.
Materials:
1x red cabbage leaf
1x 600 mL beaker
1x 100 mL measuring cylinder
1x safety glasses
1x tripod, wire gauze, Bunsen burner
18 x test tubes + labels
2x test tube rack
5 x 50 mL beakers
Hydrochloric Acid
Sulfuric Acid
Sodium Hydroxide
Sodium Carbonate
Potassium Hydroxide
Table salt
Soda Water
White vinegar
Nitric Acid
Universal Indicator
Glass stirring rod
Ph chart
Method:
1. Warning: Wear safety glasses!
2. Warning: 0.1 mol L1 NaOH is caustic. Avoid skin contact.
Clean up spills immediately.
3. Warning: 0.1 mol L1 HCl is corrosive. Avoid skin contact.
Clean up spills immediately.
4. Transfer 200 mL of water into a 600 mL beaker. Add a leaf of
shredded red cabbage. Boil the mixture gently until a richly coloured
extract is formed. Allow to cool, then pour off the reddish-purple indicator
solution.
5. Test the indicator by adding it to 3 mL samples of the following
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solutions:
Hydrochloric Hydroxide
Acid Table salt
Sulfuric Acid Soda Water
Sodium White vinegar
Hydroxide Nitric Acid
Sodium
Carbonate
Potassium
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Results:
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Discussion:
The experiment was conducted successfully as the aim was answered. The
experiment cannot be deemed reliable as it was no repeated many times due to
time constraints. We also did not get to discuss the results in class due to time
constraints. The apparatus was uncontaminated as it was washed and dried
before using the glassware. This ensured that no other substance can affect the
experiment. However, the experiment can be deemed valid because it only had
one independent variable. This meant that we were able to distinguish the slight
colour difference between natural indicator and universal indicator.
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Conclusion:
From the results it can be seen that natural indicator can work just like the
universal indicator as it has similar properties.
Introduction:
Carbon dioxide exists in equilibrium when the bottle is sealed.
CO2(g) C02(aq)
When the bottle is opened, there is a change in the conditons. This means that
according to Le Chateliers principle, system will try to readjust the change by
shifting the equilibrium to the side which minimises the change.
Aim:
to observe the mass changes of carbon dioxide loss when softdrink is
decarbonated
Materials:
375mL of sealed coca cola bottle
500g digital weighing scale
Hydrochloric acid (1Molar)
Method:
1. Take a 375mL sealed coke bottle and measure the mass on the
mass scale and record the initial mass in the table below.
2. Break the seal carefully and keep the lid onto the bottle loose so
that water vapour does not come out.
3. Leave it for two days in the room at 25 degrees.
4. Measure the mass of the coke bottle on the digital weighing scale
and record on the table.
5. Add 3 grams of HCL(aq) to the bottle, close the lid and shake it.
Carefully open the bottle and allow the CO2(g) to evaporate and weigh the
bottle again.
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Results:
Mass of sealed bottle 327.2
grams
Calculations:
m
n=
Mm
2
n=
48.01
V ( gas)
n=
V ( SLC )
V
0.04165798792=
24.79
V =1.032701521
Discussion:
The experiment was conducted successfully as the aim was answered. It was
fairly accurate as the electronic balance was used gave readings to 2 decimal
places. However we assumed that all mass lost was due to CO2 escaping vessel,
but some water vapor may have also escaped. To prevent this a control should
have been used (a beaker filled with distilled water) in order to account for this
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mass loss. Also we assumed the experiment was carried out at 25C for
calculation, however this temperature could not be accurately maintained and
results may have been affected by this. The experiment was deemed reliable as
the results were compared with other groups in class ans they got similar results.
Conclusion:
From the results it can clearly be seen that the mass change was successfully
measured through de carbonating a soft drink.
Introduction:
Many household substances are used for different purposes. This is why, they
have different chemicals, with different pH. To check the pH, data logger and pH
probe is used.
Aim:
To measure the pH of household substances using a data logger and pH probe.
Materials:
Data logger Magnesium sulfate
pH probe Vinegar
3 beakers Methylated spirits
Stock solutions Sugar soap
Bleach Lemon detergent
Shampoo Lemon juice
Window cleaner
Variables:
Controlled: pH probe used, data logger, beaker, same amount of chemicals used
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Method:
1. Turn the data logger on, and connect the pH probe wire to the data
logger machine. Calibrate the data logger, using 3 different pH solutions,
(pH = 4,7,9)
2. Fill, 30mL of each of the solutions in the beakers.
3. Place the pH probe into the beaker. Ensure that the bottom part of
the probe is in the solution. Record the pH into the table, wash the probe
with water and dry it.
4. Repeat step 4 for all the solutions.
Risk Assessment:
Do not allow bleach to contact the skin, eyes or clothes as it can cause irritations
to the skin. Methylated spirits, are highly flammable and it may cause
drowsiness. To avoid this, keep it away from face and gases.
Results:
4 4.04
7 7.04
9 9.03
Household pH
substance
Bleach 13.1
3
Shampoo 6.34
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1M magnesium 6.9
sulfate
Vinegar 1.79
Conclusion:
From the results, it can be seen that the household substances vary from a pH of
1 to pH of 13.
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Discussion:
The aim was successfully answered; hence the experiment can be called
successful. The pH probes are highly accurate compared to pH chart as it gives
the reading to 2 decimal places. This experiment can also be called valid
because there was only one independent variable which was tested against. This
can also be called reliable, because other groups got the same results, which we
got.
However, limitations to this experiment include calibration error. The probe was
not perfectly calibrated as there was 0.4 error. Further improvements can include
using an uncontaminated beaker containing uncontaminated household
substances.
Introduction:
Indicators have been used to test the acidity or basicity of a substance. This
experiment tests the pH of salt solutions using a Universal indicator.
Aim:
Materials:
Potassiu Magnesiu Water
m nitrate m carbonate Stirring
Ammoniu Magnesiu rod
m acetate m Sulfate Universal
Sodium Table salt indicator
acetate Sodium Test tube
Copper hydrogen rack
carbonate carbonate
Magnesiu 9 thin
m chloride test tubes
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Method:
1. Place approximately 2 grams of each salt in the test tubes and add
5mL of water.
2. Mix the solution with a stirring rod
3. Add 3 drops of universal indicator in each test-tube.
4. Check the pH of the solution using a pH chart.
5. Record results.
Variables:
Results:
Ammonium 6 7
acetate
Sodium 8 8
acetate
Copper 7 8
carbonate
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Magnesium 5 7
chloride
Magnesium 7 9
Carbonate
Magnegium 9 7
sulfate
Sodium 8 8
hydrogen
carbonate
Table salt 7 6.5
Conclusion:
From the results it can be seen that pH of the salts vary, when in solution.
Discussion:
The experiment can be deemed success as it answers the aim. It can also be
considered reliable, as the results were consistent with other groups. It can also
be considered accurate as the test tubes were washed and cleaned, before it was
used. It was also, valid because there is only one variable which changes
throughout the experiment.
*GOOD TO KNOW:
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Introduction:
Aim:
To find the exact concentration of 25mL HCl required to neutralize the reaction
Hypothesis:
It will take about 25mL of sodium carbonate standard to titrate with 25mL of HCl.
Materials:
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Method:
Results:
Amount of Sodium
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carbonate standard
added
Trial 1 25mL
Trial 2 24.6mL
Trial 3 24.7mL
Trial 4 24.6mL
n
CALCULATIONS:
C=
v
0.050= n/0.250
n=0.0125 moles
m
n= Mm
0.0125=m/105.99
Concentration part:
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Conclusion:
From the results it can be seen that it takes about 24.65mL of sodium carbonate
to neutralize the HCl acid.
Discussion:
Anhydrous (normal) Na2CO3 was used because it is stable and does not gain
mass by absorbing water from air. Therefore, its composition and mass is
accurately known. All equipment was free of foreign contaminants and was
washed with the correct liquids. All volumes were measured from the bottom of
the meniscus to increase the accuracy. No splashing or loss of liquid occurred
during the transfer of liquids. Hence accurate and valid as measurements were
also close to stoichiometric values. Overall experiment is valid, as all the
variables were controlled, to determine the endpoint of titration. The
experimental design is reliable because it was compared with other member of
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the class and consistent results were achieved and it also accounted for
theoretically expected results.
Limitations to this experiment include using a pH probe and data logger, to see
the titration curve. This allows to determine the equivalence point and the
endpoint of the reaction.
Esterification practical
Introduction:
Alcohols and alkanoic acids, when reacted form an ester and water molecules.
The ester formed, is insoluble in water. This is why,
it causes the stinky smell.
Hypothesis:
Aim:
Materials:
Pear shaped flask
Beaker
Tripod
Wire gauze
Bunsen burner
Retort stand
2 x boss heads
2 x clamps
Condenser
Boiling chips (heat ones)
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Method:
3 Warning: Wear safety glasses!
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Risk assessment:
Alcohols and alkanoic acids are volatile. They can rapidly evaporate
so they should be kept away from flame.
Substances used in experiment are highly corrosive so safety
glasses/gloves worn
Sulfuric acid is corrosive. Clean up spills immediately
Variables:
Results:
Butanol
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Conclusion:
From the results it can be seen that mixing alcohol and alkanoic acids produce an
ester and water
Discussion:
Concentrated sulfuric acid was used because it speeds up the rate of reaction
and it is a dehydrating agent. The boiling chips were placed into the pear shaped
flask because it prevents bubbling and spreads the heat evenly. Reflux was used
to prevent the escape of any volatile vapors, allowing us to perform the reaction
at higher temperatures, boost the reaction rate and shift left or right to favour
ester yield. Water bath was used to ensure safety, and prevent any volatile
substances like the reactants from igniting because of the flame.
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Introduction:
There are many different types of chemical reactions. Some of them include
precipitation reactions, and acid carbonate reactions. Each of these can be
visible at a macroscopic level. This experiment tests for common anions, through
chemical reactions.
Aim:
Materials:
Test solutions: Na2SO4 distilled
Pb(NO3)2 Na2CO3 water
Ba(NO3)2 Na3PO4 water
HNO3 NaCl bath
AgNO3 4 test test tube
NaOH tubes holders
test tube
Anion solutions: rack
Variables:
Independent: test solution changes
Controlled: adding 10mL of both the anion solutions and test solutions, same
height and width of test tube, distilled water, water bath, test tube holders, same
environment
Risk Assessment:
Risk Hazard Prevention
Some chemicals are They can burn the skin To prevent it, wear safety
corrosive and poisonous glasses and wash hands
if it contacts with it.
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Method:
1. Add 10 drops of each of the anion solutions to each of 4 test tubes.
2. Add 10 drops of HNO3 to each of the test tubes and warm gently.
3. Record the results.
4. Use these results to describe a test for one particular anion.
5. Thoroughly clean all test tubes with distilled water between tests.
6. For the remaining three anions, put 10 drops in each of 3 test tubes,
add 5 drops of HNO3 and then add 5 drops of Ag+.
7. Record the results in the table below. Write NP if no precipitate
forms, and write ppt if precipitate forms and give its colour.
8. Repeat steps 67 with Pb2+ and then Ba2+
9. After the Ba2+ test add 10 drops of NaOH to each of the test tubes
and record any changes
Results:
Test Solutions
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White
precipitat
e formed
at the
bottom
Discussion:
This experiment involves testing anions by reacting them with cation solutions.
Each anion reacted with a test solution.
Conclusion:
From the results, it can be seen that different anions produce different
substances.
Introduction:
Qualitative analysis is the process of identifying the substances present in a
sample of matter. There are many possible tests, and in this experiment several
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tests including flame tests and precipitation reactions will be used. Some metal
ions emit characteristic colours of light when heated in the blue flame of a
Bunsen burner. Flame tests are therefore useful in identifying some cations. In
precipitation reactions two ionic solutions are mixed with a solid precipitate being
formed. The nature of chemical tests for identifying ions must be such that no
two ions give the same results. By conducting appropriate tests, the identity of
the ion or ions in an unknown sample may be determined.
Aim:
To identify cations, present in the solution using precipitation reactions.
Materials:
Cation solutions:
Pb(NO3)2
Ba(NO3)2
FeSO4
CuSO4
CaCl2
FeCl3
Test solutions:
Na2SO4
HCl
NaOH
Acidified KMnO4 (additional test)
NaCl
KI
6 watch glasses
5mL 4M HCl
Variables:
Independent: cation solutions
Controlled: amount of each solution added, same width, height of test tubes,
environment, temperature,
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Risk Assessment:
Risk Hazard Prevention
HCl Is corrosive and can cause burns Prevent direct contact with skin or
on skin clothes
Method:
1. Add 10 drops of the Pb2+ solution to each of 6 watch glasses.
2. Add 10 drops of the test solution to each of the watch glasses. If no
precipitate forms, try adding a few more drops.
3. Record the results in the table below. Write NP if no precipitate
forms, and write ppt if precipitate forms and give its colour.
4. Thoroughly clean all watch glasses with distilled water.
5. Repeat steps 2-4 with the other test solutions listed in the materials.
Results:
TEST SOLUTIONS
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Conclusion:
From the results it can be seen that the cations have distinct precipitates when it
reacts with test solutions
Discussion:
This experiment deals with reacting cation solutions with test solutions. When
they react, certain cations like lead produce a precipitate which are distinct to
others. The results demonstrate how most of the precipitation reactions produce
a white precipitate. This means that some cations can be hard to deduce from
these tests.
This experiment can be called valid as only one variable changed and the others
remained same. The experiment can also be considered reliable as other groups
got the same results as us. Accuracy does not really matter in this experiment
because it is a qualitative experiment except for the fact that the drops were
from the dropper. Limitations to the experiment includes using test/cation
solutions which may have been contaminated by other students. Further
improvements to this experiment can include effective time management, and
placing the watch glass on top of a white paper so that the precipitate can be
easily seen.
Flame Tests
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Aim:
To observe a range of colours that cations produce in flame tests
Materials:
Bunsen Burner
Matchbox
6 spray bottles each containing 0.05M aqueous (iron III chloride,
Calcium chloride, barium nitrate, barium chloride, copper II chloride)
Variables:
Independent: chemical composition of solutions being tested
Risk Assessment:
Hazard Risk Prevention
Practical Reports
Method:
1. Set up a Bunsen burner to blue flame, like
the one shown in diagram.
2. Spray iron III chloride in the blue flame.
3. Observe the colour and record results.
4. Repeat steps 2 and 3 for other solutions.
Results:
Compound Ions Present in Colour
compound
Conclusion:
From the results it can be seen that different cations produce different colour
flames.
Discussion:
The experiment is deemed to be a success because it answers the aim. The
results show that different cations produce different colours in flame tests. The
results are reliable because other group got the same results as us. Moreover,
the experiment can also be considered valid as only one variable changes
(chemical composition of solution). Therefore, it can be said that the flame colour
present is directly as a result of the cations present. The accuracy of experiment
is dependent on the number of sprays squirted into the flame. This limits the
accuracy of the experiment. This is not really considered as the aim was only to
observe the range of colours of different cations.
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Limitations to this experiment include that flame tests cannot detect low
concentrations of ions. Moreover, flame tests may not be distinguishable as
background light may conceal colours shown in the flame.
Sulfates in fertiliser
Aim:
to use gravimetric analysis to determine the sulphate content of a lawn fertiliser.
Materials:
0.6 g solid soluble Hotplate
fertiliser Glass rod
1M hydrochloric acid Watch glass
15Ml BaCl2 Filter paper
Electronic balance Buchner funnel
250ml beaker Flask
Burette Adaptor
Tubing
Risk Assessment:
Variables:
Method:
1. Weigh out accurately approximately 0.6003 grams of the powdered
lawn fertiliser into a clean 250ml beaker. Record the mass of fertilise. Add
25ml of deionised water. Stir to dissolve the crystals.
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Results:
Practical Reports
m
n=
Mm
1.1097
n=
233.37
n=0.00475510991moles
For Sulfate:
m
n=
Mm
m
0.00475510991=
96.07
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0.4568234092
x 100=76.09918527
0.6003
Conclusion:
From the results it can be seen that about 76% of the fertiliser contains sulfate
ions.
Discussion:
Through conducting physical and chemical tests, the aim of the experiment was
successfully answered.
By placing the precipitate in the oven, any water molecules that are present will
evaporate, and thus accurate results can be obtained.
The experiment can be deemed reliable as other groups received similar mass of
precipitate to us, and hence would have received similar percentage of sulfate
concentration. The experiment is considered valid as there are no real variables
that were changed. The electronic balance was highly accurate (4 decimal
places) so the experiment can be deemed accurate.