Professional Documents
Culture Documents
2.930.1460
Table of contents
1 About these Short Instructions 1
2 Introduction 2
2.1 Instrument description ......................................................... 2
2.2 Intended use ......................................................................... 4
2.3 Safety instructions ................................................................ 4
2.3.1 General notes on safety ........................................................... 4
2.3.2 Electrical safety ........................................................................ 4
2.3.3 Tubing and capillary connections ............................................. 5
2.3.4 Flammable solvents and chemicals ........................................... 6
2.3.5 Recycling and disposal ............................................................. 6
2.4 Symbols and conventions .................................................... 6
4 Installation 11
4.1 Setting up the instrument .................................................. 11
4.1.1 Packaging .............................................................................. 11
4.1.2 Checks .................................................................................. 11
4.1.3 Location ................................................................................ 11
4.2 Removing transport locking screws ................................. 11
4.3 Connecting the drainage tubing and leak sensor ............ 13
4.3.1 Installing the drainage tubing ................................................ 13
4.3.2 Connecting the leak sensor .................................................... 14
4.4 Connecting the eluent bottle ............................................. 15
4.5 Connecting the eluent degasser ........................................ 17
4.6 Installing the high-pressure pump .................................... 17
4.7 Installing an inline filter ..................................................... 17
4.8 Installing the pulsation absorber ...................................... 17
4.9 Injection valve ..................................................................... 17
4.10 Suppressor .......................................................................... 17
4.10.1 Inserting the rotors ................................................................ 18
4.10.2 Connecting the suppressor .................................................... 19
4.11 Metrohm CO2 Suppressor (MCS) ....................................... 22
4.11.1 Connecting the MCS ............................................................. 22
4.11.2 Installing adsorption cartridges .............................................. 22
5 Operation 35
6 Warranty (guarantee) 36
7 Accessories 38
Index 40
Table of figures
Figure 1 Front ................................................................................................. 8
Figure 2 Rear .................................................................................................. 9
Figure 3 Removing the transport locking screws ............................................ 12
Figure 4 Suppressor connection capillaries ................................................. 20
Figure 5 Connecting the MCS ....................................................................... 22
2 Introduction
Leak sensor
The leak sensor detects leaking liquid that collects in the instrument's base
tray. Liquid that leaks in the instrument is routed to the base tray using
drainage tubing and detected there.
Eluent degasser
The eluent degasser removes gas bubbles and dissolved gases from the
eluent.
High-pressure pump
The intelligent and low-pulsation high-pressure pump pumps the eluent
through the system. It is equipped with a chip where its technical specifi-
cations and "life history" (operating hours, service data, etc.) are saved.
Inline filter
Inline filters protect the separation column reliably from potential contami-
nation from the eluent. The small filter pads with 2 m pore size can be
replaced quickly and easily. They remove particles from the solutions, such
as bacteria and algae.
Pulsation absorber
The pulsation absorber protects the separation column from damage
caused by pressure fluctuations when switching the injection valve, and
reduces interfering pulsations during highly sensitive measurements.
Injection valve
The injection valve connects the eluent path to the sample path. By a
quick and precise switching of the valve a quantity of sample solution
defined by the size of the sample loop is injected and flushed to the sepa-
ration column with the eluent.
Suppressor
The suppressor consists of a suppressor drive, a rotor and, where applica-
ble, an adapter. The suppressor drive gives you the flexibility to use differ-
ent rotors according to the principle "one drive many rotors". With
appropriate adapters, the rotor for the sample preparation module (SPM
Rotor) or suppressor rotors with different capacities and construction can
be easily exchanged. The rotors are not included in the instrument's scope
of delivery. A rotor suitable for the application must be ordered separately.
Detector
Metrohm offers a series of different detectors for various analysis tasks. A
suitable detector type must be ordered as a separate accessory.
Sample degasser
The sample degasser removes gas bubbles and dissolved gases from the
sample.
Separation column
The intelligent separation column separates different components accord-
ing to their interactions with the column. Metrohm separation columns
are equipped with a chip where their technical specifications and history
(start-up, operating hours, etc) are stored.
WARNING
This instrument has left the factory in a flawless state in terms of technical
safety. To maintain this state and ensure non-hazardous operation of the
instrument, the following instructions must be observed carefully.
WARNING
WARNING
Mains voltage
WARNING
WARNING
CAUTION
Leaks in tubing and capillary connections are a safety risk. Tighten all
connections well by hand. Avoid applying excessive force to tubing
connections. Damaged tubing ends lead to leakage. Appropriate tools
can be used to loosen connections.
Check the connections regularly for leakage. If the instrument is used
mainly in unattended operation, then weekly inspections are manda-
tory.
WARNING
WARNING
This symbol draws attention to a possible hazard due
to electrical current.
WARNING
This symbol draws attention to a possible hazard due
to heat or hot instrument parts.
WARNING
This symbol draws attention to a possible biological
hazard.
CAUTION
This symbol draws attention to possible damage to
instruments or instrument parts.
NOTE
This symbol highlights additional information and
tips.
3.1 Front
Figure 1 Front
3.2 Rear
Figure 2 Rear
21 Power socket
Power socket for connecting the power
cable and power switch for switching the
instrument on and off.
4 Installation
4.1.2 Checks
Immediately after receipt, check whether the shipment has arrived com-
plete and without damage by comparing it with the delivery note.
4.1.3 Location
The instrument has been developed for operation indoors and may not be
used in explosive environments.
Place the instrument in a location of the laboratory which is suitable for
operation, free of vibrations, protected from corrosive atmosphere, and
contamination by chemicals.
The instrument should be protected against excessive temperature fluctu-
ations and direct sunlight.
Store the transport locking screws in a safe place. Reinsert the transport
locking screws each time you transport the instrument a significant dis-
tance.
CAUTION
4.10 Suppressor
The suppressor drive of the 930 Compact IC Flex can hold various rotors.
The large rotors such as the SPM Rotor A (6.2835.000) and the MSM-HC
Rotor A (6.2842.000) can be inserted directly.
Small rotors like the MSM Rotor A (6.2832.000) and the MSM-LC Rotor A
(6.2844.000) must first be fitted into the adapter (6.2842.020) which can
then be inserted into the suppressor housing.
A connecting piece (6.2835.010) is used for all rotors for connecting the
suppressor to the IC system.
NOTE
CAUTION
You need the adapter (6.2842.020) in order to insert a small rotor into the
suppressor drive.
1 out 2 in
Output capillary for the eluent. Input capillary for the eluent.
Recommended installation
Alternative installation
CAUTION
If the MCS is not used, the input and output must be sealed with the
threaded stoppers (6.2744.220).
CAUTION
The following preparatory steps absolutely must be carried out for CO2
suppression to operate correctly.
NOTE
CAUTION
If the sample degasser is not used, the input and output must be
sealed with threaded stoppers (6.2744.220).
NOTE
1 Insert the USB cable into the computer connection socket on the rear
of the instrument.
WARNING
The power supply unit must not get wet. Protect it from liquids.
The power supply cable is three-core and provided with a plug with
grounding. If another plug has to be mounted, the yellow/green conduc-
tor (IEC standard) must be connected to the protective ground (protection
class I).
Accessories For this step you need the following accessories:
For Switzerland, : Power supply cable with IEC 60320 line socket,
type C13, with SEV 1011 plug, type 12 (6.2122.020), 1.5 m
For Germany, : Power supply cable with IEC 60320 line socket, type
C13, with CEE 7 plug, type VII (6.2122.040), 1.5 m
For the USA, : Power supply cable with IEC 60320 line socket, type
C13, with NEMA 5-15 plug, type 498 (6.2122.070), 1.5 m
After being switched on, the LED on the front of the instrument
flashes. The instrument conducts a system test and establishes a con-
nection to the software. Once the system test is complete and the
connection to the software has been established, the LED lights up
continuously.
CAUTION
The guard column and separation column must not be installed for the
initial start-up.
Make sure that a coupling (6.2744.040) is being used instead of the
columns.
3 Starting equilibration
Start the equilibration in MagIC Net: Workplace Run Equi-
libration Start HW.
Use the syringe to aspirate eluent until there are no more air
bubbles in the eluent.
CAUTION
New guard columns are filled with solution and sealed with stoppers or
caps on both sides.
Before inserting the guard column, ensure that this solution can be
mixed with the eluent being used (follow information from the manu-
facturer).
NOTE
The guard column may not be connected until after the instrument has
already been put into operation once (see Chapter 4.16, page 28). The
guard column and separation column have to be replaced by a coupling
(6.2744.040) until then.
CAUTION
New separation columns are filled with solution and sealed with stop-
pers on both sides. Before inserting the column, ensure that this solu-
tion can be mixed with the eluent being used (follow information from
the manufacturer).
NOTE
The separation column may not be connected until after the instrument
has already been put into operation once (see Chapter 4.16, page 28).
The guard column and separation column have to be replaced by a
coupling (6.2744.040) until then.
4.19 Conditioning
After installation, after each time the instrument is switched on and after
each time the eluent is changed, the system has to be conditioned with
eluent long enough that a stable baseline is attained.
NOTE
CAUTION
Ensure that the configured flow is not higher than the flow permit-
ted for the corresponding column (refer to the column leaflet and
the chip data record).
3 Starting equilibration
Start the equilibration in MagIC Net: Workplace Run Equi-
libration Start HW.
5 Operation
The 930 Compact IC Flex SeS/Deg is operated solely using the MagIC Net
software. You can find information on operating the software in the tuto-
rial for MagIC Net or in the online help.
6 Warranty (guarantee)
Metrohm guarantees that the deliveries and services it provides are free of
defects in materials, design or manufacturing.
The general warranty period is 36 months (exclusions below) from the
date of delivery, or 18 months in the event of continuous operation. The
warranty remains valid on the condition that the servicing is provided by a
service organization authorized by Metrohm at defined intervals and with
a defined scope.
The warranty period for anion suppressors of the type "MSM" is 120
months from the date of delivery or 60 months in the case of continuous
operation.
The warranty period for IC separation columns is 90 days after start-up.
For third-party components that are recognizable as such, the manufac-
turer's warranty regulations apply.
For instruments sold under the Metrohm NIRSystems brand, a full 16-
month warranty is applicable. In the event of continuous operation, the
warranty period is reduced by half.
Consumables and materials with limited storage life and glass breakage in
the case of electrodes or other glass parts are excluded from the warranty.
Warranty claims cannot be asserted if the ordering party has failed to
meet its payment obligations according to schedule.
During the warranty period, Metrohm undertakes either to replace free of
charge or to credit the purchaser for any modules or components that can
be shown to be faulty. Any transport or customs fees that may apply are
the responsibility of the ordering party.
The precondition for this is that the ordering party has to specify the arti-
cle number, the article designation, an adequate error description, the
delivery date and (if applicable) the serial number or chip data in the Sup-
port Tracker. Metrohm then decides whether a replacement or a credit
note is to be issued or whether the faulty part has to be returned using
the Return Material Authorization (RMA). If a replacement or credit note is
issued, the ordering party undertakes to store the faulty part for at least
24 months in accordance with the current storage directives (in compli-
ance with ESD guidelines) and to hold it in readiness for onsite inspection
or for return shipment to Metrohm. Metrohm reserves the right to invoice
the ordering party for these articles, including retroactively, in the event of
noncompliance with these preconditions.
The same warranty periods that are specified for a corresponding new
part apply to parts that are replaced or repaired within the above-men-
tioned warranty periods. However, replacement or repair of a part does
not extend the warranty period of the entire system.
Deficiencies arising from circumstances that are not the responsibility of
Metrohm, such as improper storage or improper use, etc., are expressly
excluded from the warranty.
Metrohm also offers a 120-month spare parts availability guarantee and a
60-month PC software support warranty, calculated from the date on
which the product is withdrawn from the market. The content of this war-
ranty is the ability of the customer to obtain functioning spare parts or
appropriate software support at market prices during the time of the war-
ranty period. This does not apply for software products sold under the
Metrohm NIRSystems brand.
If Metrohm AG is unable to meet this obligation due to circumstances
beyond the control of Metrohm AG, then the ordering party shall be
offered alternative solutions at preferential conditions.
7 Accessories
Up-to-date information on the scope of delivery and optional accessories
for your instrument can be found on the Internet.
NOTE
2
Click on .
The Search webpage will be displayed.
3 Enter a search term relating to the instrument into the search field
and click on Find.
The search results will be displayed.
4 In the search results, select the Devices tab (if it is not already
selected) and then click on the Metrohm article number of the
required instrument (e.g. 2.852.0050).
The page with information pertaining to the searched article is dis-
played.
6
Click on .
3 Enter the article number and click on the Generate PDF command.
The PDF file with the accessories data will be created in the language
selected.
Index
A Guard column P
Adsorption cartridges Installation ......................... 30 Power connection .................... 27
Connection ........................ 22 Rinse .................................. 30 Power supply cable ................... 27
Aspiration tubing for eluent ...... 16 Pulsation absorber
H Installation ......................... 17
B High-pressure pump
Baseline Protection .......................... 12 R
Conditioning ...................... 34 Rinse
I Guard column .................... 30
C IC column Separation column ............. 32
Cartridges See also "Separation column"
Connection ........................ 22 ........................................... 31 S
Column Injection valve ............................ 3 Safety instructions ...................... 4
See also "Separation column" Installation ......................... 17 Sample degasser
........................................... 31 Inline filter ................................ 17 Installation ......................... 25
Computer connection ............... 26 Installation Separation column
Conditioning ............................ 34 Drainage tubing ................. 13 Installation ......................... 31
Connect Eluent bottle ....................... 15 Protection ...................... 3, 17
To computer ...................... 26 Guard column .................... 30 Rinse .................................. 32
To power supply ................. 27 Injection valve .................... 17 Service ....................................... 4
Leak sensor ........................ 14 Suppressor
D MCS ................................... 22 Install rotor ......................... 17
Degasser Pulsation absorber .............. 17 Installation ......................... 17
Sample degasser ................. 25 Sample degasser ................. 25 Suppressor drive
Drainage tubing Separation column ............. 31 See also: Suppressor ........... 17
Installation ......................... 13 Suppressor ......................... 17 Switch on ................................. 27
E L T
Electrostatic charge .................... 5 Leak sensor Transport locking screws .......... 11
Eluent Installation ......................... 14
Aspirate .............................. 16 Leak-tightness .......................... 29 V
Eluent bottle Vacuum pump
Installation ......................... 15 M Protection .......................... 12
Equilibration ....................... 29, 33 Mains voltage ............................. 5 Valve
MCS See also "Injection valve" .... 17
F Capillary connection ........... 22
Filter Connection for cartridges ... 22 W
See also "Inline filter" .......... 17 Installation ......................... 22 Warranty .................................. 36
G
Guarantee ................................ 36