X

Bruker D8 Discover/Advanced
Detector
Scientillation : Point detector,
Resolution 0.0002 degree
Scan mode: theta/2theta scan,
rocking curve,
2theta scan (GIXRD)

Vantec-1: Line detector,

Resolution 0.00067 degree
Scan mode: theta/2theta scan

Source: Ceramic sealed tube

Copper K alpha radiation
Wavelenth = 1.54 anstrons
Spot size:

Sample stage: Fixed (No Phi scan or Chi scan)

 X
1) X?
2) X?
3) ?
4) ?
5) ?
6) ?
7) X?
8) ??
(1)X?

X/
:

1
sputterZnO
XZnO

2
ZnO rod
XZnORocking curverod


(2)X?

(ceramic-sealed tube)1.6kW
X
X(
0.5cm50nm)

(rotating anode tube)18kW



beam time


X

X

X
(2)X?
X
X

(SAXS)2thetaX

Phi scan/Chi scanX

(broadening)
X

2Theta/Omega

Phi
Chi

2Theta
Omega
(3)? ( page10-12)

(4)? ( page9)

(5)?
XZnO
ZnO XRD
2theta2080(10)
0.02-0.05
2theta(>2)0.05

-
X3000

Intensity
(10%30)30
10

20-80 = ()
0.02

= 10 60
(8020)
= 0.2s
0.02 2Theta

- S/N
Signal/Nosise
24

(6)?

2cm Sample
Environment
holder
Temperature 12.5-300K
35-45% (room026) 5cm
Humidity
Unclear (chamber)
Pressure 10-4-10-5
6cm

1.
2. 1.5cm X 1.5cm
3. 3cm X 2cm
4.1.5mm
5.

6.(Al2O3)
101.96/g1g

7.

(7)X? ( page13)

(8)?

TEL 03-5712121 #56144,
E-mail luyihsuan.mse00g@nctu.edu.tw
FB https://www.facebook.com/nctuepd8?ref=hl !

026

Pin
X
Pin



3 cm1.5
mm

Pin
Pin

5 cm


Pin
3mm

()




WAG(2theta-Omega Scan)
Detector

(
)

incident
detector
beam

diffracted
beam


GIXRD (2Theta Scan)
Detector

X
100 nm

incident
detector
beam


diffracted
beam

e.g.
Given In WAG mode In GIXRD mode
=69.1
Si (100) plane =69.1
=34.55
// surface =68.1
=34.55 =34.55 =1
Given 2= 69.1 =1
=69.1
=34.55

Correct geometry WRONG geometry!! Plane correction -->

correct geometry


Rocking Curve
Detector2ThetaDetector

2Theta (2)
= .

diffracted detector
beam
incident
beam

 X

X

2000
1500(3) 4000(8)
500/1 500/1
GIXRD GIXRD
WAG Rocking curve WAG Rocking curve



300/10


300/10 800/30 1000/20


300/10 800/30 800/30

90%10%100%
33
34
1
WAG10GIXRD Rocking curve30

()
88
500
20